CN109497610A - A kind of low-temperature heat cigarette with minty taste - Google Patents
A kind of low-temperature heat cigarette with minty taste Download PDFInfo
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- CN109497610A CN109497610A CN201811518597.3A CN201811518597A CN109497610A CN 109497610 A CN109497610 A CN 109497610A CN 201811518597 A CN201811518597 A CN 201811518597A CN 109497610 A CN109497610 A CN 109497610A
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- oil
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- cooling
- temperature heat
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 30
- 238000001816 cooling Methods 0.000 claims abstract description 49
- 239000003094 microcapsule Substances 0.000 claims abstract description 43
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 31
- 230000002101 lytic effect Effects 0.000 claims abstract description 30
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000003546 flue gas Substances 0.000 claims abstract description 25
- 238000004026 adhesive bonding Methods 0.000 claims abstract description 22
- 239000007800 oxidant agent Substances 0.000 claims abstract description 22
- 230000001590 oxidative effect Effects 0.000 claims abstract description 22
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 21
- 244000246386 Mentha pulegium Species 0.000 claims abstract description 18
- 235000016257 Mentha pulegium Nutrition 0.000 claims abstract description 18
- 235000004357 Mentha x piperita Nutrition 0.000 claims abstract description 18
- 235000001050 hortel pimenta Nutrition 0.000 claims abstract description 18
- 239000000853 adhesive Substances 0.000 claims abstract description 15
- 230000001070 adhesive effect Effects 0.000 claims abstract description 15
- 239000003205 fragrance Substances 0.000 claims abstract description 13
- 239000011159 matrix material Substances 0.000 claims abstract description 10
- 238000000889 atomisation Methods 0.000 claims abstract description 6
- 230000008859 change Effects 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims description 33
- 238000002156 mixing Methods 0.000 claims description 16
- 238000010438 heat treatment Methods 0.000 claims description 15
- 239000007864 aqueous solution Substances 0.000 claims description 14
- 239000000725 suspension Substances 0.000 claims description 14
- 239000007921 spray Substances 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 230000004044 response Effects 0.000 claims description 9
- 239000004006 olive oil Substances 0.000 claims description 8
- 235000008390 olive oil Nutrition 0.000 claims description 8
- 239000000243 solution Substances 0.000 claims description 8
- 239000003921 oil Substances 0.000 claims description 6
- 235000019198 oils Nutrition 0.000 claims description 6
- 239000001856 Ethyl cellulose Substances 0.000 claims description 5
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 claims description 5
- 108010010803 Gelatin Proteins 0.000 claims description 5
- 239000000443 aerosol Substances 0.000 claims description 5
- 235000019325 ethyl cellulose Nutrition 0.000 claims description 5
- 229920001249 ethyl cellulose Polymers 0.000 claims description 5
- 229920000159 gelatin Polymers 0.000 claims description 5
- 239000008273 gelatin Substances 0.000 claims description 5
- 235000019322 gelatine Nutrition 0.000 claims description 5
- 235000011852 gelatine desserts Nutrition 0.000 claims description 5
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims description 5
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 5
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 5
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 5
- 239000000123 paper Substances 0.000 claims description 5
- 229920000747 poly(lactic acid) Polymers 0.000 claims description 5
- -1 polyethylene terephthalate Polymers 0.000 claims description 5
- 239000004626 polylactic acid Substances 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 239000001525 mentha piperita l. herb oil Substances 0.000 claims description 4
- 229920001223 polyethylene glycol Polymers 0.000 claims description 4
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 3
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 3
- VUNOFAIHSALQQH-UHFFFAOYSA-N Ethyl menthane carboxamide Chemical compound CCNC(=O)C1CC(C)CCC1C(C)C VUNOFAIHSALQQH-UHFFFAOYSA-N 0.000 claims description 3
- 239000000944 linseed oil Substances 0.000 claims description 3
- 235000021388 linseed oil Nutrition 0.000 claims description 3
- 229940041616 menthol Drugs 0.000 claims description 3
- 239000008159 sesame oil Substances 0.000 claims description 3
- 235000011803 sesame oil Nutrition 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 3
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 2
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 2
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 2
- 235000006484 Paeonia officinalis Nutrition 0.000 claims description 2
- 244000170916 Paeonia officinalis Species 0.000 claims description 2
- 235000019482 Palm oil Nutrition 0.000 claims description 2
- 235000019483 Peanut oil Nutrition 0.000 claims description 2
- 239000004698 Polyethylene Substances 0.000 claims description 2
- 235000019484 Rapeseed oil Nutrition 0.000 claims description 2
- 235000019486 Sunflower oil Nutrition 0.000 claims description 2
- 235000019498 Walnut oil Nutrition 0.000 claims description 2
- 239000004676 acrylonitrile butadiene styrene Substances 0.000 claims description 2
- 239000005030 aluminium foil Substances 0.000 claims description 2
- 239000010495 camellia oil Substances 0.000 claims description 2
- 239000000919 ceramic Substances 0.000 claims description 2
- 235000005687 corn oil Nutrition 0.000 claims description 2
- 239000002285 corn oil Substances 0.000 claims description 2
- 239000008169 grapeseed oil Substances 0.000 claims description 2
- 239000002540 palm oil Substances 0.000 claims description 2
- 239000000312 peanut oil Substances 0.000 claims description 2
- 239000004033 plastic Substances 0.000 claims description 2
- 229920003023 plastic Polymers 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- 210000000582 semen Anatomy 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 239000003549 soybean oil Substances 0.000 claims description 2
- 235000012424 soybean oil Nutrition 0.000 claims description 2
- 239000002600 sunflower oil Substances 0.000 claims description 2
- 230000007704 transition Effects 0.000 claims description 2
- 239000008170 walnut oil Substances 0.000 claims description 2
- 244000061176 Nicotiana tabacum Species 0.000 claims 3
- ZOJBYZNEUISWFT-UHFFFAOYSA-N allyl isothiocyanate Chemical compound C=CCN=C=S ZOJBYZNEUISWFT-UHFFFAOYSA-N 0.000 claims 1
- 229920001577 copolymer Polymers 0.000 claims 1
- 235000019508 mustard seed Nutrition 0.000 claims 1
- 239000002304 perfume Substances 0.000 claims 1
- 239000005020 polyethylene terephthalate Substances 0.000 claims 1
- 229920000139 polyethylene terephthalate Polymers 0.000 claims 1
- 235000013599 spices Nutrition 0.000 claims 1
- 239000010410 layer Substances 0.000 abstract description 55
- 241000208125 Nicotiana Species 0.000 abstract description 18
- 230000000694 effects Effects 0.000 abstract description 14
- 239000011229 interlayer Substances 0.000 abstract description 6
- 238000004090 dissolution Methods 0.000 abstract description 4
- 238000005461 lubrication Methods 0.000 abstract description 3
- 210000000697 sensory organ Anatomy 0.000 abstract description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 22
- 210000000214 mouth Anatomy 0.000 description 16
- 238000000034 method Methods 0.000 description 10
- 238000012545 processing Methods 0.000 description 8
- 239000000654 additive Substances 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 4
- 238000009833 condensation Methods 0.000 description 4
- 230000005494 condensation Effects 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 239000013068 control sample Substances 0.000 description 3
- 238000004299 exfoliation Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 240000002853 Nelumbo nucifera Species 0.000 description 2
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 2
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 2
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 description 1
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 239000000828 canola oil Substances 0.000 description 1
- 235000019519 canola oil Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920002523 polyethylene Glycol 1000 Polymers 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000014860 sensory perception of taste Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F47/00—Smokers' requisites not otherwise provided for
Landscapes
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The present invention provides a kind of low-temperature heat cigarette with minty taste, including atomization matrix section interconnected and cooling mouth stick；The structure of cooling mouth stick is hollow cylindrical tubulose structure, ecto-entad successively includes shell, gluing oxidant layer, cooling layer, gluing oxidant layer bonds together shell and cooling layer, there are the thermosensitive type microcapsules for including lytic agent and the flavouring essence for tobacco containing peppermint in gluing oxidant layer, thermosensitive type microcapsules start to discharge lytic agent and flavouring essence for tobacco up to after responding temperature, to change the bond state and fragrance state of shell and the interlayer that cools down, increases the surface area of cooling layer and change flue gas stream path.Under the influence of the lytic agent that the present invention is discharged by thermosensitive type microcapsules is to multiple actions such as lubrication, the dissolutions of adhesive, reduce the viscosity of cooling layer and shell, achieve the effect that cooling layer falls off from shell with this, flue gas cool-down significant effect, flavouring essence for tobacco fragrance containing peppermint, sense organ cooling effect are preferable simultaneously.
Description
Technical field
The present invention relates to heat tobacco product technical field of not burning, specifically a kind of low-temperature heat with minty taste
Cigarette.
Background technique
Heating the cigarette that do not burn is to be atomized matrix section by electric heater unit to be heated to 200 DEG C -400 DEG C, to produce
The raw smog for being similar to traditional cigarette is aspirated for consumer, such usage mode will introduce a problem, it may be assumed that the temperature of flue gas
Excessively high, in the case where filter rod segments do not use cooling means, flue gas, which enters oral temperature, can achieve 70 DEG C or more, even more
Height has seriously affected the consumption experience of consumer.Therefore a kind of new type low temperature heating cigarette is designed, consumer can be significantly reduced
The temperature for sucking flue gas, is very desirable.
Flavouring essence for tobacco containing peppermint is food, daily use chemicals, one of most common fragrance in tobacco, has pure peppermint wind
Taste, cool feeling is powerful, and fragrance is pure and fresh clear, refreshing, brings except the enjoyment in the sense of taste to consumer, in aspiration procedure
In cooling taste, moreover it is possible to be not felt by the temperature of sucking flue gas indirectly in sensory experience, sense organ cooling effect is preferable.
Summary of the invention
The invention patent to solve the above problems, provides a kind of low-temperature heat volume with minty taste
Cigarette, by being rationally designed to its mouth stick, can be significantly reduced flue-gas temperature and increasing peppermint fragrance.
A kind of low-temperature heat cigarette with minty taste, including atomization matrix section interconnected and cooling mouth stick,
In
It is atomized matrix section, for generating aerosol after heating；
Cool down mouth stick, and structure is hollow cylindrical tubulose structure, and ecto-entad successively includes shell, gluing oxidant layer, drop
Warm layer, has the thermosensitive type microcapsules for including lytic agent and flavouring essence for tobacco in the gluing oxidant layer, and thermosensitive type microcapsules are up to ringing
Start to discharge lytic agent and flavouring essence for tobacco after answering temperature, thus change the bond state and fragrance state of shell and the interlayer that cools down,
Increase the surface area of cooling layer and change flue gas stream path, while also increasing suction fragrance.
Further, the response temperature of the thermosensitive type microcapsules is 55 DEG C -100 DEG C, after reaching response temperature, the heat
Quick type microcapsules start to discharge lytic agent.
Further, the lytic agent is fat-soluble solvent, including but not limited to Semen setariae oil, rapeseed oil, peanut oil, fire fiber crops
Oil, corn oil, olive oil, camellia oil, palm oil, canola oil, sunflower oil, soybean oil, sesame oil, linseed oil (flax
Oil), the combination of grape seed oil, walnut oil, one such or several substance such as peony seed oil.
Further, the flavouring essence for tobacco containing peppermint include but is not limited to Mint Essence, it is menthol, N-Ethyl-p-menthane-3-carboxamide, thin
One of lotus vegetable oil or combinations thereof.
Further, the thermosensitive type microcapsules account for the 10%-25% of adhesive total amount, in order to have after microcapsules rupture
Enough lytic agents release the viscosity to reduce adhesive.
Further, the material of the shell includes but is not limited to fibrous paper, plastics, ceramics.
Further, the cooling layer is film or thin slice with phase transition function, including polylactic acid, poly terephthalic acid
The mixing of one or more of glycol ester, acrylonitrile-butadiene-styrene copolymer, polyethylene and aluminium foil.
Further, it is designed to 0.5N- for bonding the bonding force that the gluing oxidant layer of shell and the layer that cools down generates
2N, in order to which the layer that cools down in nature or mechanical processing process will not fall off from the shell easily.
Further, the thermosensitive type microcapsules preparation method the following steps are included:
(1) gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG (1000-3000) are regard as wall material, according to (3-
10): (0.5-1): (0.5-1): the weight ratio of (0.8-1.5) is added to the water, be sufficiently stirred under the conditions of 60-75 DEG C into
Row dissolution is prepared into the wall material aqueous solution that wall material solid content is 8-25%；
(2) lytic agent is added in wall material aqueous solution by the 1%-6% of wall material aqueous solution weight, while by flavouring essence for tobacco
Additive amount is added in wall material aqueous solution by the 10%-45% of the lytic agent, and is sufficiently stirred under the conditions of 60-75 DEG C
It mixes, forms oil-in-water mixing suspension；
(3) powder processed is dried in above-mentioned mixing suspension using spray dryer to handle, wherein in spray dryer
Hopper and nozzle need to carry out heat treatment, and temperature is controlled at 60-80 DEG C or so, in hopper and spray after avoiding mixing suspension cooling
Mouth etc. condensation.
The beneficial effects of the present invention are:
(1) contradiction between flue gas cool-down and mechanization production is solved by introducing thermosensitive type microcapsules, it may be assumed that the drop
Gluing oxidant layer in warm mouth stick must have enough bonding forces, so that the shell and cooling layer are compound than stronger, certainly
Under right state especially during mechanization production, when equipment blade cuts the cooling pipe, the cooling layer be will not fall off,
Because if falling off, blade cooling layer very difficult to cut off, to will lead to equipment downtime；And it is non-ignitable to aspirate heating in consumer
During burning cigarette, and need gluing oxidant layer bonding force smaller, the cooling layer can fall off from shell, partial exfoliation, production
Raw fold or ripple glaze structure to increase surface area and change flue gas stream path with this, reach apparent flue gas cool-down effect.
In the scheme only with adhesive bonds, this balance is difficult to control, and by introducing thermosensitive type microcapsules, it is aspirating
Heating is not burnt during cigarette, and flue-gas temperature can allow the PEG structure collapse in thermosensitive type microcapsules to rupture, to release molten
Solve agent, by lytic agent to multiple actions such as lubrication, the dissolutions of adhesive under the influence of, reduce cool down layer and shell viscosity, with
This achievees the effect that cooling layer falls off from shell, partial exfoliation, generates fold or ripple glaze structure, and flue gas cool-down effect is aobvious
It writes.
(2) the technical program introduces the flavouring essence for tobacco containing peppermint, the package and shell of one side thermosensitive type microcapsules simultaneously
The sealing space that body and cooling interlayer are formed, can effectively reduce the escape of peppermint fragrance during cigarette storage, in aspiration procedure,
Microcapsules structure collapse, and cooling layer fall off, so that peppermint fragrance sufficiently escapes, fragrance is more longlasting, more rich, on the other hand
Flavouring essence for tobacco containing peppermint can provide refrigerant suction experience to consumer, although flue-gas temperature, energy cannot be reduced directly
Consumer is enough allowed to be not felt by the temperature of sucking flue gas indirectly in sensory experience, sense organ cooling effect is preferable.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of low-temperature heat cigarette of the present invention；
Fig. 2 is the structural schematic diagram of cooling mouth stick in low-temperature heat cigarette of the present invention；
Fig. 3 is the schematic cross-section of cooling mouth stick in low-temperature heat cigarette of the present invention.
Appended drawing reference is as follows in figure: 1- low-temperature heat cigarette；2- is atomized matrix section；3- cooling mouth stick；301- shell；302-
Gluing oxidant layer；303- cooling layer
Specific embodiment
Below in conjunction with the attached drawing in the present invention, the technical solution in the present invention is clearly and completely described.
Embodiment one
As shown in Figure 1-3, a kind of low-temperature heat cigarette 1 with minty taste, comprising: atomization matrix section 2, for heating
After generate aerosol；Cool down mouth stick 3, and for reducing the flue-gas temperature for entering oral cavity, structure is hollow cylindrical tubulose structure,
It is made of shell 301, gluing oxidant layer 302, cooling layer 303, shell 301 and cooling layer 303 are bonded in one by gluing oxidant layer 302
It rises.
It include thermosensitive type microcapsules in the gluing oxidant layer, for changing the bonding of shell and the interlayer that cools down in aspiration procedure
State improves flue gas cool-down efficiency.The thermosensitive type microcapsules response temperature is 60 DEG C or so, described after reaching response temperature
Microcapsules start to discharge lytic agent and flavouring essence for tobacco；The lytic agent selects olive oil, and the flavouring essence for tobacco containing peppermint is by thin
Lotus brain, N-Ethyl-p-menthane-3-carboxamide, peppermint oil dementholized are formed according to 1:0.3:0.8, and the thermosensitive type microcapsules account for the 15% of adhesive total amount, with
Convenient for there is enough lytic agents to release the viscosity to reduce adhesive, and offer peppermint fragrance after microcapsules rupture；
The case material is fibrous paper, and the cooling layer is made of polylactic acid, for bonding the adhesive of shell and the layer that cools down
The bonding force that layer generates is designed to 1N, will not be easily from described in order to cool down layer in nature or mechanical processing process
It falls off on shell.
Wherein the thermosensitive type microcapsules preparation method the following steps are included:
(1) using gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG1000 as wall material, according to 5:0.5:0.5:
1 weight ratio is added to the water, and is sufficiently stirred and is dissolved under the conditions of 60-75 DEG C, is prepared into wall material solid content and is
10% solution；
(2) olive oil is added in wall material aqueous solution by the 3% of wall material solution weight, while by flavouring essence for tobacco additive amount
It is added in wall material aqueous solution by the 20% of the lytic agent, and is still sufficiently stirred under the conditions of 60-75 DEG C, form water
Wrap the mixing suspension of oil；
(3) powder processed is dried in above-mentioned mixing suspension using spray dryer to handle, it is preferred that emphasis is spray dryer
Hopper and nozzle need to carry out heat treatment, temperature is controlled at 60-80 DEG C or so, after avoiding mixing suspension cooling in hopper and
Nozzle etc. condensation.
Embodiment two
As shown in Figure 1-3, a kind of low-temperature heat cigarette 1 with minty taste, comprising: atomization matrix section 2, for heating
After generate aerosol；Cool down mouth stick 3, and for reducing the flue-gas temperature for entering oral cavity, structure is hollow cylindrical tubulose structure,
It is made of shell 301, gluing oxidant layer 302, cooling layer 303.
It include thermosensitive type microcapsules in the gluing oxidant layer, for changing the bonding of shell and the interlayer that cools down in aspiration procedure
State improves flue gas cool-down efficiency.The thermosensitive type microcapsules response temperature is 60 DEG C or so, described after reaching response temperature
Microcapsules start to discharge lytic agent；The lytic agent selects olive oil, and the flavouring essence for tobacco containing peppermint is by menthol, peppermint acyl
Amine, peppermint oil dementholized are formed according to 0.8:0.7:1, and the thermosensitive type microcapsules account for the 20% of adhesive total amount, in order to microcapsules
There are enough lytic agents to release the viscosity to reduce adhesive after rupture；The case material is fibrous paper, the drop
Warm layer is tool polylactic acid, and the bonding force that the gluing oxidant layer for bonding shell and the layer that cools down generates is designed to 1.5N, with
It will not fall off from the shell easily convenient for the layer that cools down in nature or mechanical processing process.
The preparation methods of the thermosensitive type microcapsules the following steps are included:
(1) using gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG2000 as wall material, according to 8:0.6:0.7:
1.2 weight ratio is added to the water, and is sufficiently stirred and is dissolved under the conditions of 60-75 DEG C, is prepared into wall material solid content and is
15% solution；
(2) olive oil is added in wall material aqueous solution by the 5% of wall material solution weight, while by flavouring essence for tobacco additive amount
It is added in wall material aqueous solution by the 20% of the lytic agent, and is still sufficiently stirred under the conditions of 60-75 DEG C, form water
Wrap the mixing suspension of oil；
(3) powder processed is dried in above-mentioned mixing suspension using spray dryer to handle, it is preferred that emphasis is spray dryer
Hopper and nozzle need to carry out heat treatment, temperature is controlled at 60-80 DEG C or so, after avoiding mixing suspension cooling in hopper and
Nozzle etc. condensation.
Embodiment three
As shown in Figure 1-3, a kind of low-temperature heat cigarette 1 with minty taste, comprising: atomization matrix section 2, for heating
After generate aerosol；Cool down mouth stick 3, and for reducing the flue-gas temperature for entering oral cavity, structure is hollow cylindrical tubulose structure,
It is made of shell 301, gluing oxidant layer 302, cooling layer 303.
It include thermosensitive type microcapsules in the gluing oxidant layer, for changing the bonding of shell and the interlayer that cools down in aspiration procedure
State improves flue gas cool-down efficiency.The thermosensitive type microcapsules response temperature is 60 DEG C or so, described after reaching response temperature
Microcapsules start to discharge lytic agent；The lytic agent selects olive oil, and the flavouring essence for tobacco containing peppermint is made of peppermint oil dementholized,
The thermosensitive type microcapsules account for the 12% of adhesive total amount, in order to there is enough lytic agents to release use after microcapsules rupture
To reduce the viscosity of adhesive；The case material is fibrous paper, and the cooling layer is tool polylactic acid, for bonding shell and drop
The bonding force that the gluing oxidant layer of warm layer generates is designed to 0.8N, in order to drop in nature or mechanical processing process
Warm layer will not fall off from the shell easily.
The preparation methods of the thermosensitive type microcapsules the following steps are included:
(1) using gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG2000 as wall material, according to 10:1:1:
The weight ratio of 0.8:0.6:0.7:0.8 is added to the water, and is sufficiently stirred and is dissolved under the conditions of 60-75 DEG C, is prepared into
The solution that wall material solid content is 20%；
(2) olive oil is added in wall material aqueous solution by the 5% of wall material solution weight, while by flavouring essence for tobacco additive amount
It is added in wall material aqueous solution by the 20% of the lytic agent, and is still sufficiently stirred under the conditions of 60-75 DEG C, form water
Wrap the mixing suspension of oil；
(3) powder processed is dried in above-mentioned mixing suspension using spray dryer to handle, it is preferred that emphasis is spray dryer
Hopper and nozzle need to carry out heat treatment, temperature is controlled at 60-80 DEG C or so, after avoiding mixing suspension cooling in hopper and
Nozzle etc. condensation.
When with continuous production 1h, equipment downtime number is measured cooling pipe processing performance, is entered with flue gas as evaluation index
Temperature when oral cavity evaluates cooling effect, the physical property and temperature reduction performance test result of above three embodiments as index
It is shown in Table 1:
The cooling mouth stick combination property analysis result of table 1
| Sample | Processing performance | Cooling effect | Peppermint fragrance |
| Control sample | 14 | 54.5℃ | Nothing |
| Embodiment one | 8 | 45.2℃ | Preferably |
| Embodiment two | 10 | 44.6℃ | Preferably |
| Embodiment three | 12 | 46.1℃ | Generally |
Wherein, control sample is free of thermosensitive type microcapsules, for bonding the gluing oxidant layer of shell 301 and the layer 303 that cools down
302 bonding forces generated are designed to 0.5N.
It can be seen that control sample in the case where being added without thermosensitive type microcapsules according to above-mentioned results of performance analysis, even if
Processing performance is reduced, can not meet cooling effect well, due to introducing thermosensitive type microcapsules in above three embodiments,
During cigarette is not burnt in suction heating, flue-gas temperature can allow the PEG structure collapse in thermosensitive type microcapsules to rupture, to release
Release lytic agent, by lytic agent to multiple actions such as lubrication, the dissolutions of adhesive under the influence of, reduce cool down layer and shell
Viscosity can make the layer partial exfoliation that cool down, and increase the surface area that flue gas is contacted with the layer that cools down, extend smoke path, have
Certain cooling effect, thermosensitive type microcapsule content is higher in embodiment two, and cooling effect is preferable, but causes processing performance comparison real
It is a bit weaker to apply example one, in general, embodiment one and two resultant effect of embodiment are all preferable.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Belong to those skilled in the art in the technical scope disclosed by the present invention, any changes or substitutions that can be easily thought of, all answers
It is included within the scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection scope in claims.
Claims (9)
1. a kind of low-temperature heat cigarette with minty taste, it is characterised in that: including atomization matrix section (2) interconnected and
Cool down mouth stick (3), wherein
It is atomized matrix section (2), for generating aerosol after heating；
Cool down mouth stick (3), structure is hollow cylindrical tubulose structure, and ecto-entad successively includes shell (301), gluing oxidant layer
(302), cool down layer (303), gluing oxidant layer (302) bonds together shell (301) and cooling layer (303), the adhesive
(302) have the thermosensitive type microcapsules for including lytic agent and the flavouring essence for tobacco containing peppermint in layer, and thermosensitive type microcapsules are reaching response
Start to discharge lytic agent and flavouring essence for tobacco after temperature, to change the bond state and perfume (or spice) between shell (301) and cooling layer (303)
Gaseity increases the surface area of cooling layer (303) and changes flue gas stream path, while also increasing suction fragrance.
2. as described in claim 1 with the low-temperature heat cigarette of minty taste, it is characterised in that: the thermosensitive type microcapsules
Responding temperature is 55 DEG C -100 DEG C.
3. as described in claim 1 with the low-temperature heat cigarette of minty taste, it is characterised in that: the lytic agent is fat-soluble
Solvent, including but not limited to Semen setariae oil, rapeseed oil, peanut oil, fiery sesame oil, corn oil, olive oil, camellia oil, palm oil, mustard
Seed oil, sunflower oil, soybean oil, sesame oil, linseed oil, grape seed oil, walnut oil, peony seed oil etc. are one such or several
The combination of kind substance.
4. as described in claim 1 with the low-temperature heat cigarette of minty taste, it is characterised in that: the cigarette containing peppermint is fragrant
Essence includes but is not limited to one of Mint Essence, menthol, N-Ethyl-p-menthane-3-carboxamide, peppermint oil dementholized or combinations thereof.
5. as described in claim 1 with the low-temperature heat cigarette of minty taste, it is characterised in that: the thermosensitive type microcapsules account for
The 10%-25% of adhesive total amount.
6. as described in claim 1 with the low-temperature heat cigarette of minty taste, it is characterised in that: the material of the shell (301)
Material includes but is not limited to fibrous paper, plastics, ceramics.
7. as described in claim 1 with the low-temperature heat cigarette of minty taste, it is characterised in that: the cooling layer (303) is
Film or thin slice with phase transition function, including polylactic acid, polyethylene terephthalate, acrylonitrile-butadiene-styrene (ABS)
The mixing of one or more of copolymer, polyethylene and aluminium foil.
8. as described in claim 1 with the low-temperature heat cigarette of minty taste, it is characterised in that: for bonding shell (301)
The bonding force generated with the gluing oxidant layer (302) of cooling layer (303) is designed to 0.5N-2N.
9. as described in claim 1 with the low-temperature heat cigarette of minty taste, it is characterised in that: the thermosensitive type microcapsules
Preparation method the following steps are included:
(1) gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG (1000-3000) are regard as wall material, according to (3-10):
(0.5-1): (0.5-1): the weight ratio of (0.8-1.5) is added to the water, and it is molten that progress is sufficiently stirred under the conditions of 60-75 DEG C
Solution is prepared into the wall material aqueous solution that wall material solid content is 8-25%；
(2) lytic agent is added in wall material aqueous solution by the 1%-6% of wall material aqueous solution weight, while flavouring essence for tobacco is added
Amount is added in wall material aqueous solution by the 10%-45% of the lytic agent.And it is sufficiently stirred under the conditions of 60-75 DEG C, shape
At oil-in-water mixing suspension；
(3) powder processed is dried in above-mentioned mixing suspension using spray dryer to handle, wherein in the hopper of spray dryer
And nozzle need to carry out heat treatment, temperature is controlled at 60-80 DEG C or so.
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| CN201811518597.3A CN109497610B (en) | 2018-12-12 | 2018-12-12 | Low-temperature heating cigarette with mint taste |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811518597.3A CN109497610B (en) | 2018-12-12 | 2018-12-12 | Low-temperature heating cigarette with mint taste |
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| CN109497610B CN109497610B (en) | 2021-07-06 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110680006A (en) * | 2019-11-08 | 2020-01-14 | 湖北中烟工业有限责任公司 | Aromatized hollow bar and production method thereof |
| CN113424986A (en) * | 2021-07-26 | 2021-09-24 | 云南养瑞科技集团有限公司 | Fragrance-carrying cooling filter tip rod and preparation method thereof |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB201114675D0 (en) * | 2011-08-25 | 2011-10-12 | British American Tobacco Co | Smoking article filter |
| CN103865650B (en) * | 2014-03-20 | 2015-10-21 | 中国热带农业科学院农产品加工研究所 | A kind of cigarette temperature sensitivity aroma essence microcapsule and preparation method thereof |
| CN107087811B (en) * | 2017-05-26 | 2019-10-11 | 湖北中烟工业有限责任公司 | With the low temperature cigarette for reducing flue-gas temperature and preventing mouth stick heat from collapsing |
| CN107960680B (en) * | 2017-12-26 | 2023-12-26 | 云南巴菰生物科技股份有限公司 | Paper tube capable of reducing smoke temperature and releasing fragrance and application thereof |
| CN108576918A (en) * | 2018-01-08 | 2018-09-28 | 湖北中烟工业有限责任公司 | A kind of low temperature cigarette with temperature descending section |
| CN108523220A (en) * | 2018-06-20 | 2018-09-14 | 湖北中烟工业有限责任公司 | A kind of improved cooling filter stick and the low temperature cigarette containing the filter stick |
-
2018
- 2018-12-12 CN CN201811518597.3A patent/CN109497610B/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110680006A (en) * | 2019-11-08 | 2020-01-14 | 湖北中烟工业有限责任公司 | Aromatized hollow bar and production method thereof |
| CN110680006B (en) * | 2019-11-08 | 2022-04-29 | 湖北中烟工业有限责任公司 | Aromatized hollow bar and production method thereof |
| CN113424986A (en) * | 2021-07-26 | 2021-09-24 | 云南养瑞科技集团有限公司 | Fragrance-carrying cooling filter tip rod and preparation method thereof |
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