CN103830119B - A kind of with the preparation method of the natural silk glue protein astringent that is substrate - Google Patents
A kind of with the preparation method of the natural silk glue protein astringent that is substrate Download PDFInfo
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- CN103830119B CN103830119B CN201410087211.3A CN201410087211A CN103830119B CN 103830119 B CN103830119 B CN 103830119B CN 201410087211 A CN201410087211 A CN 201410087211A CN 103830119 B CN103830119 B CN 103830119B
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Abstract
The invention discloses a kind of with the preparation method of the natural silk glue protein astringent that is substrate, by the raw material production of sericine, disintegrating process, dissolving and astringent preparing process, obtain easy, natural, noresidue, without degeneration high-purity sericine, with this substrate, not only sericin astringent can be prepared, also the sericin cosmetic products such as pomade, frost, hair-setting agent can be made.
Description
Technical field
The present invention relates generally to cosmetic field, particularly relates to a kind of with the preparation method of the natural silk glue protein astringent that is substrate.
Background technology
Sericine is the important content of non-spun silk industrialization in multi-field utilization.Along with the raising of living standards of the people and the reinforcement of environmental protection consumer products demand, the new material of All Pure Nature pure silk glue should belong to emerging non-spun silk industry in the utilization in the fields such as cosmetic, medicine, health care, and at home and abroad market potential is huge.
Large quantifier elimination shows, sericine holds easily absorbed by the body; Be rich in the mankind's 18 kinds of essential amino acids and natural moisture preserving composition, play moisturizing, wrinkle resistant, whitening function; Easily form chelate with the heavy metal such as copper, hydrargyrum, restraint of tyrosinase isoreactivity, plays antioxidation, keeps food safety effect; Be rich in many carboxyls, water-retaining property is strong, digestibility is low, plays the active function etc. reducing digestive system canceration material.
China's sericine source is main at present reclaims from the white sericine filature, refining liquid, and cumbersome, efficiency are low, cost is high, sericin purity is low, seriously polluted, and added value is not high, also have larger distance with multi-field application widely.
All Pure Nature, pure sericine are that cosmetic product innovation area has outstanding specific function material.The present invention is demonstrated by silkworm district, the Applied economy trait expression of popularization autonomous innovation selection-breeding is better, raise simple, that functional characteristic is excellent All Pure Nature, pure cultivated silkworm breed variety, low cost, the pure Cocoon of safe and efficient, a large amount of production All Pure Natures, and prepare All Pure Nature noresidue with the short-cut method of low cost, without degeneration, high-quality sericine substrate, be directly used in high added value, the top grade of noresidue, the innovation of natural cosmetic product.Not only widen the new way that silkworm silk utilizes, enrich and improve the life requirement of people, and bring huge economy, society, ecological benefits to silkworm raiser, associated production and trading enterprise.
Summary of the invention
The object of the invention is just to provide a kind of with the preparation method of the natural silk glue protein astringent that is substrate.
The present invention is achieved by the following technical solutions:
A preparation method for the astringent being substrate with natural silk glue protein, comprises the following steps:
(1) stripping of Cocoon: be placed on small straw bundles to spin cocoons 10-13 day, harvesting of cocoon is gently adopted and is put down gently, cocoon drying 2-2.5h under 55-60 DEG C of constant temperature, manual directly stripping Cocoon shell; Clean under 60-70 DEG C of clear water again, drain rear 78-80 DEG C of cocoon drying 2-3h;
(2) Crushing of Ultrafine of cocoon shell: peel manually, from the cocoon shell of above-mentioned oven dry, is ground into 140-160 object sericin powder with atomizer;
(3) dissolving of sericin powder: the aqueous sodium carbonate 8-9ml getting distilled water 85-95ml, sericin powder 1-2g, 1-1.2%, mixing, at 75-85 DEG C, dissolve 3-3.2h, 140-160 order filter screen filtration, filtrate is sericin aqueous solution;
(4) preparation of astringent: described astringent is made up of each raw material of following weight percentage ratio:
Water 80-84%, sericin aqueous solution 10-13%, remaining be dehydrated alcohol; After above-mentioned each raw material mixing, adjustment PH is 6.5-7.5, obtains described astringent.
Advantage of the present invention is:
The present invention, by the raw material production of sericine, disintegrating process, dissolving and astringent preparing process, obtains easy, natural, noresidue, without degeneration high-purity sericine.With this substrate, not only sericin astringent can be prepared, also the sericin cosmetic products such as pomade, frost, hair-setting agent can be made.
Detailed description of the invention
Embodiment 1
A preparation method for the astringent being substrate with natural silk glue protein, comprises the following steps:
(1) stripping of Cocoon: be placed on small straw bundles to spin cocoons 10-13 day, harvesting of cocoon is gently adopted and is put down gently, cocoon drying 2-2.5h under 55-60 DEG C of constant temperature, manual directly stripping Cocoon shell; Clean under 60-70 DEG C of clear water again, drain rear 78-80 DEG C of cocoon drying 2-3h;
(2) Crushing of Ultrafine of cocoon shell: peel manually, from the cocoon shell of above-mentioned oven dry, is ground into 140-160 object sericin powder with atomizer;
(3) dissolving of sericin powder: the aqueous sodium carbonate 8-9ml getting distilled water 85-95ml, sericin powder 1-2g, 1-1.2%, mixing, at 75-85 DEG C, dissolve 3-3.2h, 140-160 order filter screen filtration, filtrate is sericin aqueous solution;
(4) preparation of astringent: described astringent is made up of each raw material of following weight percentage ratio:
Water 80-84%, sericin aqueous solution 10-13%, remaining be dehydrated alcohol; After above-mentioned each raw material mixing, adjustment PH is 6.5-7.5, obtains described astringent.
Claims (1)
1., with a preparation method for the natural silk glue protein astringent that is substrate, it is characterized in that comprising the following steps:
(1) stripping of Cocoon: be placed on small straw bundles to spin cocoons 10-13 day, harvesting of cocoon is gently adopted and is put down gently, cocoon drying 2-2.5h under 55-60 DEG C of constant temperature, manual directly stripping Cocoon shell; Clean under 60-70 DEG C of clear water again, drain rear 78-80 DEG C of cocoon drying 2-3h;
(2) Crushing of Ultrafine of cocoon shell: peel manually, from the cocoon shell of above-mentioned oven dry, is ground into 140-160 object sericin powder with atomizer;
(3) dissolving of sericin powder: the aqueous sodium carbonate 8-9ml getting distilled water 85-95ml, sericin powder 1-2g, 1-1.2%, mixing, at 75-85 DEG C, dissolve 3-3.2h, 140-160 order filter screen filtration, filtrate is sericin aqueous solution;
(4) preparation of astringent: described astringent is made up of each raw material of following weight percentage ratio:
Water 80-84%, sericin aqueous solution 10-13%, remaining be dehydrated alcohol; After above-mentioned each raw material mixing, adjustment pH is 6.5-7.5, obtains described astringent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410087211.3A CN103830119B (en) | 2014-03-11 | 2014-03-11 | A kind of with the preparation method of the natural silk glue protein astringent that is substrate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410087211.3A CN103830119B (en) | 2014-03-11 | 2014-03-11 | A kind of with the preparation method of the natural silk glue protein astringent that is substrate |
Publications (2)
| Publication Number | Publication Date |
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| CN103830119A CN103830119A (en) | 2014-06-04 |
| CN103830119B true CN103830119B (en) | 2016-03-23 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410087211.3A Active CN103830119B (en) | 2014-03-11 | 2014-03-11 | A kind of with the preparation method of the natural silk glue protein astringent that is substrate |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106473960A (en) * | 2016-11-24 | 2017-03-08 | 江苏爱西施科技服务咨询股份有限公司 | A kind of preparation method of the cosmetic water containing sericin |
| CN106667789A (en) * | 2017-03-19 | 2017-05-17 | 安徽省农业科学院蚕桑研究所 | Preparation method of natural pure-sericin liquid shampoo |
| CN107823102A (en) * | 2017-12-14 | 2018-03-23 | 佛山市万良商贸有限公司 | A kind of silk gum moisturiser and preparation method thereof |
| CN107802585A (en) * | 2017-12-14 | 2018-03-16 | 佛山市万良商贸有限公司 | A kind of silk gum condensation and preparation method thereof |
| CN108743446A (en) * | 2018-06-28 | 2018-11-06 | 中国科学院新疆理化技术研究所 | A kind of ultrafiltration membrane preparation method of cocoon sericin protein and its application |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1456177A (en) * | 2003-02-19 | 2003-11-19 | 屈清辉 | Method and apparatus for producing fibroin powder |
| CN101856318A (en) * | 2010-04-27 | 2010-10-13 | 浙江省农业科学院 | Preparation method of pure-natural, high-purity and invariable green sericin powder |
| CN102961298A (en) * | 2012-12-21 | 2013-03-13 | 李卫旗 | Manufacturing method of body lotion by taking Pullulan polysaccharide and sericin bioactive peptide as main raw materials |
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2014
- 2014-03-11 CN CN201410087211.3A patent/CN103830119B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1456177A (en) * | 2003-02-19 | 2003-11-19 | 屈清辉 | Method and apparatus for producing fibroin powder |
| CN101856318A (en) * | 2010-04-27 | 2010-10-13 | 浙江省农业科学院 | Preparation method of pure-natural, high-purity and invariable green sericin powder |
| CN102961298A (en) * | 2012-12-21 | 2013-03-13 | 李卫旗 | Manufacturing method of body lotion by taking Pullulan polysaccharide and sericin bioactive peptide as main raw materials |
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| CN103830119A (en) | 2014-06-04 |
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