CN109363254A - A kind of low-temperature heat cigarette - Google Patents

A kind of low-temperature heat cigarette Download PDF

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Publication number
CN109363254A
CN109363254A CN201811518594.XA CN201811518594A CN109363254A CN 109363254 A CN109363254 A CN 109363254A CN 201811518594 A CN201811518594 A CN 201811518594A CN 109363254 A CN109363254 A CN 109363254A
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China
Prior art keywords
oil
layer
shell
cooling
low
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Granted
Application number
CN201811518594.XA
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Chinese (zh)
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CN109363254B (en
Inventor
刘冰
陈义坤
罗诚浩
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Priority to CN201811518594.XA priority Critical patent/CN109363254B/en
Publication of CN109363254A publication Critical patent/CN109363254A/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F47/00Smokers' requisites not otherwise provided for

Abstract

The present invention provides a kind of low-temperature heat cigarette, including atomization matrix section interconnected and cooling mouth stick, wherein atomization matrix section is for generating aerosol after heating;The structure of cooling mouth stick is hollow cylindrical tubulose structure, ecto-entad successively includes shell, gluing oxidant layer, cooling layer, gluing oxidant layer bonds together shell and cooling layer, there are the thermosensitive type microcapsules for including lytic agent in the gluing oxidant layer, thermosensitive type microcapsules start to discharge lytic agent up to after responding temperature, to change the bond state of shell and the interlayer that cools down, increases the surface area of cooling layer and change flue gas stream path.The present invention is by introducing thermosensitive type microcapsules, flue-gas temperature can allow the PEG structure collapse in thermosensitive type microcapsules to rupture in aspiration procedure, to release lytic agent, by lytic agent to multiple actions such as lubrication, the dissolutions of adhesive under the influence of, reduce the viscosity of cooling layer and shell, achieve the effect that cooling layer falls off from shell with this, flue gas cool-down significant effect.

Description

A kind of low-temperature heat cigarette
Technical field
The present invention relates to heat tobacco product technical field of not burning, specifically a kind of low-temperature heat cigarette.
Background technique
Heating the cigarette that do not burn is to be atomized matrix section by electric heater unit to be heated to 200 DEG C -400 DEG C, to produce The raw smog for being similar to traditional cigarette is aspirated for consumer, such usage mode will introduce a problem, it may be assumed that the temperature of flue gas Excessively high, in the case where filter rod segments do not use cooling means, flue gas, which enters oral temperature, can achieve 70 DEG C or more, even more Height has seriously affected the consumption experience of consumer.Therefore a kind of new type low temperature heating cigarette is designed, consumer can be significantly reduced The temperature for sucking flue gas, is very desirable.
Summary of the invention
The invention patent to solve the above problems, provides a kind of low-temperature heat cigarette, by its mouth stick It is rationally designed, can be significantly reduced flue-gas temperature.
A kind of low-temperature heat cigarette, including atomization matrix section interconnected and cooling mouth stick, wherein
It is atomized matrix section, for generating aerosol after heating;
Cool down mouth stick, and structure is hollow cylindrical tubulose structure, and ecto-entad successively includes shell, gluing oxidant layer, drop Warm layer, has the thermosensitive type microcapsules for including lytic agent in the gluing oxidant layer, and thermosensitive type microcapsules are up to opening after response temperature Begin release lytic agent, to change the bond state of shell and the interlayer that cools down, increase the surface area of cooling layer and change flue gas gas Flow path.
Further, the response temperature of the thermosensitive type microcapsules is 55 DEG C -100 DEG C, after reaching response temperature, the heat Quick type microcapsules start to discharge lytic agent.
Further, the lytic agent is fat-soluble solvent, including but not limited to Semen setariae oil, rapeseed oil, peanut oil, fire fiber crops Oil, corn oil, olive oil, camellia oil, palm oil, canola oil, sunflower oil, soybean oil, sesame oil, linseed oil (flax Oil), the combination of grape seed oil, walnut oil, one such or several substance such as peony seed oil.
Further, the thermosensitive type microcapsules account for the 10%-25% of adhesive total amount, in order to have after microcapsules rupture Enough lytic agents release the viscosity to reduce adhesive.
Further, the material of the shell includes but is not limited to fibrous paper, plastics, ceramics.
Further, the cooling layer is film or thin slice with phase transition function, including polylactic acid, poly terephthalic acid The mixing of one or more of glycol ester, acrylonitrile-butadiene-styrene copolymer, polyethylene and aluminium foil.
Further, it is designed to 0.5N- for bonding the bonding force that the gluing oxidant layer of shell and the layer that cools down generates 2N, in order to which the layer that cools down in nature or mechanical processing process will not fall off from the shell easily.
Further, the thermosensitive type microcapsules preparation method the following steps are included:
(1) gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG (1000-3000) are regard as wall material, according to (3- 10): (0.5-1): (0.5-1): the weight ratio of (0.8-1.5) is added to the water, be sufficiently stirred under the conditions of 60-75 DEG C into Row dissolution is prepared into the wall material aqueous solution that wall material solid content is 8-25%;
(2) lytic agent is added in wall material aqueous solution by the 1%-6% of wall material aqueous solution weight, and in 60-75 DEG C of item It is sufficiently stirred under part, forms oil-in-water mixing suspension;
(3) powder processed is dried in above-mentioned mixing suspension using spray dryer to handle, wherein in spray dryer Hopper and nozzle need to carry out heat treatment, and temperature is controlled at 60-80 DEG C or so, in hopper and spray after avoiding mixing suspension cooling Mouth etc. condensation.
The beneficial effects of the present invention are: by introduce thermosensitive type microcapsules solve flue gas cool-down and mechanization production it Between contradiction, it may be assumed that it is described cooling mouth stick in gluing oxidant layer must have enough bonding forces so that the shell and cooling layer It is compound than stronger, in its natural state especially during mechanization production, equipment blade cut the cooling pipe when, institute Stating cooling layer will not fall off, because if falling off, blade cooling layer very difficult to cut off, to will lead to equipment downtime;And Consumer's suction heating is not burnt during cigarette, and needs gluing oxidant layer bonding force smaller, and the cooling layer can be from shell On fall off, partial exfoliation, generate fold or ripple glaze structure, flue gas stream path to increase surface area and is changed with this, is reached Apparent flue gas cool-down effect.In the scheme only with adhesive bonds, this balance is difficult to control, and passes through introducing Thermosensitive type microcapsules, during cigarette is not burnt in suction heating, flue-gas temperature can allow the PEG skeleton in thermosensitive type microcapsules to collapse Collapse rupture, to release lytic agent, by lytic agent to multiple actions such as lubrication, the dissolutions of adhesive under the influence of, reduce drop The viscosity of warm layer and shell, with this reach cooling layer fall off from shell, partial exfoliation, the effect for generating fold or ripple glaze structure Fruit, flue gas cool-down significant effect.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of low-temperature heat cigarette of the present invention;
Fig. 2 is the structural schematic diagram of cooling mouth stick in low-temperature heat cigarette of the present invention;
Fig. 3 is the schematic cross-section of cooling mouth stick in low-temperature heat cigarette of the present invention.
Appended drawing reference is as follows in figure: 1- low-temperature heat cigarette;2- is atomized matrix section;3- cooling mouth stick;301- shell;302- Gluing oxidant layer;303- cooling layer
Specific embodiment
Below in conjunction with the attached drawing in the present invention, the technical solution in the present invention is clearly and completely described.
Embodiment one
As shown in Figure 1-3, a kind of low-temperature heat cigarette 1, comprising: atomization matrix section 2, for generating aerosol after heating; Cool down mouth stick 3, and for reducing the flue-gas temperature for entering oral cavity, structure is hollow cylindrical tubulose structure, by shell 301, glue Adhesive layer 302, cooling layer 303 form, and gluing oxidant layer 302 bonds together shell 301 and cooling layer 303.
It include thermosensitive type microcapsules in the gluing oxidant layer, for changing the bonding of shell and the interlayer that cools down in aspiration procedure State improves flue gas cool-down efficiency.The thermosensitive type microcapsules response temperature is 60 DEG C or so, described after reaching response temperature Microcapsules start to discharge lytic agent;The lytic agent selects olive oil, and the thermosensitive type microcapsules account for the 15% of adhesive total amount, In order to there is enough lytic agents to release the viscosity to reduce adhesive after microcapsules rupture;The case material is fibre Paper is tieed up, the cooling layer is made of polylactic acid, the bonding force quilt that the gluing oxidant layer for bonding shell and the layer that cools down generates 1N is designed to, in order to which the layer that cools down in nature or mechanical processing process will not fall off from the shell easily.
Wherein the thermosensitive type microcapsules preparation method the following steps are included:
(1) using gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG1000 as wall material, according to 5:0.5:0.5: 1 weight ratio is added to the water, and is sufficiently stirred and is dissolved under the conditions of 60-75 DEG C, is prepared into wall material solid content and is 10% solution;
(2) olive oil is added in wall material aqueous solution by the 3% of wall material solution weight, and still in 60-75 DEG C of condition Under be sufficiently stirred, form oil-in-water mixing suspension;
(3) powder processed is dried in above-mentioned mixing suspension using spray dryer to handle, it is preferred that emphasis is spray dryer Hopper and nozzle need to carry out heat treatment, temperature is controlled at 60-80 DEG C or so, after avoiding mixing suspension cooling in hopper and Nozzle etc. condensation.
Embodiment two
As shown in Figure 1-3, a kind of low-temperature heat cigarette 1, comprising: atomization matrix section 2, for generating aerosol after heating; Cool down mouth stick 3, and for reducing the flue-gas temperature for entering oral cavity, structure is hollow cylindrical tubulose structure, by shell 301, glue Adhesive layer 302, cooling layer 303 form.
It include thermosensitive type microcapsules in the gluing oxidant layer, for changing the bonding of shell and the interlayer that cools down in aspiration procedure State improves flue gas cool-down efficiency.The thermosensitive type microcapsules response temperature is 60 DEG C or so, described after reaching response temperature Microcapsules start to discharge lytic agent;The lytic agent selects olive oil, and the thermosensitive type microcapsules account for the 20% of adhesive total amount, In order to there is enough lytic agents to release the viscosity to reduce adhesive after microcapsules rupture;The case material is fibre Paper is tieed up, the cooling layer is tool polylactic acid, and the bonding force that the gluing oxidant layer for bonding shell and the layer that cools down generates is set 1.5N is counted into, in order to which the layer that cools down in nature or mechanical processing process will not fall off from the shell easily.
The preparation methods of the thermosensitive type microcapsules the following steps are included:
(1) using gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG2000 as wall material, according to 8:0.6:0.7: 1.2 weight ratio is added to the water, and is sufficiently stirred and is dissolved under the conditions of 60-75 DEG C, is prepared into wall material solid content and is 15% solution;
(2) olive oil is added in wall material aqueous solution by the 5% of wall material solution weight, and still in 60-75 DEG C of condition Under be sufficiently stirred, form oil-in-water mixing suspension;
(3) powder processed is dried in above-mentioned mixing suspension using spray dryer to handle, it is preferred that emphasis is spray dryer Hopper and nozzle need to carry out heat treatment, temperature is controlled at 60-80 DEG C or so, after avoiding mixing suspension cooling in hopper and Nozzle etc. condensation.
Embodiment three
As shown in Figure 1-3, a kind of low-temperature heat cigarette 1, comprising: atomization matrix section 2, for generating aerosol after heating; Cool down mouth stick 3, and for reducing the flue-gas temperature for entering oral cavity, structure is hollow cylindrical tubulose structure, by shell 301, glue Adhesive layer 302, cooling layer 303 form.
It include thermosensitive type microcapsules in the gluing oxidant layer, for changing the bonding of shell and the interlayer that cools down in aspiration procedure State improves flue gas cool-down efficiency.The thermosensitive type microcapsules response temperature is 60 DEG C or so, described after reaching response temperature Microcapsules start to discharge lytic agent;The lytic agent selects olive oil, and the thermosensitive type microcapsules account for the 12% of adhesive total amount, In order to there is enough lytic agents to release the viscosity to reduce adhesive after microcapsules rupture;The case material is fibre Paper is tieed up, the cooling layer is tool polylactic acid, and the bonding force that the gluing oxidant layer for bonding shell and the layer that cools down generates is set 0.8N is counted into, in order to which the layer that cools down in nature or mechanical processing process will not fall off from the shell easily.
The preparation methods of the thermosensitive type microcapsules the following steps are included:
(1) using gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG2000 as wall material, according to 10:1:1: The weight ratio of 0.8:0.6:0.7:0.8 is added to the water, and is sufficiently stirred and is dissolved under the conditions of 60-75 DEG C, is prepared into The solution that wall material solid content is 20%;
(2) olive oil is added in wall material aqueous solution by the 5% of wall material solution weight, and still in 60-75 DEG C of condition Under be sufficiently stirred, form oil-in-water mixing suspension;
(3) powder processed is dried in above-mentioned mixing suspension using spray dryer to handle, it is preferred that emphasis is spray dryer Hopper and nozzle need to carry out heat treatment, temperature is controlled at 60-80 DEG C or so, after avoiding mixing suspension cooling in hopper and Nozzle etc. condensation.
When with continuous production 1h, equipment downtime number is measured cooling pipe processing performance, is entered with flue gas as evaluation index Temperature when oral cavity evaluates cooling effect, the physical property and temperature reduction performance test result of above three embodiments as index It is shown in Table 1:
The cooling mouth stick combination property analysis result of table 1
Sample Processing performance Cooling effect
Control sample 14 54.5℃
Embodiment one 8 45.2℃
Embodiment two 10 44.6℃
Embodiment three 12 46.1℃
Wherein, control sample is free of thermosensitive type microcapsules, for bonding the gluing oxidant layer of shell 301 and the layer 303 that cools down 302 bonding forces generated are designed to 0.5N.
It can be seen that control sample in the case where being added without thermosensitive type microcapsules according to above-mentioned results of performance analysis, even if Processing performance is reduced, can not meet cooling effect well, due to introducing thermosensitive type microcapsules in above three embodiments, During cigarette is not burnt in suction heating, flue-gas temperature can allow the PEG structure collapse in thermosensitive type microcapsules to rupture, to release Release lytic agent, by lytic agent to multiple actions such as lubrication, the dissolutions of adhesive under the influence of, reduce cool down layer and shell Viscosity can make the layer partial exfoliation that cool down, and increase the surface area that flue gas is contacted with the layer that cools down, extend smoke path, have Certain cooling effect, thermosensitive type microcapsule content is higher in embodiment two, and cooling effect is preferable, but leads to processing performance slightly worse one A bit, in general, embodiment one and two resultant effect of embodiment are all preferable.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any Belong to those skilled in the art in the technical scope disclosed by the present invention, any changes or substitutions that can be easily thought of, all answers It is included within the scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection scope in claims.

Claims (8)

1. a kind of low-temperature heat cigarette, it is characterised in that: including atomization matrix section (2) interconnected and cool down mouth stick (3), In
It is atomized matrix section (2), for generating aerosol after heating;
Cool down mouth stick (3), structure is hollow cylindrical tubulose structure, and ecto-entad successively includes shell (301), gluing oxidant layer (302), cool down layer (303), gluing oxidant layer (302) bonds together shell (301) and cooling layer (303), the adhesive (302) have the thermosensitive type microcapsules for including lytic agent in layer, and thermosensitive type microcapsules are starting release dissolution up to after responding temperature Agent, to change the bond state between shell (301) and cooling layer (303), increase the surface area of cooling layer (303) and change cigarette Gas air flow path.
2. low-temperature heat cigarette as described in claim 1, it is characterised in that: the response temperature of the thermosensitive type microcapsules is 55 ℃-100℃。
3. low-temperature heat cigarette as described in claim 1, it is characterised in that: the lytic agent is fat-soluble solvent, including but not It is limited to Semen setariae oil, rapeseed oil, peanut oil, fiery sesame oil, corn oil, olive oil, camellia oil, palm oil, canola oil, sunflower seed Oil, soybean oil, sesame oil, linseed oil, grape seed oil, walnut oil, peony seed oil etc. be one such or the group of several substances It closes.
4. low-temperature heat cigarette as described in claim 1, it is characterised in that: the thermosensitive type microcapsules account for adhesive total amount 10%-25%.
5. low-temperature heat cigarette as described in claim 1, it is characterised in that: the material of the shell 301 includes but is not limited to fibre Tie up paper, plastics, ceramics.
6. low-temperature heat cigarette as described in claim 1, it is characterised in that: the cooling layer (303) is with phase transition function Film or thin slice, including polylactic acid, polyethylene terephthalate, acrylonitrile-butadiene-styrene copolymer, polyethylene And the mixing of one or more of aluminium foil.
7. low-temperature heat cigarette as described in claim 1, it is characterised in that: for bonding shell (301) and cooling down layer (303) The bonding force that the gluing oxidant layer (302) generates is designed to 0.5N-2N.
8. low-temperature heat cigarette as described in claim 1, it is characterised in that: the preparation method of the thermosensitive type microcapsules include with Lower step:
(1) gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG (1000-3000) are regard as wall material, according to (3-10): (0.5-1): (0.5-1): the weight ratio of (0.8-1.5) is added to the water, and it is molten that progress is sufficiently stirred under the conditions of 60-75 DEG C Solution is prepared into the wall material aqueous solution that wall material solid content is 8-25%;
(2) lytic agent is added in wall material aqueous solution by the 1%-6% of wall material aqueous solution weight, and under the conditions of 60-75 DEG C It is sufficiently stirred, forms oil-in-water mixing suspension;
(3) powder processed is dried in above-mentioned mixing suspension using spray dryer to handle, wherein in the hopper of spray dryer And nozzle need to carry out heat treatment, temperature is controlled at 60-80 DEG C or so.
CN201811518594.XA 2018-12-12 2018-12-12 Low-temperature heating cigarette Active CN109363254B (en)

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CN109363254B CN109363254B (en) 2021-02-19

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Publication number Priority date Publication date Assignee Title
CN112137163A (en) * 2019-06-28 2020-12-29 湖北中烟工业有限责任公司 Blending material and preparation method and application thereof
WO2020258466A1 (en) * 2019-06-28 2020-12-30 湖北中烟工业有限责任公司 Phase-change material, preparation method therefor and use thereof
CN112220109A (en) * 2019-06-28 2021-01-15 湖北中烟工业有限责任公司 Phase change material and preparation method and application thereof

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CN107087811A (en) * 2017-05-26 2017-08-25 湖北中烟工业有限责任公司 With reduction flue-gas temperature and the low temperature cigarette for preventing that mouth rod heat from collapsing
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Cited By (3)

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CN112137163A (en) * 2019-06-28 2020-12-29 湖北中烟工业有限责任公司 Blending material and preparation method and application thereof
WO2020258466A1 (en) * 2019-06-28 2020-12-30 湖北中烟工业有限责任公司 Phase-change material, preparation method therefor and use thereof
CN112220109A (en) * 2019-06-28 2021-01-15 湖北中烟工业有限责任公司 Phase change material and preparation method and application thereof

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