CN106176256A - A kind of preparation method of facial film - Google Patents
A kind of preparation method of facial film Download PDFInfo
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- CN106176256A CN106176256A CN201610584405.3A CN201610584405A CN106176256A CN 106176256 A CN106176256 A CN 106176256A CN 201610584405 A CN201610584405 A CN 201610584405A CN 106176256 A CN106176256 A CN 106176256A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses the preparation method of a kind of facial film, after the method includes modulating the facial mask liquid without preservative or essence, its fill is contained in the facial film bag of mask carriers, after fill, described facial film bag is put into and microwave vacuum dryer carries out microwave vacuum drying, after the water content of the facial film in facial film bag reaches setting value, stop being dried, then described facial film bag is carried out vacuum seal, obtain finished product.The facial film preparation method of the present invention uses the technology that microwave vacuum drying combines with vacuum packaging, can obtain preservative free by this preparation method, aseptic and contain the facial film of high active ingredient.
Description
Technical field
The present invention relates to cosmetic field, be specifically related to the preparation method of a kind of facial film.
Background technology
Along with the development of global economy and living standards of the people and the raising of total quality, increasing people starts to make
Applying some make up, especially for the daily nursing of face skin, and along with the development of society, cosmetics are required also to get over by people
Coming the highest, people more want to use the cosmetics with the most active and preservative free.In existing cosmetics, make except daily
Cream class cosmetics, facial film is also a kind of daily face skin required product of nursing.The form of facial film mainly has mud cream
Type, tear-pull, gel-type, four kinds of wet paper towel type.Wet paper towel formula is exactly typically the face paper infiltrating essence of mmic package,
It is divided into by material: non-woven fabrics, silkworm silk, cotton, terylene, blending, tencel, biological fiber etc..Wet paper towel profile film is using method
The simplest, and there is the uniform feature of nutrition distribution pattern, so such facial film class facial film that to be range the widest.
Facial film common on market mainly has the functions such as cleaning, replenishing water and preserving moisture, whitening, old, the Sage Extract of removing wrinkle and resisting aging,
These facial films the most inevitably introduce some by many aspects such as raw material, dispensing, packaging material
Microorganism, inherently contain rich in protein, polysaccharide, oligosaccharide, vitamin etc. in facial mask essence easily cause in addition
The composition of microbial reproduction, this is easy to cause antibacterial amount reproduction in facial film, from causing the rotten of facial film.Therefore at facial film
Production process will be added different types of preservative to suppress breeding or the killing microorganisms of microorganism.In cosmetics
Using preservative Main Function is to prevent microorganism from growing in the product, keeps the stable in properties of skin care item and use of uncapping
After be unlikely to deteriorate.The skin care item that moisture is the most more need preservative.
It addition, along with the progress of science and technology, increasing active component is used for facial film series products, specifically includes that life
Long factor type, activated protein class, active polypeptide class, vitamins and some Polyphenols have the material of antioxidant activity.This
A little materials easily lose activity in wet paper towel profile film.Therefore a kind of without preservative in exploitation, and activity therein becomes
The facial film being unlikely to deteriorate and the high development for mask product of production efficiency is divided to be extremely important.
Summary of the invention
The present invention is directed to existing wet paper towel profile film generally contain preservative with can not add changeableness (going bad) activity become
Point deficiency, it is provided that the new preparation process of a kind of facial film, preservative free can be obtained by this preparation method, aseptic and containing height
The facial film of active component, it is simple that this facial film has processing technique, and production cost is low, and production efficiency is high, and consumer is acceptant
Etc. advantage.
The present invention is by the following technical solutions:
The preparation method of a kind of facial film, comprises the following steps:
After facial mask liquid without preservative or essence are modulated, its fill is contained in the facial film bag of mask carriers,
After fill, described facial film bag is put into and microwave vacuum dryer carries out microwave vacuum drying, treat the facial film in facial film bag
Water content reach setting value after, stop be dried, then described facial film bag is carried out vacuum seal, obtains finished product.
Preferably, this facial mask liquid or essence contain somatomedin class, activated protein class, active polypeptide class, vitamin
Class, polyphenols or other there is the material of antioxidant activity function.From the point of view of the using effect of facial film, the preparation of the present invention
Method is more suitable for the preparation facial film containing above active substance.
Preferably, described facial mask liquid or essence can be commercially available conventional facial mask liquid or essence, it is also possible to be containing
The facial mask liquid of the composition of the high activity changeablenesss such as EGF (epidermal growth factor) or essence, it is also possible to be easy containing vitamin C etc.
The facial mask liquid of oxidizing component or essence, it is also possible to be facial mask liquid or the essence of the compositions apt to deteriorate such as fruit and vegetable juice.This
Method is especially suitable for facial mask liquid or the essence of rear three kinds of compositions.
Preferably, described facial mask liquid or essence contain macromole water conservation material, and this macromole water conservation material includes transparent
Matter acid, Herba bromi japonici polysaccharide, collagen protein, sodium alginate, xanthan gum etc. therein one or more.The preparation method of the present invention is suitableeer
Closing the preparation facial film containing these macromolecular substances, rate of drying ratio is very fast, and cost is relatively low, and production efficiency is high.
Preferably, after microwave vacuum drying, the water content (mass fraction) of described facial film is less than or equal to 3%, has this and contains
The facial film of the water yield can not only extend its shelf-life so that it is can keep aseptic, additionally it is possible to after its fast rehydrating, keeps it relatively
The active component of high-load.Water content of membrane is more than 3% face to face, and the activity of the active substance in facial film is the most relatively low.
Preferably, described mask carriers is non-woven fabrics, silkworm silk, cotton, terylene, blending, tencel, biological fiber or other are normal
Face-mask material.
Preferably, described facial film bag is aluminium foil bag or the composite facial mask bag based on aluminium foil bag.
Preferably, facial mask liquid or the loading amount of essence in each facial film bag are 20～30mL, and facial mask liquid or essence are firm
It is impregnated with well face paper and not water clock.
Preferably, so that mask carriers can load more nutritional labeling or active component equably, described
The gradient in microwave vacuum dryer put into by film bag is 5 degree of-20 degree.
Preferably, the temperature of described microwave vacuum drying is 30-50 DEG C.
Preferably, the vacuum of described microwave vacuum drying is :-0.1MPa vacuum-0.09MPa, preferably-
0.09MPa, interval ratio 3:1, preferably microwave operational 15s, intermittently 5s, microwave power 18-25W/g (quality be facial mask liquid or
The quality of essence).Intermittently than selection extremely important, inappropriate interval increases than not only energy consumption, and easily causes office
Portion's temperature is too high, then facial film and facial film bag can be made to be charred, affect the activity of active component in facial film.The highest drying effect of vacuum
The best, the present invention is directed to this special raw material of facial film, use above match vacuum, interval than and microwave power.
Using method: when product uses, it is only necessary to open packaging, pours 20-30ml pure water or sterilized water into, places 3-
5min, facial film will rehydration rapidly, then facial film is applied on skin, carries out normal skin nursing.
Preferably, facial film uses vacuum sealer to seal after drying, and vacuum is less than 1000Pa.
Preferably, above-mentioned production stage completes under cleanliness factor is 100,000 grades of environment.
The present invention also provides for a kind of facial film using said method to prepare, containing somatomedin class, work in this facial film
Property protide, active polypeptide class, vitamins, polyphenols or other there is the material of antioxidant activity function.
A technical scheme in technique scheme has the advantages that
(1) the facial film preparation method of the present invention uses the technology that microwave vacuum drying combines with vacuum packaging, wherein, micro-
Ripple vacuum drying technique has dry yield height, quality is good, processing cost is low, can accurately control the advantages such as moisture simultaneously, this
When being dried under external low-temp low-pressure, oxygen content is low, and the oxidation reaction of the composition in facial film weakens and slows down, thus ensure that in facial film
The activity of effective ingredient；Vacuum-packed technique can reduce facial film bag internal oxygen Gas content, thus improves effective ingredient in facial film
Activity.Preservative free can be obtained, aseptic and facial film containing high active ingredient by this preparation method.
(2) the invention provides a kind of brand-new facial film form, this mask product is a kind of vacuum-packed face paper, makes
Obtaining the facial film wide variety in cosmetics, the development of facial film is extremely important by this.
(3) present invention is according to the characteristic of facial film, selects microwave vacuum drying technology to be dried by facial film, and have employed
The baking temperature matched and vacuum and microwave intensity, make facial film have the water content less than or equal to 3% after drying, have
The facial film of this water content can not only extend its shelf-life so that it is can keep aseptic, additionally it is possible to after its fast rehydrating, keeps
The active component of its high level.
(4) present invention uses the technology that vacuum packaging combines with microwave vacuum drying technology, can preferably realize prolonging
Changeableness or the shelf-life of oxidizable composition and do not use the effect of preservative in long facial film.It addition, use vacuum packaging
Technology can also make facial mask liquid or the more preferable uniform load of essence on carrier, thus after rehydration use time, can lock
More nutritional labeling and active component etc..
(5) the facial film processing technique of the present invention is simple, and production efficiency is high, and cost is relatively low, and facial film bag is directly placed into microwave
In vacuum dryer, it is not necessary to extra packaging material sterilization steps etc., improve production efficiency.
Accompanying drawing explanation
Fig. 1: room temperature storage contains the cytoactive of EGF facial film after 1 year.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated:
Embodiment 1 does not contains making and the sanitary index detection thereof of preservative common essence facial film
After modulating without preservative essence, poured in the facial film bag containing mask carriers, be sufficiently impregnated with, often
Individual facial film bag pours into essence 25ml, facial film bag inclination 15 degree is put into and carry out microwave in microwave vacuum dryer after fill
Vacuum drying, control temperature is between 30-50 DEG C, and vacuum is-0.09MPa, interval ratio 3:1, microwave operational 15s, intermittently 5s,
Microwave power is 18W/g, after being dried (facial film water content 2% mass percent), uses vacuum sealer sealing so that face
Vacuum in film bag is less than 1000Pa, gets product.
Comparative example 1
After modulating without preservative essence, poured in the facial film bag containing mask carriers, be sufficiently impregnated with, often
Individual facial film bag pours into essence 25ml, facial film bag inclination 15 degree is put into and carry out vacuum in vacuum freeze drier after fill
Lyophilization, controls temperature and is-65 DEG C, after lyophilizing completes (facial film water content 2% mass percent), get product.
Comparative example 2
After modulating without preservative essence, poured in the facial film bag containing mask carriers, be sufficiently impregnated with, often
Individual facial film bag pours into essence 25ml, facial film bag inclination 15 degree is put into and carry out microwave in microwave vacuum dryer after fill
Vacuum drying, control temperature is between 30-50 DEG C, and vacuum is-0.09MPa, interval ratio 3:1, microwave operational 15s, intermittently 5s,
Microwave power is 18W/g, after being dried (facial film water content 5% mass percent), uses vacuum sealer sealing so that face
Vacuum in film bag is less than 1000Pa, gets product.
After finished product room temperature in embodiment 1, comparative example 1 and comparative example 2 is placed 3 years, according in GB/T 7918.1-87
The detection method of total plate count measures total plate count in product, and testing result is as follows:
Table 1 is without preservative facial film total number of bacteria measurement result
Even if from the testing result of table 1 it can be seen that not adding preservative agent, the facial film produced by the inventive method can be steady
Surely preserve 3 years and do not have microorganism to pollute, meet national cosmetic sanitary index, and the facial film of Vacuum Freezing & Drying Technology production
And the total number of bacteria in comparative example 2 facial film is higher than the total number of bacteria of the facial film in embodiment 1.
Embodiment 2 contains making and the Activity determination thereof of EGF facial film
After facial mask liquid (containing EGF 20ng/ml) containing EGF being modulated, poured into the facial film bag containing mask carriers
In, it being sufficiently impregnated with, each facial film bag pours into essence 20ml, after fill, facial film bag inclination 20 degree is put into microwave vacuum and does
Carrying out microwave vacuum drying in dry machine, control temperature is between 30-40 DEG C, and vacuum is-0.09MPa, interval ratio 3:1, microwave
Work 15s, intermittently 5s, microwave power is 20W/g, after being dried (facial film water content 1% mass percent), uses vacuum seal
Mouth machine sealing so that the vacuum in facial film bag is less than 1000Pa, gets product.
After finished product room temperature is placed 1 year, according to EGF activity determination method in pharmacopeia, use fibroblast detection product
Promoting the activity of cell proliferation, using 20ng/ml EGF as positive control, testing result is as shown in Figure 1.
From figure 1 it appears that the facial film prepared by the present invention, room temperature storage is after 1 year, and it is higher that EGF still retains
Activity, can effectively facilitate fibroblast proliferation, and common facial film is (manufacture method with microwave vacuum drying facial film, simply
Do not carry out microwave vacuum drying) illustrate that this manufacture method can effectively extend the shelf-life of product, keep changeableness in product to become
The activity divided.
Embodiment 3 contains making and the oxidation resistance detection thereof of vitamin C facial film
To contain after ascorbic facial mask liquid (ascorbic mass percent is 2%) modulates, be poured into containing face
In the facial film bag of membrane carrier, being sufficiently impregnated with, each facial film bag pours into essence 30ml, after fill, facial film bag is tilted 18 degree
Putting into and carry out microwave vacuum drying in microwave vacuum dryer, control temperature is between 30-40 DEG C, and vacuum is-0.09MPa,
Interval ratio 3:1, microwave operational 15s, intermittently 5s, microwave power is 22W/g, (facial film water content 2% percent mass after being dried
Than), use vacuum sealer sealing so that the vacuum in facial film bag is less than 1000Pa, gets product.
Comparative example 3
To contain after ascorbic facial mask liquid (ascorbic mass percent is 2%) modulates, be poured into containing face
In the facial film bag of membrane carrier, being sufficiently impregnated with, each facial film bag pours into essence 30ml, after fill, facial film bag is tilted 18 degree
Putting into and carry out microwave vacuum drying in microwave vacuum dryer, control temperature is between 30-40 DEG C, and vacuum is-0.09MPa,
Interval ratio 3:1, microwave operational 15s, intermittently 5s, microwave power is 22W/g, (facial film water content 2% percent mass after being dried
Than), use the conventional method sealing of facial film, get product.
Comparative example 4
To contain after ascorbic facial mask liquid (ascorbic mass percent is 2%) modulates, be poured into containing face
In the facial film bag of membrane carrier, being sufficiently impregnated with, each facial film bag pours into essence 30ml, after fill, facial film bag is tilted 18 degree
Putting into and carry out microwave vacuum drying in microwave vacuum dryer, control temperature is between 30-40 DEG C, and vacuum is-0.09MPa,
Interval ratio 3:1, microwave operational 15s, intermittently 5s, microwave power is 22W/g, (facial film water content 5% percent mass after being dried
Than), use vacuum sealer sealing so that the vacuum in facial film bag is less than 1000Pa, gets product.
After finished product facial film room temperature is placed 2 years, open packaging and add 30ml pure water, place 5min, tie up with containing of fresh configuration
Raw element C mass percent be 2% facial mask liquid be comparison, use 2, it is ascorbic that 6-dichloroindophenol method measures reduced form therein
Content, measurement result shows: in the facial mask liquid of fresh configuration, Vc content is 1.95%, and room temperature is placed in the embodiment 1 of 2 years
In facial film, Vc content is 1.80%, and the facial film Vc content in comparative example 3 is 1.2%, and the facial film Vc content in comparative example 4 is
1.4%.The facial film that as can be seen from the above results prepared by the inventive method has preferable protective effect to reduced ascorbic acid, permissible
Preserve without the oxidation causing Vc for a long time.
The embodiment 4 making containing fruit and vegetable juice facial film
After facial mask liquid containing fruit and vegetable juice is modulated, poured in the facial film bag containing mask carriers, be sufficiently impregnated with, often
Individual facial film bag pours into essence 25ml, facial film bag inclination 25 degree is put into and carry out microwave in microwave vacuum dryer after fill
Vacuum drying, control temperature is between 30-50 DEG C, and vacuum is-0.09MPa, interval ratio 3:1, microwave operational 15s, intermittently 5s,
Microwave power is 25W/g, after being dried (facial film water content 1% mass percent), uses vacuum sealer sealing so that face
Vacuum in film bag is less than 1000Pa, gets product.Fruit and vegetable juice active component in this finished product can fine must retain, finished product
Long shelf-life.
The embodiment 5 making containing macromole water conservation material facial film
After facial mask liquid (containing EGF 20ng/ml) containing EGF and hyaluronic acid, Herba bromi japonici polysaccharide is modulated, poured into and contained
In having the facial film bag of mask carriers, being sufficiently impregnated with, each facial film bag pours into essence 20ml, is tilted by facial film bag after fill
To put into for 25 degree and microwave vacuum dryer carries out microwave vacuum drying, control temperature between 40-50 DEG C, vacuum is-
0.09MPa, interval ratio 3:1, microwave operational 15s, intermittently 5s, microwave power is 22W/g, (facial film water content 1% after being dried
Mass percent), use vacuum sealer sealing so that the vacuum in facial film bag is less than 1000Pa, gets product.This enforcement
The preparation method of example is more suitable for the preparation facial film containing macromole water conservation material, and rate of drying ratio is very fast, and cost is relatively low, produces effect
Rate is high.
The using method of facial film of the present invention: when product uses, it is only necessary to open packaging, pour 20-30ml pure water or nothing into
Bacterium water, places 3-5min, facial film will rehydration rapidly, then facial film is applied on skin, carries out normal skin nursing.
Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention are not by above-described embodiment
Limit, the change made under other any spirit without departing from the present invention and principle, modify, substitute, combine, simplify,
All should be the substitute mode of equivalence, within being included in protection scope of the present invention.
Claims (10)
1. a preparation method for facial film, is characterized in that: after the facial mask liquid without preservative or essence being modulated, filled
Described facial film bag containing in the facial film bag of mask carriers, is put into after fill that to carry out microwave in microwave vacuum dryer true by dress
Empty it is dried, after the water content of the facial film in facial film bag in reaches setting value, stops dry, then described facial film bag is carried out very
Empty sealing, obtains finished product.
2. preparation method as claimed in claim 1, is characterized in that: containing somatomedin class, work in this facial mask liquid or essence
Property protide, active polypeptide class, vitamins, polyphenols or other there is the material of antioxidant activity function.
3. preparation method as claimed in claim 1, is characterized in that: in this facial mask liquid or essence containing epidermal growth factor or
Person's vitamin C or fruit and vegetable juice.
4. preparation method as claimed in claim 1, is characterized in that: described facial mask liquid or essence contain macromole water conservation thing
Matter, this macromole water conservation material includes hyaluronic acid, Herba bromi japonici polysaccharide, collagen protein, sodium alginate, the one of xanthan gum or many
Kind.
5. preparation method as claimed in claim 1, is characterized in that: described mask carriers be non-woven fabrics, silkworm silk, cotton, terylene,
Blending, tencel, biological fiber or other conventional face-mask materials；Preferred: inclining in microwave vacuum dryer put into by facial film bag
Gradient is 5 degree of-20 degree；Preferably, the loading amount of the facial mask liquid in each facial film bag or essence is 20 ~ 30mL.
6. preparation method as claimed in claim 1, is characterized in that: the temperature of described microwave vacuum drying is 30-50 DEG C.
7. preparation method as claimed in claim 1, is characterized in that: the vacuum of described microwave vacuum drying is :-0.1MPa
Vacuum-0.09MPa, interval ratio 3:1, microwave power is 18-25W/g.
8. profit requires the preparation method described in 1, it is characterized in that: facial film uses vacuum sealer to seal after drying, and vacuum is less than
1000Pa。
9. use the facial film that the method according to any one of claim 1 ~ 8 prepares.
10. facial film as claimed in claim 9, is characterized in that: the water content of described facial film is less than or equal to 3%.
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| CN201610584405.3A CN106176256B (en) | 2016-07-21 | 2016-07-21 | A kind of preparation method of facial mask |
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| CN201610584405.3A CN106176256B (en) | 2016-07-21 | 2016-07-21 | A kind of preparation method of facial mask |
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| CN106176256B CN106176256B (en) | 2019-02-26 |
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Cited By (7)
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| CN107440923A (en) * | 2017-08-08 | 2017-12-08 | 何维 | A kind of sterile reparation facial mask of anti-aging |
| CN108578301A (en) * | 2018-07-24 | 2018-09-28 | 高昕文 | A kind of pro-skin is retained the preparation method of anti-back suction facial mask |
| CN109276457A (en) * | 2018-11-28 | 2019-01-29 | 大连美图生物科技有限公司 | It is a kind of to contain the facial mask film cloth and preparation method thereof for solidifying essence |
| CN110251420A (en) * | 2019-07-05 | 2019-09-20 | 广州奥蓓斯化妆品有限公司 | A kind of facial mask and its manufacture craft |
| CN110946768A (en) * | 2018-09-26 | 2020-04-03 | 森田生医股份有限公司 | Biological fiber dry facial mask and drying method thereof |
| CN112006965A (en) * | 2020-09-02 | 2020-12-01 | 杭州骏远生物科技有限公司 | Preparation process of Chinese herbal medicine mask |
| CN113244139A (en) * | 2020-02-11 | 2021-08-13 | 和康生物科技股份有限公司 | Mask base and mask set |
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| CN110946768A (en) * | 2018-09-26 | 2020-04-03 | 森田生医股份有限公司 | Biological fiber dry facial mask and drying method thereof |
| CN110946768B (en) * | 2018-09-26 | 2022-08-19 | 森田生医股份有限公司 | Biological fiber dry mask and drying method thereof |
| CN109276457A (en) * | 2018-11-28 | 2019-01-29 | 大连美图生物科技有限公司 | It is a kind of to contain the facial mask film cloth and preparation method thereof for solidifying essence |
| CN110251420A (en) * | 2019-07-05 | 2019-09-20 | 广州奥蓓斯化妆品有限公司 | A kind of facial mask and its manufacture craft |
| CN113244139A (en) * | 2020-02-11 | 2021-08-13 | 和康生物科技股份有限公司 | Mask base and mask set |
| CN112006965A (en) * | 2020-09-02 | 2020-12-01 | 杭州骏远生物科技有限公司 | Preparation process of Chinese herbal medicine mask |
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| CN106176256B (en) | 2019-02-26 |
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