CN106667789A - Preparation method of natural pure-sericin liquid shampoo - Google Patents

Preparation method of natural pure-sericin liquid shampoo Download PDF

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Publication number
CN106667789A
CN106667789A CN201710180605.7A CN201710180605A CN106667789A CN 106667789 A CN106667789 A CN 106667789A CN 201710180605 A CN201710180605 A CN 201710180605A CN 106667789 A CN106667789 A CN 106667789A
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CN
China
Prior art keywords
silk
cocoon
parts
silk gum
preparation
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710180605.7A
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Chinese (zh)
Inventor
李冰
叶崇军
陈复生
夏家凤
舒蕊
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Sericultural Research Institute Anhui Academy Of Agricultural Sciences
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Sericultural Research Institute Anhui Academy Of Agricultural Sciences
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Priority to CN201710180605.7A priority Critical patent/CN106667789A/en
Publication of CN106667789A publication Critical patent/CN106667789A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Zoology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a preparation method of natural pure-sericin liquid shampoo. The preparation method comprises the following steps: peeling off silkworm cocoons from a paper cocooning frame in 8 days after mounting a cocooning frame on a sericin variety of silkworms, avoiding collision among the silkworm cocoons during a peeling process, drying the silkworm cocoons for 2 hours under 50 DEG C of a constant temperature, and directly peeling off sericin cocoon layers of the silkworm cocoons; washing once by using water, removing impurities, drying the silkworm cocoons for 2 hours under 80 DEG C of a temperature after draining, and sieving through a 100-mesh sieve after smashing, thus obtaining sericin powder; mixing 100 ml of distilled water with 5 g of the sericin powder, uniformly stirring under 80 DEG C, dissolving for 3 hours, centrifuging, removing sediment, mixing with core masterbatches of a flexible detergent, wool fat, pearly slurry, water, salt, deep sea fish oil, essence, spearmint and wire drawing powder according to proportions, uniformly stirring, dissolving, emulsifying, standing and cooling, thus obtaining the natural pure-sericin liquid shampoo. According to the preparation method disclosed by the invention, not only is the scrap removing effect of existent commercially available liquid shampoo be obtained, but also the functions of moisturizing, moistening hairs, resisting bacteria, relieving itching, blacking the hairs and shining the hairs are obtained, and the effect of the liquid shampoo is broadened.

Description

A kind of preparation method of natural pure silk glue protein shampoo
Technical field
The present invention relates to daily necessities field, and in particular to a kind of preparation method of natural pure silk glue protein shampoo.
Background technology
Sericin confrontation skin can play moisturizing, wrinkle resistant, whitening function, and chelating is easily formed with the heavy metal such as copper, mercury Thing, suppresses the property such as tyrosinase, plays anti-oxidant, keeps food security effect;Rich in many carboxyls, water-retaining property is strong, digestibility is low, Play active function of reduction digestive system canceration material etc..All Pure Nature pure silk glue is in cosmetics, health products, medicine and other fields tool Have broad application prospects and market.
With the continuous improvement of living standard, people pursue more naturalization, synthesis to washing shield product requirement pursuit higher Change, the commodity of functionalization.Shampoo on the market can not fully meet wanting for consumer in terms of security, feature at present Ask.Natural pure silk glue protein coordinates phosphatide oil, water source protease, coconut oil, deep-sea mineral salt etc. with its unique physicochemical property Active ingredient shampoo, it is not only natural harmless, also there is good effect on the functional characteristics such as moisturizing, black hair, antibacterial.
The content of the invention
To solve the above problems, the invention provides a kind of preparation method of natural pure silk glue protein shampoo, safe nothing Evil, functional characteristic are good.
To achieve the above object, the technical scheme taken of the present invention is:
A kind of preparation method of natural pure silk glue protein shampoo, comprises the following steps:
The preparation of S1, silk gum mother liquor
The treatment of S11, silk gum cocoon husk as raw material:Silk gum kind silkworm be placed on small straw bundles to spin cocoons the 8th day after stripping silk cocoon from paper cocooning frame, Silk cocoon is avoided to collide during harvesting of cocoon, cocoon drying 2h under 50 DEG C of constant temperature directly peels off the silk gum cocoon layer of silk cocoon;Cleaned with water one time The removal of impurity is gone, 80 DEG C of cocoon drying 2h after draining;
The crushing of S12, silk gum cocoon shell:Above-mentioned silk gum cocoon shell is crushed with micronizer, 100 mesh sieves are crossed, silk gum is obtained Powder;
The configuration of S13, natural silk sol solution:100ml distilled water, silk gum powder 5g mixing are taken, in dissolving 3h at 80 DEG C, 5000rpm is centrifuged 30min, and removal precipitation is silk gum mother liquor;
The preparation of S2, silk gum shampoo
S21, the silk gum aqueous solution and flexible abstergent core master batch by obtained by above-mentioned preparation, lanolin, pearlite slurry, water, After salt, deep sea fish oil, essence, spearmint, wire drawing powder mix in proportion, uniform stirring, will to 10-12h is dissolved at 60-80 DEG C The above-mentioned solution stand for having emulsified prepares natural silk gum shampoo by cooling down 12-24 hours.
Wherein, each group is divided into the step S21:
6-10 parts of flexible abstergent core master batch, lanolin 0.4-0.8 parts, pearlite slurry 1-2 parts, water 80-90 parts, salt 3-4 Part, deep sea fish oil 0.04-0.08 parts, essence 0.001-0.002 parts, spearmint 0.8-1.2 parts, 0.2-0.4 parts of wire drawing powder, silk gum Aqueous solution 0.1-0.2 parts.
The invention has the advantages that:
The anti-dandruff effect of the existing shampoo in market is not only adhered to, while also having moisturizing profit hair, anti-bacterial, anti-itching, black hair bright The effect of hair, makes effect of shampoo be expanded.
Specific embodiment
In order that objects and advantages of the present invention become more apparent, the present invention is carried out further with reference to embodiments Describe in detail.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to limit this hair It is bright.
Embodiment 1
A kind of preparation method of natural pure silk glue protein shampoo, comprises the following steps:
The preparation of S1, silk gum mother liquor
The treatment of S11, silk gum cocoon husk as raw material:Silk gum kind silkworm be placed on small straw bundles to spin cocoons the 8th day after stripping silk cocoon from paper cocooning frame, Silk cocoon is avoided to collide during harvesting of cocoon, cocoon drying 2h under 50 DEG C of constant temperature directly peels off the silk gum cocoon layer of silk cocoon;Cleaned with water one time The removal of impurity is gone, 80 DEG C of cocoon drying 2h after draining;
The crushing of S12, silk gum cocoon shell:Above-mentioned silk gum cocoon shell is crushed with micronizer, 100 mesh sieves are crossed, silk gum is obtained Powder;
The configuration of S13, natural silk sol solution:100ml distilled water, silk gum powder 5g mixing are taken, in dissolving 3h at 80 DEG C, 5000r/h is centrifuged 30min, and removal precipitation is silk gum mother liquor;
The preparation of S2, silk gum shampoo
S21, weigh 0.1 part of the silk gum aqueous solution, 6 parts of flexible abstergent core master batch, lanolin 0.4 obtained by above-mentioned preparation Part, 1 part of pearlite slurry, 80 parts of water, 3 parts of salt, 0.04 part of deep sea fish oil, 0.001 part of essence, 0.8 part of spearmint, 0.2 part of wire drawing powder After mixing, to 10-12h is dissolved, the above-mentioned solution stand that will have been emulsified cools down 12-24 hours i.e. to uniform stirring at 60-80 DEG C Natural silk gum shampoo can be prepared.
Embodiment 2
The preparation of S1, silk gum mother liquor
The treatment of S11, silk gum cocoon husk as raw material:Silk gum kind silkworm be placed on small straw bundles to spin cocoons the 8th day after stripping silk cocoon from paper cocooning frame, Silk cocoon is avoided to collide during harvesting of cocoon, cocoon drying 2h under 50 DEG C of constant temperature directly peels off the silk gum cocoon layer of silk cocoon;Cleaned with water one time The removal of impurity is gone, 80 cocoon drying 2h after draining;
The crushing of S12, silk gum cocoon shell:Above-mentioned silk gum cocoon shell is crushed with micronizer, 100 mesh sieves are crossed, silk gum is obtained Powder;
The configuration of S13, natural silk sol solution:100ml distilled water, silk gum powder 5g mixing are taken, in dissolving 3h at 80 DEG C, 5000r/h is centrifuged 30min, and removal precipitation is silk gum mother liquor;
The preparation of S2, silk gum shampoo
S21, weigh 0.2 part of silk gum mother liquor, 10 parts of flexible abstergent core master batch, lanolin 0.8 obtained by above-mentioned preparation Part, 2 parts of pearlite slurry, 90 parts of water, 4 parts of salt, 0.08 part of deep sea fish oil, 0.002 part of essence, 1.2 parts of spearmint, 0.4 part of wire drawing powder After mixing, to 10-12h is dissolved, the above-mentioned solution stand that will have been emulsified cools down 12-24 hours i.e. to uniform stirring at 60-80 DEG C Natural silk gum shampoo can be prepared.
Embodiment 3
The preparation of S1, silk gum mother liquor
The treatment of S11, silk gum cocoon husk as raw material:Silk gum kind silkworm be placed on small straw bundles to spin cocoons the 8th day after stripping silk cocoon from paper cocooning frame, Silk cocoon is avoided to collide during harvesting of cocoon, cocoon drying 2h under 50 DEG C of constant temperature directly peels off the silk gum cocoon layer of silk cocoon;Cleaned with water one time The removal of impurity is gone, 80 DEG C of cocoon drying 2h after draining;
The crushing of S12, silk gum cocoon shell:Above-mentioned silk gum cocoon shell is crushed with micronizer, 100 mesh sieves are crossed, silk gum is obtained Powder;
The configuration of S13, natural silk sol solution:100ml distilled water, silk gum powder 5g mixing are taken, in dissolving 3h at 80 DEG C, 5000r/h is centrifuged 30min, and removal precipitation is silk gum mother liquor;
The preparation of S2, silk gum shampoo
S21, weigh 0.15 part of silk gum mother liquor liquid, 8 parts of flexible abstergent core master batch, lanolin obtained by above-mentioned preparation 0.6 part, 1.5 parts of pearlite slurry, 85 parts of water, 3.5 parts of salt, 0.06 part of deep sea fish oil, 0.0015 part of essence, 1 part of spearmint, wire drawing powder After 0.3 part of mixing, uniform stirring is to 10-12h is dissolved at 60-80 DEG C, and the above-mentioned solution stand cooling 12-24 that will have been emulsified is small When can prepare natural silk gum shampoo.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should It is considered as protection scope of the present invention.

Claims (2)

1. a kind of preparation method of natural pure silk glue protein shampoo, it is characterised in that comprise the following steps:
The preparation of S1, silk gum mother liquor
The treatment of S11, silk gum cocoon husk as raw material:Silk gum kind silkworm be placed on small straw bundles to spin cocoons the 8th day after stripping silk cocoon from paper cocooning frame, harvesting of cocoon During avoid silk cocoon from colliding, cocoon drying 2h under 50 DEG C of constant temperature directly peels off the silk gum cocoon layer of silk cocoon;A removal is cleaned with water Impurity, 80 DEG C of cocoon drying 2h after draining;
The crushing of S12, silk gum cocoon shell:100 mesh sieves are crossed after above-mentioned silk gum cocoon shell is crushed with micronizer, sericin powder is obtained End;
The configuration of S13, natural silk sol solution:100ml distilled water, silk gum powder 5g mixing are taken, in dissolving 3h at 80 DEG C, 5000rpm is centrifuged 30min, and removal precipitation is the silk gum aqueous solution;
The preparation of S2, silk gum shampoo
S21, by the silk gum aqueous solution and flexible abstergent core master batch, lanolin, pearlite slurry, water, salt, depth obtained by above-mentioned preparation After ocean fish oil, essence, spearmint, wire drawing powder mix in proportion, uniform stirring will be emulsified to 10-12h is dissolved at 60-80 DEG C Good above-mentioned solution stand is cooled down 12-24 hours and can prepare natural silk gum shampoo.
2. a kind of preparation method of natural pure silk glue protein shampoo as claimed in claim 1, it is characterised in that the step Each group is divided into S21:
6-10 parts of flexible abstergent core master batch, lanolin 0.4-0.8 parts, pearlite slurry 1-2 parts, water 80-90 parts, salt 3-4 parts, depth 0.04-0.08 parts of ocean fish oil, essence 0.001-0.002 parts, spearmint 0.8-1.2 parts, 0.2-0.4 parts of wire drawing powder, silk gum it is water-soluble Liquid 0.1-0.2 parts.
CN201710180605.7A 2017-03-19 2017-03-19 Preparation method of natural pure-sericin liquid shampoo Pending CN106667789A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108041115A (en) * 2017-12-19 2018-05-18 牟小林 A kind of food compounding moisturizer containing silk gum and preparation method thereof
CN113842331A (en) * 2021-11-17 2021-12-28 广州宝丝捷生物科技有限公司 Novel soothing, nursing, refreshing and anti-dandruff shampoo and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102860977A (en) * 2012-10-12 2013-01-09 苏州谷力生物科技有限公司 Liquid shampoo for damaged hair
CN103830119A (en) * 2014-03-11 2014-06-04 安徽省农业科学院蚕桑研究所 Preparation method of toning lotion taking natural sericin as matrix
CN103876955A (en) * 2012-12-19 2014-06-25 南通富尔生物制品有限公司 Silkworm chrysalis protein shampoo
CN104622782A (en) * 2015-02-04 2015-05-20 广西壮族自治区环境保护科学研究院 Fermented traditional Chinese medicine detergent and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102860977A (en) * 2012-10-12 2013-01-09 苏州谷力生物科技有限公司 Liquid shampoo for damaged hair
CN103876955A (en) * 2012-12-19 2014-06-25 南通富尔生物制品有限公司 Silkworm chrysalis protein shampoo
CN103830119A (en) * 2014-03-11 2014-06-04 安徽省农业科学院蚕桑研究所 Preparation method of toning lotion taking natural sericin as matrix
CN104622782A (en) * 2015-02-04 2015-05-20 广西壮族自治区环境保护科学研究院 Fermented traditional Chinese medicine detergent and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108041115A (en) * 2017-12-19 2018-05-18 牟小林 A kind of food compounding moisturizer containing silk gum and preparation method thereof
CN113842331A (en) * 2021-11-17 2021-12-28 广州宝丝捷生物科技有限公司 Novel soothing, nursing, refreshing and anti-dandruff shampoo and preparation method thereof

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