CN106176256B - A kind of preparation method of facial mask - Google Patents
A kind of preparation method of facial mask Download PDFInfo
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- CN106176256B CN106176256B CN201610584405.3A CN201610584405A CN106176256B CN 106176256 B CN106176256 B CN 106176256B CN 201610584405 A CN201610584405 A CN 201610584405A CN 106176256 B CN106176256 B CN 106176256B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a kind of preparation methods of facial mask, this method includes after the facial mask liquid or Essence that will be free of preservative modulate, it will be in its filling facial mask bag containing mask carriers, the facial mask bag is put into microwave vacuum dryer after filling and carries out micro-wave vacuum, after the water content of facial mask in facial mask bag reaches setting value, stop drying, vacuum seal then is carried out to the facial mask bag, obtains finished product.The technology that facial mask preparation method of the invention is combined using micro-wave vacuum with vacuum packaging, can obtain preservative free, facial mask sterile and containing high active ingredient by the preparation method.
Description
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of preparation method of facial mask.
Background technique
With the development of the global economy with the raising of living standards of the people and total quality, more and more people start to make
It applies some make up, especially for the daily nursing of face skin, and with the development of society, people require also to get over to cosmetics
Come it is higher, people more want using have preferably activity and preservative free cosmetics.In existing cosmetics, make in addition to daily
Creams class cosmetics, facial mask are also a kind of daily required product of face skin nursing.The form of facial mask mainly has mud cream
Type, tear-pull, gel-type, four kinds of hygenic towelette type.Hygenic towelette formula is generally exactly the face paper for infiltrating Essence of mmic package,
It is divided by material: non-woven fabrics, silk, cotton, terylene, blended, tencel, biological fiber etc..Hygenic towelette type facial mask is application method
It is most simple, and have the characteristics that nutrition distribution pattern is uniform, so such facial mask is the most wide a kind of facial mask of use scope.
Common facial mask mainly has the function of cleaning, replenishing water and preserving moisture, whitening, the old, Sage Extract of removing wrinkle and resisting aging etc. in the market,
These facial masks inevitably introduce certain amount by many aspects such as raw material, ingredient, packaging materials in process of production
Microorganism, protein inherently rich in, polysaccharide, oligosaccharides, the vitamin etc. in facial mask essence easily cause in addition
The ingredient of microbial reproduction, this is easy to cause bacterium mass propagation in facial mask, from causing the rotten of facial mask.Therefore in facial mask
Different types of preservative will be added in production process to inhibit the breeding of microorganism or kill microorganism.In cosmetics
The use of preservative main function is to prevent microorganism from growing in the product, keeps the property of skin care item stable and use of uncapping
After be unlikely to deteriorate.The more skin care item of moisture more need preservative.
In addition, more and more active constituents are used for facial mask class product with the progress of science and technology, life is specifically included that
Long factor type, activated protein class, active peptides class, vitamins and some Polyphenols have the substance of antioxidant activity.This
A little substances are easy to lose activity in hygenic towelette type facial mask.Therefore a kind of in exploitation to be free of preservative, and activity therein at
The facial mask being unlikely to deteriorate and high production efficiency is divided to be extremely important the development of mask product.
Summary of the invention
The present invention for existing hygenic towelette type facial mask generally contain preservative and cannot add mutability it is (rotten) it is active at
Point deficiency, a kind of new preparation process of facial mask is provided, preservative free can be obtained by this preparation method, it is sterile and containing height
The facial mask of active constituent, this facial mask have processing technology simple, and production cost is low, high production efficiency, and consumer is acceptant
The advantages that.
The invention adopts the following technical scheme:
A kind of preparation method of facial mask, comprising the following steps:
By the facial mask liquid without preservative or after Essence modulates, by its filling facial mask bag containing mask carriers,
The facial mask bag is put into microwave vacuum dryer after filling and carries out micro-wave vacuum, to the facial mask in facial mask bag
Water content reach setting value after, stop drying, then to the facial mask bag carry out vacuum seal, obtain finished product.
Preferably, contain growth factor class, activated protein class, active peptides class, vitamin in the facial mask liquid or Essence
Class, polyphenols or other substances with antioxidant activity function.From the point of view of the using effect of facial mask, preparation of the invention
Method, which is more suitable, prepares the facial mask containing the above active material.
Preferably, the facial mask liquid or Essence can be commercially available conventional facial mask liquid or Essence, be also possible to containing
The facial mask liquid or Essence of the ingredients of high activities mutability such as EGF (epidermal growth factor) are also possible to easy containing vitamin C etc.
Perhaps Essence is also possible to the facial mask liquid or Essence of the ingredient apt to deteriorate such as juice to the facial mask liquid of oxidizing component.This
The facial mask liquid or Essence of three kinds of ingredients after method is especially suitable for.
Preferably, the facial mask liquid or Essence contain macromolecular water conservation substance, and it includes transparent which, which is retained substance,
Matter acid, oat polysaccharide, collagen, sodium alginate, xanthan gum etc. are one such or a variety of.Preparation method of the invention is more suitable
Facial mask of the preparation containing these macromolecular substances is closed, rate of drying is than very fast, and cost is relatively low, high production efficiency.
Preferably, after micro-wave vacuum, the water content (mass fraction) of the facial mask is less than or equal to 3%, contains with this
The facial mask of water can not only extend its shelf-life, can keep sterile, additionally it is possible to after its fast rehydrating, keep its compared with
The active constituent of high-content.Water content of membrane is greater than 3% face to face, and the activity of the active material in facial mask is lower.
Preferably, the mask carriers be non-woven fabrics, silk, cotton, terylene, blended, tencel, biological fiber or other often
Face-mask material.
Preferably, the facial mask bag is aluminium foil bag or the composite facial mask bag based on aluminium foil bag.
Preferably, the facial mask liquid in each facial mask bag or the loading amount of Essence are 20~30mL, and facial mask liquid or Essence are rigid
It is impregnated with face paper well without water clock.
Preferably, in order to enable mask carriers can equably load more nutritional ingredients or active constituent, the face
It is 5 degree of -20 degree that film bag, which is put into the gradient in microwave vacuum dryer,.
Preferably, the temperature of the micro-wave vacuum is 30-50 DEG C.
Preferably, the vacuum degree of the micro-wave vacuum are as follows: -0.1MPa ﹤ Zhen Kong Du≤- 0.09MPa, preferably -
0.09MPa, intermittently than 3:1, preferably microwave operational 15s, interval 5s, microwave power 18-25W/g (quality be facial mask liquid or
The quality of Essence).The selection of interval ratio is extremely important, and inappropriate interval increases than not only energy consumption, but also be easy to cause office
Portion's temperature is excessively high, then facial mask and facial mask bag can be made to be charred, influence the activity of active constituent in facial mask.The higher drying effect of vacuum degree
Better, the present invention is directed to this special raw material of facial mask, using the vacuum degree to match above, intermittently compares and microwave power.
Application method: product pours into 20-30ml pure water or sterile water in use, only need to open packaging, places 3-
5min, facial mask will rapid rehydration, then by facial mask apply carry out normal skin nursing on the skin.
Preferably, it is sealed after facial mask is dry using vacuum sealer, vacuum degree is less than 1000Pa.
Preferably, above-mentioned production stage is completed in the case where cleanliness is 100,000 grades of environment.
The present invention also provides a kind of facial mask being prepared using the above method, contain growth factor class, work in the facial mask
Property protide, active peptides class, vitamins, polyphenols or other substances with antioxidant activity function.
A technical solution in above-mentioned technical proposal has the following beneficial effects:
(1) technology that facial mask preparation method of the invention is combined using micro-wave vacuum with vacuum packaging, wherein micro-
Wave vacuum drying technique has many advantages, such as that dry yield is high, high-quality, processing cost is low, while can accurately control moisture, this
Oxygen content is low when dry under external low-temp low-pressure, and the oxidation reaction decrease of the ingredient in facial mask slows down, to ensure that in facial mask
Effective component activity;Vacuum-packed technique can reduce facial mask bag internal oxygen Gas content, to improve effective component in facial mask
Activity.Preservative free, facial mask sterile and containing high active ingredient can be obtained by the preparation method.
(2) the present invention provides a kind of completely new facial mask form, which is a kind of vacuum-packed face paper, is made
The facial mask wide variety in cosmetics is obtained, this is extremely important to the development of facial mask.
(3) present invention selects microwave vacuum drying technology that facial mask is dried, and use according to the characteristic of facial mask
The drying temperature and vacuum degree and microwave intensity to match makes the water content for having less than or equal to 3% after facial mask is dry, has
The facial mask of the water content can not only extend its shelf-life, can keep sterile, additionally it is possible to after its fast rehydrating, keep
The active constituent of its high level.
(4) technology that the present invention is combined using vacuum packaging with microwave vacuum drying technology, can preferably realize and prolong
The shelf-life of mutability or oxidizable ingredient and the effect without using preservative in long facial mask.In addition, using vacuum packaging
Technology can also make facial mask liquid or the better uniform load of Essence on carrier, thus in use, can lock after rehydration
More nutritional ingredient and active constituent etc..
(5) facial mask processing technology of the invention is simple, and high production efficiency, cost is relatively low, and facial mask bag is directly placed into microwave
In vacuum dryer, additional packaging material sterilization steps etc. are not needed, production efficiency is improved.
Detailed description of the invention
Fig. 1: the cell activity of the facial mask containing EGF after room temperature storage 1 year.
Specific embodiment
Below with reference to embodiment, the present invention is further illustrated:
Production and its sanitary index detection of the embodiment 1 without the common Essence facial mask of preservative
After being modulated without preservative Essence, is poured into the facial mask bag containing mask carriers, be sufficiently impregnated, often
A facial mask bag pours into Essence 25ml, and 15 degree of the inclination of facial mask bag are put into microwave vacuum dryer after filling and carries out microwave
Vacuum drying controls temperature between 30-50 DEG C, and vacuum degree is -0.09MPa, intermittently than 3:1, microwave operational 15s, interval 5s,
Microwave power is 18W/g, after the completion of drying (2% mass percent of facial mask water content), is sealed using vacuum sealer, so that face
Vacuum degree in film bag is less than 1000Pa to get finished product.
Comparative example 1
After being modulated without preservative Essence, is poured into the facial mask bag containing mask carriers, be sufficiently impregnated, often
A facial mask bag pours into Essence 25ml, and 15 degree of the inclination of facial mask bag are put into vacuum freeze drier after filling and carries out vacuum
Freeze-drying, controlled at -65 DEG C, (2% mass percent of facial mask water content) is after the completion of freeze-drying to get finished product.
Comparative example 2
After being modulated without preservative Essence, is poured into the facial mask bag containing mask carriers, be sufficiently impregnated, often
A facial mask bag pours into Essence 25ml, and 15 degree of the inclination of facial mask bag are put into microwave vacuum dryer after filling and carries out microwave
Vacuum drying controls temperature between 30-50 DEG C, and vacuum degree is -0.09MPa, intermittently than 3:1, microwave operational 15s, interval 5s,
Microwave power is 18W/g, after the completion of drying (5% mass percent of facial mask water content), is sealed using vacuum sealer, so that face
Vacuum degree in film bag is less than 1000Pa to get finished product.
After finished product in embodiment 1, comparative example 1 and comparative example 2 is placed at room temperature for 3 years, according in GB/T 7918.1-87
Total plate count in the detection method measurement product of total plate count, testing result are as follows:
Table 1 is free of preservative facial mask total number of bacteria measurement result
Can be seen that the facial mask produced by the method for the invention even if not adding preservative agent from the testing result of table 1 can be steady
Surely 3 years are saved without microbial contamination, meets national cosmetic sanitary index, and the facial mask of Vacuum Freezing & Drying Technology production
And the total number of bacteria in 2 facial mask of comparative example is higher than the total number of bacteria of the facial mask in embodiment 1.
The production of 2 facial mask containing EGF of embodiment and its Activity determination
After facial mask liquid (20ng/ml containing EGF) containing EGF is modulated, the facial mask bag containing mask carriers is poured into
It is interior, it is sufficiently impregnated, each facial mask bag pours into Essence 20ml, is put into microwave vacuum for 20 degree of the inclination of facial mask bag after filling and does
Micro-wave vacuum is carried out in dry machine, controls temperature between 30-40 DEG C, vacuum degree is -0.09MPa, intermittently than 3:1, microwave
Work 15s, interval 5s, microwave power 20W/g, after the completion of drying (1% mass percent of facial mask water content), using vacuum seal
Mouth machine sealing, so that the vacuum degree in facial mask bag is less than 1000Pa to get finished product.
After finished product is placed at room temperature for 1 year, according to EGF activity determination method in pharmacopeia, using fibroblast testing product
Promote the activity of cell Proliferation, using 20ng/ml EGF as positive control, testing result is as shown in Figure 1.
From figure 1 it appears that the facial mask prepared through the invention, after room temperature storage 1 year, EGF still retains higher
Activity, can effectively facilitate fibroblast proliferation, and common facial mask is (production method with micro-wave vacuum facial mask, only
Without micro-wave vacuum) illustrate that this production method can effectively extend the shelf-life of product, keep product in mutability at
The activity divided.
The production of 3 facial mask containing vitamin C of embodiment and its oxidation resistance detection
It will contain after ascorbic facial mask liquid (ascorbic mass percent be 2%) modulates, be poured into containing face
It in the facial mask bag of membrane carrier, is sufficiently impregnated, each facial mask bag pours into Essence 30ml, and facial mask bag tilted 18 degree after filling
It being put into microwave vacuum dryer and carries out micro-wave vacuum, control temperature between 30-40 DEG C, vacuum degree is -0.09MPa,
Interval is than 3:1, microwave operational 15s, interval 5s, microwave power 22W/g, (2% mass percentage of facial mask water content after the completion of drying
Than), it is sealed using vacuum sealer, so that the vacuum degree in facial mask bag is less than 1000Pa to get finished product.
Comparative example 3
It will contain after ascorbic facial mask liquid (ascorbic mass percent be 2%) modulates, be poured into containing face
It in the facial mask bag of membrane carrier, is sufficiently impregnated, each facial mask bag pours into Essence 30ml, and facial mask bag tilted 18 degree after filling
It being put into microwave vacuum dryer and carries out micro-wave vacuum, control temperature between 30-40 DEG C, vacuum degree is -0.09MPa,
Interval is than 3:1, microwave operational 15s, interval 5s, microwave power 22W/g, (2% mass percentage of facial mask water content after the completion of drying
Than), it is sealed using the conventional method of facial mask to get finished product.
Comparative example 4
It will contain after ascorbic facial mask liquid (ascorbic mass percent be 2%) modulates, be poured into containing face
It in the facial mask bag of membrane carrier, is sufficiently impregnated, each facial mask bag pours into Essence 30ml, and facial mask bag tilted 18 degree after filling
It being put into microwave vacuum dryer and carries out micro-wave vacuum, control temperature between 30-40 DEG C, vacuum degree is -0.09MPa,
Interval is than 3:1, microwave operational 15s, interval 5s, microwave power 22W/g, (5% mass percentage of facial mask water content after the completion of drying
Than), it is sealed using vacuum sealer, so that the vacuum degree in facial mask bag is less than 1000Pa to get finished product.
After finished product facial mask is placed at room temperature for 2 years, packaging plus 30ml pure water are opened, places 5min, with fresh configuration containing dimension
It is control that raw element C mass percent, which is 2% facial mask liquid, and it is ascorbic to measure reduced form therein using 2,6- dichloroindophenol method
Content, measurement result show: Vc content is 1.95% in the facial mask liquid of fresh configuration, in the embodiment 1 for being placed at room temperature for 2 years
Vc content is 1.80% in facial mask, and the facial mask Vc content in comparative example 3 is 1.2%, and the facial mask Vc content in comparative example 4 is
1.4%.The facial mask of the method for the present invention preparation has preferable protective effect to reduced ascorbic acid as can be seen from the above results, can be with
The oxidation saved for a long time without causing Vc.
The production of 4 juice facial mask containing fruits and vegetables of embodiment
After facial mask liquid containing juice is modulated, is poured into the facial mask bag containing mask carriers, be sufficiently impregnated, often
A facial mask bag pours into Essence 25ml, and 25 degree of the inclination of facial mask bag are put into microwave vacuum dryer after filling and carries out microwave
Vacuum drying controls temperature between 30-50 DEG C, and vacuum degree is -0.09MPa, intermittently than 3:1, microwave operational 15s, interval 5s,
Microwave power is 25W/g, after the completion of drying (1% mass percent of facial mask water content), is sealed using vacuum sealer, so that face
Vacuum degree in film bag is less than 1000Pa to get finished product.Juice active constituent in the finished product fine can must retain, finished product
Long shelf-life.
The production of the water conservation substance facial mask containing macromolecular of embodiment 5
After facial mask liquid (20ng/ml containing EGF) containing EGF and hyaluronic acid, oat polysaccharide is modulated, is poured into and contained
Have in the facial mask bag of mask carriers, be sufficiently impregnated, each facial mask bag pours into Essence 20ml, tilts facial mask bag after filling
25 degree are put into microwave vacuum dryer and carry out micro-wave vacuum, control temperature between 40-50 DEG C, and vacuum degree is-
0.09MPa, intermittently than 3:1, microwave operational 15s, interval 5s, microwave power 22W/g, (facial mask water content 1% after the completion of drying
Mass percent), it is sealed using vacuum sealer, so that the vacuum degree in facial mask bag is less than 1000Pa to get finished product.This implementation
The preparation method of example is more suitable for preparing the facial mask containing macromolecular water conservation substance, and rate of drying is than very fast, and cost is relatively low, production effect
Rate is high.
The application method of facial mask of the present invention: product pours into 20-30ml pure water or nothing in use, only need to open packaging
Bacterium water, place 3-5min, facial mask will rapid rehydration, then by facial mask apply carry out normal skin nursing on the skin.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention,
It should be equivalent substitute mode, be included within the scope of the present invention.
Claims (7)
1. a kind of preparation method of facial mask, it is characterized in that: being filled after the facial mask liquid for being free of preservative or Essence are modulated
Fill the facial mask bag containing mask carriers in, it is filling after by the facial mask bag be put into microwave vacuum dryer carry out microwave it is true
Sky is dry, after the water content of the facial mask in facial mask bag reaches setting value, stops drying, after micro-wave vacuum, the face
The water content of film is less than or equal to 3%, then carries out vacuum seal to the facial mask bag, obtains finished product;
Contain epidermal growth factor or vitamin C or juice in the facial mask liquid or Essence;Alternatively,
The facial mask liquid or Essence contain macromolecular water conservation substance, and macromolecular water conservation substance includes that hyaluronic acid, oat are more
Sugar, collagen, sodium alginate, xanthan gum it is one or more;
The temperature of the micro-wave vacuum is 30-50 DEG C, the vacuum degree of the micro-wave vacuum are as follows: -0.1MPa ﹤ vacuum degree
≤ -0.09MPa, intermittently than 3:1, microwave power 18-25W/g;
Above-mentioned production stage is completed in the case where cleanliness is 100,000 grades of environment.
2. preparation method as described in claim 1, it is characterized in that: the mask carriers be non-woven fabrics, silk, cotton, terylene,
Blended, tencel, biological fiber or other common face-mask materials.
3. preparation method as described in claim 1, it is characterized in that: facial mask bag is put into the gradient in microwave vacuum dryer is
5 degree of -20 degree.
4. preparation method as described in claim 1, it is characterized in that: the loading amount of facial mask liquid or Essence in each facial mask bag is
20~30mL.
5. preparation method as described in claim 1, it is characterized in that: being sealed after facial mask is dry using vacuum sealer, vacuum degree
Less than 1000Pa.
6. the facial mask being prepared using method according to any one of claims 1 to 5.
7. facial mask as claimed in claim 6, it is characterized in that: the water content of the facial mask is less than or equal to 3%.
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CN107440923A (en) * | 2017-08-08 | 2017-12-08 | 何维 | A kind of sterile reparation facial mask of anti-aging |
CN108578301A (en) * | 2018-07-24 | 2018-09-28 | 高昕文 | A kind of pro-skin is retained the preparation method of anti-back suction facial mask |
CN110946768B (en) * | 2018-09-26 | 2022-08-19 | 森田生医股份有限公司 | Biological fiber dry mask and drying method thereof |
CN109276457A (en) * | 2018-11-28 | 2019-01-29 | 大连美图生物科技有限公司 | It is a kind of to contain the facial mask film cloth and preparation method thereof for solidifying essence |
CN110251420A (en) * | 2019-07-05 | 2019-09-20 | 广州奥蓓斯化妆品有限公司 | A kind of facial mask and its manufacture craft |
CN113244139A (en) * | 2020-02-11 | 2021-08-13 | 和康生物科技股份有限公司 | Mask base and mask set |
CN112006965A (en) * | 2020-09-02 | 2020-12-01 | 杭州骏远生物科技有限公司 | Preparation process of Chinese herbal medicine mask |
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CN101167691A (en) * | 2007-10-30 | 2008-04-30 | 张定忠 | Method for preparing natural oblongas juice beautifying face pack |
CN102920830A (en) * | 2012-11-28 | 2013-02-13 | 华南师范大学 | Method for effectively extracting polyphenol from Longan seed |
CN103735426A (en) * | 2014-01-09 | 2014-04-23 | 浙江奥林医疗用品有限公司 | Method for preparing gypsum facial mask |
CN104905170A (en) * | 2015-05-15 | 2015-09-16 | 四川食为天农业有限公司 | Production method of freeze-dried active red-heart kiwifruit slices |
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