CN109430661A - A kind of preparation method of syrup of plum underflow - Google Patents

A kind of preparation method of syrup of plum underflow Download PDF

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Publication number
CN109430661A
CN109430661A CN201910005911.6A CN201910005911A CN109430661A CN 109430661 A CN109430661 A CN 109430661A CN 201910005911 A CN201910005911 A CN 201910005911A CN 109430661 A CN109430661 A CN 109430661A
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China
Prior art keywords
concentration
plum
syrup
tank
underflow
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Pending
Application number
CN201910005911.6A
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Chinese (zh)
Inventor
强会芳
高民权
张海强
况增军
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SHANNXI SHENGHUA PHARMACEUTICAL CO Ltd
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SHANNXI SHENGHUA PHARMACEUTICAL CO Ltd
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Priority to CN201910005911.6A priority Critical patent/CN109430661A/en
Publication of CN109430661A publication Critical patent/CN109430661A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Preparation Of Fruits And Vegetables (AREA)

Abstract

The present invention relates to a kind of preparation methods of syrup of plum underflow, comprising the following steps: S1 stock: weighs dark plum medicine materical crude slice, uctus Crataegi, licorice piece by weight ratio;S2 leaching material: weighed raw material medicine materical crude slice is put into heat reflux extracting-inspissator extractor, is soaked in water;S3 decoction-concentration: the feed liquid in extractor is heated to boiling, and keeps feed liquid fluidized state, and feed liquid is put into heat reflux extracting-inspissator concentration tank and carries out circumfluence distillation concentration;S4 alcohol precipitation: the concentrate being concentrated to get is placed in Alcohol-settling tank, and ethanol in proper amount is added, is stirred, and room temperature is stood, and lower sediment thing is discharged, takes supernatant;S5 secondary concentration: by supernatant be placed in heat reflux extracting-inspissator concentration tank in, carry out ethyl alcohol recycling after, then carry out secondary pressure concentration to get.Compared with prior art, the present invention has not feed change fruit color odor type, is not likely to produce precipitating, denaturalization phenomenon, and later period allotment is without the advantages of adding corrigent.

Description

A kind of preparation method of syrup of plum underflow
Technical field
The present invention relates to a kind of preparation methods of syrup of plum underflow, belong to food processing technology field.
Background technique
Syrup of plum is most ancient one of the traditional beverages in China, according to inventor Qin Dynasty necromancer Xu Fu is passed, because it has life Saliva quenches the thirst, spleen benefiting and stimulating the appetite, refreshes the mind, restoring the multi-efficiencies such as body energy, and is appreciated and liked by Emperor Qin deeply, is bestowed the name called " the public drink of Xu ".Syrup of plum original formulation increases a small amount of Radix Glycyrrhizae when to the Qing Dynasty, so far syrup of plum using dark plum and hawthorn as raw material Formula enters China's ancient prescription ranks.In the integration of drinking and medicinal herbs kind that national healths in 2012 and family planning committee member announce, dark plum, mountain Short, bristly hair or beard, Radix Glycyrrhizae are arranging.
Traditional processing production syrup of plum is filtered out residue, obtains dope using decoction method that is, by after raw material mixing infusion, after Water is added into dope again in phase, sugar is deployed.The syrup of plum dope that conventional method is processed, it is more muddy, it is long-term to place It has a large amount of precipitatings to generate, and due to closed container not being used to produce, dope is easily rotten, cannot achieve large-scale production.It is existing Carbon dioxide extraction method is mostly used for enterprise's processing syrup of plum, technical process is to carry out each raw material respectively to decoct mentioning It takes, extract, being concentrated, dextrin is added dusting, obtaining extract monocrystal, down-stream enterprise mixes each extraction raw material powder in proportion Match, be dissolved in water, corrigent adjusts mouthfeel and forms.Carbon dioxide extraction method is conducive to syrup of plum and accomplishes scale production, but most Big deficiency is to change the special efficacy of ancient prescription tanning, and intermediate monocrystal is had no result color odor type, and a large amount of food need to be added in later period allotment Additive carries out mouthfeel correction, is unfavorable for human health.
Summary of the invention
(1) technical problems to be solved
For technical problem of the existing technology, the present invention provides one kind and is suitable for industrialized production, not feed change Fruit color odor type is not likely to produce precipitating, denaturalization phenomenon, and syrup of plum underflow preparation method of the later period allotment without adding corrigent.
(2) technical solution
In order to achieve the above object, The technical solution adopted by the invention is as follows:
A kind of preparation method of syrup of plum underflow, which comprises the following steps:
S1, stock: by weight, weighing dark plum medicine materical crude slice 60-70, uctus Crataegi 30-35, licorice piece 2-5, spare;
S2, leaching material: raw material medicine materical crude slice weighed in S1 is put into heat reflux extracting-inspissator extractor, water logging is added Bubble;
S3, decoction-concentration: heat reflux extracting-inspissator extractor steam valve is opened, the feed liquid in extractor is carried out Heating keeps feed liquid fluidized state until feed liquid is boiled, and feed liquid is put into heat reflux extracting-inspissator concentration tank and carries out heat Refluxing extraction concentration;
S4, alcohol precipitation: concentrate obtained in S3 being placed in Alcohol-settling tank, then ethanol in proper amount is added into Alcohol-settling tank, is stirred Mixing, room temperature are stood, and lower sediment thing is discharged, takes supernatant spare;
S5, secondary concentration: supernatant obtained in S4 is placed in heat reflux extracting-inspissator concentration tank, is opened dense The steam valve of contracting tank heat exchanger heats liquid in concentration tank, carries out ethyl alcohol recycling, after completing ethyl alcohol recycling, then to concentration Juice in tank carries out secondary pressure and is concentrated to get syrup of plum underflow of the present invention.
Further, in the step S3, after feed liquid boils 10-30 minutes, then by feed liquid be put into heat reflux extracting-concentration The concentration tank of device carries out circumfluence distillation concentration.
Further, before the step S5, further include the steps that being filtered obtained supernatant, i.e., by supernatant It is placed in again after 5 μm of bag filters filter in heat reflux extracting-inspissator concentration tank.
Further, in the S2, amount of water is 3-4 times of raw material gross weight, and soaking time is 3-5 hours.
Further, in the S3, when heating to the feed liquid in extractor, control steam pressure is 0.1 ± 0.05mpa, It is 85 ± 3 DEG C that temperature in concentration tank is controlled in circumfluence distillation concentration process, vacuum degree 0.03-0.06mpa, after reduced pressure Obtained concentrate relative density at 90 ± 5 DEG C is 1.10-1.15.
Further, in the S4, ethyl alcohol is food-grade ethanol, and mixed liquor concentration of alcohol is in Alcohol-settling tank after addition ethyl alcohol 75%-85%, room temperature time of repose are 6-12 hours.
Further, in the S5, in ethyl alcohol recycling and secondary pressure concentration process, controlling temperature in concentration tank is 65- 85 DEG C, vacuum degree 0.01-0.07mpa, obtained underflow relative density at 50 ± 3 DEG C is after secondary pressure concentration 1.20-1.22。
(3) beneficial effect
The present invention combines conventional preparation techniques with modernization of Chinese medicine process equipment, compared with prior art, have with Lower advantage:
1, step of preparation process leaching material, decoction-concentration, alcohol precipitation, secondary concentration and later period storage of the present invention are closed Lower in container to carry out, product is unlikely to deteriorate, it can be achieved that large-scale production.
2, pectin is separated with jam using ethanol precipitation, be not easy that precipitating is precipitated, effectively increase syrup of plum after allotment The transparency of product.
3, not feed change fruit color odor type has the distinctive mouthfeel of traditional syrup of plum, taste, without adding food after allotment Additive corrects taste, reduces food safety risk.
Detailed description of the invention
Fig. 1 is a kind of process flow chart of the preparation method of syrup of plum underflow of the present invention.
Specific embodiment
The present invention is described in further details with embodiment with reference to the accompanying drawing.
Embodiment 1
As shown in Figure 1, a kind of preparation method of syrup of plum underflow of the present invention, has follow steps:
S1, stock: by weight, weighing 65 ㎏ of dark plum medicine materical crude slice, 32 ㎏ of uctus Crataegi, licorice piece 3 ㎏, spare;
S2, leaching material: raw material medicine materical crude slice weighed in S1 is put into heat reflux extracting-inspissator extractor, water logging is added Bubble, amount of water are institute 3 times of additions raw material gross weight, and soaking time is 4 hours, and it is effective to be conducive to raw material medicine materical crude slice for such operation Ingredient is precipitated in subsequent decoction step;
S3, decoction-concentration: opening heat reflux extracting-inspissator extractor steam valve, and control steam pressure is 0.1mpa heats the feed liquid in extractor, until feed liquid is boiled, feed liquid is boiled after twenty minutes, continues to keep boiling-like Feed liquid is put into heat reflux extracting-concentration tank concentration tank and carries out circumfluence distillation concentration, in circumfluence distillation concentration process by state Controlling temperature in concentration tank is 85 DEG C, vacuum degree 0.04mpa, obtained after reduced pressure relative density at 90 DEG C be 1.10 it is dense Contracting liquid so operates, it is ensured that and raw material medicine materical crude slice effective component is sufficiently fried, prevents decocting liquid bumping excessive, and reduces decocting liquid volume, Advantageous subsequent alcohol precipitation process carries out.
S4, alcohol precipitation: concentrate obtained in S3 is placed in Alcohol-settling tank, then food-grade ethanol is added into Alcohol-settling tank, is stirred Mixing is mixed, mixed liquor concentration of alcohol 80% in Alcohol-settling tank is made, room temperature stands 8 hours, and lower sediment thing is discharged, takes supernatant standby With so operation can be such that pectin and pulp in concentrate is sufficiently separated, improve product transparency, be not easy that precipitating is precipitated.
S5, filtering impurity elimination: the supernatant that S4 is obtained is filtered through 5 μm of bag filters, is so operated, it is ensured that dense The impurity such as pectin contained in contracting liquid are effectively removed.
S6, secondary concentration: will be filtered off in the hot extracting-inspissator concentration tank that flows back of miscellaneous supernatant merging in S5, It opens concentration tank heat exchanger steam valve to heat liquid in concentration tank, carries out ethyl alcohol recycling, after completing ethyl alcohol recycling, then it is right Juice in concentration tank carries out secondary pressure concentration, and ethyl alcohol recycling controls temperature in concentration tank in secondary pressure concentration process It is 65 DEG C, vacuum degree 0.06mpa, the underflow that relative density is 1.20 at 50 DEG C is obtained after secondary pressure concentration, then examined, It can be put in storage after filling, labeling, so operate, not only ensure that foodsafety, but also be conducive to later period storage.
Down-stream enterprise is when being further processed syrup of plum product, it is only necessary to add water, sugar etc. and simply be deployed, not have to needle again Corrigent is added to syrup of plum unique oral sensations.
Embodiment 2
The present embodiment is identical as 1 preparation step of embodiment, and difference is the related skill that raw material weight proportioning of soup processed is used to preparation Art technological parameter is different, and raw material taken amount and specific process parameter are as follows:
Raw material weight: 62 ㎏ of dark plum medicine materical crude slice, 34 ㎏ of uctus Crataegi, 2 ㎏ of licorice piece
Technological parameter: in S2, extractor amount of water by 4 times of addition raw material gross weight, soaking time is 3 hours;S3 In, controlling steam pressure when feed liquid in heating extraction tank is 0.15mpa, after feed liquid boils 30 minutes, then feed liquid is put into heat and is returned It flows extracting-inspissator concentration tank and carries out circumfluence distillation concentration, control temperature in concentration tank in circumfluence distillation concentration process It is 86 DEG C, vacuum degree 0.03mpa, the concentrate obtained after reduced pressure relative density at 95 DEG C is 1.15;In S4, to alcohol After food-grade ethanol is added in heavy tank, mixed liquor concentration of alcohol is 75% in Alcohol-settling tank, and room temperature time of repose is 10 hours;S6 In, in ethyl alcohol recycling and secondary pressure concentration process, controlling temperature in concentration tank is 80 DEG C, vacuum degree 0.02mpa, secondary to subtract The syrup of plum underflow obtained after pressure concentration relative density at 53 DEG C is 1.22.
Embodiment 3
The present embodiment is with Examples 1 and 2 difference, the preparing craft technical parameter of raw material weight proportioning of soup processed and use It is different:
Raw material weight: 68 ㎏ of dark plum medicine materical crude slice, 31 ㎏ of uctus Crataegi, 4 ㎏ of licorice piece
Technological parameter: in S2, extractor amount of water by 3.5 times of addition raw material gross weight, soaking time is 5 hours; In S3, controlling steam pressure when feed liquid in heating extraction tank is 0.095mpa, and feed liquid is boiled after ten minutes, then feed liquid is put into heat Extracting-inspissator concentration tank that flows back carries out circumfluence distillation concentration, and temperature in concentration tank is controlled in circumfluence distillation concentration process Degree is 83 DEG C, vacuum degree 0.06mpa, and the concentrate obtained after reduced pressure relative density at 85 DEG C is 1.12;In S4, to After food-grade ethanol is added in Alcohol-settling tank, mixed liquor concentration of alcohol is 85% in Alcohol-settling tank, and room temperature time of repose is 7 hours;S6 In, in ethyl alcohol recycling and secondary pressure concentration process, controlling temperature in concentration tank is 70 DEG C, vacuum degree 0.07mpa, secondary to subtract The syrup of plum underflow obtained after pressure concentration relative density at 47 DEG C is 1.21.
Syrup of plum underflow and tradition tanning syrup of plum dope and dioxy as shown in the table for 1-3 of embodiment of the present invention preparation Change carbon and extract monocrystal Testing index contrast table:
It can thus be seen that the syrup of plum underflow of the method for the present invention preparation has had both traditional tanning dope and carbon dioxide extraction The advantages of taking monocrystal, feed change fruit color odor type, is not likely to produce precipitating, long shelf-life, and later period allotment is rectified without addition Taste agent, effectively reduces food safety risk, is a kind of excellent production method of syrup of plum intermediate suitable for industrialized production.
The above described is only a preferred embodiment of the present invention, being not the limitation for doing other forms to the present invention, appoint What those skilled in the art changed or be modified as possibly also with the technology contents of the disclosure above equivalent variations etc. Imitate embodiment.But without departing from the technical solutions of the present invention, according to the technical essence of the invention to above embodiments institute Any simple modification, equivalent variations and the remodeling made, still fall within the protection scope of technical solution of the present invention.

Claims (7)

1. a kind of preparation method of syrup of plum underflow, which comprises the following steps:
S1, stock: by weight, weighing dark plum medicine materical crude slice 60-70, uctus Crataegi 30-35, licorice piece 2-5, spare;
S2, leaching material: raw material medicine materical crude slice weighed in S1 is put into heat reflux extracting-inspissator extractor, is soaked in water;
S3, decoction-concentration: heat reflux extracting-inspissator extractor steam valve is opened, the feed liquid in extractor is added Heat keeps feed liquid fluidized state until feed liquid is boiled, and feed liquid is put into heat reflux extracting-inspissator concentration tank progress heat and is returned Stream extracts concentration;
S4, alcohol precipitation: concentrate obtained in S3 being placed in Alcohol-settling tank, then ethanol in proper amount is added into Alcohol-settling tank, is stirred, Room temperature is stood, and lower sediment thing is discharged, takes supernatant spare;
S5, secondary concentration: supernatant obtained in S4 is placed in heat reflux extracting-inspissator concentration tank, concentration tank is opened The steam valve of heat exchanger heats liquid in concentration tank, carries out ethyl alcohol recycling, after completing ethyl alcohol recycling, then in concentration tank Juice carry out secondary pressure be concentrated to get syrup of plum underflow of the present invention.
2. a kind of preparation method of syrup of plum underflow according to claim 1, which is characterized in that in the step S3, material After liquid boils 10-30 minutes, then feed liquid is put into heat reflux extracting-inspissator concentration tank and carries out circumfluence distillation concentration.
3. a kind of preparation method of syrup of plum underflow according to claim 1, which is characterized in that before the step S5, also Include the steps that being filtered obtained supernatant, i.e., supernatant is placed in heat after 5 μm of bag filters filter again and is returned It flows in extracting-inspissator concentration tank.
4. a kind of preparation method of syrup of plum underflow according to claim 1, which is characterized in that in the S2, amount of water It is 3-4 times of raw material gross weight, soaking time is 3-5 hours.
5. a kind of preparation method of syrup of plum underflow according to claim 1, which is characterized in that in the S3, to extraction When feed liquid in tank heats, control steam pressure is 0.1 ± 0.05mpa, is controlled in concentration tank in circumfluence distillation concentration process Temperature is 85 ± 3 DEG C, and vacuum degree 0.03-0.06mpa, obtained concentrate is relatively close at 90 ± 5 DEG C after reduced pressure Degree is 1.10-1.15.
6. a kind of preparation method of syrup of plum underflow according to claim 1, which is characterized in that in the S4, ethyl alcohol is Food-grade ethanol, it is 75%-85% that mixed liquor concentration of alcohol in Alcohol-settling tank, which is added after ethyl alcohol, and room temperature time of repose is that 6-12 is small When.
7. a kind of preparation method of syrup of plum underflow according to claim 1, which is characterized in that in the S5, ethyl alcohol is returned Receive and secondary pressure concentration process in, controlling temperature in concentration tank is 65-85 DEG C, vacuum degree 0.01-0.07mpa, secondary to subtract Obtained underflow relative density at 50 ± 3 DEG C is 1.20-1.22 after pressure concentration.
CN201910005911.6A 2019-01-04 2019-01-04 A kind of preparation method of syrup of plum underflow Pending CN109430661A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112586639A (en) * 2020-12-15 2021-04-02 广东健力宝股份有限公司 Concentrated plum juice and plum juice beverage

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101584488A (en) * 2009-06-22 2009-11-25 北京燕京饮料有限公司 Pure natural sweet-sour plum juice and its preparing method
CN101744327A (en) * 2008-12-10 2010-06-23 天津鑫恒阳进出口贸易有限公司 Plum beverage and preparation method thereof
CN201969379U (en) * 2010-12-13 2011-09-14 曾粉美 Hot-reflux extraction and concentration mechanism
CN104705762A (en) * 2015-03-07 2015-06-17 湖北卫尔康现代中药有限公司 Plum juice effervescent tablet
CN107582600A (en) * 2017-06-26 2018-01-16 安徽永生堂药业有限责任公司 A kind of banlangen granules, banlangen keli and preparation method thereof
CN108157698A (en) * 2017-12-25 2018-06-15 宁夏喜力食品有限公司 A kind of compound plum juice drink and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101744327A (en) * 2008-12-10 2010-06-23 天津鑫恒阳进出口贸易有限公司 Plum beverage and preparation method thereof
CN101584488A (en) * 2009-06-22 2009-11-25 北京燕京饮料有限公司 Pure natural sweet-sour plum juice and its preparing method
CN201969379U (en) * 2010-12-13 2011-09-14 曾粉美 Hot-reflux extraction and concentration mechanism
CN104705762A (en) * 2015-03-07 2015-06-17 湖北卫尔康现代中药有限公司 Plum juice effervescent tablet
CN107582600A (en) * 2017-06-26 2018-01-16 安徽永生堂药业有限责任公司 A kind of banlangen granules, banlangen keli and preparation method thereof
CN108157698A (en) * 2017-12-25 2018-06-15 宁夏喜力食品有限公司 A kind of compound plum juice drink and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112586639A (en) * 2020-12-15 2021-04-02 广东健力宝股份有限公司 Concentrated plum juice and plum juice beverage

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Application publication date: 20190308