CN106074217B - Body temperature is moulded into type skin caring material and skin nursing film and preparation method certainly - Google Patents
Body temperature is moulded into type skin caring material and skin nursing film and preparation method certainly Download PDFInfo
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- CN106074217B CN106074217B CN201610383052.0A CN201610383052A CN106074217B CN 106074217 B CN106074217 B CN 106074217B CN 201610383052 A CN201610383052 A CN 201610383052A CN 106074217 B CN106074217 B CN 106074217B
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8129—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
It is moulded into type skin caring material certainly the present invention relates to a kind of body temperature in the skin nursing products such as facial mask, eye mask, lip film and body temperature is moulded into type skin nursing film and preparation method certainly.Body temperature of the invention is made of following material from being moulded into type skin caring material: the body temperature that a. is made of thermo-sensitive gel is from moulding material;B. the skin-care function material for being used to generate skin nursing role that can be blended in a.It includes thermo-sensitive gel make the body temperature from the solidification temperature of type skin caring material is moulded into 20-30 DEG C or more, condensing temperature at 25-10 DEG C or less.The present invention can be suitable for different skin surface, good, easy to use with skin conjugation.
Description
Technical field
The present invention relates to a kind of body temperature in the skin nursing products such as facial mask, eye mask, lip film to protect from type skin is moulded into
Reason material and body temperature are moulded into type skin nursing film and preparation method certainly.
Background technique
Facial mask is widely used by people as a kind of beautifying technique.The beautification function of facial mask is protected from the skin of early stage
It is wet, supplement the nutrients or dispel skin oil and fat and cutin, be extended to skin-whitening, reduce wrinkle and restored skin vigor
Effect.The principle of facial mask is exactly to be contacted using the short time for being covered in skin interior barrier skin with external environment, improves skin table
Face temperature, expands pore, promotes sweat gland secretion and metabolism, is conducive to dispel epidermal cell metabolism product and accumulation
Oil substances, to reach cleaning action;Because the gain of heat acts on, moisture content and nutrition is made to accelerate the cutin that penetrates to the skin
Layer achievees the purpose that supplement moisture content and nutrition.
Facial mask mainly includes matrix and nutritional ingredient two large divisions.Its mesostroma is the carrier of facial mask, common matrix
There are hydrogel, non-woven fabrics etc.;Nutritional ingredient is then varied, such as animal and plant extracts, amino acid, essential oil etc..It is presently commercially available
There are many type of facial mask, can be divided into four classes: powder face pack, cream pack, removing facial mask and molding facial mask by material.Powder face pack
For it is a kind of it is fine and smooth, uniformly, the mixing powdery substance of free from admixture, it is non-stimulated to skin, when use by suitable facial mask powder with
Water concocting is at paste, coated on face, with the evaporation of moisture, forms one layer of thicker membranoid substance in face;Cream pack is big
Mostly containing more clay constituents (such as kaolin, diatomite), emollient oil components and various skin-protecting functions at
Point etc., when use is also to be applied directly to face, cannot need to generally be cleaned with water-absorbing sponge at film stripping after use;Release surface
Film is generally ointment shape and gel, is thrown off facial mask, facial dirt, skin after it is dry coated on face when use
Bits are also adhered on facial mask while being broken away, and achieve the purpose that cleaning skin;Facial mask is formed, is that facial mask liquid is immersed into Non-woven fabrics
Matrix on, cloth need to only be pasted to jail in face when use, after 15-20 minutes, facial mask liquid is gradually absorbed drying, and cloth is removed
?.Facial mask is formed because of its favor simple and easy to use by consumer, is a kind of facial mask the most widely used at present.
Facial mask, especially current most commonly used molding facial mask, deposits following problem in use: (1) forming facial mask because of shape
Shape is fixed, and when use can not be bonded everyone face completely, especially at portion now, wing of nose periphery and mouth two sides position,
Cannot well with skin attachement;(2) forming the matrix of facial mask is mostly non-woven fabrics, and the toughness under hygrometric state and patch skin are not
Height requires face that must remain stationary when use, once having relaxation to will result in facial mask is detached from skin.(3) facial mask is formed
In undertake trophism facial mask liquid viscosity it is usually all relatively low, viscosity lower than cream pack and remove facial mask in ointment
With the viscosity of gel, facial mask liquid is easy unrestrained and flows to neck in use.
In view of the above-mentioned problems, the invention of facial mask is also being continuously improved.In early stage, inventor is once to patch from the structure of facial mask
Conjunction problem is solved.There is patent (US 922420) and adapt to facial mask blocking the different shape demand of nose and cheek, it will
Facial mask is made into different size and shapes to adapt to different shapes of face;Having patent (US 1862588) to increase by one on facial mask can
Prominent nasal assembly that is adjusting and can removing makes facial mask be close to eye and nose, while increasing dismountable chin strap to maintain fitting chin
Profile, this kind of chin strap still using in subsequent many facial mask inventions.Although these additional components can effectively solve
Fitting problem, but facial mask structure is become complicated, while use is also inconvenient.Subsequent invention again facial mask body in shape
Moulding is carried out, is such as respectively provided with opening in the corresponding position of human face eyes, nose, mouth, or design is a variety of different to cut
The position of trace is allowed to more docile.Recently there is 3D facial mask again, there is patent (104721061 A of CN) to make using 3D technology three-dimensional
Mask sheet can preferably be bonded with individual face, but because of individual difference, everyone shape of face and difference in size compared with
Greatly, do not have wide applicability.
Summary of the invention
The technical problem to be solved by the invention is to provide one kind can be suitable for different skin surface and skin
Skin conjugation is good, body temperature easy to use is moulded into type skin caring material and skin nursing film and preparation method certainly.
Temperature sensitive high molecular material is that one kind changes with ambient temperature, and the material of solution-gel transformation can occur for aqueous solution.
The gel formed by temperature sensitive high molecular material, referred to as thermo-sensitive gel.
Body temperature of the invention is moulded into type skin caring material certainly and is made of following material:
A. the body temperature being made of thermo-sensitive gel is from moulding material;
B. the skin-care function material for being used to generate skin nursing role that can be blended in a;
It includes thermo-sensitive gel make the body temperature from be moulded into the solidification temperature of type skin caring material 20-30 DEG C with
Upper, condensing temperature is at 25-10 DEG C or less.
The body temperature is made of from moulding material the mixing of temperature sensitive high molecular material, added material and deionized water, in which: temperature sensitive
Mass percent shared by high molecular material is 10-60%;Mass percent shared by added material is 0-25%;Remaining for go from
Sub- water.Preferably, the mass percent of temperature sensitive high molecular material is 25-35%, and the mass percent of added material is 0-
15%.The skin-care function quality of materials is 0-20% of the body temperature from moulding material quality, preferably 0.01-5%.Body temperature is certainly
The solidification temperature and condensing temperature for being moulded into type skin caring material can obtain and the routine test to above-mentioned mass ratio selects
?.
Temperature sensitive high score material in the thermo-sensitive gel is one or more combinations below: cellulose and its derivates,
Chitosan and phosphoglycerol, xylan, n-isopropyl acrylamide, poloxamer (Poloxamer), polyethylene glycol/polylactic acid-
Hydroxyacetic acid (PEG/PLGA), polyethylene glycol/polylactic acid-three sections of copolymers of hydroxyacetic acid/polyethylene glycol (PEG-PLGA-PEG).
The carrier added material be sodium chloride, potassium chloride, disodium hydrogen phosphate, sodium dihydrogen phosphate, cyclodextrin, glycerine,
One or more kinds of combinations of polyvinyl alcohol (PVA), polyethylene glycol (PEG), kaolin, diatomite etc..
Body temperature of the invention includes that thermo-sensitive gel material and skin protect from type skin nursing film is moulded into including at least there is one layer
Manage the modeling shaping membrane certainly of ingredient.It further, can also include at least one layer of flexible substrate layer in conjunction with from modeling shaping membrane.
Preferably, the flexible substrate layer is non-woven fabrics, silk fabric, plumage velvet, fiber cloth, bamboo carbon cloth, negative ion cloth, flower bud
The silk any one or more of combination of cloth.
Preferably, the body temperature is moulded into type skin nursing film certainly and moulds shaping membrane and one layer of flexible substrate layer group certainly by one layer
At.
Preferably, the body temperature includes two sheets of flexible substrate layer and is clipped in two sheets of flexible substrate from type skin nursing film is moulded into
One layer between layer forms from modeling shaping membrane.
Body temperature of the invention from be moulded into type skin nursing film as facial mask, nose film, eye mask, lip film, cervacoria or face with
One of neck integration facial mask.
The preparation method of thermo-sensitive gel material of the present invention, comprising the following steps:
(a) the temperature sensitive high molecular material of aforementioned ratio, added material and deionized water are mixed, and
It stirs evenly;
(b) it under the conditions of 1-15 DEG C, places 1 to 24 hour, is liquid to its liquefaction;
(c) it is placed in more than in the environment of thermo-sensitive gel solidification temperature, liquid curing is gel state, i.e.,
For thermo-sensitive gel material.
Body temperature of the invention from be moulded into type skin nursing film preparation method the first string the following steps are included:
(a) thermo-sensitive gel material liquid after freezing is uniformly mixed with skin caring ingredient;
(b) flexible substrate layer is dipped in the mixed liquor in (a), soaking time about 1 minute;
(c) then take out to be placed in makes gel solidification complete facial mask system more than from the environment of modeling shaping membrane solidification temperature
It is standby.
Body temperature of the invention from be moulded into type skin nursing film preparation method second scheme the following steps are included:
(a) thermo-sensitive gel material liquid after freezing is uniformly mixed with skin caring ingredient;
(b) mixed liquor prepared by step (a) is coated in the flexible substrate layer as internal layer, coating thickness 0.1-3mm,
It is formed from modeling shaping membrane;
(c) flexible substrate layer as outer layer is covered in from modeling shaping membrane again;
(d) be placed in is more than to make the i.e. finished surface film preparation of gel solidification from the environment of modeling shaping membrane solidification temperature.
Body temperature of the invention from be moulded into type skin nursing film preparation method third scheme the following steps are included:
(a) thermo-sensitive gel is placed in lower than cryogenic liquefaction in the environment of thermo-sensitive gel transition temperature;
(b) after mixing by liquid thermo-sensitive gel and skin caring ingredient material, it is placed in and changes lower than thermo-sensitive gel
The environment of temperature;
(c) (b) resulting materials are placed in more than the paste face in the environment of thermo-sensitive gel transition temperature, that is, forming gelation
Film.
The present invention has the following advantages that effect compared with existing facial mask:
1) body temperature of the present invention can be bonded completely from type facial mask is moulded into skin, and can be by design requirement certain
Occur obvious solidification effect in time, realize facial mask according to the function of the face contour plastotype of user, effectively realize facial mask with
Eye circumference, wing of nose two sides, mouth and the perfect fitting at chin position.
2) body temperature of the present invention can produce certain convergent force from type facial mask is moulded into use, effectively tight
Skin is caused, beauty functions are improved;Elastic gel after solidifying simultaneously effectively prevent facial movement and facial mask is caused to fall off.
3) body temperature of the present invention is from type facial mask is moulded into, because that can liquefy again after its cryogenic freezing, it is not necessary to worry production
Or in transportational process temperature change influence;And can freeze again makes its liquefaction in use, then plastotype again, weight
It is multiple to use.
4) skin caring ingredient can be locked by thermo-sensitive gel layer, be had from type facial mask is moulded by body temperature of the present invention
Effect solves the problems, such as skin caring ingredient trickle down and overflow.
Specific embodiment
Body temperature of the present invention can be prepared as molding facial mask, cream pack, removing from type skin caring material is moulded into
Any one of facial mask and powder face pack.
When as forming surface film, generally it is made of body temperature from moulding material, skin caring material and flexible substrate layer.Skin
Nursing material is any one of nutrient solution used in common facial mask, such as animal and plant extracts, amino acid, essential oil etc.;It is soft
Property substrate layer can be nonwoven layer, silk layer of cloth, plumage velvet layer, scrim cloth, bamboo charcoal layer of cloth, anion layer of cloth, lace layer of cloth
Any one or more of combination.
It, can be by body temperature from moulding material and such existing facial mask when as cream pack, removing facial mask and when powder face pack
Finished product is compound.
Embodiment 1
(1) facial mask type: molding facial mask.
(2) body temperature is from moulding material ingredient: poloxamer (Poloxamer) 407, weight percentage 30%;Remaining is to go
Ionized water.
(3) skin caring material: essential oil, dosage are body temperature from the 3% of moulding material quality.
(4) substrate layer is selected: silk fabric.
(5) body temperature is prepared from moulding material: (a) body temperature is from each components in certain proportion mixing of moulding material, and stirs evenly;(b) exist
It under the conditions of 1-15 DEG C, places 1 to 24 hour, is liquid to its liquefaction.(c) room temperature (20 DEG C or more) are placed in, liquid curing is solidifying
Colloidal state, as body temperature are from moulding material.
(6) facial mask is prepared using method as described below: (a) by body temperature liquid after freezing from moulding material and skin nursing
After mixing, be placed in (4-8 DEG C) of cold compartment of refrigerator freezing 3 minutes or more ensures its liquefaction to material;(b) by flexible substrate layer
It is dipped in the mixed liquor in (a), soaking time about 1 minute;(c) then taking out 1-10 minutes in the environment of being placed in more than 20 DEG C makes
Gel solidification is formed from modeling shaping membrane, that is, completes the production of facial mask.
(7) application method of facial mask is as follows: (a) being placed in cold compartment of refrigerator (4-8 DEG C) facial mask using preceding, freezes 3 minutes
Ensure its liquefaction above;(b) by facial mask taking-up spread on face after, with hand press facial mask, make its according to user's face contour at
Type, back film starts to solidify within 3 minutes, fits in skin surface completely;(c) after twenty minutes, it takes facial mask off, completes a skin care
Journey.
Embodiment 2
Difference from Example 1 is:
(2) body temperature is from moulding material ingredient are as follows: poloxamer (Poloxamer) 407, weight percentage 35%;Remaining is
Deionized water.
(4) substrate layer is selected: fiber cloth.
Remaining content with it is same as Example 1, repeat no more.
Embodiment 3
Difference from Example 1 is:
(2) body temperature is from moulding material ingredient: cellulose and its derivates, weight percentage 35%;Remaining is deionized water.
(4) substrate layer is selected: plumage velvet.
Remaining content with it is same as Example 1, repeat no more.
Embodiment 4
Difference from Example 1 is:
(2) body temperature is from moulding material ingredient :/polyethylene glycol/polylactic acid-hydroxyacetic acid polyethylene glycol (PEG-PLGA-PEG),
Weight percentage 35%;Remaining is deionized water.
(4) substrate layer is selected: bamboo carbon cloth.
Remaining content with it is same as Example 1, repeat no more.
Embodiment 5
Difference from Example 1 is:
(2) body temperature is from moulding material ingredient: poloxamer (Poloxamer) 407, weight percentage 30%, sodium chloride,
Weight percentage 1%;Remaining is deionized water.
(4) substrate layer is selected: non-woven fabrics.
(6) facial mask is prepared using method as described below: (a) by body temperature liquid after freezing from moulding material and skin nursing
After mixing, be placed in (4-8 DEG C) of cold compartment of refrigerator freezing 3 minutes or more ensures its liquefaction to material;(b) step (a) is made
Standby mixed liquor is coated in flexible substrate layer, coating thickness 0.1-3mm;(c) 1-10 minutes in the environment of being placed in more than 20 DEG C
Make the i.e. finished surface film preparation of gel solidification.
Remaining content with it is same as Example 1, repeat no more.
Embodiment 6
Difference from Example 5 is:
(2) body temperature is from moulding material ingredient: polyethylene glycol/polylactic acid-hydroxyacetic acid/polyethylene glycol (PEG-PLGA-PEG),
Weight percentage 30%;Potassium chloride, weight percentage 0.5%;Remaining is deionized water.
(4) substrate layer is selected: fiber cloth
Remaining content with it is same as Example 5, repeat no more.
Embodiment 7
Difference from Example 5 is:
(2) body temperature is from moulding material ingredient: cellulose and its derivates, weight percentage 20%;N- isopropyl propionamide,
Weight percentage 10%,;Disodium hydrogen phosphate, weight percentage 0.5%;Remaining is deionized water.
(4) substrate layer is selected: functional facial mask cloth
Remaining content with it is same as Example 5, repeat no more.
Embodiment 8
Difference from Example 5 is:
(2) body temperature is from moulding material ingredient: chitosan, weight percentage 30%;Phosphoglycerol, weight percentage
5%,;Polyethylene glycol (PEG), weight percentage 3%;Remaining is deionized water.
(4) substrate layer is selected: bamboo carbon cloth
Remaining content with it is same as Example 5, repeat no more.
Embodiment 9
Difference from Example 5 is:
(2) body temperature is from moulding material ingredient: xylan, weight percentage 25%;N- isopropyl propionamide, weight percent contain
Amount 10%,;Sodium dihydrogen phosphate, weight percentage 1%;Remaining is deionized water.
(4) substrate layer is selected: negative ion cloth
Remaining content with it is same as Example 5, repeat no more.
Embodiment 10
Difference from Example 5 is:
(4) substrate layer is selected: internal layer is silk fabric, and outer layer is non-woven fabrics.
(6) facial mask is prepared using method as described below: (a) by body temperature liquid after freezing from moulding material ingredient and skin
Nurse material after mixing, being placed in (4-8 DEG C) of cold compartment of refrigerator freezing 3 minutes or more ensures its liquefaction;(b) by step
(a) mixed liquor prepared is coated on the substrate layer as internal layer, coating thickness 0.1-3mm, is formed and is needed from modeling shaping membrane (c)
When, then the substrate layer as outer layer is covered in from modeling shaping membrane;(d) make to coagulate within 1-10 minutes in the environment of being placed in more than 20 DEG C
Adhesive curing, that is, finished surface film preparation.
This facial mask when in use, may be selected, ectonexine with the contact surface of face.Remaining content with it is same as Example 5,
It repeats no more.
Embodiment 11
Difference from Example 10 is:
(2) body temperature is from moulding material ingredient: chitosan, weight percentage 30%;Phosphoglycerol, weight percentage 5%,
Remaining is deionized water.
(4) substrate layer is selected: internal layer is bamboo carbon cloth, and outer layer is lace cloth.
Remaining content with it is same as in Example 10, repeat no more.
Embodiment 12
Difference from Example 10 is:
(2) body temperature is from moulding material ingredient: poloxamer (Poloxamer) 407, weight percentage 20%;N- isopropyl
Propionamide, weight percentage 10%;Glycerine, weight percentage 5%, remaining is deionized water.
(4) substrate layer is selected: internal layer is negative ion cloth, and outer layer is fiber cloth.
Remaining content with it is same as in Example 10, repeat no more.
Embodiment 13
Difference from Example 10 is:
(2) body temperature is from moulding material ingredient: xylan, weight percentage 20%;N-isopropyl acrylamide, weight percent
Content 10%;Cyclodextrin, weight percentage 2%, remaining is deionized water.
(4) substrate layer is selected: internal layer is plumage velvet, and outer layer is non-woven fabrics.
Remaining content with it is same as in Example 10, repeat no more.
Embodiment 14
Difference from Example 10 is:
(2) body temperature is from moulding material ingredient: polyethylene glycol/polylactic acid-hydroxyacetic acid (PEG-PLGA), weight percentage
30%;N-isopropyl acrylamide, weight percentage 5%;Polyvinyl alcohol (PVA), weight percentage 5%;Remaining is to go
Ionized water.
(4) substrate layer is selected: internal layer is negative ion cloth, and outer layer is fiber cloth.
Remaining content with it is same as in Example 10, repeat no more.
Embodiment 15
Difference from Example 10 is:
(2) body temperature is from moulding material ingredient: polyethylene glycol/polylactic acid-hydroxyacetic acid/polyethylene glycol (PEG-PLGA-PEG),
Weight percentage 25%;N-isopropyl acrylamide, weight percentage 10%;Glycerine, weight percentage 5%;Its
Remaining is deionized water.
(4) substrate layer is selected: internal layer is non-woven fabrics, and outer layer is fiber cloth.
Remaining content with it is same as in Example 10, repeat no more.
Embodiment 16
(1) facial mask type: cream pack
(2) body temperature is from moulding material ingredient: poloxamer (Poloxamer) 407, weight percentage 30%;Polyvinyl alcohol
(PVA), weight content 5%;Remaining is deionized water.
(3) facial mask liquid ingredient: essential oil.
(4) body temperature is prepared from moulding material: (a) body temperature is from each components in certain proportion mixing of moulding material, and stirs evenly;(b) exist
It under the conditions of 1-15 DEG C, places 1 to 24 hour, is liquid to its liquefaction.(c) room temperature (20 DEG C or more) are placed in, liquid curing is solidifying
Colloidal state, as body temperature are from moulding material.
(5) facial mask preparation flow: (a) body temperature is placed in (4-8 DEG C) of cold compartment of refrigerator freezing 3 minutes or more from moulding material
Ensure its liquefaction;It (b) is by volume that 100:3 volume ratio is uniformly mixed from moulding material and skin caring material by body temperature;(c) so
Taking out afterwards makes the i.e. finished surface film preparation of gel solidification for 1-10 minutes in the environment of being placed in more than 20 DEG C.
(6) application method of facial mask is as follows: (a) being placed in cold compartment of refrigerator (4-8 DEG C) facial mask using preceding, freezes 3 minutes
More than;(b) facial mask taking-up is spread on into face;(c) after 30 minutes, face mask layer is removed, cleaning face completes a skin care process.
Embodiment 17
With embodiment 16 the difference is that:
(2) body temperature is from moulding material ingredient: poloxamer (Poloxamer) 407, weight percentage 30%;Sodium chloride, weight
Measure percentage composition 1%;, polyethylene glycol (PEG), weight percentage 5%;Remaining is deionized water.
Remaining content is identical as with embodiment 16, repeats no more.
Embodiment 18
With embodiment 16 the difference is that:
(2) body temperature is from moulding material ingredient: n-isopropyl acrylamide, weight percentage 25%;Chitosan, weight percent
Content 5%;Polyethylene glycol (PEG), weight percentage 5%;Remaining is deionized water.
Remaining content is identical as with embodiment 16, repeats no more.
Embodiment 19
With embodiment 16 the difference is that:
(2) body temperature is from moulding material ingredient: n-isopropyl acrylamide, weight percentage 25%;Phosphoglycerol, weight hundred
Divide content 5%;Glycerine, weight percentage 5%, kaolin, weight percentage 5%;Remaining is deionized water.
Remaining content is identical as with embodiment 16, repeats no more.
Embodiment 20
With embodiment 16 the difference is that:
(2) body temperature is from moulding material ingredient: polyethylene glycol/polylactic acid-hydroxyacetic acid/polyethylene glycol (PEG-PLGA-PEG),
Weight percentage 30%;Glycerine, weight percentage 5%;Diatomite, weight percentage 5%;Remaining is deionization
Water.
Remaining content is identical as with embodiment 16, repeats no more.
Embodiment 21
(1) facial mask type: cream pack.
(2) body temperature is from moulding material: poloxamer (Poloxamer) 407, weight percentage 30%;Remaining is deionization
Water.
(3) skin-care function material: essential oil, dosage are body temperature from the 3% of moulding material quality.
(4) preparation flow of cream pack material: (a) body temperature is placed in (4-8 DEG C) of cold compartment of refrigerator freezing 3 from moulding material
Minute or more ensure its liquefaction;(b) after mixing by liquid thermo-sensitive gel and skin caring ingredient material, it is cold to be placed in refrigerator
It hides the freezing of (4-8 DEG C) of room 3 minutes or more;(c) (b) resulting materials are placed 1-10 minutes in the environment of more than 20 DEG C,
Form the facial mask mixture of gelation.
(5) application method of facial mask is as follows: facial mask mixture made of step (4) (a) being placed in refrigerator cold-storage using preceding
Room (4-8 DEG C) 3 minutes or more ensures its liquefaction;(b) it is drawn off spreading on face;(c) after 20-30 minutes, facial mask, cleaning are removed
Face completes a skin care process.
Claims (11)
1. a kind of body temperature is moulded into type skin caring material certainly, which is characterized in that be made of following material:
A. the body temperature being made of thermo-sensitive gel is from moulding material;
B. the skin-care function material for being used to generate skin nursing role that can be blended in a;
It includes thermo-sensitive gel make the body temperature from the solidification temperature of type skin caring material is moulded into 20-30 DEG C, liquefaction temperature
Degree is at 1-15 DEG C;The thermo-sensitive gel is poloxamer;Thermo-sensitive gel is cold in the environment of being lower than thermo-sensitive gel transition temperature
Freeze liquefaction, solidifies in the environment of being more than thermo-sensitive gel transition temperature.
2. body temperature according to claim 1 is from being moulded into type skin caring material, it is characterised in that: the body temperature is from moulding material
It is made of the thermo-sensitive gel that temperature sensitive high molecular material, added material and deionized water are mixed to form, in which: temperature sensitive high molecular material
Shared mass percent is 10-60%;Mass percent shared by added material is 0-25%;Remaining is deionized water;The skin
Skin nursing function quality of materials is 0-20 % of the body temperature from moulding material quality;The added material is sodium chloride, potassium chloride, phosphoric acid
Disodium hydrogen, sodium dihydrogen phosphate, cyclodextrin, glycerine, polyvinyl alcohol (PVA), polyethylene glycol (PEG), kaolin, diatomite one
Kind or a variety of combinations.
3. body temperature according to claim 2 is moulded into type skin caring material certainly, it is characterised in that: temperature sensitive high molecular material
Mass percent is preferably 25-35%, and the mass percent of added material is 0-15%.
4. a kind of body temperature is from being moulded into type skin nursing film, it is characterised in that: including at least there is one layer of body temperature described in claim 1
From being moulded into type skin caring material.
5. body temperature according to claim 4 is moulded into type skin nursing film certainly, it is characterised in that: further include having at least one layer soft
Property substrate layer.
6. body temperature according to claim 5 is moulded into type skin nursing film certainly, it is characterised in that: the flexible substrate layer is nothing
Woven fabric, silk fabric, plumage velvet, fiber cloth, bamboo carbon cloth, negative ion cloth, any one or more of combination of lace cloth.
7. the preparation method that body temperature described in a kind of claim 5 is moulded into type skin nursing film certainly, comprising the following steps:
(a) thermo-sensitive gel material liquid after freezing is uniformly mixed with skin caring ingredient;
(b) mixed liquor prepared by step (a) is coated in the flexible substrate layer as internal layer, coating thickness 0.1-3 mm, shape
At modeling shaping membrane certainly;
(c) flexible substrate layer as outer layer is covered in from modeling shaping membrane again;
(d) be placed in is more than to make the i.e. finished surface film preparation of gel solidification from the environment of modeling shaping membrane solidification temperature.
8. the preparation method that body temperature described in a kind of claim 5 is moulded into type skin nursing film certainly, comprising the following steps:
(a) thermo-sensitive gel material liquid after freezing is uniformly mixed with skin caring ingredient;
(b) mixed liquor prepared by step (a) is coated in the flexible substrate layer as internal layer, coating thickness 0.1-3 mm, shape
At modeling shaping membrane certainly;
(c) be placed in is more than to make the i.e. finished surface film preparation of gel solidification from the environment of modeling shaping membrane solidification temperature.
9. the preparation method that body temperature described in a kind of claim 4 is moulded into type skin nursing film certainly, comprising the following steps:
(a) thermo-sensitive gel is placed in lower than cryogenic liquefaction in the environment of thermo-sensitive gel transition temperature;
(b) after mixing by liquid thermo-sensitive gel and skin caring ingredient, it is placed in the ring lower than thermo-sensitive gel transition temperature
Border;
(c) (b) resulting materials are placed in more than in the environment of thermo-sensitive gel transition temperature, that is, form the cream pack of gelation.
10. the preparation method that body temperature described in a kind of claim 1 is moulded into type skin caring material certainly, comprising the following steps:
(a) thermo-sensitive gel is placed in lower than cryogenic liquefaction in the environment of thermo-sensitive gel transition temperature;
(b) after mixing by liquid thermo-sensitive gel and skin-care function material, it is placed in lower than thermo-sensitive gel transition temperature
Environment;
(c) (b) resulting materials are placed in more than the skin nursing material in the environment of thermo-sensitive gel transition temperature, that is, forming gelation
Material.
11. the body temperature of claim 4-6 any one from be moulded into type skin nursing film be used as prepare facial mask, nose film, eye mask, lip
The purposes of film, cervacoria or face facial mask integrated with neck.
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CN108478485A (en) * | 2018-05-04 | 2018-09-04 | 邵立坤 | A kind of temperature-sensitive hydrogel facial mask and preparation method thereof |
CN108635284A (en) * | 2018-08-17 | 2018-10-12 | 佛山市森昂生物科技有限公司 | A kind of Temperature Control Type biology base facial mask |
KR102123483B1 (en) * | 2018-11-30 | 2020-06-16 | 충남대학교산학협력단 | Manufacturing method for thermo-sensitive hydrogel type mask pack and mask pack manufactured by the same |
CN112168717B (en) * | 2020-10-06 | 2023-12-01 | 广东碧素堂生物科技有限公司 | Hydrogel-based slow-release mask and preparation method and application method thereof |
CN115363964A (en) * | 2021-05-18 | 2022-11-22 | 华南理工大学 | Borneol-based temperature-sensitive hydrogel eye mask for relieving eye problems and preparation method thereof |
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