CN109464355A - A kind of free modular facemask powder and preparation method thereof - Google Patents
A kind of free modular facemask powder and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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Abstract
The invention discloses a kind of free modular facemask powders and preparation method thereof, it is related to cosmetic field, the present invention chooses Radix Salviae Miltiorrhizae, nutmeg, the root of Dahurain angelica, Radix Angelicae Sinensis, rhizoma typhonii, almond, dandelion, Prunella vulgaris, Cortex Phellodendri, semen brassicae, honeysuckle, the bletilla striata, cape jasmine, mulberry leaf, cortex moutan, radix saposhnikoviae, the coptis, the raw material as facemask powder such as chrysanthemum, with clearing heat and detoxicating, cool blood detumescence, activating microcirculation and removing stasis medicinal, dampness removing face cleaning and other effects, for the external application Chinese medicine for commonly using treatment face acnes on tcm clinical practice, it is also common antibacterial anti-inflammatory class facial mask raw material, and single medicinal material is individually extracted using cold ethanol reflux extraction, extract is obtained using freeze-drying, effective component will be guessed by retaining to greatest extent, and suitable medicinal substances extract is selected according to personal considerations, carry out the independent assortment of facemask powder, traditional Chinese medicine has been given full expression to vary with each individual, one One side's of people is specific.
Description
Technical field
The present invention relates to cosmetic fields, and in particular to facial mask technical field particularly relates to a kind of free modular facial mask
Powder and preparation method thereof.
Background technique
Acne is a kind of inflammatory dermatoses for involving hair follicle and sebaceous glands, and morbidity is vigorous except puberty endocrine, also
It is closely related with the mental elements such as anxiety, depression, the increase with present life stress and the habitual bad habit stayed up late,
Causing most people endocrine to get muddled causes the generation rate of face acnes to increase, to influence the beauty of the appearance of entire people
It is beautiful.
Facial mask is known as reinforced effect cosmetic since active constituent content is higher, due to its formula and makes
It is different from everyday skincare with method, is easier to be absorbed by human skin.Facial mask can be divided into gel, paste according to the difference of dosage form
Shape and powdered type, powdered facial mask does not have to directly smear, but is reconciled with water, is tuned into paste, is applied to face.To
After it is dry, washing can be passed through as paste facial mask, peeling, wiping are removed, since the storage of powdered facial mask is convenient, storage
Time is long, and the visibility of raw material is strong, and is widely used.
Inventor has found that the existing face mask of traditional Chinese medicine with treatment acne is in the face mask of traditional Chinese medicine of research treatment acne
Fixed composition prescription, cannot vary with each individual, and most of ingredient is that Chinese medicine is directly prepared into superfine powder, slowly effective, absorb effect
Rate is low, even with Chinese medical extract, decocting method is mostly used to extract, and temperature is high when extraction, containing the more medicine of saccharide compound
Material concentrate drying is more troublesome and heated time is long, often results in the loss and destruction of part effective component.
Summary of the invention
In view of this, it is an object of the invention to propose a kind of free modular facemask powder and preparation method thereof.
Preparation method based on a kind of free modular facemask powder that above-mentioned purpose one purpose of the present invention is to provide, including
Following steps take each single medicinal material respectively, and cold ethanol reflux extraction is respectively adopted per medicinal material simply and extracts at least 3
Secondary, each extraction time 2-3h mixes extracting solution, is successively concentrated by low-temperature reduced-pressure, and freeze-drying obtains facial mask freeze-dried powder.
In some optional embodiments, the temperature of the cold ethanol reflux extraction is 50-60 DEG C, and concentration of alcohol is
75-90%, solid-liquid ratio 1:4-5.
In some optional embodiments, the temperature of the low-temperature reduced-pressure concentration is 50-60 DEG C, enrichment factor 85-90%.
In some optional embodiments, the temperature of the freeze-drying is subzero 17-25 DEG C.
From the above it can be seen that a kind of preparation method of free modular facemask powder provided by the invention, use are low
Temperature is extracted and concentration (within 60 DEG C), and the use of ethyl alcohol is Extraction solvent, has the advantage that (1) low temperature extracts, can maximum limit
Degree retains the effective component in medicinal material, is allowed to destroy.(2) low temperature (within 60 DEG C) is concentrated and using powder processed is lyophilized, and is concentrated
Process be not in concentrate it is sticky and gelatinization phenomenon, while in medicinal material volatile component not because be heated at high temperature volatilization loss, protect
Demonstrate,prove product quality.(3) pure Chinese medicinal preparation is solvent using ethyl alcohol, and impurity is less and active constituent content is high.
It is a further object of the present invention to provide a kind of free modular facemask powder, the facemask powder uses described free group
The preparation method of box-like facemask powder is prepared.
In some optional embodiments, the facemask powder is to be taken by different medicinal substances extracts according to different acne symptoms
With being composed, wherein the medicinal substances extract includes Radix Salviae Miltiorrhizae, nutmeg, the root of Dahurain angelica, Radix Angelicae Sinensis, rhizoma typhonii, almond, dandelion, summer
Withered grass, Cortex Phellodendri, semen brassicae, honeysuckle, the bletilla striata, cape jasmine, mulberry leaf, cortex moutan, radix saposhnikoviae, the coptis and chrysanthemum.
In some optional embodiments, the facemask powder application method are as follows: take medicinal substances extract to mix respectively, combined amount is
0.8-1g/ times, 12-15mL blender is added into extract, is uniformly mixed, face paper is impregnated in the solution, wait mention
Face paper is unfolded after taking object to absorb and applies in face；Face paper, cleaning face are plucked after 15-20min.
In some optional embodiments, the blender is pure water, hydromel or lemon juice.
From the above it can be seen that a kind of free modular facemask powder provided by the invention, medicinal material selects independent assortment,
Accomplish to vary with each individual, Radix Salviae Miltiorrhizae, nutmeg, the root of Dahurain angelica, Radix Angelicae Sinensis, rhizoma typhonii, almond, dandelion, Prunella vulgaris, Cortex Phellodendri, semen brassicae, gold and silver
Flower, the bletilla striata, cape jasmine, mulberry leaf, cortex moutan, radix saposhnikoviae, the coptis, chrysanthemum etc..Be respectively provided with it is clearing heat and detoxicating, cool blood detumescence, activating microcirculation and removing stasis medicinal,
Dampness removing face cleaning and other effects is the external application Chinese medicine and common antibacterial anti-inflammatory class facial mask that treatment face acnes are commonly used on tcm clinical practice
Raw material, single medicinal material individually extract, and select suitable medicinal substances extract according to personal considerations, have given full expression to traditional Chinese medicine due to people
It is different, one side of a people specific.
Detailed description of the invention
Fig. 1 is the Different Extraction Method Content of Chlorogenic Acid high-efficient liquid phase chromatogram of honeysuckle of the embodiment of the present invention；
Fig. 2 is each medicinal substances extract schematic diagram of the embodiment of the present invention；
Fig. 3 is that face paper of the embodiment of the present invention absorbs facemask powder solution processes schematic diagram；
Fig. 4 is the schematic diagram after face paper of the embodiment of the present invention absorbs.
Specific embodiment
To make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with specific embodiment, and reference
Attached drawing, the present invention is described in more detail.
In order to overcome prior art Chinese medicine mask for acne powder, 1) it is directly prepared into superfine powder, slowly effective, absorption efficiency is low；
2) it is extracted using decocting method, temperature is high when extraction, when the more medicinal material concentrate drying containing saccharide compound is more troublesome and is heated
Between it is long, often result in the loss of part effective component and the deficiency destroyed, one purpose of the present invention is to provide a kind of independent assortment
The preparation method of formula facemask powder, includes the following steps, takes each single medicinal material respectively, and cold ethanol is respectively adopted per medicinal material simply and returns
Stream extraction method extracts at least 3 times, and each extraction time 2-3h mixes extracting solution, is successively concentrated by low-temperature reduced-pressure, cold
It is lyophilized dry, obtains facial mask freeze-dried powder.
In some optional embodiments, the preparation method of a kind of free modular facemask powder provided by the invention, specifically such as
Under: each single medicinal material is taken respectively, medicinal material is cleaned, is screened, after dissection, drains removing superficial moisture on medicinal materials, then by medicinal material section
The coarse powder for being ground into granularity 5-10 mesh is carried out, is on the one hand conducive to the extraction of subsequent medicinal material effective component, on the other hand anti-tablet
Powder caused by degree is too thin is flown upward, and medicinal material coarse powder is added in the ethyl alcohol that concentration is 80% by the waste of medicinal material, keeps feed liquid
Than then carrying out cold ethanol refluxing extraction 3 times at 55 DEG C of temperature for 1:4-5, extraction time is respectively 3h, 2h and 2h, so
Afterwards by after 3 extracting solution filterings, merge to obtain total extract, total extract is concentrated at 50-60 DEG C using being concentrated under reduced pressure
Volume is the 10-15% of total extract, and concentrate is placed at subzero 19 DEG C and is freeze-dried, facial mask freeze-dried powder is obtained.
It is extracted using low temperature and (within 60 DEG C) is concentrated, and the use of ethyl alcohol is Extraction solvent, have the advantage that (1) is low
Temperature is extracted, and can be retained the effective component in medicinal material to greatest extent, is allowed to destroy.(2) low temperature (within 60 DEG C) is concentrated and adopts
With freeze-drying powder, concentration process is not in that concentrate is sticky and gelatinization phenomenon, at the same in medicinal material volatile component not because of high temperature
Volatile loss on heating guarantees product quality.(3) pure Chinese medicinal preparation is solvent using ethyl alcohol, and impurity is less and active constituent content
It is high.
In order to overcome the face mask of traditional Chinese medicine for treating acne in the prior art, it is fixed composition prescription, cannot varies with each individual, originally
The another object of invention is to provide a kind of free modular facemask powder, and facemask powder uses the system of the free modular facemask powder
Preparation Method is prepared.The facemask powder is can to carry out matched combined according to different acne symptoms by different medicinal substances extracts,
In, medicinal substances extract include Radix Salviae Miltiorrhizae, nutmeg, the root of Dahurain angelica, Radix Angelicae Sinensis, rhizoma typhonii, almond, dandelion, Prunella vulgaris, Cortex Phellodendri, semen brassicae,
Honeysuckle, the bletilla striata, cape jasmine, mulberry leaf, cortex moutan, radix saposhnikoviae, the coptis and chrysanthemum are illustrated in figure 2 medicinal substances extract powder, extraction
Powder is dark yellow powder, the granularity of powder is in 250-300 since there are different colors for the difference between medicinal material on the whole
Between mesh.
When in use, it according to the difference of the state of individual physique and acne conditions, is chosen from medicinal substances extract different
Medicinal substances extract is combined use as facemask powder, then mixes the facemask powder taken, combined amount is maintained at 0.8-1g/
It is secondary, 12-15mL pure water, hydromel or lemon juice are added into mixed extract, is uniformly mixed, face paper is impregnated
It is absorbed in the solution, as shown in figure 3, the face paper of script white has absorbed facial mask liquid (should be dark yellow) and become face
Face paper is unfolded after facial mask liquid is absorbed in color, as shown in figure 4, the face paper of white changes colour because adsorbing coloured facial mask liquid, and
From the color change of face paper, the color of entire face paper is uniformly distributed, and the region accumulated or color is overweight does not occur,
Illustrate that the dissolubility of facemask powder is preferable, and is absorbed and infiltrate by face paper.Then the face paper for being adsorbed with facial mask liquid is applied in face
Portion；Face paper is plucked after 15-20min, cleaning face carries out subsequent maintenance.
Medicinal material selects independent assortment, accomplishes to vary with each individual, Radix Salviae Miltiorrhizae, nutmeg, the root of Dahurain angelica, Radix Angelicae Sinensis, rhizoma typhonii, almond, Pu Gong
English, Prunella vulgaris, Cortex Phellodendri, semen brassicae, honeysuckle, the bletilla striata, cape jasmine, mulberry leaf, cortex moutan, radix saposhnikoviae, the coptis, chrysanthemum etc..It is respectively provided with
Clearing heat and detoxicating, cool blood detumescence, activating microcirculation and removing stasis medicinal, dampness removing face cleaning and other effects are the external application that treatment face acnes are commonly used on tcm clinical practice
Chinese medicine and common antibacterial anti-inflammatory class facial mask raw material, single medicinal material individually extract, and select suitable medicinal material extract according to personal considerations
Object, given full expression to traditional Chinese medicine vary with each individual, one side of a people it is specific.
In order to verify the content for using cold ethanol reflux extraction to extract medicinal ingredient, the present embodiment inventor selects medicine
Representative medicinal material honeysuckle is object in material series extract, is mark with antibiotic effective ingredient chlorogenic acid in honeysuckle
Standard measures honeysuckle alcohol reflux extract, and with green in honeysuckle flower water decoction extract and honeysuckle ethanol percolation extract
Determination of Chlorogenic Acid is as a control group.
Chromatographiccondition:: WatersNavepak C18 column, Navepak C18 column, mobile phase are methanol-acetonitrile-
0.4% phosphoric acid solution (15 ︰, 15 ︰ 70), flow velocity: 1.0ml/min, Detection wavelength: 327nm, 25 DEG C of column temperature.
Contrast solution preparation: it takes control sample that 50% methanol is added to prepare the solution of 0.319mg/ml, uses high-efficient liquid phase color
Spectrometry establishes calibration curve equation.
Three kinds of extract same procedures are configured to suitable concentration solution, high effective liquid chromatography for measuring chlorogenic acid peak area,
Calibration curve equation is substituted into, test map is as shown in Figure 1, chlorogenic acid raw material all occurs in the chlorogenic acid that three kinds of extracting methods are extracted
Distinctive wave crest, and occur without other apparent miscellaneous peaks, illustrate that extract purity is higher.Three kinds of extracting method product yields and have
Imitate ingredient chlorogenic acid content such as table 1.
1 three kinds of extracting method product yields of table and active ingredient chlorogenic acid content
| Extracting method | Product recovery rate (extract quality/quality of medicinal material × 100%) | Chlorogenic acid content |
| Water boiling and extraction | 18.32% | 3.11% |
| Cold ethanol refluxing extraction | 13.21% | 5.21% |
| Ethanol percolation extracts | 10.92% | 3.41% |
Upper Biao Ke get, water extraction products obtained therefrom yield is high, but water extract impurity is more and water extraction Content of Chlorogenic Acid compared with
Low, diacolation product recovery rate is low, and chlorogenic acid content is also relatively low.Comprehensively consider in conjunction with the map of Fig. 1, cold ethanol refluxing extraction
Method is more excellent.
Analysis of experiments can be carried out to the effectiveness of the other drugs facemask powder of preparation of the embodiment of the present invention simultaneously:
1) data and method
Face acnes patient 120 are chosen, as research object, is randomly assigned as mask for acne group and control group each 60
Example, mask for acne group patients with mild (I grade) 32, moderate patient (II grade) 28, control group patients with mild (I grade) 29, in
Degree patient (II grade) 31.Mask for acne group: male 29, the age (14-26) year, average age (19 ± 2) year；Female 31, year
Year in age (15-25), average age (18 ± 2.5) year；Control group: male 28, the age (14-25) year, average age (19.3 ±
3.1) year, female 32, year at age (15-24), average age (18 ± 2.8) year.Two groups of genders, age and course of disease indifference (P >
0.05)。
2) treatment method
Mask for acne group: patient elder generation face cleaning, hot towel apply on the surface 2-3min, patients with mild (I grade) selection Radix Salviae Miltiorrhizae, Pork and beans
The cool, root of Dahurain angelica, dandelion, Prunella vulgaris, Cortex Phellodendri, semen brassicae, honeysuckle, the bletilla striata, cape jasmine, mulberry leaf, radix saposhnikoviae, the coptis, chrysanthemum extract
As facemask powder, (II grade) selection Radix Salviae Miltiorrhizae of moderate patient, nutmeg, the root of Dahurain angelica, Radix Angelicae Sinensis, rhizoma typhonii, almond, dandelion, Prunella vulgaris,
Cortex Phellodendri, semen brassicae, honeysuckle, the bletilla striata, cape jasmine, mulberry leaf, cortex moutan, radix saposhnikoviae, the coptis and chrysanthemum are as facemask powder, total amount 0.8-
1g/ times, hydromel 12-15mL is then added, is uniformly mixed, face paper is impregnated in the solution, after object to be extracted absorbs
Expansion face paper is simultaneously applied in face；Face paper, cleaning face, frequency of use: when using for the first time are plucked after 15-20 minutes
Then continuous use 3 days is changed to primary, 28 days as a treatment course on the two.
Control group: patient's acne spots embrocate Clindamycin Gel (Xiamen Jinri Pharmaceutical Co., Ltd's production, national drug standard
H20040314), the course for the treatment of and frequency of use and routine care are identical as mask for acne group.
3) statistical method
Statistical analysis is carried out using statistic software SPSS 18.0, P < 0.05 is that difference is statistically significant.Two groups of treatments
Front and back curative effect compares, and is shown in Table 2.
2 two groups for the treatment of conditioies of table
Mask for acne group cure rate, total effective rate are apparently higher than control group.
It should be understood by those ordinary skilled in the art that: the discussion of any of the above embodiment is exemplary only, not
It is intended to imply that the scope of the present disclosure (including claim) is limited to these examples；Under thinking of the invention, above embodiments
Or can also be combined between the technical characteristic in different embodiments, step can be realized with random order, and be existed such as
Many other variations of the upper different aspect of the invention, for simplicity, they are not provided in details.
The embodiment of the present invention be intended to cover fall into all such replacements within the broad range of appended claims,
Modifications and variations.Therefore, all within the spirits and principles of the present invention, any omission, modification, equivalent replacement, the improvement made
Deng should all be included in the protection scope of the present invention.
Claims (8)
1. a kind of preparation method of free modular facemask powder, which is characterized in that include the following steps, take each simple respectively
Material is respectively adopted cold ethanol reflux extraction per medicinal material simply and extracts at least 3 times, and each extraction time 2-3h will be mentioned
It takes liquid to mix, is successively concentrated by low-temperature reduced-pressure, freeze-drying obtains facial mask freeze-dried powder.
2. the preparation method of free modular facemask powder according to claim 1, which is characterized in that the cold ethanol returns
The temperature for flowing extraction method is 50-60 DEG C, concentration of alcohol 75-90%, solid-liquid ratio 1:4-5.
3. the preparation method of free modular facemask powder according to claim 1, which is characterized in that the low-temperature reduced-pressure is dense
The temperature of contracting is 50-60 DEG C, enrichment factor 85-90%.
4. the preparation method of free modular facemask powder according to claim 1, which is characterized in that the freeze-drying
Temperature is subzero 17-25 DEG C.
5. a kind of free modular mask for acne powder, which is characterized in that the facemask powder is any described using claim 1-4
The preparation method of free modular facemask powder is prepared.
6. free modular facemask powder according to claim 5, which is characterized in that the facemask powder is mentioned by different medicinal materials
Take object according to different acne symptoms carry out matched combined form, wherein the medicinal substances extract include Radix Salviae Miltiorrhizae, nutmeg, the root of Dahurain angelica,
Radix Angelicae Sinensis, rhizoma typhonii, almond, dandelion, Prunella vulgaris, Cortex Phellodendri, semen brassicae, honeysuckle, the bletilla striata, cape jasmine, mulberry leaf, cortex moutan, radix saposhnikoviae,
The coptis and chrysanthemum.
7. free modular facemask powder according to claim 5, which is characterized in that the facemask powder application method are as follows: point
Medicinal substances extract is not taken to mix, combined amount is 0.8-1g/ times, and 12-15mL blender is added into extract, is stirred
It is even, face paper is impregnated in the solution, object to be extracted is unfolded face paper and applies in face after absorbing；Facial mask is plucked after 15-20min
Paper, cleaning face.
8. free modular facemask powder according to claim 5, which is characterized in that the blender is pure water, honey
Water or lemon juice.
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| CN114099390A (en) * | 2021-12-22 | 2022-03-01 | 广东工业大学 | Facial mask liquid containing mesona chinensis benth extracting solution and preparation method thereof |
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| 邢俊波 等: ""正交实验法优选金银花中绿原酸提取工艺的研究"", 《时珍国医国药》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110841000A (en) * | 2019-12-04 | 2020-02-28 | 菏泽市圣医医疗科技有限公司 | Traditional Chinese medicine mask powder capable of expelling toxin and removing acne and preparation method thereof |
| CN114099390A (en) * | 2021-12-22 | 2022-03-01 | 广东工业大学 | Facial mask liquid containing mesona chinensis benth extracting solution and preparation method thereof |
| CN114099390B (en) * | 2021-12-22 | 2023-05-16 | 广东工业大学 | Mask liquid containing mesona chinensis benth extract and preparation method thereof |
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