CN103735426A - Method for preparing gypsum facial mask - Google Patents
Method for preparing gypsum facial mask Download PDFInfo
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- CN103735426A CN103735426A CN201410009753.9A CN201410009753A CN103735426A CN 103735426 A CN103735426 A CN 103735426A CN 201410009753 A CN201410009753 A CN 201410009753A CN 103735426 A CN103735426 A CN 103735426A
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Abstract
The invention relates to a method for preparing a gypsum facial mask, and belongs to the living field of cosmetics. The method sequentially comprises the following steps: preparing mixed glue: stirring and mixing polyvinyl alcohol gel, a starch glue solution and food gum in a weight ratio of (2-4):1:1 to prepare the mixed glue; preparing primary glue of gypsum: mixing gypsum powder and the mixed glue in a weight ratio of 1:(0.5-0.9), sufficiently stirring with water until the baume degree is 82-98 degrees Be to obtain the primary glue of gypsum; preparing secondary glue of gypsum: mixing the primary glue of gypsum, the mixed glue and water in a mass ratio of (9-12):6:1, and stirring to obtain the secondary glue of gypsum; guiding gauze: guiding gauze through a cloth guiding barrel in a suspending manner, and sizing with the secondary glue of gypsum; baking: baking the gypsum gauze obtained after cloth guiding and sizing; cutting and packaging: and cutting the baked gypsum gauze into a single gypsum facial mask, and packaging. The gypsum facial mask is safe and reliable to use, can be used for clearing heat and promoting skin to heat and perspire and pores to puff, and is especially effective to oily skin and skin with acne or hidrocystoma, inflammation and allergic phenomena.
Description
Technical field
The present invention relates to a kind of preparation method of Gypsum Fibrosum facial film, belong to cosmetics sphere of life.
Background technology
Facial film is a kind of cosmetics and skincare product applying on the face, plays effect clean, vigorous and graceful and protection face.Increasing moisture of skin is the basis of beauty and skin care, and that the skin drying out can be dried is coarse, form microgroove, pigmentation, causes many skin problems.In < < Compendium of Materia Medica > >, disclose and adopt Gypsum Fibrosum as expelling wind and clearing away heat, open plug sensible, treatment face is because of the unexpected inaccessible antiperspirant cyst producing of pore.CN103110564A (2013-5-22) discloses a kind of traditional Chinese medicinal whitening mask and preparation method thereof, comprising there being Gypsum Fibrosum powder.Yet they are all to adopt to take orally, do not disclose the preparation method of external Gypsum Fibrosum facial film at present.
Summary of the invention
The object of this invention is to provide a kind of preparation method with the Gypsum Fibrosum facial film of whitening antiinflammatory effect.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs:
A preparation method for Gypsum Fibrosum facial film, it comprises step successively:
(1) epoxy glue preparation:
Take by weight the polyvinyl alcohol of 1 part of solid granular and the hot water that 7-10 part temperature is 95-100 ℃, toward limit in described polyvinyl alcohol, add described hot water limit and stir, deposit and within 5-10 days, make polyvinyl alcohol jelly;
Take by weight 1 part of starch and 8-12 part temperature and be the hot water of 95-100 ℃, toward limit in described starch, add described hot water limit and stir, deposit and within 1-5 days, make starch glue;
Described polyvinyl alcohol jelly, starch glue and foodstuff glue are uniformly mixed and make epoxy glue by weight 2-4:1:1;
(2) Gypsum Fibrosum one-level slurry preparation: Gypsum Fibrosum powder and described epoxy glue are mixed according to weight ratio 1:0.5-0.9, and then adding water to be stirred well to Baume degrees is 82-98
°be, obtains Gypsum Fibrosum primary amine;
(3) Gypsum Fibrosum secondary slurry preparation: described Gypsum Fibrosum primary amine, described epoxy glue and water are mixed according to mass ratio 9-12:6:1, stir, obtain Gypsum Fibrosum secondary glue;
(4) selvage guide: gauze is hung and imported by selvage guide bucket, carry out starching with described Gypsum Fibrosum secondary glue;
(5) dry: the plaster gauze of gained after selvage guide starching is dried;
(6) cut, pack: the plaster gauze after drying is cut into the Gypsum Fibrosum facial film of monolithic, packing.
Advantage of the present invention is:
1. by a plurality of steps, make specific epoxy glue, then after making Gypsum Fibrosum secondary slurry with Gypsum Fibrosum powder classification, carry out starching, dry, cut and make Gypsum Fibrosum facial film, Gypsum Fibrosum powder is difficult for dropping, after Gypsum Fibrosum facial film being immersed in warm water during use, apply spray form water after putting on the face or first on the face, use 10-30min, Gypsum Fibrosum facial film soft durometer during use is moderate, and too brittle failure is not split, also can be also not soft very soon;
2. use this Gypsum Fibrosum facial film can heat clearing away, promote that skin heating is perspired and pore opens, to oily skin, length, have the skin of acne or antiperspirant cyst, inflammation and allergic phenomena effective especially;
3. when prepared by the present invention, the content of sizing material and preparation process are controlled very crucially, because Gypsum Fibrosum is met Aquatic product heat on the one hand, promote that pore opens; Must control on the other hand the heat producing when Gypsum Fibrosum facial film is used, thus safe and reliable when Gypsum Fibrosum facial film is used.
As preferably, in described step (1) starch glue, be added with the mud that accounts for described starch glue weight 2-6 ‰ and moor golden fat.
Mud is moored golden fat can increase the result of use of Gypsum Fibrosum facial film on the one hand, can extend on the other hand the holding time of Gypsum Fibrosum facial film.
As preferably, described step (1) foodstuff glue is carrageenan or Konjac glucomannan.
As preferably, the preparation of described step (1) epoxy glue:
Take by weight the polyvinyl alcohol of 1 part of solid granular and the hot water that 7-10 part temperature is 95-100 ℃, toward limit in described polyvinyl alcohol, add described hot water limit and stir, deposit and within 7 days, make polyvinyl alcohol jelly;
Take by weight 1 part of starch and 9 parts of temperature and be the hot water of 95-100 ℃, toward limit in described starch, add described hot water limit and stir, deposit and within 3 days, make starch glue;
Described polyvinyl alcohol jelly, starch glue and foodstuff glue are uniformly mixed and make epoxy glue by weight 3:1:1.
As preferably, the preparation of described step (2) Gypsum Fibrosum one-level slurry is that Gypsum Fibrosum powder and described epoxy glue are mixed according to weight ratio 1:0.6, and then adding water to be stirred well to Baume degrees is 85-95
°be, obtains Gypsum Fibrosum primary amine.
As preferably, the preparation of described step (3) Gypsum Fibrosum secondary slurry is that described Gypsum Fibrosum primary amine, described epoxy glue and water are mixed according to mass ratio 10:6:1, stirs 20-50min, obtains Gypsum Fibrosum secondary glue.
As preferably, described step (4) selvage guide specifically hangs gauze to import by selvage guide bucket, through tension adjustment frame and selvage guide cylinder, sends into Gypsum Fibrosum distribution machine center position by gauze is straight without crape; After start, open blowing lock, Gypsum Fibrosum secondary slurry is introduced and fed stock tank; Make gauze enter pincers, and open the even starching of feeding valve, driving starching be speed of a motor vehicle 9-12m/min.
During starching, also should notice at any time that gauze crape is folded, joint is wound around, and starching is wanted evenly, and gauze is without spillage; Note left and right stenter, prevent that gauze from taking off pincers, once find, go up pincers immediately.
More preferably, described gauze is the strip gauze that has been made into facial film shape.
As preferably, described bake out temperature is 120-150 ℃.
As preferably, described oven dry is that microwave vacuum is dried, and specifically plaster gauze is put into microwave vacuum tank, then carry out evacuation process to vacuum be-0.05MPa～-0.03MPa; Carry out microwave treatment, microwave frequency is 150MHz～240MHz again, and microwave treatment time is 2～5min.
In sum, the present invention has following beneficial effect:
1, use this Gypsum Fibrosum facial film can heat clearing away, promote that skin heating is perspired and pore opens, to oily skin, grow and have the skin of acne or antiperspirant cyst, inflammation and allergic phenomena effective especially;
It is safe and reliable when 2, Gypsum Fibrosum facial film is used.
The specific embodiment
Embodiment mono-
The preparation method of Gypsum Fibrosum facial film, comprises step successively:
(1) epoxy glue preparation:
Take by weight the polyvinyl alcohol of 1 part of solid granular and the hot water that 7 parts of temperature are 95 ℃, toward limit in described polyvinyl alcohol, add described hot water limit and stir, deposit and within 5 days, make polyvinyl alcohol jelly;
Take by weight 1 part of starch and 8 parts of temperature and be the hot water of 95 ℃, toward limit in described starch, add described hot water limit and stir, deposit and within 1 day, make starch glue; And the mud that past starch glue interpolation accounts for described starch glue weight 2 ‰ is moored golden fat;
Described polyvinyl alcohol jelly, starch glue and Konjac glucomannan are uniformly mixed and make epoxy glue by weight 2:1:1;
(2) Gypsum Fibrosum one-level slurry preparation: Gypsum Fibrosum powder and described epoxy glue are mixed according to weight ratio 1:0.5, and then adding water to be stirred well to Baume degrees is 82
°be, obtains Gypsum Fibrosum primary amine;
(3) Gypsum Fibrosum secondary slurry preparation: described Gypsum Fibrosum primary amine, described epoxy glue and water are mixed according to mass ratio 9:6:1, stir 20min, obtain Gypsum Fibrosum secondary glue;
(4) selvage guide: the strip gauze that is made into facial film shape is hung and imported by selvage guide bucket, through tension adjustment frame and selvage guide cylinder, send into Gypsum Fibrosum distribution machine center position without crape by gauze is straight; After start, open blowing lock, Gypsum Fibrosum secondary slurry is introduced and fed stock tank; Make gauze enter pincers, and open the even starching of feeding valve, driving starching be speed of a motor vehicle 9m/min;
During starching, also should notice at any time that gauze crape is folded, joint is wound around, and starching is wanted evenly, and gauze is without spillage; Note left and right stenter, prevent that gauze from taking off pincers, once find, go up pincers immediately;
(5) dry: by the plaster gauze of gained after selvage guide starching, in temperature, be to dry at 120 ℃;
(6) cut, pack: the plaster gauze after drying is cut into the Gypsum Fibrosum facial film of monolithic, packing.
Embodiment bis-
The preparation method of Gypsum Fibrosum facial film, comprises step successively:
(1) epoxy glue preparation:
Take by weight the polyvinyl alcohol of 1 part of solid granular and the hot water that 10 parts of temperature are 100 ℃, toward limit in described polyvinyl alcohol, add described hot water limit and stir, deposit and within 10 days, make polyvinyl alcohol jelly;
Take by weight 1 part of starch and 12 parts of temperature and be the hot water of 100 ℃, toward limit in described starch, add described hot water limit and stir, deposit and within 5 days, make starch glue; And the mud that past starch glue interpolation accounts for described starch glue weight 6 ‰ is moored golden fat;
Described polyvinyl alcohol jelly, starch glue and carrageenan are uniformly mixed and make epoxy glue by weight 4:1:1;
(2) Gypsum Fibrosum one-level slurry preparation: Gypsum Fibrosum powder and described epoxy glue are mixed according to weight ratio 1:0.9, and then adding water to be stirred well to Baume degrees is 98
°be, obtains Gypsum Fibrosum primary amine;
(3) Gypsum Fibrosum secondary slurry preparation: described Gypsum Fibrosum primary amine, described epoxy glue and water are mixed according to mass ratio 12:6:1, stir 50min, obtain Gypsum Fibrosum secondary glue;
(4) selvage guide: the strip gauze that is made into facial film shape is hung and imported by selvage guide bucket, through tension adjustment frame and selvage guide cylinder, send into Gypsum Fibrosum distribution machine center position without crape by gauze is straight; After start, open blowing lock, Gypsum Fibrosum secondary slurry is introduced and fed stock tank; Make gauze enter pincers, and open the even starching of feeding valve, driving starching be speed of a motor vehicle 12m/min;
During starching, also should notice at any time that gauze crape is folded, joint is wound around, and starching is wanted evenly, and gauze is without spillage; Note left and right stenter, prevent that gauze from taking off pincers, once find, go up pincers immediately;
(5) dry: by the plaster gauze of gained after selvage guide starching, in temperature, be to dry at 150 ℃;
(6) cut, pack: the plaster gauze after drying is cut into the Gypsum Fibrosum facial film of monolithic, packing.
Embodiment tri-
(1) epoxy glue preparation:
Take by weight the polyvinyl alcohol of 1 part of solid granular and the hot water that 8 parts of temperature are 98 ℃, toward limit in described polyvinyl alcohol, add described hot water limit and stir, deposit and within 7 days, make polyvinyl alcohol jelly;
Take by weight 1 part of starch and 9 parts of temperature and be the hot water of 98 ℃, toward limit in described starch, add described hot water limit and stir, deposit and within 3 days, make starch glue;
Described polyvinyl alcohol jelly, starch glue and Konjac glucomannan are uniformly mixed and make epoxy glue by weight 3:1:1;
(2) Gypsum Fibrosum one-level slurry preparation: Gypsum Fibrosum powder and described epoxy glue are mixed according to weight ratio 1:0.6, and then adding water to be stirred well to Baume degrees is 88
°be, obtains Gypsum Fibrosum primary amine;
(3) Gypsum Fibrosum secondary slurry preparation: described Gypsum Fibrosum primary amine, described epoxy glue and water are mixed according to mass ratio 10:6:1, stir 30min, obtain Gypsum Fibrosum secondary glue;
(4) selvage guide: strip gauze hang is imported by selvage guide bucket, through tension adjustment frame and selvage guide cylinder, send into Gypsum Fibrosum distribution machine center position without crape by gauze is straight; After start, open blowing lock, Gypsum Fibrosum secondary slurry is introduced and fed stock tank; Make gauze enter pincers, and open the even starching of feeding valve, driving starching be speed of a motor vehicle 11m/min;
During starching, also should notice at any time that gauze crape is folded, joint is wound around, and starching is wanted evenly, and gauze is without spillage; Note left and right stenter, prevent that gauze from taking off pincers, once find, go up pincers immediately;
(5) dry: by the plaster gauze of gained after selvage guide starching, in temperature, be to dry at 130 ℃;
(6) cut, pack: the plaster gauze after drying is cut by facial film shape, finally cut into the Gypsum Fibrosum facial film of monolithic, packing.
Embodiment tetra-
With embodiment mono-, different is dries is that microwave vacuum is dried, and specifically plaster gauze is put into microwave vacuum tank, then carry out evacuation process to vacuum be-0.05MPaMPa; Carry out microwave treatment, microwave frequency is 150MHz again, and microwave treatment time is 2min.
Embodiment five
With embodiment bis-, different is dries is that microwave vacuum is dried, and specifically plaster gauze is put into microwave vacuum tank, then carry out evacuation process to vacuum be-0.03MPa; Carry out microwave treatment, microwave frequency is 240MHz again, and microwave treatment time is 5min.
Embodiment six
With embodiment tri-, different is dries is that microwave vacuum is dried, and specifically plaster gauze is put into microwave vacuum tank, then carry out evacuation process to vacuum be-0.04MPa; Carry out microwave treatment, microwave frequency is 200MHz again, and microwave treatment time is 4min.
In order to understand better the present invention, the technique effect below the explanation the present invention that improves by clinical experiment report being had.
1, patient's data: select forehead, buccal portion, 60 examples, each 30 examples of men and women, age 16-35 year.Be divided at random two groups: treatment group (Chinese medicine extraction liquid adds skin nutrient) 30 examples, each 15 examples of men and women, 26 ± 7 years old age, matched group (carrageenan adds water) 30 examples, each 15 examples of men and women, 29 ± 8 years old age.
Before use, respectively organize patient's sex, age, skin symptom integration there are no significant difference (P>0.05), there is comparability.
2, experiment material:
(1) treatment group of the present invention:
Treatment group: Gypsum Fibrosum facial film used is pressed embodiment 1 preparation;
(2) matched group facial film is prepared by the following method:
Matched group:
Prescription: carrageenan 11g.
Method for making: water adds carrageenan fully to stir 5 minutes after being heated to 80-90 ℃, regulates pH value to 5.5-6.5, film forming, packing, sterilizing.
3, experimental technique:
Treatment group 1: patient lies on the back after washing one's face, is applied on the face during use after in Gypsum Fibrosum facial film immersion warm water, uses 10min.3 times weekly, be 2 weeks the course for the treatment of.
Treatment group 2: patient lies on the back, after washing one's face, first puts Gypsum Fibrosum facial film rear spray form water on the face during use, use 30min.3 times weekly, be 2 weeks the course for the treatment of.
Matched group: patient lies on the back, after washing one's face, spreads on face with matched group facial film (not drug ingredients) and embodiment 1 facial film 1., after about 15min, washes away.3 times weekly, be 2 weeks the course for the treatment of.
4, symptom scores standard: forehead, buccal, a small amount of blackhead of nose, comedo person are respectively designated as 2 minutes, forehead, nose, buccal have blackhead and the area 1/3-2/3 person of comedo Qie Zhan face to be respectively designated as 4 minutes, and forehead, nose, buccal portion and cervical region have blackhead and the area 2/3 above person of comedo Qie Zhan face to be respectively designated as 6 minutes.Blackhead, comedo obviously shoal and are designated as 1 minute, and blackhead, comedo shoal and be designated as 2 minutes, and blackhead and tamper pimple shoal and be designated as 3 minutes, and blackhead, tamper pimple and comedo disappear and be designated as 0 minute.
5, efficacy assessment standard:
First by formula-clinical symptoms integration score value improvement rate=(the rear symptom integral score value of symptom integral score value-use before using)/before using, score value * 100% calculates improvement rate, then adopts following standard rating curative effect.
Effective: symptom integral score value improvement rate >=70%;
Effective: symptom integral score value improvement rate >=50%;
Invalid: symptom has no obvious improvement or instead sees deterioration, symptom integral score value improvement rate <50%.
6, statistical procedures: total data adopts SPSS 13.0 statistics softwares to carry out statistical analysis, and mean ± standard deviation for measurement data (x ± s) represents.Before and after two groups of experimenters use, symptom score more all adopts t check, and two groups of experimenter's Clinical efficacy comparisons adopt X
2check.
7, result of the test
Before and after treatment group and matched group are used, symptom scores is relatively in Table 1, and before and after treatment group and matched group are used, curative effect is relatively in Table 2, as known from Table 2, facial film wrinkle removal total effective rate of the present invention, up to 90%, is observed without finding skin heating, flushing through treatment group, edema, the convulsion untoward reaction such as itch.
Symptom scores comparison (x ± s) before and after table 1 treatment group and matched group are used
Table 2 treatment group and the comparison of matched group curative effect
From treatment group and the matched group comparison of table 1 and table 2, standard variance P < 0.01, illustrates the evident in efficacy of this facial film.
This specific embodiment is only explanation of the invention; it is not limitation of the present invention; those skilled in the art can make to the present embodiment the modification that there is no creative contribution as required after reading this description, but as long as within the scope of claim of the present invention, are all subject to the protection of Patent Law.
Claims (10)
1. a preparation method for Gypsum Fibrosum facial film, is characterized in that comprising successively step:
(1) epoxy glue preparation:
Take by weight the polyvinyl alcohol of 1 part of solid granular and the hot water that 7-10 part temperature is 95-100 ℃, toward limit in described polyvinyl alcohol, add described hot water limit and stir, deposit and within 5-10 days, make polyvinyl alcohol jelly;
Take by weight 1 part of starch and 8-12 part temperature and be the hot water of 95-100 ℃, toward limit in described starch, add described hot water limit and stir, deposit and within 1-5 days, make starch glue;
Described polyvinyl alcohol jelly, starch glue and foodstuff glue are uniformly mixed and make epoxy glue by weight 2-4:1:1;
(2) Gypsum Fibrosum one-level slurry preparation: Gypsum Fibrosum powder and described epoxy glue are mixed according to weight ratio 1:0.5-0.9, and then adding water to be stirred well to Baume degrees is 82-98
°be, obtains Gypsum Fibrosum primary amine;
(3) Gypsum Fibrosum secondary slurry preparation: described Gypsum Fibrosum primary amine, described epoxy glue and water are mixed according to mass ratio 9-12:6:1, stir, obtain Gypsum Fibrosum secondary glue;
(4) selvage guide: gauze is hung and imported by selvage guide bucket, carry out starching with described Gypsum Fibrosum secondary glue;
(5) dry: the plaster gauze of gained after selvage guide starching is dried;
(6) cut, pack: the plaster gauze after drying is cut into the Gypsum Fibrosum facial film of monolithic, packing.
2. the preparation method of a kind of Gypsum Fibrosum facial film according to claim 1, is characterized in that: in described step (1) starch glue, be added with the mud that accounts for described starch glue weight 2-6 ‰ and moor golden fat.
3. the preparation method of a kind of Gypsum Fibrosum facial film according to claim 2, is characterized in that: described step (1) foodstuff glue is carrageenan or Konjac glucomannan.
4. the preparation method of a kind of Gypsum Fibrosum facial film according to claim 3, is characterized in that: the preparation of described step (1) epoxy glue:
Take by weight the polyvinyl alcohol of 1 part of solid granular and the hot water that 7-10 part temperature is 95-100 ℃, toward limit in described polyvinyl alcohol, add described hot water limit and stir, deposit and within 7 days, make polyvinyl alcohol jelly;
Take by weight 1 part of starch and 9 parts of temperature and be the hot water of 95-100 ℃, toward limit in described starch, add described hot water limit and stir, deposit and within 3 days, make starch glue;
Described polyvinyl alcohol jelly, starch glue and foodstuff glue are uniformly mixed and make epoxy glue by weight 3:1:1.
5. according to the preparation method of a kind of Gypsum Fibrosum facial film described in claim 1-4 any one, it is characterized in that: the preparation of described step (2) Gypsum Fibrosum one-level slurry is that Gypsum Fibrosum powder and described epoxy glue are mixed according to weight ratio 1:0.6, and then adding water to be stirred well to Baume degrees is 85-95
°be, obtains Gypsum Fibrosum primary amine.
6. the preparation method of a kind of Gypsum Fibrosum facial film according to claim 5, it is characterized in that: the preparation of described step (3) Gypsum Fibrosum secondary slurry is that described Gypsum Fibrosum primary amine, described epoxy glue and water are mixed according to mass ratio 10:6:1, stir 20-50min, obtain Gypsum Fibrosum secondary glue.
7. the preparation method of a kind of Gypsum Fibrosum facial film according to claim 6, it is characterized in that: described step (4) selvage guide specifically hangs gauze to import by selvage guide bucket, through tension adjustment frame and selvage guide cylinder, without crape, send into Gypsum Fibrosum distribution machine center position by gauze is straight; After start, open blowing lock, Gypsum Fibrosum secondary slurry is introduced and fed stock tank; Make gauze enter pincers, and open the even starching of feeding valve, driving starching be speed of a motor vehicle 9-12m/min.
8. the preparation method of a kind of Gypsum Fibrosum facial film according to claim 7, is characterized in that: described gauze is the strip gauze that has been made into facial film shape.
9. the preparation method of a kind of Gypsum Fibrosum facial film according to claim 8, is characterized in that: described bake out temperature is 120-150 ℃.
10. the preparation method of a kind of Gypsum Fibrosum facial film according to claim 8, it is characterized in that: described oven dry is that microwave vacuum is dried, specifically plaster gauze is put into microwave vacuum tank, then carry out evacuation process to vacuum be-0.05MPa～-0.03MPa; Carry out microwave treatment, microwave frequency is 150MHz～240MHz again, and microwave treatment time is 2～5min.
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| CN106176256A (en) * | 2016-07-21 | 2016-12-07 | 山东大学（威海） | A kind of preparation method of facial film |
| CN106606421A (en) * | 2015-10-21 | 2017-05-03 | 恩客斯有限公司 | Manufacturing method for gypsum skincare mask using gypsum skincare cloth, and gypsum skincare mask thereof |
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| CN107961182A (en) * | 2017-12-05 | 2018-04-27 | 浙江和也健康科技有限公司 | A kind of preparation process of konjaku biomass facial mask |
| CN108705660A (en) * | 2018-08-08 | 2018-10-26 | 沈阳甲克素科技有限公司 | Novel gypsum health care physical therapy device, preparation process and physical therapy device manufacturing mold |
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| CN107961182A (en) * | 2017-12-05 | 2018-04-27 | 浙江和也健康科技有限公司 | A kind of preparation process of konjaku biomass facial mask |
| CN108705660A (en) * | 2018-08-08 | 2018-10-26 | 沈阳甲克素科技有限公司 | Novel gypsum health care physical therapy device, preparation process and physical therapy device manufacturing mold |
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