CN109497610B - Low-temperature heating cigarette with mint taste - Google Patents
Low-temperature heating cigarette with mint taste Download PDFInfo
- Publication number
- CN109497610B CN109497610B CN201811518597.3A CN201811518597A CN109497610B CN 109497610 B CN109497610 B CN 109497610B CN 201811518597 A CN201811518597 A CN 201811518597A CN 109497610 B CN109497610 B CN 109497610B
- Authority
- CN
- China
- Prior art keywords
- cooling
- temperature
- mint
- shell
- layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 33
- 235000006679 Mentha X verticillata Nutrition 0.000 title claims abstract description 28
- 235000002899 Mentha suaveolens Nutrition 0.000 title claims abstract description 28
- 235000001636 Mentha x rotundifolia Nutrition 0.000 title claims abstract description 28
- 238000010438 heat treatment Methods 0.000 title claims abstract description 18
- 238000001816 cooling Methods 0.000 claims abstract description 79
- 239000010410 layer Substances 0.000 claims abstract description 48
- 239000003094 microcapsule Substances 0.000 claims abstract description 43
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 31
- 239000012790 adhesive layer Substances 0.000 claims abstract description 24
- 239000000853 adhesive Substances 0.000 claims abstract description 21
- 230000001070 adhesive effect Effects 0.000 claims abstract description 21
- 239000000779 smoke Substances 0.000 claims abstract description 20
- 241000208125 Nicotiana Species 0.000 claims abstract description 19
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 19
- 230000004044 response Effects 0.000 claims abstract description 12
- 239000003205 fragrance Substances 0.000 claims abstract description 11
- 239000000758 substrate Substances 0.000 claims abstract 3
- 239000000463 material Substances 0.000 claims description 24
- 239000000725 suspension Substances 0.000 claims description 14
- 239000007921 spray Substances 0.000 claims description 13
- 239000007864 aqueous solution Substances 0.000 claims description 12
- -1 oleum Helianthi Substances 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000001856 Ethyl cellulose Substances 0.000 claims description 5
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 claims description 5
- 108010010803 Gelatin Proteins 0.000 claims description 5
- 239000000443 aerosol Substances 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 235000019325 ethyl cellulose Nutrition 0.000 claims description 5
- 229920001249 ethyl cellulose Polymers 0.000 claims description 5
- 239000000835 fiber Substances 0.000 claims description 5
- 229920000159 gelatin Polymers 0.000 claims description 5
- 239000008273 gelatin Substances 0.000 claims description 5
- 235000019322 gelatine Nutrition 0.000 claims description 5
- 235000011852 gelatine desserts Nutrition 0.000 claims description 5
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims description 5
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 5
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 5
- 238000003754 machining Methods 0.000 claims description 5
- 239000001525 mentha piperita l. herb oil Substances 0.000 claims description 5
- 239000000123 paper Substances 0.000 claims description 5
- 235000019477 peppermint oil Nutrition 0.000 claims description 5
- 229920000747 poly(lactic acid) Polymers 0.000 claims description 5
- 239000004626 polylactic acid Substances 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 5
- 230000000391 smoking effect Effects 0.000 claims description 5
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 4
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 4
- 229940041616 menthol Drugs 0.000 claims description 4
- 229920001223 polyethylene glycol Polymers 0.000 claims description 4
- 235000006484 Paeonia officinalis Nutrition 0.000 claims description 2
- 244000170916 Paeonia officinalis Species 0.000 claims description 2
- 235000019482 Palm oil Nutrition 0.000 claims description 2
- 239000004698 Polyethylene Substances 0.000 claims description 2
- XECAHXYUAAWDEL-UHFFFAOYSA-N acrylonitrile butadiene styrene Chemical compound C=CC=C.C=CC#N.C=CC1=CC=CC=C1 XECAHXYUAAWDEL-UHFFFAOYSA-N 0.000 claims description 2
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 claims description 2
- 239000004676 acrylonitrile butadiene styrene Substances 0.000 claims description 2
- 239000000828 canola oil Substances 0.000 claims description 2
- 235000019519 canola oil Nutrition 0.000 claims description 2
- 239000000919 ceramic Substances 0.000 claims description 2
- 239000008169 grapeseed oil Substances 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000003921 oil Substances 0.000 claims description 2
- 235000019198 oils Nutrition 0.000 claims description 2
- 239000002540 palm oil Substances 0.000 claims description 2
- 239000004033 plastic Substances 0.000 claims description 2
- 229920003023 plastic Polymers 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- 229920000139 polyethylene terephthalate Polymers 0.000 claims description 2
- 239000005020 polyethylene terephthalate Substances 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 239000003549 soybean oil Substances 0.000 claims description 2
- 235000012424 soybean oil Nutrition 0.000 claims description 2
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 2
- FINKDHKJINNQQW-UHFFFAOYSA-N 5-methyl-2-propan-2-ylcyclohexane-1-carboxamide Chemical compound CC(C)C1CCC(C)CC1C(N)=O FINKDHKJINNQQW-UHFFFAOYSA-N 0.000 claims 1
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims 1
- 210000000582 semen Anatomy 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 14
- 238000004090 dissolution Methods 0.000 abstract description 3
- 238000005461 lubrication Methods 0.000 abstract description 3
- 230000001953 sensory effect Effects 0.000 abstract description 3
- 239000011257 shell material Substances 0.000 description 24
- 238000000034 method Methods 0.000 description 9
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 7
- 239000003546 flue gas Substances 0.000 description 7
- 239000004006 olive oil Substances 0.000 description 7
- 235000008390 olive oil Nutrition 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- 239000011159 matrix material Substances 0.000 description 6
- 210000000214 mouth Anatomy 0.000 description 5
- 244000246386 Mentha pulegium Species 0.000 description 4
- 235000016257 Mentha pulegium Nutrition 0.000 description 4
- 235000004357 Mentha x piperita Nutrition 0.000 description 4
- HSHXDCVZWHOWCS-UHFFFAOYSA-N N'-hexadecylthiophene-2-carbohydrazide Chemical compound CCCCCCCCCCCCCCCCNNC(=O)c1cccs1 HSHXDCVZWHOWCS-UHFFFAOYSA-N 0.000 description 4
- 235000001050 hortel pimenta Nutrition 0.000 description 4
- 239000013068 control sample Substances 0.000 description 3
- 239000008368 mint flavor Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000000944 linseed oil Substances 0.000 description 2
- 235000021388 linseed oil Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 210000000697 sensory organ Anatomy 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 1
- 235000019483 Peanut oil Nutrition 0.000 description 1
- 235000019484 Rapeseed oil Nutrition 0.000 description 1
- 208000021063 Respiratory fume inhalation disease Diseases 0.000 description 1
- 244000062793 Sorghum vulgare Species 0.000 description 1
- 235000019486 Sunflower oil Nutrition 0.000 description 1
- 235000019498 Walnut oil Nutrition 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000010495 camellia oil Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 235000005687 corn oil Nutrition 0.000 description 1
- 239000002285 corn oil Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000010460 hemp oil Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 235000019713 millet Nutrition 0.000 description 1
- 239000000312 peanut oil Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920002523 polyethylene Glycol 1000 Polymers 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 239000008170 walnut oil Substances 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F47/00—Smokers' requisites not otherwise provided for
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention provides a low-temperature heating cigarette with mint taste, which comprises an atomizing substrate section and a cooling filter tip, wherein the atomizing substrate section and the cooling filter tip are connected with each other; the structure of the cooling tip rod is a hollow cylindrical tubular structure and sequentially comprises a shell, an adhesive layer and a cooling layer from outside to inside, the shell and the cooling layer are bonded together by the adhesive layer, the adhesive layer is internally provided with a thermosensitive microcapsule containing a dissolving agent and tobacco essence containing mint, and the thermosensitive microcapsule starts to release the dissolving agent and the tobacco essence after reaching a response temperature, so that the bonding state and the aroma state between the shell and the cooling layer are changed, the surface area of the cooling layer is increased, and the smoke airflow path is changed. The invention reduces the viscosity of the cooling layer and the shell under the influence of multiple actions such as lubrication and dissolution of the adhesive by the dissolving agent released by the heat-sensitive microcapsule, thereby achieving the effect of dropping the cooling layer from the shell, having obvious smoke cooling effect, and simultaneously, the tobacco essence contains mint fragrance and has better sensory cooling effect.
Description
Technical Field
The invention relates to the technical field of heating non-combustible tobacco products, in particular to a low-temperature heating cigarette with mint taste.
Background
The non-combustible cigarette is heated to 200-400 ℃ by an electric heating device, so as to generate smoke similar to the traditional cigarette for a consumer to smoke, and the using mode of the non-combustible cigarette introduces a problem that: the temperature of the smoke is too high, and the temperature of the smoke entering the oral cavity can reach more than 70 ℃ or even higher under the condition that the filter stick section does not adopt a cooling means, so that the consumption experience of consumers is seriously influenced. Therefore, the novel low-temperature heating cigarette is designed, can obviously reduce the temperature of the smoke inhaled by a consumer, and is very desirable.
The mint-containing essence for cigarettes is one of the most common flavors in food, daily chemical and tobacco, has pure mint flavor, strong cool feeling, fresh and clear aroma and is refreshing and refreshing, consumers can enjoy the taste, the cool taste in the smoking process can not indirectly feel the temperature of smoke inhalation in the sensory experience, and the sensory cooling effect is better.
Disclosure of Invention
In order to solve the existing problems, the invention provides the low-temperature heating cigarette with the mint taste, and the cigarette filter tip can obviously reduce the smoke temperature and increase the mint fragrance by reasonably designing the cigarette filter tip.
A low temperature heated cigarette with mint flavor comprises an atomizing matrix section and a cooling tip rod connected with each other, wherein
An atomized matrix section for generating aerosol after heating;
the cooling filter tip is of a hollow cylindrical tubular structure and sequentially comprises a shell, an adhesive layer and a cooling layer from outside to inside, wherein the adhesive layer is internally provided with a thermosensitive microcapsule containing a dissolving agent and tobacco essence, and the thermosensitive microcapsule starts to release the dissolving agent and the tobacco essence after reaching a response temperature, so that the bonding state and the fragrance state between the shell and the cooling layer are changed, the surface area of the cooling layer is increased, the flue gas airflow path is changed, and meanwhile, the fragrance is sucked.
Further, the response temperature of the heat-sensitive microcapsule is 55-100 ℃, and the heat-sensitive microcapsule starts to release the dissolving agent after the response temperature is reached.
Further, the dissolving agent is a fat-soluble solvent, including but not limited to, one or a combination of several materials selected from the group consisting of millet oil, rapeseed oil, peanut oil, hemp seed oil, corn oil, olive oil, camellia oil, palm oil, canola oil, sunflower oil, soybean oil, sesame oil, linseed oil (linseed oil), grape seed oil, walnut oil, peony seed oil, and the like.
Further, the mint-containing tobacco flavor includes but is not limited to one or a combination of mint flavor, menthol, menthane amide and dementholized peppermint oil.
Furthermore, the heat-sensitive microcapsule accounts for 10-25% of the total amount of the adhesive, so that enough dissolving agent is released after the microcapsule is broken to reduce the viscosity of the adhesive.
Further, the material of the shell includes, but is not limited to, fiber paper, plastic, and ceramic.
Further, the cooling layer is a film or a sheet with a phase change function, and comprises one or a mixture of polylactic acid, polyethylene terephthalate, acrylonitrile-butadiene-styrene copolymer, polyethylene and aluminum foil.
Further, the adhesive force generated by the adhesive layer for bonding the housing and the cooling layer is designed to be 0.5N-2N, so that the cooling layer does not easily fall off from the housing in a natural state or during a machining process.
Further, the preparation method of the heat-sensitive microcapsule comprises the following steps:
(1) taking gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG (1000-;
(2) adding a dissolving agent which accounts for 1-6% of the weight of the wall material aqueous solution into the wall material aqueous solution, simultaneously adding tobacco essence which accounts for 10-45% of the adding amount of the dissolving agent into the wall material aqueous solution, and fully stirring at the temperature of 60-75 ℃ to form an oil-in-water mixed suspension;
(3) and drying the mixed suspension by a spray dryer to prepare powder, wherein the hopper and the nozzle of the spray dryer are required to be heated, and the temperature is controlled to be about 60-80 ℃, so that the mixed suspension is prevented from being condensed at the hopper, the nozzle and the like after being cooled.
The invention has the beneficial effects that:
(1) the contradiction between the flue gas cooling and the mechanized production is solved by introducing the heat-sensitive microcapsule, namely: the adhesive layer in the cooling tip rod has enough adhesive force, so that the shell and the cooling layer are combined firmly, and the cooling layer cannot fall off when an equipment blade cuts the cooling pipe in a natural state, particularly in a mechanized production process, and the blade is difficult to cut off the cooling layer if the falling off occurs, so that the equipment can be shut down; in the process of smoking and heating the non-combustible cigarette by a consumer, the adhesive force of the adhesive layer is required to be small, and the cooling layer can fall off from the shell, partially fall off and generate a fold or wave structure, so that the surface area is increased, the airflow path of smoke is changed, and the obvious smoke cooling effect is achieved. In the scheme of only adopting the adhesive for bonding, the balance is difficult to control, and by introducing the heat-sensitive microcapsule, in the process of smoking and heating the non-combustible cigarette, the smoke temperature can lead the PEG skeleton in the heat-sensitive microcapsule to collapse and break, so that the dissolving agent is released, the viscosity of the cooling layer and the shell is reduced under the influence of multiple actions of the dissolving agent on the lubrication, the dissolution and the like of the adhesive, the effects of the cooling layer falling off from the shell, partial falling off and generating a fold or wavy structure are achieved, and the smoke cooling effect is obvious.
(2) This technical scheme introduces the cigarette essence that contains peppermint simultaneously, the parcel of heat-sensitive type microcapsule on the one hand, and the enclosure space that forms between casing and the cooling layer, can effectively reduce the cigarette and deposit the escape of in-process peppermint fragrance, the suction in-process, the microcapsule skeleton collapses, and the cooling layer drops, make the sufficient escape of peppermint fragrance, fragrance is more lasting, more strong, on the other hand contains the cigarette essence of peppermint and can provide cool suction for the consumer and experience, although can not directly reduce the flue gas temperature, but can let the consumer experience the indirect temperature that can not experience the inhaled flue gas in the sense organ, the sense organ cooling effect is better.
Drawings
FIG. 1 is a schematic view of the structure of a low temperature heated cigarette of the present invention;
FIG. 2 is a schematic structural view of a cooling tip rod in the low-temperature heating cigarette of the present invention;
FIG. 3 is a schematic cross-sectional view of a cooling tip rod in a low temperature heated cigarette of the present invention.
The reference numbers in the figures are as follows: 1-heating the cigarette at low temperature; 2-an atomizing matrix section; 3-cooling the filter tip; 301-a housing; 302-an adhesive layer; 303-temperature lowering layer
Detailed Description
The technical solution of the present invention will be clearly and completely described below with reference to the accompanying drawings.
Example one
As shown in fig. 1 to 3, a low-temperature-heated cigarette 1 having a mint taste includes: an atomized matrix section 2 for generating aerosol after heating; the cooling filter rod 3 is used for reducing the temperature of smoke entering an oral cavity, is of a hollow cylindrical tubular structure and consists of a shell 301, an adhesive layer 302 and a cooling layer 303, and the shell 301 and the cooling layer 303 are bonded together through the adhesive layer 302.
The adhesive layer contains thermosensitive microcapsules and is used for changing the bonding state between the shell and the cooling layer in the suction process and improving the cooling efficiency of the smoke. The response temperature of the heat-sensitive microcapsule is about 60 ℃, and after the response temperature is reached, the microcapsule starts to release the dissolving agent and the tobacco essence; the dissolving agent is olive oil, the mint-containing tobacco essence is composed of menthol, menthane amide and dementholized peppermint oil according to the ratio of 1:0.3:0.8, and the thermosensitive microcapsule accounts for 15% of the total amount of the adhesive, so that enough dissolving agent is released after the microcapsule is broken to reduce the viscosity of the adhesive and provide mint fragrance; the shell is made of fiber paper, the cooling layer is made of polylactic acid, and the adhesive force generated by the adhesive layer for bonding the shell and the cooling layer is designed to be 1N, so that the cooling layer cannot easily fall off from the shell in a natural state or a machining process.
The preparation method of the heat-sensitive microcapsule comprises the following steps:
(1) adding gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG1000 as wall materials into water according to the weight part ratio of 5:0.5:0.5:1, and fully stirring at 60-75 ℃ for dissolving to prepare a solution with the solid content of the wall materials being 10%;
(2) adding olive oil into the wall material aqueous solution according to 3% of the weight of the wall material solution, simultaneously adding the tobacco essence into the wall material aqueous solution according to 20% of the dissolving agent, and fully stirring at the temperature of 60-75 ℃ to form an oil-in-water mixed suspension;
(3) drying the mixed suspension by a spray dryer to prepare powder, wherein the spray dryer is mainly characterized in that a hopper and a nozzle of the spray dryer are heated, the temperature is controlled to be about 60-80 ℃, and the mixed suspension is prevented from being condensed at the hopper, the nozzle and the like after being cooled.
Example two
As shown in fig. 1 to 3, a low-temperature-heated cigarette 1 having a mint taste includes: an atomized matrix section 2 for generating aerosol after heating; the cooling filter rod 3 is used for reducing the temperature of the smoke entering the oral cavity, is of a hollow cylindrical tubular structure, and consists of a shell 301, an adhesive layer 302 and a cooling layer 303.
The adhesive layer contains thermosensitive microcapsules and is used for changing the bonding state between the shell and the cooling layer in the suction process and improving the cooling efficiency of the smoke. The response temperature of the heat-sensitive microcapsule is about 60 ℃, and the microcapsule starts to release the dissolving agent after the response temperature is reached; the dissolving agent is olive oil, the mint-containing tobacco essence is composed of menthol, menthane amide and dementholized peppermint oil according to the ratio of 0.8:0.7:1, and the thermosensitive microcapsule accounts for 20% of the total amount of the adhesive, so that enough dissolving agent is released after the microcapsule is broken to reduce the viscosity of the adhesive; the shell is made of fiber paper, the cooling layer is made of polylactic acid, and the adhesive force generated by the adhesive layer for bonding the shell and the cooling layer is designed to be 1.5N, so that the cooling layer cannot easily fall off from the shell in a natural state or a machining process.
The preparation method of the heat-sensitive microcapsule comprises the following steps:
(1) adding gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG2000 as wall materials into water according to the weight part ratio of 8:0.6:0.7:1.2, and fully stirring at the temperature of 60-75 ℃ for dissolving to prepare a solution with the solid content of the wall materials being 15%;
(2) adding olive oil into the wall material aqueous solution according to 5% of the weight of the wall material solution, simultaneously adding the tobacco essence into the wall material aqueous solution according to 20% of the dissolving agent, and fully stirring at the temperature of 60-75 ℃ to form an oil-in-water mixed suspension;
(3) drying the mixed suspension by a spray dryer to prepare powder, wherein the spray dryer is mainly characterized in that a hopper and a nozzle of the spray dryer are heated, the temperature is controlled to be about 60-80 ℃, and the mixed suspension is prevented from being condensed at the hopper, the nozzle and the like after being cooled.
EXAMPLE III
As shown in fig. 1 to 3, a low-temperature-heated cigarette 1 having a mint taste includes: an atomized matrix section 2 for generating aerosol after heating; the cooling filter rod 3 is used for reducing the temperature of the smoke entering the oral cavity, is of a hollow cylindrical tubular structure, and consists of a shell 301, an adhesive layer 302 and a cooling layer 303.
The adhesive layer contains thermosensitive microcapsules and is used for changing the bonding state between the shell and the cooling layer in the suction process and improving the cooling efficiency of the smoke. The response temperature of the heat-sensitive microcapsule is about 60 ℃, and the microcapsule starts to release the dissolving agent after the response temperature is reached; the dissolving agent is olive oil, the mint-containing tobacco essence is composed of dementholized peppermint oil, and the thermosensitive microcapsule accounts for 12% of the total amount of the adhesive, so that enough dissolving agent is released after the microcapsule is broken to reduce the viscosity of the adhesive; the shell material is fiber paper, the cooling layer is polylactic acid, and the adhesive force generated by the adhesive layer for bonding the shell and the cooling layer is designed to be 0.8N, so that the cooling layer cannot easily fall off from the shell in a natural state or a machining process.
The preparation method of the heat-sensitive microcapsule comprises the following steps:
(1) adding gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG2000 as wall materials into water according to the weight ratio of 10:1:1:0.8:0.6:0.7:0.8, and fully stirring at the temperature of 60-75 ℃ for dissolving to prepare a solution with the solid content of the wall materials being 20%;
(2) adding olive oil into the wall material aqueous solution according to 5% of the weight of the wall material solution, simultaneously adding the tobacco essence into the wall material aqueous solution according to 20% of the dissolving agent, and fully stirring at the temperature of 60-75 ℃ to form an oil-in-water mixed suspension;
(3) drying the mixed suspension by a spray dryer to prepare powder, wherein the spray dryer is mainly characterized in that a hopper and a nozzle of the spray dryer are heated, the temperature is controlled to be about 60-80 ℃, and the mixed suspension is prevented from being condensed at the hopper, the nozzle and the like after being cooled.
When 1h with continuous production, equipment number of times of shutting down is as the evaluation index, weighs cooling tube processing properties, and the temperature when the flue gas gets into the oral cavity is as the index, evaluates the cooling effect, and the physical properties and the cooling performance test result of above-mentioned three embodiments are seen in Table 1:
TABLE 1 analysis result of comprehensive performance of cooling tip
| Sample (I) | Processability (M-Y-Y | Cooling effect | Mint fragrance |
| Control sample | 14 | 54.5℃ | Is free of |
| Example one | 8 | 45.2℃ | Is preferably used |
| Example two | 10 | 44.6℃ | Is preferably used |
| EXAMPLE III | 12 | 46.1℃ | In general |
Wherein the control sample does not contain the heat-sensitive type microcapsule, and the adhesive force generated by the adhesive layer 302 for bonding the case 301 and the temperature decreasing layer 303 is designed to be 0.5N.
From the above results of the performance analysis, it can be seen that the control sample, without the addition of the heat-sensitive microcapsules, even if the processing performance is reduced, the cooling effect cannot be well satisfied, and because the heat-sensitive microcapsules are introduced in the three embodiments, in the process of smoking and heating the non-combustible cigarette, the temperature of smoke can collapse and crack the PEG skeleton in the heat-sensitive microcapsule, thereby releasing the dissolving agent, reducing the viscosity of the cooling layer and the shell under the influence of multiple actions of the dissolving agent on the lubrication, the dissolution and the like of the adhesive, enabling the cooling layer to partially fall off, increasing the surface area of the flue gas contacting the cooling layer, prolonging the path of the flue gas, having certain cooling effect, higher content of the heat-sensitive microcapsules in the second embodiment and better cooling effect, but the processing performance is slightly poorer than that of the first embodiment, and the first embodiment and the second embodiment have better comprehensive effects in view of combination.
The above description is only an embodiment of the present invention, but the scope of the present invention is not limited thereto, and any changes or substitutions that can be easily conceived by those skilled in the art within the technical scope of the present invention are included in the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.
Claims (7)
1. A low-temperature heating cigarette with mint taste is characterized in that: comprises an atomizing substrate section (2) and a cooling nozzle rod (3) which are connected with each other, wherein
An aerosol-generating section (2) for generating aerosol upon heating;
the cooling tip rod (3) is of a hollow cylindrical tubular structure and sequentially comprises a shell (301), an adhesive layer (302) and a cooling layer (303) from outside to inside, the shell (301) and the cooling layer (303) are bonded together by the adhesive layer (302), a thermosensitive microcapsule containing a dissolving agent and tobacco essence containing mint is arranged in the adhesive layer (302), and the thermosensitive microcapsule starts to release the dissolving agent and the tobacco essence after reaching a response temperature, so that the bonding state and the fragrance state between the shell (301) and the cooling layer (303) are changed, the surface area of the cooling layer (303) is increased, the smoke airflow path is changed, and meanwhile, the smoking fragrance is increased; the dissolving agent is a fat-soluble solvent selected from one or more of semen Setariae oil, oleum Rapae, oleum Arachidis Hypogaeae, oleum Sesami, oleum Maydis, oleum Olivarum, oleum Camelliae Japonicae, palm oil, canola oil, oleum Helianthi, soybean oil, oleum Sesami, oleum Lini, grapeseed oil, oleum Juglandis, and peony seed oil; the adhesive force generated by the adhesive layer (302) for bonding the housing (301) and the cooling layer (303) is designed to be 0.5N-2N, so that the cooling layer does not easily fall off the housing in a natural state or during machining.
2. The low-temperature-heated cigarette having a mint taste according to claim 1, wherein: the response temperature of the heat-sensitive microcapsule is 55-100 ℃.
3. The low-temperature-heated cigarette having a mint taste according to claim 1, wherein: the tobacco essence containing mint comprises one or the combination of mint essence, menthol, menthane carboxamide and dementholized peppermint oil.
4. The low-temperature-heated cigarette having a mint taste according to claim 1, wherein: the heat-sensitive microcapsule accounts for 10-25% of the total amount of the adhesive.
5. The low-temperature-heated cigarette having a mint taste according to claim 1, wherein: the material of the shell (301) comprises fiber paper, plastic or ceramic.
6. The low-temperature-heated cigarette having a mint taste according to claim 1, wherein: the cooling layer (303) is a film or a sheet with a phase change function, and is selected from one or a mixture of polylactic acid, polyethylene terephthalate, acrylonitrile-butadiene-styrene copolymer and polyethylene.
7. The low-temperature-heated cigarette having a mint taste according to claim 1, wherein: the preparation method of the heat-sensitive microcapsule comprises the following steps:
(1) taking gelatin, ethyl cellulose, hydroxypropyl methyl cellulose and PEG (1000-;
(2) adding a dissolving agent which accounts for 1-6% of the weight of the wall material aqueous solution into the wall material aqueous solution, simultaneously adding tobacco essence which accounts for 10-45% of the adding amount of the dissolving agent into the wall material aqueous solution, and fully stirring at the temperature of 60-75 ℃ to form an oil-in-water mixed suspension;
(3) and drying the mixed suspension by a spray dryer to prepare powder, wherein a hopper and a nozzle of the spray dryer are required to be heated, and the temperature is controlled to be 60-80 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811518597.3A CN109497610B (en) | 2018-12-12 | 2018-12-12 | Low-temperature heating cigarette with mint taste |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811518597.3A CN109497610B (en) | 2018-12-12 | 2018-12-12 | Low-temperature heating cigarette with mint taste |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109497610A CN109497610A (en) | 2019-03-22 |
| CN109497610B true CN109497610B (en) | 2021-07-06 |
Family
ID=65752222
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811518597.3A Active CN109497610B (en) | 2018-12-12 | 2018-12-12 | Low-temperature heating cigarette with mint taste |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109497610B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110680006B (en) * | 2019-11-08 | 2022-04-29 | 湖北中烟工业有限责任公司 | Aromatized hollow bar and production method thereof |
| CN113424986B (en) * | 2021-07-26 | 2023-07-04 | 云南养瑞科技集团有限公司 | Fragrant cooling filter tip rod and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013027066A2 (en) * | 2011-08-25 | 2013-02-28 | British American Tobacco (Investments) Limited | Smoking article filter |
| CN103865650A (en) * | 2014-03-20 | 2014-06-18 | 中国热带农业科学院农产品加工研究所 | Temperature sensibility liquor-fragrance essence microcapsule for cigarette and preparation method thereof |
| CN107087811A (en) * | 2017-05-26 | 2017-08-25 | 湖北中烟工业有限责任公司 | With reduction flue-gas temperature and the low temperature cigarette for preventing that mouth rod heat from collapsing |
| CN107960680A (en) * | 2017-12-26 | 2018-04-27 | 云南巴菰生物科技有限公司 | A kind of paper tube that can be reduced flue-gas temperature and discharge fragrance and application thereof |
| CN108523220A (en) * | 2018-06-20 | 2018-09-14 | 湖北中烟工业有限责任公司 | A kind of improved cooling filter stick and the low temperature cigarette containing the filter stick |
| CN108576918A (en) * | 2018-01-08 | 2018-09-28 | 湖北中烟工业有限责任公司 | A kind of low temperature cigarette with temperature descending section |
-
2018
- 2018-12-12 CN CN201811518597.3A patent/CN109497610B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013027066A2 (en) * | 2011-08-25 | 2013-02-28 | British American Tobacco (Investments) Limited | Smoking article filter |
| CN103865650A (en) * | 2014-03-20 | 2014-06-18 | 中国热带农业科学院农产品加工研究所 | Temperature sensibility liquor-fragrance essence microcapsule for cigarette and preparation method thereof |
| CN107087811A (en) * | 2017-05-26 | 2017-08-25 | 湖北中烟工业有限责任公司 | With reduction flue-gas temperature and the low temperature cigarette for preventing that mouth rod heat from collapsing |
| CN107960680A (en) * | 2017-12-26 | 2018-04-27 | 云南巴菰生物科技有限公司 | A kind of paper tube that can be reduced flue-gas temperature and discharge fragrance and application thereof |
| CN108576918A (en) * | 2018-01-08 | 2018-09-28 | 湖北中烟工业有限责任公司 | A kind of low temperature cigarette with temperature descending section |
| CN108523220A (en) * | 2018-06-20 | 2018-09-14 | 湖北中烟工业有限责任公司 | A kind of improved cooling filter stick and the low temperature cigarette containing the filter stick |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109497610A (en) | 2019-03-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US11439178B2 (en) | Smokeless cigarette having decreased vapor temperature and preventing heat-caused collapse of cigarette holder | |
| CN107259639B (en) | A kind of smoking article and its manufacturing method | |
| WO2019100545A1 (en) | Low-temperature cigarette and preparation method therefor | |
| KR102436742B1 (en) | Cigarettes used in circumferentially heated non-combustible cigarettes | |
| CN109043654A (en) | It is a kind of to heat not burning cigarette and its component | |
| CN109497610B (en) | Low-temperature heating cigarette with mint taste | |
| JP2018518156A (en) | Aerosol-generating article with a highly breathable detachable freshener delivery element | |
| CN113662239A (en) | An aerosol-generating article flavored with a core segment | |
| CN109363254B (en) | Low-temperature heating cigarette | |
| CN109349682A (en) | It is a kind of for heating the cigarette for the cigarette that do not burn | |
| JP7372979B2 (en) | Water-based flavor liquid for electronic cigarettes | |
| CN216393032U (en) | An aerosol-generating article flavored with a core segment | |
| WO2021218893A1 (en) | Heating smokable product and heat-not-burn system | |
| CN111053277B (en) | Heated non-combustible aerosol-generating article | |
| CN108652073A (en) | A kind of low temperature cigarette and preparation method thereof with the loose integrated tobacco segment of multilayer | |
| JP2022506157A (en) | Smoking substitute consumables | |
| CN111567870B (en) | Flavoring and moisturizing tube for heating cigarettes and preparation method thereof | |
| CN109497609B (en) | Cigarette holder rod containing cooling agent and capable of being heated and not combusted | |
| CN107692318A (en) | A kind of tobacco juice for electronic smoke and preparation method | |
| CN108741206A (en) | The low temperature cigarette and preparation method of loose integrated tobacco segment with high thermal conductivity | |
| CN108523242A (en) | The low temperature cigarette and preparation method thereof of loose integrated tobacco segment with herbal | |
| WO2024011649A1 (en) | Aerosol generating product having flavored support section | |
| JP7286727B2 (en) | Double-use cigarette with high smoke volume and method and use thereof | |
| CN108420124A (en) | A kind of low temperature cigarette and preparation method thereof with pungent fragrant loose integrated tobacco segment | |
| JP2023538513A (en) | fragrance glycosides |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |