CN109497609B - Cigarette holder rod containing cooling agent and capable of being heated and not combusted - Google Patents

Cigarette holder rod containing cooling agent and capable of being heated and not combusted Download PDF

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Publication number
CN109497609B
CN109497609B CN201811518596.9A CN201811518596A CN109497609B CN 109497609 B CN109497609 B CN 109497609B CN 201811518596 A CN201811518596 A CN 201811518596A CN 109497609 B CN109497609 B CN 109497609B
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cooling
layer
agent
cooling agent
shell
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CN109497609A (en
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刘冰
黄龙
陈义坤
刘磊
罗诚浩
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China Tobacco Hubei Industrial LLC
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China Tobacco Hubei Industrial LLC
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/04Tobacco smoke filters characterised by their shape or structure
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F47/00Smokers' requisites not otherwise provided for

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  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The invention provides a heating non-combustion cigarette holder rod containing cooling agents, which comprises a shell, an adhesive layer and a cooling layer, wherein the shell and the cooling layer are bonded together by the adhesive layer to form a hollow cylindrical tubular structure, the adhesive layer contains a raising agent and the cooling agents, the raising agent consists of an acidic matrix and an alkaline matrix, and is used for generating gas through the reaction of the acidic matrix and the alkaline matrix in the smoking process and changing the bonding state between the shell and the cooling layer. According to the invention, the swelling agent is introduced into the adhesive layer, so that in the process of smoking and heating non-combustible cigarettes, the temperature of smoke can enable the heat-sensitive organic acid microcapsules in the swelling agent to be broken, so that the acidic matrix is released, the gas is accelerated to be released through chemical reaction with the alkaline matrix, and the shell and the cooling layer are torn under the pressure of the gas, so that the effect of dropping the cooling layer from the shell is achieved, the smoke cooling effect is remarkable, and meanwhile, the cooling agent is introduced, so that cool smoking experience can be provided for consumers.

Description

Cigarette holder rod containing cooling agent and capable of being heated and not combusted
Technical Field
The invention relates to the technical field of heating non-combustible tobacco products, in particular to a heating non-combustible cigarette holder rod containing a cooling agent.
Background
The non-combustible cigarette is heated to 200-400 ℃ by an electric heating device, so as to generate smoke similar to the traditional cigarette for a consumer to smoke, and the using mode of the non-combustible cigarette introduces a problem that: the temperature of the smoke is too high, and the temperature of the smoke entering the oral cavity can reach more than 70 ℃ or even higher under the condition that the filter stick section does not adopt a cooling means, so that the consumption experience of consumers is seriously influenced. Therefore, it is highly desirable to design a cooling filter rod for heating a non-combustible cigarette, thereby reducing the temperature of the smoke inhaled by the consumer.
The cooling agent can provide cool taste for consumers in the smoking process, the smoking experience is good, the cooling agent is often used in the traditional cigarettes, the application of the cooling agent in heating the non-combustible cigarettes has not been reported, the cooling agent not only can provide cool feeling, but also can not indirectly sense the temperature of smoke inhalation in sensory experience, and the sensory cooling effect is very obvious.
Disclosure of Invention
In order to solve the problems, the invention provides a cigarette holder rod containing a cooling agent and capable of heating and non-combusting, and the cigarette holder rod can obviously reduce the temperature of smoke by reasonably designing the holder rod.
A heating non-combustion cigarette holder rod containing a cooling agent comprises a shell, an adhesive layer and a cooling layer, wherein the shell and the cooling layer are bonded together by the adhesive layer to form a hollow cylindrical tubular structure, the adhesive layer contains a swelling agent and the cooling agent, the swelling agent is composed of an acidic substrate and an alkaline substrate and is used for generating gas through reaction of the acidic substrate and the alkaline substrate in a smoking process, the bonding state between the shell and the cooling layer is changed, the surface area of the cooling layer is increased, the airflow path of smoke is changed, and therefore the cooling efficiency of the smoke is improved, and the cooling agent is used for providing a cool feeling.
Further, the acid matrix is a thermosensitive organic acid microcapsule, including but not limited to one or a combination of several of thermosensitive citric acid microcapsules, thermosensitive malic acid microcapsules and thermosensitive tartaric acid microcapsules.
Further, the response temperature of the heat-sensitive organic acid microcapsule is 55-100 ℃, and the microcapsule starts to release the organic acid after the response temperature is reached.
Further, the basic substrate is salt powder containing carbonate, bicarbonate or oxalate ions.
Furthermore, the amount of the leavening agent accounts for 5-30% of the total amount of the adhesive, so that enough gas is generated during chemical reaction, and the viscosity of the adhesive is not influenced.
Further, the cooling agent is prepared from the following powder materials in parts by weight:
Figure BDA0001902669550000021
further, the amount of the cooling agent accounts for 1% -10% of the total amount of the adhesive, so that the adhesive is not influenced while sufficient cooling feeling is provided.
Further, the shell material includes, but is not limited to, fiber paper, plastic, ceramic, and the like.
Further, the cooling layer is a film or a sheet with a phase change function, and comprises one or a mixture of polylactic acid, polyethylene terephthalate, acrylonitrile-butadiene-styrene copolymer, polyethylene and aluminum foil.
Further, the shell and the temperature reduction layer must have a gas permeability of less than 20CU, so that the gas generated by the chemical reaction between the acidic matrix and the basic matrix in the leavening agent can generate sufficient escaping force.
Further, the adhesive force generated by the adhesive layer for bonding the housing and the cooling layer is designed to be 0.5N-2N, so that the cooling layer does not easily fall off from the housing in a natural state or during a machining process.
The invention has the beneficial effects that: (1) the technical scheme solves the contradiction between the smoke cooling and the mechanized production by introducing the leavening agent, namely: the adhesive layer in the cooling tip rod has enough adhesive force, so that the shell and the cooling layer are combined firmly, and the cooling layer cannot fall off when an equipment blade cuts the cooling tip rod in a natural state, particularly in a mechanized production process, and the blade is difficult to cut off the cooling layer if the falling off occurs, so that equipment can be shut down; in the process of smoking and heating the non-combustible cigarette by a consumer, the adhesive force of the adhesive layer is required to be small, and the cooling layer can fall off from the shell, partially fall off and generate a fold or wave structure, so that the cooling surface area is increased, the smoke airflow path is changed, and the obvious smoke cooling effect is achieved. In the scheme of only adopting the adhesive for bonding, the balance is difficult to control, and by introducing the swelling agent, in the process of smoking and heating the non-combustible cigarette, the smoke temperature can lead the heat-sensitive organic acid microcapsules in the swelling agent to be broken so as to release the acid matrix, and accelerate the release of gas through the chemical reaction with the alkaline matrix, and tear the shell and the cooling layer under the pressure of the gas, so that the effects of falling off, partial falling off and generating a fold or wave structure of the cooling layer from the shell are achieved, and the smoke cooling effect is obvious. (2) The cooling agent is introduced simultaneously in the technical scheme, cool smoking experience can be provided for consumers, the smoke temperature can not be directly reduced, the temperature of the smoke sucked by the consumers can not be indirectly sensed in sense organ experience, and the sense organ cooling effect is good.
Drawings
FIG. 1 is a schematic view of the structure of a filter rod for heating a non-combustible cigarette according to the present invention;
figure 2 is a schematic cross-sectional view of a filter rod for heating a non-combustible cigarette according to the present invention.
The reference numbers in the figures are as follows: 301-a housing; 302-an adhesive layer; 303-temperature lowering layer
Detailed Description
The technical solution of the present invention will be clearly and completely described below with reference to the accompanying drawings.
Example one
As shown in fig. 1 and 2, a cigarette holder rod containing cooling agents which is not burned by heat is composed of a shell 301, an adhesive layer 302 and a cooling layer 303, wherein the adhesive layer 302 is used for bonding the shell 301 and the cooling layer 303 together.
The filter tip is of a hollow cylindrical tubular structure, the adhesive layer 302 contains a raising agent and a cooling agent, and the raising agent is used for changing the bonding state between the shell and the cooling layer in the pumping process and improving the cooling efficiency of smoke. The swelling agent is a heat-sensitive citric acid microcapsule and sodium bicarbonate powder, the weight ratio of the swelling agent to the sodium bicarbonate powder is 4:1, the usage amount of the swelling agent accounts for 12% of the total amount of the adhesive, the usage amount of the cooling agent accounts for 2% of the total amount of the adhesive, the swelling agent and the cooling agent are added into the adhesive and uniformly stirred and mixed for later use, the shell 301 is made of fiber paper, and the cooling layer 303 is a polylactic acid film with a phase change function; the housing 301 and the cooling layer 303 have no air permeability, and the adhesive force generated by the adhesive layer 302 for bonding the housing 301 and the cooling layer 303 is designed to be 1N.
Example two
As shown in fig. 1 and 2, a cigarette holder rod containing cooling agents which is not burned by heat is composed of a shell 301, an adhesive layer 302 and a cooling layer 303, wherein the adhesive layer 302 is used for bonding the shell 301 and the cooling layer 303 together.
The filter tip is of a hollow cylindrical tubular structure, the adhesive layer 302 contains a raising agent and a cooling agent, and the raising agent is used for changing the bonding state between the shell and the cooling layer in the pumping process and improving the cooling efficiency of smoke. The swelling agent is heat-sensitive citric acid microcapsules and sodium bicarbonate powder, the weight ratio of the swelling agent to the sodium bicarbonate powder is 2:1, the usage amount of the swelling agent accounts for 8% of the total amount of the adhesive, the cooling agent accounts for 4% of the total amount of the adhesive, the substances are added into the adhesive and uniformly stirred and mixed for later use, the shell 301 and the cooling layer 303 do not have air permeability, and the adhesive force generated by the adhesive layer 302 for bonding the shell 301 and the cooling layer 303 is designed to be 1.5N.
EXAMPLE III
As shown in fig. 1 and 2, a cigarette holder rod containing cooling agents which is not burned by heat is composed of a shell 301, an adhesive layer 302 and a cooling layer 303, wherein the adhesive layer 302 is used for bonding the shell 301 and the cooling layer 303 together.
The filter tip is of a hollow cylindrical tubular structure, the adhesive layer 302 contains a raising agent and a cooling agent, and the raising agent is used for changing the bonding state between the shell and the cooling layer in the pumping process and improving the cooling efficiency of smoke. The swelling agent is a heat-sensitive citric acid microcapsule and sodium bicarbonate powder, the weight ratio of the swelling agent to the sodium bicarbonate powder is 0.5:1, the usage amount of the swelling agent accounts for 20% of the total amount of the adhesive, the cooling agent accounts for 5% of the total amount of the adhesive, the swelling agent and the cooling agent are added into the adhesive and uniformly stirred and mixed for later use, the shell 301 is made of fiber paper, and the cooling layer 303 is a polylactic acid film with a phase change function; the housing 301 and the cooling layer 303 have no air permeability, and the adhesive force generated by the adhesive layer 302 for bonding the housing 301 and the cooling layer 303 is designed to be 0.6N.
The cooling agent in the above embodiment is composed of the following powder materials in parts by weight:
Figure BDA0001902669550000051
when 1h of continuous production is used, equipment shutdown times is used as an evaluation index, the machining performance of the cooling pipe is measured, the temperature of flue gas entering an oral cavity is used as an index, the cooling effect is evaluated, and the test results of the physical performance, the cooling performance and the cooling degree of the three embodiments are shown in table 1:
TABLE 1 analysis result of comprehensive performance of cooling tip
Sample (I) Processability (M-Y-Y Cooling effect Degree of cooling
Comparison sample (without leavening agent) 14 54.5℃ Is free of
Example one 10 45.2℃ In general
Example two 8 43.7℃ Is preferably used
EXAMPLE III 14 44.1℃ Is preferably used
Wherein the control sample does not contain a raising agent and a cooling agent, and the adhesive force generated by the adhesive layer 302 for bonding the case 301 and the cooling layer 303 is designed to be 0.5N.
According to the performance analysis results, the control sample can not well meet the cooling effect even if the processing performance is reduced under the condition that the leavening agent is not added, and in the third embodiment, the processing performance is influenced due to the existence of a large amount of leavening agents, but the cooling effect is better; in the first embodiment, the acidic matrix thermosensitive citric acid microcapsule exists excessively, and cannot react completely with the alkaline matrix sodium bicarbonate, so that the generated gas amount is reduced, and certain processing performance is influenced; the second embodiment has good comprehensive conditions of processing performance and cooling effect, when smoke enters the cooling mouth rod, because the smoke temperature is higher, the acid matrix thermosensitive citric acid microcapsules are broken and release citric acid, the citric acid is contacted with the alkaline matrix sodium bicarbonate and quickly reacts, the content of the citric acid can be fully reacted with each other, gas quickly escapes, the cooling layer is separated from the shell to a greater extent, the cooling surface area is obviously increased, meanwhile, the airflow can be cut, the airflow path is prolonged, the collision probability of the gas is increased, and the smoke temperature is reduced to the maximum extent.
The above description is only an embodiment of the present invention, but the scope of the present invention is not limited thereto, and any changes or substitutions that can be easily conceived by those skilled in the art within the technical scope of the present invention are included in the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.

Claims (9)

1. A cigarette holder rod containing a cooling agent and not burning by heating is characterized in that: the cooling device comprises a shell, an adhesive layer and a cooling layer, wherein the shell and the cooling layer are bonded together by the adhesive layer to form a hollow cylindrical tubular structure, the adhesive layer comprises a swelling agent and a cooling agent, the swelling agent consists of an acidic matrix and an alkaline matrix and is used for generating gas through reaction of the acidic matrix and the alkaline matrix in a pumping process, the bonding state between the shell and the cooling layer is changed, the surface area of the cooling layer is increased, the path of flue gas flow is changed, and therefore the cooling efficiency of flue gas is improved, and the cooling agent is used for providing a cool feeling; the acid matrix is a thermosensitive organic acid microcapsule, and the thermosensitive organic acid microcapsule comprises one or more of thermosensitive citric acid microcapsule, thermosensitive malic acid microcapsule and thermosensitive tartaric acid microcapsule.
2. A heat non-combustible cigarette holder rod containing a cooling agent as set forth in claim 1, wherein: the response temperature of the heat-sensitive organic acid microcapsule is 55-100 ℃, and the microcapsule starts to release the organic acid after the response temperature is reached.
3. A heat non-combustible cigarette holder rod containing a cooling agent as set forth in claim 1, wherein: the alkaline substrate is salt powder containing carbonate, bicarbonate or oxalate ions.
4. A heat non-combustible cigarette holder rod containing a cooling agent as set forth in claim 1, wherein: the amount of the leavening agent accounts for 5-30% of the total amount of the adhesive.
5. A heat non-combustible cigarette holder rod containing a cooling agent as set forth in claim 1, wherein: the cooling agent is prepared from the following powder materials in parts by weight:
70 portions of menthol
Menthol 20 parts
Xylitol 2 parts
Erythritol 3 parts
5 parts of menthane carboxamide.
6. A heat non-combustible cigarette holder rod containing a cooling agent as set forth in claim 1, wherein: the dosage of the cooling agent accounts for 1 to 10 percent of the total amount of the adhesive.
7. A heat non-combustible cigarette holder rod containing a cooling agent as set forth in claim 1, wherein: the shell material comprises fiber paper, plastic or ceramic.
8. A heat non-combustible cigarette holder rod containing a cooling agent as set forth in claim 1, wherein: the cooling layer is a film or a sheet with a phase change function, and the material of the cooling layer comprises one or a mixture of polylactic acid, polyethylene terephthalate, acrylonitrile-butadiene-styrene copolymer and polyethylene.
9. A heat non-combustible cigarette holder rod containing a cooling agent as set forth in claim 1, wherein: the adhesive force generated by the adhesive layer for bonding the case and the cooling layer is designed to be 0.5N-2N.
CN201811518596.9A 2018-12-12 2018-12-12 Cigarette holder rod containing cooling agent and capable of being heated and not combusted Active CN109497609B (en)

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Publication number Priority date Publication date Assignee Title
WO2020258466A1 (en) * 2019-06-28 2020-12-30 湖北中烟工业有限责任公司 Phase-change material, preparation method therefor and use thereof
CN115053980A (en) * 2022-06-29 2022-09-16 湖北中烟工业有限责任公司 Aroma coated carrier, preparation method and production equipment thereof, and cigarette without burning during heating

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2183091Y (en) * 1993-08-02 1994-11-23 陈堃明 Cigarette capable of reducing temp. of smoke
CN102835735A (en) * 2012-09-17 2012-12-26 川渝中烟工业有限责任公司 Temperature-sensitive micro capsule as well as preparation method and application of temperature-sensitive micro capsule
CN103060093A (en) * 2012-12-28 2013-04-24 华宝食用香精香料(上海)有限公司 Fragrance-invigorating and moisture-retention particles in cigarette and their preparation method and use
CN104010531A (en) * 2011-12-30 2014-08-27 菲利普莫里斯生产公司 Aerosol-generating article for use with an aerosol-generating device

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018201123A1 (en) * 2017-04-28 2018-11-01 Celanese International Corporation Cellulose acetate film for aerosol-generating device

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2183091Y (en) * 1993-08-02 1994-11-23 陈堃明 Cigarette capable of reducing temp. of smoke
CN104010531A (en) * 2011-12-30 2014-08-27 菲利普莫里斯生产公司 Aerosol-generating article for use with an aerosol-generating device
CN102835735A (en) * 2012-09-17 2012-12-26 川渝中烟工业有限责任公司 Temperature-sensitive micro capsule as well as preparation method and application of temperature-sensitive micro capsule
CN103060093A (en) * 2012-12-28 2013-04-24 华宝食用香精香料(上海)有限公司 Fragrance-invigorating and moisture-retention particles in cigarette and their preparation method and use

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