CN109371688B - 一种绿色环保柔软剂及其制备方法 - Google Patents
一种绿色环保柔软剂及其制备方法 Download PDFInfo
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- CN109371688B CN109371688B CN201811049451.9A CN201811049451A CN109371688B CN 109371688 B CN109371688 B CN 109371688B CN 201811049451 A CN201811049451 A CN 201811049451A CN 109371688 B CN109371688 B CN 109371688B
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- 239000004902 Softening Agent Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title abstract description 17
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 27
- 229920013822 aminosilicone Polymers 0.000 claims abstract description 26
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 20
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 20
- 108700004121 sarkosyl Proteins 0.000 claims abstract description 20
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims abstract description 20
- 229940045885 sodium lauroyl sarcosinate Drugs 0.000 claims abstract description 20
- HJVAFZMYQQSPHF-UHFFFAOYSA-N 2-[bis(2-hydroxyethyl)amino]ethanol;boric acid Chemical compound OB(O)O.OCCN(CCO)CCO HJVAFZMYQQSPHF-UHFFFAOYSA-N 0.000 claims abstract description 18
- RKISUIUJZGSLEV-UHFFFAOYSA-N n-[2-(octadecanoylamino)ethyl]octadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(=O)NCCNC(=O)CCCCCCCCCCCCCCCCC RKISUIUJZGSLEV-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000003756 stirring Methods 0.000 claims description 56
- 239000003921 oil Substances 0.000 claims description 25
- 238000010438 heat treatment Methods 0.000 claims description 16
- 238000001816 cooling Methods 0.000 claims description 15
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 14
- 239000008367 deionised water Substances 0.000 claims description 9
- 229910021641 deionized water Inorganic materials 0.000 claims description 9
- 229910021529 ammonia Inorganic materials 0.000 claims description 7
- 238000005303 weighing Methods 0.000 claims description 7
- 238000004321 preservation Methods 0.000 claims description 6
- 239000010499 rapseed oil Substances 0.000 claims description 5
- ZYNDJIBBPLNPOW-UHFFFAOYSA-N eurucic acid methyl ester Natural products CCCCCCCCC=CCCCCCCCCCCCC(=O)OC ZYNDJIBBPLNPOW-UHFFFAOYSA-N 0.000 claims description 2
- ZYNDJIBBPLNPOW-KHPPLWFESA-N methyl erucate Chemical compound CCCCCCCC\C=C/CCCCCCCCCCCC(=O)OC ZYNDJIBBPLNPOW-KHPPLWFESA-N 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 5
- 235000019198 oils Nutrition 0.000 abstract description 23
- 239000004744 fabric Substances 0.000 abstract description 7
- 235000019484 Rapeseed oil Nutrition 0.000 abstract description 5
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 5
- 239000002979 fabric softener Substances 0.000 abstract description 2
- 238000009776 industrial production Methods 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 29
- 238000012360 testing method Methods 0.000 description 9
- 230000007613 environmental effect Effects 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 239000004753 textile Substances 0.000 description 4
- 239000002131 composite material Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
- D06M13/342—Amino-carboxylic acids; Betaines; Aminosulfonic acids; Sulfo-betaines
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
Description
项目 | 柔软度平均分 |
实施例1 | 9.0 |
实施例2 | 9.2 |
实施例3 | 9.3 |
实施例4 | 9.2 |
实施例5 | 9.1 |
对比例1 | 7.2 |
对比例2 | 8.1 |
对比例3 | 4.8 |
对比例4 | 8.6 |
对比例5 | 7.5 |
项目 | △lgρ |
实施例1 | 5.22 |
实施例2 | 5.28 |
实施例3 | 5.34 |
实施例4 | 5.29 |
实施例5 | 5.24 |
对比例1 | 4.56 |
对比例2 | 4.78 |
对比例3 | 3.14 |
对比例4 | 5.12 |
对比例5 | 4.35 |
项目 | 毛细效应时间(s) |
实施例1 | 37 |
实施例2 | 35 |
实施例3 | 33 |
实施例4 | 35 |
实施例5 | 36 |
对比例1 | 51 |
对比例2 | 45 |
对比例3 | 69 |
对比例4 | 41 |
对比例5 | 55 |
项目 | 抗菌率(%) |
实施例1 | 97.7 |
实施例2 | 98.3 |
实施例3 | 98.8 |
实施例4 | 98.5 |
实施例5 | 97.9 |
对比例1 | 78.5 |
对比例2 | 83.2 |
对比例3 | 52.1 |
对比例4 | 96.6 |
对比例5 | 79.4 |
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201811049451.9A CN109371688B (zh) | 2018-09-10 | 2018-09-10 | 一种绿色环保柔软剂及其制备方法 |
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CN201811049451.9A CN109371688B (zh) | 2018-09-10 | 2018-09-10 | 一种绿色环保柔软剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN109371688A CN109371688A (zh) | 2019-02-22 |
CN109371688B true CN109371688B (zh) | 2020-12-29 |
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CN201811049451.9A Active CN109371688B (zh) | 2018-09-10 | 2018-09-10 | 一种绿色环保柔软剂及其制备方法 |
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Country | Link |
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CN (1) | CN109371688B (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111074630A (zh) * | 2019-12-26 | 2020-04-28 | 苏州福彬新科化学有限公司 | 一种具有高抗静电性能的抗静电柔软剂 |
JP7126297B1 (ja) | 2021-07-06 | 2022-08-26 | 竹本油脂株式会社 | 合成繊維用処理剤及び合成繊維 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103321053A (zh) * | 2013-06-19 | 2013-09-25 | 江苏金太阳纺织科技有限公司 | 一种多功能柔软剂及其制备方法 |
CN105421080A (zh) * | 2015-12-23 | 2016-03-23 | 常熟市淼泉盛达助剂厂 | 一种织物柔软剂 |
CN108103783A (zh) * | 2017-11-30 | 2018-06-01 | 安徽宏远无纺布业有限公司 | 一种用于布料的新型柔软剂 |
CN108221390A (zh) * | 2017-12-13 | 2018-06-29 | 上海氟聚化学产品股份有限公司 | 一种丝绸织物用亲水柔软剂及其制备方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102014203865A1 (de) * | 2014-03-04 | 2015-09-10 | Henkel Ag & Co. Kgaa | Rohstoff und seine Verwendung |
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2018
- 2018-09-10 CN CN201811049451.9A patent/CN109371688B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103321053A (zh) * | 2013-06-19 | 2013-09-25 | 江苏金太阳纺织科技有限公司 | 一种多功能柔软剂及其制备方法 |
CN105421080A (zh) * | 2015-12-23 | 2016-03-23 | 常熟市淼泉盛达助剂厂 | 一种织物柔软剂 |
CN108103783A (zh) * | 2017-11-30 | 2018-06-01 | 安徽宏远无纺布业有限公司 | 一种用于布料的新型柔软剂 |
CN108221390A (zh) * | 2017-12-13 | 2018-06-29 | 上海氟聚化学产品股份有限公司 | 一种丝绸织物用亲水柔软剂及其制备方法 |
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Address after: 201600 area F, building 1, 120 Rongjiang Road, Songjiang District, Shanghai Patentee after: Shanghai Yunji Chemical New Materials Co.,Ltd. Address before: No.216 GANGYE Road, Xiaokunshan Town, Songjiang District, Shanghai, 201616 Patentee before: SHANGHAI YUNJI CHEMICAL NEW MATERIAL CO.,LTD. |
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Effective date of registration: 20240514 Address after: Room 101, Building 5, No. 855 Dingsheng Road, Songjiang District, Shanghai, 2016 Patentee after: Shanghai Weidye Technology Co.,Ltd. Country or region after: China Address before: 201600 area F, building 1, 120 Rongjiang Road, Songjiang District, Shanghai Patentee before: Shanghai Yunji Chemical New Materials Co.,Ltd. Country or region before: China |