CN109371688A - 一种绿色环保柔软剂及其制备方法 - Google Patents
一种绿色环保柔软剂及其制备方法 Download PDFInfo
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- CN109371688A CN109371688A CN201811049451.9A CN201811049451A CN109371688A CN 109371688 A CN109371688 A CN 109371688A CN 201811049451 A CN201811049451 A CN 201811049451A CN 109371688 A CN109371688 A CN 109371688A
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- 239000004902 Softening Agent Substances 0.000 title claims abstract description 42
- 230000001681 protective effect Effects 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- -1 amido silicon Chemical compound 0.000 claims abstract description 33
- 150000001412 amines Chemical class 0.000 claims abstract description 28
- 239000003921 oil Substances 0.000 claims abstract description 27
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 27
- 239000010703 silicon Substances 0.000 claims abstract description 27
- QYDYPVFESGNLHU-UHFFFAOYSA-N elaidic acid methyl ester Natural products CCCCCCCCC=CCCCCCCCC(=O)OC QYDYPVFESGNLHU-UHFFFAOYSA-N 0.000 claims abstract description 24
- QYDYPVFESGNLHU-KHPPLWFESA-N methyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC QYDYPVFESGNLHU-KHPPLWFESA-N 0.000 claims abstract description 24
- 229940073769 methyl oleate Drugs 0.000 claims abstract description 24
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 22
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 22
- HJVAFZMYQQSPHF-UHFFFAOYSA-N 2-[bis(2-hydroxyethyl)amino]ethanol;boric acid Chemical compound OB(O)O.OCCN(CCO)CCO HJVAFZMYQQSPHF-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000002994 raw material Substances 0.000 claims abstract description 19
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims abstract description 15
- RKISUIUJZGSLEV-UHFFFAOYSA-N n-[2-(octadecanoylamino)ethyl]octadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(=O)NCCNC(=O)CCCCCCCCCCCCCCCCC RKISUIUJZGSLEV-UHFFFAOYSA-N 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000002156 mixing Methods 0.000 claims description 27
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 22
- 229910021529 ammonia Inorganic materials 0.000 claims description 11
- 238000001816 cooling Methods 0.000 claims description 9
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 8
- 239000005977 Ethylene Substances 0.000 claims description 8
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 7
- 229910052708 sodium Inorganic materials 0.000 claims description 7
- 239000011734 sodium Substances 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 4
- 125000000400 lauroyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 238000004321 preservation Methods 0.000 claims 2
- 229920002545 silicone oil Polymers 0.000 claims 2
- 239000004744 fabric Substances 0.000 abstract description 8
- 230000003115 biocidal effect Effects 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 230000010148 water-pollination Effects 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 30
- 238000012360 testing method Methods 0.000 description 10
- 239000000243 solution Substances 0.000 description 7
- BACYUWVYYTXETD-UHFFFAOYSA-N N-Lauroylsarcosine Chemical compound CCCCCCCCCCCC(=O)N(C)CC(O)=O BACYUWVYYTXETD-UHFFFAOYSA-N 0.000 description 5
- 239000007998 bicine buffer Substances 0.000 description 5
- 239000000835 fiber Substances 0.000 description 5
- 239000004753 textile Substances 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 208000015220 Febrile disease Diseases 0.000 description 1
- 108010077895 Sarcosine Proteins 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000002242 deionisation method Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000010499 rapseed oil Substances 0.000 description 1
- 229940048098 sodium sarcosinate Drugs 0.000 description 1
- ZUFONQSOSYEWCN-UHFFFAOYSA-M sodium;2-(methylamino)acetate Chemical compound [Na+].CNCC([O-])=O ZUFONQSOSYEWCN-UHFFFAOYSA-M 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
- D06M13/342—Amino-carboxylic acids; Betaines; Aminosulfonic acids; Sulfo-betaines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
Description
项目 | 柔软度平均分 |
实施例1 | 9.0 |
实施例2 | 9.2 |
实施例3 | 9.3 |
实施例4 | 9.2 |
实施例5 | 9.1 |
对比例1 | 7.2 |
对比例2 | 8.1 |
对比例3 | 4.8 |
对比例4 | 8.6 |
对比例5 | 7.5 |
项目 | △lgρ |
实施例1 | 5.22 |
实施例2 | 5.28 |
实施例3 | 5.34 |
实施例4 | 5.29 |
实施例5 | 5.24 |
对比例1 | 4.56 |
对比例2 | 4.78 |
对比例3 | 3.14 |
对比例4 | 5.12 |
对比例5 | 4.35 |
项目 | 毛细效应时间(s) |
实施例1 | 37 |
实施例2 | 35 |
实施例3 | 33 |
实施例4 | 35 |
实施例5 | 36 |
对比例1 | 51 |
对比例2 | 45 |
对比例3 | 69 |
对比例4 | 41 |
对比例5 | 55 |
项目 | 抗菌率(%) |
实施例1 | 97.7 |
实施例2 | 98.3 |
实施例3 | 98.8 |
实施例4 | 98.5 |
实施例5 | 97.9 |
对比例1 | 78.5 |
对比例2 | 83.2 |
对比例3 | 52.1 |
对比例4 | 96.6 |
对比例5 | 79.4 |
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811049451.9A CN109371688B (zh) | 2018-09-10 | 2018-09-10 | 一种绿色环保柔软剂及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811049451.9A CN109371688B (zh) | 2018-09-10 | 2018-09-10 | 一种绿色环保柔软剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN109371688A true CN109371688A (zh) | 2019-02-22 |
CN109371688B CN109371688B (zh) | 2020-12-29 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201811049451.9A Active CN109371688B (zh) | 2018-09-10 | 2018-09-10 | 一种绿色环保柔软剂及其制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN109371688B (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111074630A (zh) * | 2019-12-26 | 2020-04-28 | 苏州福彬新科化学有限公司 | 一种具有高抗静电性能的抗静电柔软剂 |
JP7126297B1 (ja) | 2021-07-06 | 2022-08-26 | 竹本油脂株式会社 | 合成繊維用処理剤及び合成繊維 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103321053A (zh) * | 2013-06-19 | 2013-09-25 | 江苏金太阳纺织科技有限公司 | 一种多功能柔软剂及其制备方法 |
CN105421080A (zh) * | 2015-12-23 | 2016-03-23 | 常熟市淼泉盛达助剂厂 | 一种织物柔软剂 |
US20160348305A1 (en) * | 2014-03-04 | 2016-12-01 | Henkel Ag & Co. Kgaa | Raw material and use thereof to reduce creases in textiles |
CN108103783A (zh) * | 2017-11-30 | 2018-06-01 | 安徽宏远无纺布业有限公司 | 一种用于布料的新型柔软剂 |
CN108221390A (zh) * | 2017-12-13 | 2018-06-29 | 上海氟聚化学产品股份有限公司 | 一种丝绸织物用亲水柔软剂及其制备方法 |
-
2018
- 2018-09-10 CN CN201811049451.9A patent/CN109371688B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103321053A (zh) * | 2013-06-19 | 2013-09-25 | 江苏金太阳纺织科技有限公司 | 一种多功能柔软剂及其制备方法 |
US20160348305A1 (en) * | 2014-03-04 | 2016-12-01 | Henkel Ag & Co. Kgaa | Raw material and use thereof to reduce creases in textiles |
CN105421080A (zh) * | 2015-12-23 | 2016-03-23 | 常熟市淼泉盛达助剂厂 | 一种织物柔软剂 |
CN108103783A (zh) * | 2017-11-30 | 2018-06-01 | 安徽宏远无纺布业有限公司 | 一种用于布料的新型柔软剂 |
CN108221390A (zh) * | 2017-12-13 | 2018-06-29 | 上海氟聚化学产品股份有限公司 | 一种丝绸织物用亲水柔软剂及其制备方法 |
Non-Patent Citations (6)
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《简明化学试剂手册》编写组: "《简明化学试剂手册》", 31 January 1991, 上海科学技术出版社 * |
冯胜: "《精细化工手册(下)》", 31 March 1995, 广东科技出版社 * |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111074630A (zh) * | 2019-12-26 | 2020-04-28 | 苏州福彬新科化学有限公司 | 一种具有高抗静电性能的抗静电柔软剂 |
JP7126297B1 (ja) | 2021-07-06 | 2022-08-26 | 竹本油脂株式会社 | 合成繊維用処理剤及び合成繊維 |
JP2023008773A (ja) * | 2021-07-06 | 2023-01-19 | 竹本油脂株式会社 | 合成繊維用処理剤及び合成繊維 |
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