CN109348549A - 一种SnO2/改性碳纳米管复合电热薄膜及其制备方法 - Google Patents
一种SnO2/改性碳纳米管复合电热薄膜及其制备方法 Download PDFInfo
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- CN109348549A CN109348549A CN201811138474.7A CN201811138474A CN109348549A CN 109348549 A CN109348549 A CN 109348549A CN 201811138474 A CN201811138474 A CN 201811138474A CN 109348549 A CN109348549 A CN 109348549A
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- China
- Prior art keywords
- carbon nano
- film
- electric
- modified carbon
- tube
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 40
- -1 modified carbon nano-tube compound Chemical class 0.000 title claims abstract description 21
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical class [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 97
- 239000002243 precursor Substances 0.000 claims abstract description 46
- 238000010438 heat treatment Methods 0.000 claims abstract description 42
- 239000000243 solution Substances 0.000 claims abstract description 40
- 239000007788 liquid Substances 0.000 claims abstract description 30
- 239000011259 mixed solution Substances 0.000 claims abstract description 20
- 150000001875 compounds Chemical class 0.000 claims abstract description 14
- 239000002904 solvent Substances 0.000 claims abstract description 4
- 238000005485 electric heating Methods 0.000 claims description 83
- 239000010408 film Substances 0.000 claims description 83
- 239000010409 thin film Substances 0.000 claims description 80
- 239000002041 carbon nanotube Substances 0.000 claims description 50
- 229910021393 carbon nanotube Inorganic materials 0.000 claims description 50
- 239000002048 multi walled nanotube Substances 0.000 claims description 35
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 24
- 239000000758 substrate Substances 0.000 claims description 23
- 238000006243 chemical reaction Methods 0.000 claims description 22
- 238000001035 drying Methods 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 13
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 12
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 11
- 239000012153 distilled water Substances 0.000 claims description 11
- 239000002184 metal Substances 0.000 claims description 11
- 229910052751 metal Inorganic materials 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical group O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 10
- 229910052799 carbon Inorganic materials 0.000 claims description 9
- 230000004048 modification Effects 0.000 claims description 9
- 238000012986 modification Methods 0.000 claims description 9
- 238000005119 centrifugation Methods 0.000 claims description 8
- 229910044991 metal oxide Inorganic materials 0.000 claims description 8
- 150000004706 metal oxides Chemical class 0.000 claims description 8
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 7
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 6
- FPCJKVGGYOAWIZ-UHFFFAOYSA-N butan-1-ol;titanium Chemical compound [Ti].CCCCO.CCCCO.CCCCO.CCCCO FPCJKVGGYOAWIZ-UHFFFAOYSA-N 0.000 claims description 5
- 239000012266 salt solution Substances 0.000 claims description 5
- TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 4
- 229910021626 Tin(II) chloride Inorganic materials 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 4
- 239000001119 stannous chloride Substances 0.000 claims description 4
- 235000011150 stannous chloride Nutrition 0.000 claims description 4
- 229960004756 ethanol Drugs 0.000 claims description 3
- 235000019441 ethanol Nutrition 0.000 claims description 3
- PJXISJQVUVHSOJ-UHFFFAOYSA-N indium(III) oxide Inorganic materials [O-2].[O-2].[O-2].[In+3].[In+3] PJXISJQVUVHSOJ-UHFFFAOYSA-N 0.000 claims description 3
- GCTFWCDSFPMHHS-UHFFFAOYSA-M Tributyltin chloride Chemical compound CCCC[Sn](Cl)(CCCC)CCCC GCTFWCDSFPMHHS-UHFFFAOYSA-M 0.000 claims description 2
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 claims description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 2
- 239000004246 zinc acetate Substances 0.000 claims description 2
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 claims 1
- 238000003756 stirring Methods 0.000 abstract description 13
- 239000000126 substance Substances 0.000 abstract description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 238000004134 energy conservation Methods 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000002604 ultrasonography Methods 0.000 description 15
- 238000003760 magnetic stirring Methods 0.000 description 13
- 238000001514 detection method Methods 0.000 description 11
- 230000000052 comparative effect Effects 0.000 description 9
- 239000011521 glass Substances 0.000 description 8
- 238000005303 weighing Methods 0.000 description 8
- 238000005516 engineering process Methods 0.000 description 7
- 239000012535 impurity Substances 0.000 description 7
- 238000004321 preservation Methods 0.000 description 7
- 239000000428 dust Substances 0.000 description 6
- 238000001914 filtration Methods 0.000 description 6
- 238000000227 grinding Methods 0.000 description 6
- 230000006641 stabilisation Effects 0.000 description 6
- 238000011105 stabilization Methods 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- 230000008901 benefit Effects 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000002131 composite material Substances 0.000 description 4
- 229910003481 amorphous carbon Inorganic materials 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 230000005611 electricity Effects 0.000 description 3
- 238000011068 loading method Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 206010037660 Pyrexia Diseases 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 241000894007 species Species 0.000 description 2
- 229910001887 tin oxide Inorganic materials 0.000 description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910021591 Copper(I) chloride Inorganic materials 0.000 description 1
- 206010054949 Metaplasia Diseases 0.000 description 1
- 239000004642 Polyimide Substances 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 235000009470 Theobroma cacao Nutrition 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 244000240602 cacao Species 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical compound [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000027950 fever generation Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- XLYOFNOQVPJJNP-ZSJDYOACSA-N heavy water Substances [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 1
- 230000015689 metaplastic ossification Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910021392 nanocarbon Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000000554 physical therapy Methods 0.000 description 1
- 229920001721 polyimide Polymers 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000027756 respiratory electron transport chain Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229920003169 water-soluble polymer Polymers 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
- H05B3/10—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor
- H05B3/12—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor characterised by the composition or nature of the conductive material
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
- H05B3/10—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor
- H05B3/12—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor characterised by the composition or nature of the conductive material
- H05B3/14—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor characterised by the composition or nature of the conductive material the material being non-metallic
- H05B3/145—Carbon only, e.g. carbon black, graphite
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B2203/00—Aspects relating to Ohmic resistive heating covered by group H05B3/00
- H05B2203/017—Manufacturing methods or apparatus for heaters
Landscapes
- Carbon And Carbon Compounds (AREA)
Abstract
Description
方块电阻/(Ω/□) | 发射率 | 发热效率/% | 通220V电压稳定发热温度/℃ |
85 | 0.9 | 92 | 320±10 |
方块电阻/(Ω/□) | 发射率 | 发热效率/% | 通220V电压稳定发热温度/℃ |
92 | 0.9 | 92 | 302±10 |
方块电阻/(Ω/□) | 发射率 | 发热效率/% | 通220V电压稳定发热温度/℃ |
95 | 0.9 | 92 | 305±10 |
方块电阻/(Ω/□) | 发射率 | 发热效率/% | 通220V电压稳定发热温度/℃ |
92 | 0.9 | 91 | 298±10 |
方块电阻/(Ω/□) | 发射率 | 发热效率/% | 通220V电压稳定发热温度/℃ |
98 | 0.9 | 92 | 305±10 |
Claims (9)
Priority Applications (1)
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CN201811138474.7A CN109348549B (zh) | 2018-09-28 | 2018-09-28 | 一种SnO2/改性碳纳米管复合电热薄膜及其制备方法 |
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CN201811138474.7A CN109348549B (zh) | 2018-09-28 | 2018-09-28 | 一种SnO2/改性碳纳米管复合电热薄膜及其制备方法 |
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CN109348549A true CN109348549A (zh) | 2019-02-15 |
CN109348549B CN109348549B (zh) | 2021-07-02 |
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Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1850641A (zh) * | 2006-05-26 | 2006-10-25 | 上海大学 | 碳纳米管/二氧化锡复合电催化电极的制备方法 |
CN101582303A (zh) * | 2009-03-24 | 2009-11-18 | 新奥光伏能源有限公司 | 一种新型结构的透明导电薄膜及其制备方法 |
CN101718732A (zh) * | 2009-12-09 | 2010-06-02 | 黑龙江大学 | 碳掺杂硼氮纳米管/半导体氧化物复合材料及其制备方法和应用 |
CN101787502A (zh) * | 2010-01-19 | 2010-07-28 | 中国科学院化学研究所 | 制备金属、金属氧化物或金属氢氧化物与碳纳米管复合物的方法 |
CN104310790A (zh) * | 2014-09-28 | 2015-01-28 | 中国建材国际工程集团有限公司 | 大面积透明导电膜玻璃的制备方法 |
CN106517812A (zh) * | 2016-11-04 | 2017-03-22 | 燕山大学 | 绒面透明导电的FTO/Gr‑CNTs复合薄膜及其制备方法 |
CN107074547A (zh) * | 2014-10-17 | 2017-08-18 | 国立研究开发法人产业技术综合研究所 | 碳纳米管复合膜及该复合膜的制造方法 |
KR20170141112A (ko) * | 2017-04-18 | 2017-12-22 | (주)씨엔티솔루션 | 탄소나노튜브가 포함된 복합소재 발열체 및 그 제조방법 |
-
2018
- 2018-09-28 CN CN201811138474.7A patent/CN109348549B/zh active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1850641A (zh) * | 2006-05-26 | 2006-10-25 | 上海大学 | 碳纳米管/二氧化锡复合电催化电极的制备方法 |
CN101582303A (zh) * | 2009-03-24 | 2009-11-18 | 新奥光伏能源有限公司 | 一种新型结构的透明导电薄膜及其制备方法 |
CN101718732A (zh) * | 2009-12-09 | 2010-06-02 | 黑龙江大学 | 碳掺杂硼氮纳米管/半导体氧化物复合材料及其制备方法和应用 |
CN101787502A (zh) * | 2010-01-19 | 2010-07-28 | 中国科学院化学研究所 | 制备金属、金属氧化物或金属氢氧化物与碳纳米管复合物的方法 |
CN104310790A (zh) * | 2014-09-28 | 2015-01-28 | 中国建材国际工程集团有限公司 | 大面积透明导电膜玻璃的制备方法 |
CN107074547A (zh) * | 2014-10-17 | 2017-08-18 | 国立研究开发法人产业技术综合研究所 | 碳纳米管复合膜及该复合膜的制造方法 |
CN106517812A (zh) * | 2016-11-04 | 2017-03-22 | 燕山大学 | 绒面透明导电的FTO/Gr‑CNTs复合薄膜及其制备方法 |
KR20170141112A (ko) * | 2017-04-18 | 2017-12-22 | (주)씨엔티솔루션 | 탄소나노튜브가 포함된 복합소재 발열체 및 그 제조방법 |
Non-Patent Citations (3)
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MOHAMMAD REZA GOLOBOSTANFARD , HOSSEIN ABDIZADEH ECT: "Carbon nanotube/indium tin oxide hybrid transparent conductive film: Effect of nanotube diameter", 《SOLAR ENERGY MATERIALS & SOLAR CELLS》 * |
于华荣,成荣明 等: "碳纳米管负载纳米Fe2O3的研究", 《无机化学学报》 * |
吴玉程,宋林云等: "碳纳米管负载纳米TiO2复合材料的制备即组织结构表征", 《功能材料》 * |
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CN109348549B (zh) | 2021-07-02 |
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Effective date of registration: 20230117 Address after: 410400 Xingwang Road, Wushi Industrial Park, Pingjiang County, Yueyang City, Hunan Province Patentee after: Pingjiang Yuefeng Electric Heating Technology Co.,Ltd. Address before: 230000 Room 203, building 2, phase I, e-commerce Park, Jinggang Road, Shushan Economic Development Zone, Hefei City, Anhui Province Patentee before: Hefei Jiuzhou Longteng scientific and technological achievement transformation Co.,Ltd. Effective date of registration: 20230117 Address after: 230000 Room 203, building 2, phase I, e-commerce Park, Jinggang Road, Shushan Economic Development Zone, Hefei City, Anhui Province Patentee after: Hefei Jiuzhou Longteng scientific and technological achievement transformation Co.,Ltd. Address before: 224051 middle road of hope Avenue, Yancheng City, Jiangsu Province, No. 1 Patentee before: YANCHENG INSTITUTE OF TECHNOLOGY |
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