CN109453051A - Facial mask and preparation method thereof is repaired in a kind of whitening - Google Patents
Facial mask and preparation method thereof is repaired in a kind of whitening Download PDFInfo
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- CN109453051A CN109453051A CN201811469866.1A CN201811469866A CN109453051A CN 109453051 A CN109453051 A CN 109453051A CN 201811469866 A CN201811469866 A CN 201811469866A CN 109453051 A CN109453051 A CN 109453051A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/447—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof containing sulfur
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention belongs to cosmetic technical fields, and in particular to facial mask and preparation method thereof is repaired in a kind of whitening.It includes following components and its mass percent that facial mask is repaired in whitening of the present invention: moisturizer 3.5%~5.5%, thickener 0.08%~0.15%, antioxidant 0.2%~0.5%, function composition 1.2%~1.8%, polyvinyl alcohol 0.5%~0.8%, sorbic acid 0.01%~0.03%, triethanolamine 0.01%~0.05%, essence 0.01%~0.03%, water 91.14%~94.49%.Whitening repair surface film component of the present invention is simple, and external moisturizing is anti-oxidant, prevents the dry line of skin surface microgroove from generating；It internally prevents collagen aging and new collagen is promoted to generate, promote deep moisturizing water lock power, increase plumpness and elastic sensation.In addition, the stability that facial mask is repaired in whitening of the present invention is high, there is good whitening effect, and can prevent to repair ultraviolet damage.
Description
Technical field
The invention belongs to cosmetic technical fields, and in particular to facial mask and preparation method thereof is repaired in a kind of whitening.
Background technique
The effect of facial mask is mainly clean skin and beauty, by smearing, facial mask forms thin film on the skin, by certain
After the drying of time, with washing away for facial mask, the dirt, scurf and cutin of skin can be washed off, while facial mask can completely cut off
Skin and outside air increase the temperature of skin, and pore expansion, skin can absorb the nutritional ingredient in facial mask, improve
Skin, the effect of reaching beauty.Relative to other skin care item types, the effect of facial mask, is more extensive, and using effect is more fast
Speed.Therefore, facial mask is increasingly by the favor of the majority of consumers.Divide from its product form and usage mode, currently on the market
Facial mask mainly have four major types: exfoliated, clay/gypsum mould, cream type and face paste type.
Peel off pack is often the product of transparent gel-form, and therefore, the selection of film forming agent and the determination of formula are removings
Key element in the preparation of type facial mask, generally will select film forming preferable, and the film forming agent of effect is smeared in dispersion with higher.
The substance specific gravity of powdery class is larger in clay/gypsum mould facial mask formula, smears white powdered, the powder usually added that comes
Shape substance is mainly pearl powder.The main formula of cream type and face paste type facial mask is also by film forming agent, emulsifier, moisturizer and function
Imitate four kinds of base substance compositions such as ingredient.Other than above-mentioned four kinds of facial mask types, there are also South Korea is derived from recent years, in Made in China
The Wash-free mask of Cheng great Re, also referred to as good night facial mask, it has disposable characteristic overnight, because of appearance easy to use and tempting
It is allowed to be pursued.
With the further subdivision of Cosmetic Market and the change of people's nursing skin habit, mask product has become daily
Skin care products in life, it is also more and more extensive to the research of facial mask both at home and abroad, deep.Currently, both at home and abroad to the research master of facial mask
It will the formula comprising facial mask and its preparation process, formula technique and using effect, facial mask functional raw material and specific aim use effect
Fruit etc..
Chinese patent application CN107929223A discloses a kind of skin whitening reparation facial mask, the skin whitening repair surface
Film includes face paper and facial mask liquid, and the facial mask liquid includes umbilical cord stem cells extract, oat peptide, Wild soybean peptide, moisturizer, plant
Object extract and water.Although facial mask is repaired in the skin whitening of the invention, skin injury can be repaired, promotes Skin Cell raw
It is long, soften tender skin, increase skin elasticity, there is preferable skin effect, still, the umbilical cord stem cells extract contained is not easy
It obtains.
Chinese patent CN104586731B, which discloses a kind of snail and is full of profit whitening, repairs facial mask, by the original of following parts by weight
Material is made: 50-60 parts of water, 0.1-0.5 parts of allantoin, and 5-10 parts of glycerol, 1-10 parts of butanediol, 1-10 parts of pentanediol, oxybenzene first
0.1-0.3 parts of ester, 0.05-0.3 parts of Sodium Hyaluronate, 0.1-0.3 parts of carbomer, 0.05-0.3 parts of xanthan gum, trehalose 1-4
Part, 1-4 parts of seaweed extracted liquor, 1-10 parts of snail extract, 2-8 parts of witch hazel distillate, 0.1-0.5 parts of Jojoba esters, sweet tea
1-4 parts of dish alkali, 1-4 parts of hydrolyzed vegetable protein, 0.1-0.5 parts of dipotassium glycyrrhizinate, 0.1-0.5 parts of glycyrrhetinic acid, Fourstamen Stephania Root extracts
0.1-1 parts of object, 1-4 parts of glucan, 0.1-3 parts of Trenaxmine, 1-4 parts of niacinamide, 0.1-1 parts of arabo-ascorbic acid, triethanolamine
0.1-3 parts, 0.01 part of methylisothiazolinone, 0.01-0.05 parts of essence.Although the effect of the invention facial mask is preferable,
Ingredient is numerous.
Currently, there are complicated components for existing facial mask, using effect is bad, and stability and ultraviolet light repair function are paid no attention to
The problems such as thinking.
Summary of the invention
In view of the deficiencies of the prior art, the purpose of the present invention is to provide a kind of whitenings to repair facial mask and preparation method thereof.
Whitening repair surface film component provided by the invention is simple, and raw material is easy to get, and it is anti-oxidant externally to play moisturizing, prevents skin surface microgroove
Dry line generates, and keeps the careful smooth effect of surface appearance；Internally playing prevents collagen aging and new collagen is promoted to generate, and mentions
Deep moisturizing water lock power is risen, the effect of plumpness and elastic sensation from inside to outside is increased.In addition to this, whitening provided by the invention
Repair surface membrane stability is high, and has good whitening effect, and ultraviolet damage effect is repaired in prevention.
The technical scheme is that
A kind of whitening reparation facial mask, including following components and its mass percent:
Moisturizer 3.5%~5.5%, thickener 0.08%~0.15%, antioxidant 0.2%~0.5%, function combination
Object 1.2%~1.8%, polyvinyl alcohol 0.5%~0.8%, sorbic acid 0.01%~0.03%, triethanolamine 0.01%~
0.05%, essence 0.01%~0.03%, water 91.14%~94.49%.
Further, facial mask is repaired in the whitening, is made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%,
Sorbic acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%.
Further, the moisturizer is made of Sodium Hyaluronate and glycerol 0.02~0.04:1~3 in mass ratio.
Further, the moisturizer is made of Sodium Hyaluronate and glycerol 0.03:2 in mass ratio.
Further, the antioxidant by L-cysteine hydrochloride and parthenolide 3~5:10 in mass ratio~
12 compositions.
Further, the antioxidant is by L-cysteine hydrochloride and parthenolide 4:11 group in mass ratio
At.
Further, the function composition by chitosan oligosaccharide, fibroin albumen and yeast-beta glucan in mass ratio 10~
12:4~6:1~2 are made.
Further, the function composition is by chitosan oligosaccharide, fibroin albumen and yeast-beta glucan in mass ratio 10:
5:1 is made.
The function composition the preparation method comprises the following steps: take chitosan oligosaccharide, add water, the additional amount of water is the 27- of chitosan oligosaccharide quality
32 times, stirring is completely dissolved to chitosan oligosaccharide, sequentially adds fibroin albumen, yeast-beta glucan, is stirred, mixing speed 800-
1200r/min, mixing time 20-25min, obtains mixed material, by gained mixed material be spray-dried to get.
Further, the thickener is by sodium carboxymethylcellulose and konjaku glucan 7~10:2~4 group in mass ratio
At.
Further, the thickener is made of sodium carboxymethylcellulose and konjaku glucan 8:3 in mass ratio.
In addition, steps are as follows the present invention also provides the preparation method that facial mask is repaired in whitening:
S1 takes thickener, adds water, and stirring stands 10~15h, obtain swelling solution to being completely dissolved；
Moisturizer, polyvinyl alcohol, sorbic acid are added into swelling solution obtained by step S1 by S2, are stirred and heated to 70~80
DEG C, 22~30min is kept the temperature, mixed material is obtained；
Mixed material obtained by step S2 is cooled to 40~45 DEG C by S3, and triethanolamine, antioxidant, function combination is added
Object, essence, are stirred until homogeneous, and are down to room temperature, discharging to get.
In the present invention, not only had by certain mass than the thickener formed by sodium carboxymethylcellulose and konjaku glucan
There are good thickening properties, keep the influence of the viscosity with temperature of products obtained therefrom little, additionally it is possible to enhance functional component and product
Heat-resistant stability, cold-resistant stability and centrifugal stability；In addition to this, it also has good film forming, enhances product
Performance of keeping humidity, can also prevent bacteria attack, extend period of storage.
It is an unexpected discovery of the invention that L-cysteine hydrochloride and parthenolide combination, can play significant antioxygen
Change effect, can effective skin whitening, accelerate the metabolism of skin.
In the present invention, combined chitosan oligosaccharide, fibroin albumen and yeast-beta glucan by certain mass function than made of
Object can not only further enhance the stability of product with thickener collective effect, additionally it is possible to it interacts with antioxidant,
Further enhance the whitening effect of product；In addition to this, it can also make product have good ultraviolet injury repair and promotion
The effect of cellular energy metabolism.
Chitosan oligosaccharide, fibroin albumen and yeast-beta glucan are combined using method of the invention, three can be made to generate function
Synergistic effect on energy, simultaneously, additionally it is possible to which function composition made from the method is used for by the undesirable property for covering original material
Whitening repair facial mask, can enhance product whitening effect and ultraviolet injury repair effect.
Compared with prior art, present invention has the advantage that
(1) whitening repair surface film component provided by the invention is simple, and raw material is easy to get, highly-safe, and has good steady
It is qualitative.
(2) whitening provided by the invention repair facial mask can effective skin whitening, accelerate the metabolism of skin, make skin
Skin bleaches the absorption that is greasy, while can promoting nutritional ingredient that attenuates.
(3) whitening provided by the invention repairs facial mask externally to play moisturizing anti-oxidant, prevents the dry line of skin surface microgroove raw
At the holding careful smooth effect of surface appearance；Internally playing prevents collagen aging and new collagen is promoted to generate, and promotes deep layer
Moisturizing water lock power increases the effect of plumpness and elastic sensation from inside to outside.
(4) whitening provided by the invention repairs facial mask and has the function of ultraviolet injury repair and promote cellular energy metabolism,
Have the effect of preventing to repair ultraviolet damage significantly.
(5) simple production process of facial mask is repaired in whitening provided by the invention, and condition is controllable, process stabilizing, is easy to industry
Metaplasia produces, and pollution-free, environmentally protective.
Specific embodiment
The following describes the present invention further through the description of specific embodiments, but it is to limit of the invention that this, which is not,
System, those skilled in the art's basic thought according to the present invention can make various modifications or improvements, but without departing from this
The basic thought of invention, is all within the scope of the present invention.
In the present invention, konjaku glucomannan is purchased from Henan Qi Nuo food ingredient Co., Ltd, article No.: myj；Polyvinyl alcohol
It is purchased from Guangzhou Ju Lang Chemical Co., Ltd., article No.: PVA-224；Yeast-beta glucan is purchased from the gloomy not natural product in Shaanxi
Co., Ltd, model: SFM019；Parthenolide is purchased from Sigma company；Sodium carboxymethylcellulose, which is purchased from Zhejiang, rolls into a ball life
Object Technology Co., Ltd., article No.: 0018355；Chitosan oligosaccharide is purchased from Shaanxi Sen Fu natural product Co., Ltd, article No.:
KGT180801；Fibroin albumen is purchased from Xi'an Lv Ruquan Biotechnology Co., Ltd, model: 6845.
Facial mask is repaired in embodiment 1, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 3.5%, thickener 0.08%, antioxidant 0.2%, function composition 1.2%, polyvinyl alcohol 0.5%,
Sorbic acid 0.01%, triethanolamine 0.01%, essence 0.01%, water 94.49%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.02:3 in mass ratio；The thickener is made of sodium carboxymethylcellulose and konjaku glucan 7:4 in mass ratio；It is described
Antioxidant is made of L-cysteine hydrochloride and parthenolide 3:12 in mass ratio；The function composition is by shell widow
Sugar, fibroin albumen and yeast-beta glucan 10:6:2 in mass ratio are made.
The function composition the preparation method comprises the following steps: take chitosan oligosaccharide, add water, the additional amount of water is the 27 of chitosan oligosaccharide quality
Times, stirring is completely dissolved to chitosan oligosaccharide, sequentially adds fibroin albumen, yeast-beta glucan, is stirred, mixing speed 800r/
Min, mixing time 20min, obtains mixed material, by gained mixed material be spray-dried to get.
The whitening repair facial mask the preparation method comprises the following steps:
S1 takes thickener, adds water, and stirring stands 10h, obtain swelling solution to being completely dissolved；
Moisturizer, polyvinyl alcohol, sorbic acid are added into swelling solution obtained by step S1 by S2, are stirred and heated to 70 DEG C, protect
Warm 22min, obtains mixed material；
Mixed material obtained by step S2 is cooled to 40 DEG C by S3, and triethanolamine, antioxidant, function composition, perfume (or spice) is added
Essence is stirred until homogeneous, and is down to room temperature, discharging to get.
Facial mask is repaired in embodiment 2, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 5.5%, thickener 0.15%, antioxidant 0.5%, function composition 1.8%, polyvinyl alcohol 0.8%,
Sorbic acid 0.03%, triethanolamine 0.05%, essence 0.03%, water 91.14%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.04:1 in mass ratio；The thickener is made of sodium carboxymethylcellulose and konjaku glucan 10:2 in mass ratio；Institute
Antioxidant is stated to be made of L-cysteine hydrochloride and parthenolide 5:10 in mass ratio；The function composition is by shell widow
Sugar, fibroin albumen and yeast-beta glucan 12:4:1 in mass ratio are made.
The function composition the preparation method comprises the following steps: take chitosan oligosaccharide, add water, the additional amount of water is the 32 of chitosan oligosaccharide quality
Times, stirring is completely dissolved to chitosan oligosaccharide, sequentially adds fibroin albumen, yeast-beta glucan, is stirred, mixing speed 1200r/
Min, mixing time 25min, obtains mixed material, by gained mixed material be spray-dried to get.
The whitening repair facial mask the preparation method comprises the following steps:
S1 takes thickener, adds water, and stirring stands 15h, obtain swelling solution to being completely dissolved；
Moisturizer, polyvinyl alcohol, sorbic acid are added into swelling solution obtained by step S1 by S2, are stirred and heated to 80 DEG C, protect
Warm 30min, obtains mixed material；
Mixed material obtained by step S2 is cooled to 45 DEG C by S3, and triethanolamine, antioxidant, function composition, perfume (or spice) is added
Essence is stirred until homogeneous, and is down to room temperature, discharging to get.
Facial mask is repaired in embodiment 3, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%,
Sorbic acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.03:2 in mass ratio；The thickener is made of sodium carboxymethylcellulose and konjaku glucan 8:3 in mass ratio；It is described
Antioxidant is made of L-cysteine hydrochloride and parthenolide 4:11 in mass ratio；The function composition is by shell widow
Sugar, fibroin albumen and yeast-beta glucan 10:5:1 in mass ratio are made.
The function composition the preparation method comprises the following steps: take chitosan oligosaccharide, add water, the additional amount of water is the 30 of chitosan oligosaccharide quality
Times, stirring is completely dissolved to chitosan oligosaccharide, sequentially adds fibroin albumen, yeast-beta glucan, is stirred, mixing speed 1000r/
Min, mixing time 22min, obtains mixed material, by gained mixed material be spray-dried to get.
The whitening repair facial mask the preparation method comprises the following steps:
S1 takes thickener, adds water, and stirring stands 14h, obtain swelling solution to being completely dissolved；
Moisturizer, polyvinyl alcohol, sorbic acid are added into swelling solution obtained by step S1 by S2, are stirred and heated to 78 DEG C, protect
Warm 26min, obtains mixed material；
Mixed material obtained by step S2 is cooled to 43 DEG C by S3, and triethanolamine, antioxidant, function composition, perfume (or spice) is added
Essence is stirred until homogeneous, and is down to room temperature, discharging to get.
Facial mask is repaired in comparative example 1, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%,
Sorbic acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.03:2 in mass ratio；The thickener is made of sodium carboxymethylcellulose and konjaku glucan 1:1 in mass ratio；It is described
Antioxidant is made of L-cysteine hydrochloride and parthenolide 4:11 in mass ratio；The function composition is by shell widow
Sugar, fibroin albumen and yeast-beta glucan 10:5:1 in mass ratio are made.
The preparation method that the function composition, whitening repair facial mask is similar to Example 3.
Difference with embodiment 3 is that the thickener is by sodium carboxymethylcellulose and konjaku glucan 1:1 in mass ratio
Composition.
Facial mask is repaired in comparative example 2, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%,
Sorbic acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.03:2 in mass ratio；The thickener is sodium carboxymethylcellulose；The antioxidant is by L-cysteine hydrochloride
It is formed with parthenolide 4:11 in mass ratio；The function composition is pressed by chitosan oligosaccharide, fibroin albumen and yeast-beta glucan
Mass ratio 10:5:1 is made.
The preparation method that the function composition, whitening repair facial mask is similar to Example 3.
Difference with embodiment 3 is that the thickener is sodium carboxymethylcellulose.
Facial mask is repaired in comparative example 3, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%,
Sorbic acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.03:2 in mass ratio；The thickener is made of sodium carboxymethylcellulose and konjaku glucan 8:3 in mass ratio；It is described
Antioxidant is made of L-cysteine hydrochloride and parthenolide 1:1 in mass ratio；The function composition by chitosan oligosaccharide,
Fibroin albumen and yeast-beta glucan 10:5:1 in mass ratio are made.
The preparation method that the function composition, whitening repair facial mask is similar to Example 3.
Difference with embodiment 3 is that the antioxidant presses quality by L-cysteine hydrochloride and parthenolide
It is formed than 1:1.
Facial mask is repaired in comparative example 4, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%,
Sorbic acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.03:2 in mass ratio；The thickener is made of sodium carboxymethylcellulose and konjaku glucan 8:3 in mass ratio；It is described
Antioxidant is parthenolide；The function composition by chitosan oligosaccharide, fibroin albumen and yeast-beta glucan in mass ratio
10:5:1 is made.
The preparation method that the function composition, whitening repair facial mask is similar to Example 3.
Difference with embodiment 3 is that the antioxidant is parthenolide.
Facial mask is repaired in comparative example 5, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%,
Sorbic acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.03:2 in mass ratio；The thickener is made of sodium carboxymethylcellulose and konjaku glucan 8:3 in mass ratio；It is described
Antioxidant is made of L-cysteine hydrochloride and parthenolide 4:11 in mass ratio；The function composition is by shell widow
Sugar, fibroin albumen and yeast-beta glucan 1:1:1 in mass ratio composition.
The preparation method that the function composition, whitening repair facial mask is similar to Example 3.
Difference with embodiment 3 is that the function composition is pressed by chitosan oligosaccharide, fibroin albumen and yeast-beta glucan
Mass ratio 1:1:1 composition.
Facial mask is repaired in comparative example 6, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%,
Sorbic acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.03:2 in mass ratio；The thickener is made of sodium carboxymethylcellulose and konjaku glucan 8:3 in mass ratio；It is described
Antioxidant is made of L-cysteine hydrochloride and parthenolide 4:11 in mass ratio；The function composition is by chitosan oligosaccharide
It is formed with fibroin albumen 10:5 in mass ratio.
The preparation method that the function composition, whitening repair facial mask is similar to Example 3.
Difference with embodiment 3 is that the function composition is made of chitosan oligosaccharide and fibroin albumen 10:5 in mass ratio.
Facial mask is repaired in comparative example 7, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%,
Sorbic acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.03:2 in mass ratio；The thickener is made of sodium carboxymethylcellulose and konjaku glucan 8:3 in mass ratio；It is described
Antioxidant is made of L-cysteine hydrochloride and parthenolide 4:11 in mass ratio；The function composition is by shell widow
Sugar, fibroin albumen and yeast-beta glucan 10:5:1 in mass ratio composition.
The preparation method that facial mask is repaired in the whitening is similar to Example 3.
Difference with embodiment 3 is that the function composition is pressed by chitosan oligosaccharide, fibroin albumen and yeast-beta glucan
Mass ratio 10:5:1 composition, i.e., function composition is only mixed by chitosan oligosaccharide, fibroin albumen and yeast-beta glucan.
Facial mask is repaired in comparative example 8, a kind of whitening
The whitening is repaired facial mask and is made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%,
Sorbic acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%；The moisturizer is by Sodium Hyaluronate and glycerol
The composition of 0.03:2 in mass ratio；The thickener is made of sodium carboxymethylcellulose and konjaku glucan 8:3 in mass ratio；It is described
Antioxidant is made of L-cysteine hydrochloride and parthenolide 4:11 in mass ratio；The function composition is by shell widow
Sugar, fibroin albumen and oat-beta glucan 10:5:1 in mass ratio are made.
The preparation method that the function composition, whitening repair facial mask is similar to Example 3.
Difference with embodiment 3 is that the function composition is pressed by chitosan oligosaccharide, fibroin albumen and oat-beta glucan
Mass ratio 10:5:1 is made.
Test example one, safety evaluatio
1, tested material: facial mask is repaired in embodiment 1, embodiment 2, embodiment 3, whitening made from comparative example 1-8.2, tested right
As:
110 women trial volunteers, the age 25-50 years old, subjects skin health, no skin disease allergies, meet by
Examination person volunteers inclusion criteria.
3, test method:
110 women trial volunteers are randomly divided into 11 groups, respectively embodiment 1-3 group, comparative example 1-8 group, every group
10 people repair facial mask using whitening made from embodiment 1-3, comparative example 1-8 respectively.
Qualified spot tester is selected, with closed patch experiment method, 0.020g tested material is added in spot tester, external application
Special adhesive tape is covered on subject back, removes tested material afterwards for 24 hours, respectively remove after 0.5h, 6h, 12h, for 24 hours, 48h observe skin
Skin reaction.
4, test result:
Human skin patch test result is shown: each group subject passes through the whitening reparation of embodiment 1-3, comparative example 1-8
The patch test of facial mask, 0.5h, 6h, 12h, for 24 hours, 48h observe dermoreaction, it is bad anti-that all subjects do not occur skin
It answers, it is safe that this illustrates that whitening reparation facial mask produced by the present invention uses.
Test example two, stability test test
1, test material: embodiment 1, embodiment 2, embodiment 3, comparative example 1, comparative example 2, comparative example 6 and comparative example 7 are made
Facial mask is repaired in standby whitening.
2, test method:
(1) heat-resistant stability investigate: by whitening repair facial mask 40 DEG C constant temperature 24 hours, restore room temperature after, observe product
Whether there is or not separation, layering, deposited phenomenons, if phenomena such as without separation, layering, precipitating, for qualification, conversely, being then unqualified.
(2) resist cold study on the stability: whitening being repaired facial mask at -15 DEG C after 24 hours, after restoring room temperature, observation is produced
Whether there is or not separation, layering, deposited phenomenons for product, if phenomena such as without separation, layering, precipitating, for qualification, conversely, being then unqualified.
(3) centrifugal stability is investigated: the whitening prepared reparation film sample being placed in centrifuge, with 3000r/
The rotation speed of min rotates 30min, takes out and observe the separation and layering situation of film sample.
3, test result:
Test result is as shown in table 1.
Table 1: stability test result
As can be seen from Table 1, after 24 hours study on the stability, comparative example 1, comparative example 6, is compared comparative example 2
The heat-resistant stability of the reparation facial mask of whitening made from example 7 and cold-resistant stability are unqualified, occur separating and being layered after centrifugation
Phenomenon, and whitening produced by the present invention repairs facial mask and does not occur separation, layering, deposited phenomenon, this illustrates whitening reparation of the present invention
Facial mask is with good stability.
Test example three, whitening effect evaluation
1, given the test agent: facial mask is repaired in embodiment 1, embodiment 2, embodiment 3, whitening made from comparative example 3-8.2, it tests
Method:
It chooses 135 female subjects and participates in test, the age 20-46 years old, subject's exclusion condition met " cosmetics contact
Property dermatitis diagnostic criteria and treatment principle " it is included in, exclusion criteria.Test position is inside of cranking arm, and the left and right arm of random arrangement is
Tested area before test, tests each subject's recipient site dermal melanin content using dermal melanin and ferroheme tester
All subjects are randomly divided into 9 groups according to MI value by MI value, and every group of 15 people, respectively example 1 group, implement 2 groups of embodiment
3 groups of example, 3 groups of comparative example, 4 groups of comparative example, 5 groups of comparative example, 6 groups of comparative example, 7 groups of comparative example and 8 groups of comparative example, respectively using real
Apply example 1, embodiment 2, embodiment 3, comparative example 3, comparative example 4, comparative example 5, comparative example 6, comparative example 7, beauty made from comparative example 8
White reparation facial mask, night apply once, are used continuously 12 weeks, and recipient site does not use other cosmetics during test.Utilize skin
Melanin and ferroheme tester test dermal melanin content MI value after each subject's recipient site test.It is black to test skin
It needs to clean recipient site before pigment content MI value.
3, test result:
Test result is as shown in table 2.
Table 2: influence of the facial mask to dermal melanin content MI value is repaired in whitening
| Group | Before test | After test |
| Example 1 group | 224.36 | 159.67 |
| 2 groups of embodiment | 223.98 | 156.43 |
| 3 groups of embodiment | 224.05 | 152.95 |
| 3 groups of comparative example | 223.87 | 175.94 |
| 4 groups of comparative example | 224.15 | 189.27 |
| 5 groups of comparative example | 223.58 | 182.46 |
| 6 groups of comparative example | 224.12 | 206.82 |
| 7 groups of comparative example | 224.08 | 202.59 |
| 8 groups of comparative example | 223.78 | 178.24 |
As can be seen from Table 2, the skin black of the subject of facial mask is repaired using whitening made from 1-3 of the embodiment of the present invention
Cellulose content MI value is substantially reduced, wherein the dermal melanin content of the subject of facial mask is repaired using whitening made from embodiment 3
The reduction of MI value is the most significant, and therefore, embodiment 3 is highly preferred embodiment of the present invention；Compared with comparative example 3-8 group, 3 groups of embodiment
Subject dermal melanin content MI value it is lower, it can be seen that, it is aobvious that facial mask whitening effect is repaired in whitening provided by the invention
It writes.
Test example four, the evaluation of ultraviolet injury repairing effect
1, test specimen: facial mask is repaired in embodiment 1, embodiment 2, embodiment 3, whitening made from comparative example 5-8.
2, test method:
Using blance test, Example 1, embodiment 2, embodiment 3, comparative example 5, comparative example 6, comparative example 7, comparative example
Whitening made from 8 repairs facial mask, deionized water as test specimen and makes culture medium and point 12 groups, respectively example 1 group, reality
Apply 2 groups of example, 3 groups of embodiment, 5 groups of comparative example, 6 groups of comparative example, 7 groups of comparative example, 8 groups of comparative example, blank control group.Cell is multiple
Soviet Union when to be grown in good condition, carries out cell synchronization processing.Concentration is adjusted after synchronization to be inoculated in cell plates.Second day,
It is placed under UVB irradiation unit, adds in the culture medium being grouped, continue culture and be incubated for.After being incubated for after a period of time, every hole
Test fluid in kit is added, concussion is placed at room temperature for stable fluorescent instrument detection reading.Record the flat fluorescent that each hole measures
RLU, every group of 3 multiple holes are averaged, and calculate protection ratio, meanwhile, on the basis of normal cell 100%, calculate each group fluorescence list
Position ATP percentage composition numerical value.
3, test result:
Test result is as shown in table 3.
Table 3: ultraviolet injury repairing effect evaluation result
As can be seen from Table 3, compared with blank control group, the ATP percentage composition and protection ratio of embodiment 1-3 group are bright
Aobvious to increase, this illustrates that whitening produced by the present invention repairs facial mask and has ultraviolet injury repair and promote the work of cellular energy metabolism
With.Compared with comparative example 5-8 group, 3 groups of embodiment of ultraviolet injury repairing effect is more preferable.
Claims (10)
1. facial mask is repaired in a kind of whitening, which is characterized in that including following components and its mass percent:
Moisturizer 3.5%~5.5%, thickener 0.08%~0.15%, antioxidant 0.2%~0.5%, function composition
1.2%~1.8%, polyvinyl alcohol 0.5%~0.8%, sorbic acid 0.01%~0.03%, triethanolamine 0.01%~
0.05%, essence 0.01%~0.03%, water 91.14%~94.49%.
2. facial mask is repaired in whitening as described in claim 1, which is characterized in that be made of following components and its mass percent:
Moisturizer 4.6%, thickener 0.13%, antioxidant 0.3%, function composition 1.5%, polyvinyl alcohol 0.6%, sorb
Acid 0.01%, triethanolamine 0.03%, essence 0.02%, water 92.81%.
3. facial mask is repaired in whitening as claimed in claim 1 or 2, which is characterized in that the antioxidant is by L-cysteine salt
Hydrochlorate and parthenolide 3~5:10 in mass ratio~12 composition.
4. facial mask is repaired in whitening as claimed in claim 3, which is characterized in that the antioxidant is by L-cysteine hydrochloride
It is formed with parthenolide 4:11 in mass ratio.
5. facial mask is repaired in whitening as claimed in claim 1 or 2, which is characterized in that the function composition is by chitosan oligosaccharide, fibroin
Albumen and yeast-beta glucan 10~12:4 in mass ratio~6:1~2 are made.
6. facial mask is repaired in whitening as claimed in claim 5, which is characterized in that the function composition is by chitosan oligosaccharide, fibroin egg
White and yeast-beta glucan 10:5:1 in mass ratio is made.
7. facial mask is repaired in whitening as claimed in claim 5, which is characterized in that the function composition the preparation method comprises the following steps: taking
Chitosan oligosaccharide adds water, and the additional amount of water is 27-32 times of chitosan oligosaccharide quality, and stirring is completely dissolved to chitosan oligosaccharide, sequentially adds fibroin
Albumen, yeast-beta glucan, stirring, mixing speed 800-1200r/min, mixing time 20-25min obtain mixture
Material, by gained mixed material be spray-dried to get.
8. facial mask is repaired in whitening as claimed in claim 1 or 2, which is characterized in that the thickener is by sodium carboxymethylcellulose
It is formed with konjaku glucan 7~10:2 in mass ratio~4.
9. facial mask is repaired in whitening as claimed in claim 8, which is characterized in that the thickener is by sodium carboxymethylcellulose and evil spirit
Taro glucan 8:3 in mass ratio composition.
10. as the preparation method of facial mask is repaired in the described in any item whitenings of claim 1-9, which is characterized in that including following step
It is rapid:
S1 takes thickener, adds water, and stirring stands 10~15h, obtain swelling solution to being completely dissolved；
Moisturizer, polyvinyl alcohol, sorbic acid are added into swelling solution obtained by step S1 by S2, are stirred and heated to 70~80 DEG C, protect
22~30min of temperature, obtains mixed material；
Mixed material obtained by step S2 is cooled to 40~45 DEG C by S3, and triethanolamine, antioxidant, function composition, perfume (or spice) is added
Essence is stirred until homogeneous, and is down to room temperature, discharging to get.
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