CN109303076A - A kind of air sterilizing composition - Google Patents
A kind of air sterilizing composition Download PDFInfo
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- CN109303076A CN109303076A CN201810660686.5A CN201810660686A CN109303076A CN 109303076 A CN109303076 A CN 109303076A CN 201810660686 A CN201810660686 A CN 201810660686A CN 109303076 A CN109303076 A CN 109303076A
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- A—HUMAN NECESSITIES
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- A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
- A01N35/06—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing keto or thioketo groups as part of a ring, e.g. cyclohexanone, quinone; Derivatives thereof, e.g. ketals
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- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/20—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom three- or four-membered rings
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- A—HUMAN NECESSITIES
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
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Abstract
The invention discloses a kind of air sterilizing compositions, it is related to sterilizing arts, including following raw material: hypericin, allyl sulfides, snail mucus, avocado oil, glycyrrhizic acid, 1,2-PD, natural botanical extraction liquid, compound surfactant, RO water.Disinfection sanitizer of the invention prepares simple and convenient, and stability is good, has excellent functionality, dispel taste and sterilizing, is widely used, wide market.
Description
Technical field
The present invention relates to sterilizing arts, and in particular to a kind of air sterilizing composition.
Background technique
The worsening of environment causes harmful substance in air to increase, and virus, the infection of bacterium are serious especially in air
Affect people's health daily life.It is well known that cold, influenza or the infection of the upper respiratory tract are the common diseases of winter-spring season and multiple
Disease is propagated and is mainly infected by droplet and air cross, especially the crowd is dense, air is not easy the place circulated and confined air
Between, for example, hospital, school, restaurant, hotel, public lavatory, in compartment etc., the incidence of infection is higher.Its main cause is to be attributed to
There are more pathogenic microorganisms in air, such as influenza virus, rhinovirus, Respiratory Syncytial Virus(RSV), adenovirus, hemolytic hammer
Bacterium, staphylococcus, Escherichia coli etc..Therefore, carrying out sterilizing appropriate to air is to prevent and control this cross-infection
One of important measure, gradually, air sterilizing disinfectant just comes into being, but air sterilizing disinfectant quality currently on the market
Preferable price costly, also contains artificial synthesized chemosterilant mostly, is commonly exposed to this containing chemicals
Air in, it is also possible to a certain amount of harm will cause to human body.Therefore, it is purification, sterilizing, disinfection room air, develops
A kind of cheap, safe and efficient pure and fresh sterile products of green air are particularly important out.
The patent application of Publication No. CN106259446A discloses a kind of air deodorization disinfection sanitizer, including as follows
The component of parts by weight, 6~12 parts of agar, 6~8 parts of ethylene glycol, 4~8 parts of hexachlorophene, 10~16 parts of sodium pyrosulfite, benzene first
8~12 parts of sour sodium, 6~10 parts of ferrous sulfate, 8~16 parts of fat alcohol polyethylene ether, 4~8 parts of glycerol, 4~6 parts of pentanediol, second
It is 4~6 parts of acid butyl ester, 4~6 parts of butanol, 4~6 parts of sodium acrylate, 8~12 parts of phthalic acid dibutyl ester, 8~16 parts of glycerine, different
4~12 parts of propyl alcohol, 8~20 parts of triethanolamine, 4~8 parts of polyaerylic acid, 80~100 parts of distilled water.This kind of disinfection sanitizer has
Preferable environmentally friendly property, but in practical application, disinfection effect is not fine.
The patent application for authorizing Publication No. CN102487961B, discloses a kind of air smell removing disinfectant, wraps
Include solid portion and liquid portion；The solid portion includes following components by weight percentage: sodium chlorite 1-78%, sub- chlorine
Sour potassium 0.01-50%, sodium chlorate 2-85%, calcium chlorite 1-69%, calcium chlorate 0-80%, potassium chlorate 0.1-85%, hypochlorous acid
Sodium 1-90%；The liquid portion includes following components by percentage: hydrochloric acid 0.1-36.3%, copper sulphate 0-2%, sulfuric acid
Aluminium potassium 0-15%, remaining is distilled water；This kind of air smell removing disinfectant Environmental Safety, but its bactericidal effect is not enough
It is good.
Summary of the invention
The purpose of the present invention is to provide a kind of air sterilizing composition, this kind of sterilizing composition preparation is simple
Convenient, stability is good, has excellent functionality, dispel taste and sterilizing.
In order to achieve the above object, the present invention is achieved through the following technical solutions:
A kind of air sterilizing composition, including following raw material by weight:
3-5 parts of hypericin；
4.5-5.5 parts of allyl sulfides；
2-3 parts of snail mucus；
1.5-2.5 parts of avocado oil；
3-4 parts of glycyrrhizic acid；
6-8 parts of 1,2- propylene glycol；
16-20 parts of natural botanical extraction liquid；
1-2 parts of compound surfactant；
40-50 parts of RO water；
Above-mentioned compound surfactant is made of nonionic surfactant and double property ionic surface active agents.
Further, above-mentioned sterilizing composition is made of following raw material by weight:
3 parts of hypericin；
4.5 parts of allyl sulfides；
2 parts of snail mucus；
1.5 parts of avocado oil；
3 parts of glycyrrhizic acid；
6 parts of 1,2- propylene glycol；
16 parts of natural botanical extraction liquid；
1 part of compound surfactant；
40 parts of RO water；
Above-mentioned compound surfactant is by nonionic surfactant, double property ionic surface active agents according to mass ratio 1:
2 are sufficiently blended.
Further, above-mentioned sterilizing composition is made of following raw material by weight:
5 parts of hypericin；
5.5 parts of allyl sulfides；
3 parts of snail mucus；
2.5 parts of avocado oil；
4 parts of glycyrrhizic acid；
8 parts of 1,2- propylene glycol；
20 parts of natural botanical extraction liquid；
2 parts of compound surfactant；
50 parts of RO water；
Above-mentioned compound surfactant is by nonionic surfactant, double property ionic surface active agents according to mass ratio 2:
3 are sufficiently blended.
Further, above-mentioned sterilizing composition the preparation method is as follows:
I: taking the natural botanical extraction liquid of parts by weight 34%, be heated to 41 DEG C, under stirring condition, Hypericum Chinense is first added
Element and glycyrrhizic acid are sufficiently mixed stirring, after standing 22min, are heated to 49 DEG C again, and it is mixed to be then poured slowly into snail mucus
It is even, obtain material A；
II: 1,2-PD is taken, is added in closed agitator tank, first pours into allyl sulfides, high-speed stirred 12min, then
Avocado oil is poured into again, again high-speed stirred 9min, be heated to 45 DEG C later, insulated and stirred 7.5min obtains material B；
III: taking the natural botanical extraction liquid of surplus, be added in closed agitator tank, be heated to 41 DEG C, simultaneously first
Compound surfactant and material B high-speed stirred 7.5min is added, adds material A and is sufficiently mixed stirring, heat preservation is stood
The mixing of RO water is poured into after 3.5min.
Further, above-mentioned natural botanical extraction liquid is made by following steps: by weight (3-5): (1-2) takes fresh
Patrinia villosa Juss, olive leaf, be added after being smashed to pieces 4-6 times of its weight water decoct 65-75min, ultrasonic extraction 10-
15min, the water that 4-6 times of filter residue weight is added after centrifugal filtration into filter residue decoct 75-85min, ultrasonic extraction 10-15min, from
After heart filtering, merge filtrate twice, be concentrated into the 1/5 of original volume to obtain the final product.
Further, above-mentioned natural botanical extraction liquid is made by following steps: fresh white flower is taken by weight 3:1
Field pennycress, olive leaf, the water that 4 times of its weight is added after being smashed to pieces decoct 65min, ultrasonic extraction 10min, and centrifugal filtration is backward
The water that 4 times of filter residue weight are added in filter residue decocts 75min, ultrasonic extraction 10min, after centrifugal filtration, merges filtrate twice, concentration
To original volume 1/5 to obtain the final product.
Further, above-mentioned natural botanical extraction liquid is made by following steps: fresh white flower is taken by weight 5:2
Field pennycress, olive leaf, the water that 6 times of its weight is added after being smashed to pieces decoct 75min, ultrasonic extraction 15min, and centrifugal filtration is backward
The water that 6 times of filter residue weight are added in filter residue decocts 85min, ultrasonic extraction 15min, after centrifugal filtration, merges filtrate twice, concentration
To original volume 1/5 to obtain the final product.
Preferably, above-mentioned nonionic surfactant is using sorbitan fatty acid ester, lauryl glucoside according to matter
Amount is than (1-3): (3-5) is sufficiently blended；Double property ionic surface active agents use imidazoline surfactant, coconut oleoyl amine
Propyl betaine is according to mass ratio (3-4): (1-2) is sufficiently blended.
Further, above-mentioned nonionic surfactant is sorbitan fatty acid ester, lauryl glucoside according to matter
What amount was sufficiently blended than 1:3；Double property ionic surface active agents are imidazoline surfactant, Cocoamidopropyl betaine
It is sufficiently blended according to mass ratio 3:1.
Further, above-mentioned nonionic surfactant is sorbitan fatty acid ester, lauryl glucoside according to matter
What amount was sufficiently blended than 3:5；Double property ionic surface active agents are imidazoline surfactant, cocamidopropyl propyl amide sweet tea
Dish alkali is sufficiently blended according to mass ratio 2:1.
The present invention is with following the utility model has the advantages that disinfectant of the invention passes through to the ingenious selection of raw materials for production and its system
The inventive improvements of standby technique, the collaboration of the compositions such as hypericin, allyl sulfides, snail mucus, avocado oil, glycyrrhizic acid in raw material
Interaction makes sterile products obtained have effect and advantage below:
(1) stability: raw material composition is dissolved each other, and performance is good, and easily storage, easy freezing vaporization at high temperature, suspended dispersed be not good；
(2) low cost: raw material sources are extensive, low in cost, prepare simple and convenient, high production efficiency；
(3) functional: to no skin irritation, anti-inflammatory anti-itch, and to there is preferable moisturizing moisture-keeping efficacy；
(4) dispel taste: peculiar smell effect of dispelling is good, has light faint scent, can effectively purify air, improves Interior Space makings
Amount enables to air to become faint scent pleasant, has no toxic side effect, green safe；
(5) sterilizing: there is broad-spectrum, have excellent sterilization effect for fungi, bacterium etc., kill
Bacterium speed is fast, the antibacterial time is long, and germ will not develop drug resistance, and thoroughly, anthelminthic effect is good, can be widely applied to room for disinfection
Occasions and the field such as in interior, interior, public testing.
Specific embodiment
Below with reference to embodiment, further description of the specific embodiments of the present invention, and following embodiment is only used for more
Technical solution of the present invention is clearly demonstrated, and not intended to limit the protection scope of the present invention.
It all raw materials in embodiment and its produces composition and can be obtained by disclosed commercially available channel；
Embodiment 1
The present embodiment is related to a kind of air sterilizing composition and preparation method thereof, the foliar fertilizer by it is following by weight
The raw material composition of part meter:
3 parts of hypericin；
4.5 parts of allyl sulfides；
2 parts of snail mucus；
1.5 parts of avocado oil；
3 parts of glycyrrhizic acid；
6 parts of 1,2- propylene glycol；
16 parts of natural botanical extraction liquid；
1 part of compound surfactant；
40 parts of RO water.
It the selection of natural botanical extraction liquid and compound surfactant and is produced as follows in the present embodiment:
(1) natural botanical extraction liquid: taking fresh Patrinia villosa Juss, olive leaf by weight 3:1, adds after being smashed to pieces
The water for entering 4 times of its weight decocts 65min, ultrasonic extraction 10min, and the water of 4 times of filter residue weight is added after centrifugal filtration into filter residue
It decocts 75min, ultrasonic extraction 10min, after centrifugal filtration, merges filtrate twice, be concentrated into the 1/5 of original volume to obtain the final product.
(2) compound surfactant: by nonionic surfactant, double property ionic surface active agents according to mass ratio 1:2
Composition；
Wherein, nonionic surfactant is sorbitan fatty acid ester, lauryl glucoside is filled according to mass ratio 1:3
It point is blended；
Double property ionic surface active agents are imidazoline surfactant, Cocoamidopropyl betaine according to mass ratio 3:1
Sufficiently it is blended.
The preparation method of sterilizing composition is carried out according to following general steps in the present embodiment:
I: taking the natural botanical extraction liquid of parts by weight 32%, be heated to 40 DEG C, under stirring condition, Hypericum Chinense is first added
Element and glycyrrhizic acid are sufficiently mixed stirring, after standing 20min, are heated to 48 DEG C again, and it is mixed to be then poured slowly into snail mucus
It is even, obtain material A；
II: 1,2-PD is taken, is added in closed agitator tank, first pours into allyl sulfides, high-speed stirred 10min, then
Avocado oil is poured into again, again high-speed stirred 8min, be heated to 44 DEG C later, insulated and stirred 8min obtains material B；
III: taking the natural botanical extraction liquid of surplus, be added in closed agitator tank, be heated to 40 DEG C, simultaneously first
Compound surfactant and material B high-speed stirred 8min is added, adds material A and is sufficiently mixed stirring, after heat preservation stands 3min
Pour into the mixing of RO water.
Embodiment 2
The present embodiment is related to a kind of air sterilizing composition and preparation method thereof, the foliar fertilizer by it is following by weight
The raw material composition of part meter:
3 parts of hypericin；
4.5 parts of allyl sulfides；
2 parts of snail mucus；
1.5 parts of avocado oil；
3 parts of glycyrrhizic acid；
6 parts of 1,2- propylene glycol；
16 parts of natural botanical extraction liquid；
1 part of compound surfactant；
40 parts of RO water.
It the selection of natural botanical extraction liquid and compound surfactant and is produced as follows in the present embodiment:
(1) natural botanical extraction liquid: fresh Patrinia villosa Juss, olive leaf are taken by weight 3.5:1.2, is smashed to pieces
The water that 4.5 times of its weight is added afterwards decocts 68min, ultrasonic extraction 12min, and 4.5 times of filter residues are added after centrifugal filtration into filter residue
The water of weight decocts 78min, ultrasonic extraction 11min, after centrifugal filtration, merges filtrate twice, is concentrated into the 1/5 of original volume i.e.
?.
(2) compound surfactant: by nonionic surfactant, double property ionic surface active agents according to mass ratio
1.2:2.4 composition；
Wherein, nonionic surfactant is sorbitan fatty acid ester, lauryl glucoside according to mass ratio 1.5:
3.5 are sufficiently blended；
Double property ionic surface active agents are imidazoline surfactant, Cocoamidopropyl betaine according to mass ratio 3.2:
1.3 are sufficiently blended.
The preparation method of sterilizing composition is carried out according to following general steps in the present embodiment:
I: taking the natural botanical extraction liquid of parts by weight 34%, be heated to 41 DEG C, under stirring condition, Hypericum Chinense is first added
Element and glycyrrhizic acid are sufficiently mixed stirring, after standing 22min, are heated to 49 DEG C again, and it is mixed to be then poured slowly into snail mucus
It is even, obtain material A；
II: 1,2-PD is taken, is added in closed agitator tank, first pours into allyl sulfides, high-speed stirred 12min, then
Avocado oil is poured into again, again high-speed stirred 9min, be heated to 45 DEG C later, insulated and stirred 7.5min obtains material B；
III: taking the natural botanical extraction liquid of surplus, be added in closed agitator tank, be heated to 41 DEG C, simultaneously first
Compound surfactant and material B high-speed stirred 7.5min is added, adds material A and is sufficiently mixed stirring, heat preservation is stood
The mixing of RO water is poured into after 3.5min.
Embodiment 3
The present embodiment is related to a kind of air sterilizing composition and preparation method thereof, the foliar fertilizer by it is following by weight
The raw material composition of part meter:
4 parts of hypericin；
5 parts of allyl sulfides；
2.6 parts of snail mucus；
2 parts of avocado oil；
3.5 parts of glycyrrhizic acid；
7 parts of 1,2- propylene glycol；
18 parts of natural botanical extraction liquid；
1.7 parts of compound surfactant；
45 parts of RO water.
It the selection of natural botanical extraction liquid and compound surfactant and is produced as follows in the present embodiment:
(1) natural botanical extraction liquid: fresh Patrinia villosa Juss, olive leaf are taken by weight 4:1.5, after being smashed to pieces
The water that 2 times of its weight is added decocts 70min, ultrasonic extraction 12.5min, and 5 times of filter residue weight are added after centrifugal filtration into filter residue
Water decoct 80min, ultrasonic extraction 12.5min, after centrifugal filtration, merge filtrate twice, be concentrated into the 1/5 of original volume to obtain the final product.
(2) compound surfactant: by nonionic surfactant, double property ionic surface active agents according to mass ratio
1.5:2.5 composition；
Wherein, nonionic surfactant is sorbitan fatty acid ester, lauryl glucoside is filled according to mass ratio 1:2
It point is blended；
Double property ionic surface active agents are imidazoline surfactant, Cocoamidopropyl betaine according to mass ratio 3.5:
1.5 are sufficiently blended.
The preparation method of sterilizing composition is carried out according to following general steps in the present embodiment:
I: taking the natural botanical extraction liquid of parts by weight 35%, be heated to 42 DEG C, under stirring condition, Hypericum Chinense is first added
Element and glycyrrhizic acid are sufficiently mixed stirring, after standing 23min, are heated to 50 DEG C again, and it is mixed to be then poured slowly into snail mucus
It is even, obtain material A；
II: 1,2-PD is taken, is added in closed agitator tank, first pours into allyl sulfides, high-speed stirred 13min, then
Avocado oil is poured into again, again high-speed stirred 10min, be heated to 46 DEG C later, insulated and stirred 7min obtains material B；
III: taking the natural botanical extraction liquid of surplus, be added in closed agitator tank, be heated to 42 DEG C, simultaneously first
Compound surfactant and material B high-speed stirred 7min is added, adds material A and is sufficiently mixed stirring, after heat preservation stands 4min
Pour into the mixing of RO water.
Embodiment 4
The present embodiment is related to a kind of air sterilizing composition and preparation method thereof, the foliar fertilizer by it is following by weight
The raw material composition of part meter:
4.5 parts of hypericin；
5.2 parts of allyl sulfides；
2.8 parts of snail mucus；
2.1 parts of avocado oil；
3.7 parts of glycyrrhizic acid；
7.5 parts of 1,2- propylene glycol；
19 parts of natural botanical extraction liquid；
1.9 parts of compound surfactant；
46 parts of RO water.
It the selection of natural botanical extraction liquid and compound surfactant and is produced as follows in the present embodiment:
(1) natural botanical extraction liquid: fresh Patrinia villosa Juss, olive leaf are taken by weight 4.5:1.8, is smashed to pieces
The water that 5.5 times of its weight is added afterwards decocts 72min, ultrasonic extraction 14min, and 5.5 times of filter residues are added after centrifugal filtration into filter residue
The water of weight decocts 82min, ultrasonic extraction 14min, after centrifugal filtration, merges filtrate twice, is concentrated into the 1/5 of original volume i.e.
?.
(2) compound surfactant: by nonionic surfactant, double property ionic surface active agents according to mass ratio
1.6:2.7 composition；
Wherein, nonionic surfactant is sorbitan fatty acid ester, lauryl glucoside according to mass ratio 2.5:
4.5 being sufficiently blended；
Double property ionic surface active agents are imidazoline surfactant, Cocoamidopropyl betaine according to mass ratio 3.8:
1.6 are sufficiently blended.
The preparation method of sterilizing composition is carried out according to following general steps in the present embodiment:
I: taking the natural botanical extraction liquid of parts by weight 36%, be heated to 43 DEG C, under stirring condition, Hypericum Chinense is first added
Element and glycyrrhizic acid are sufficiently mixed stirring, after standing 24min, are heated to 51 DEG C again, and it is mixed to be then poured slowly into snail mucus
It is even, obtain material A；
II: 1,2-PD is taken, is added in closed agitator tank, first pours into allyl sulfides, high-speed stirred 14min, then
Avocado oil is poured into again, again high-speed stirred 11min, be heated to 47 DEG C later, insulated and stirred 6.5min obtains material B；
III: taking the natural botanical extraction liquid of surplus, be added in closed agitator tank, be heated to 43 DEG C, simultaneously first
Compound surfactant and material B high-speed stirred 6.5min is added, adds material A and is sufficiently mixed stirring, heat preservation is stood
The mixing of RO water is poured into after 4.5min.
Embodiment 5
The present embodiment is related to a kind of air sterilizing composition and preparation method thereof, the foliar fertilizer by it is following by weight
The raw material composition of part meter:
5 parts of hypericin；
5.5 parts of allyl sulfides；
3 parts of snail mucus；
2.5 parts of avocado oil；
4 parts of glycyrrhizic acid；
8 parts of 1,2- propylene glycol；
20 parts of natural botanical extraction liquid；
2 parts of compound surfactant；
50 parts of RO water.
It the selection of natural botanical extraction liquid and compound surfactant and is produced as follows in the present embodiment:
(1) natural botanical extraction liquid: taking fresh Patrinia villosa Juss, olive leaf by weight 5:2, adds after being smashed to pieces
The water for entering 6 times of its weight decocts 75min, ultrasonic extraction 15min, and the water of 6 times of filter residue weight is added after centrifugal filtration into filter residue
It decocts 85min, ultrasonic extraction 15min, after centrifugal filtration, merges filtrate twice, be concentrated into the 1/5 of original volume to obtain the final product.
(2) compound surfactant: by nonionic surfactant, double property ionic surface active agents according to mass ratio 2:3
Composition；
Wherein, nonionic surfactant is sorbitan fatty acid ester, lauryl glucoside is filled according to mass ratio 3:5
It point is blended；
Double property ionic surface active agents are imidazoline surfactant, Cocoamidopropyl betaine according to mass ratio 2:1
Sufficiently it is blended.
The preparation method of sterilizing composition is carried out according to following general steps in the present embodiment:
I: taking the natural botanical extraction liquid of parts by weight 38%, be heated to 43 DEG C, under stirring condition, Hypericum Chinense is first added
Element and glycyrrhizic acid are sufficiently mixed stirring, after standing 25min, are heated to 52 DEG C again, and it is mixed to be then poured slowly into snail mucus
It is even, obtain material A；
II: 1,2-PD is taken, is added in closed agitator tank, first pours into allyl sulfides, high-speed stirred 15min, then
Avocado oil is poured into again, again high-speed stirred 12min, be heated to 48 DEG C later, insulated and stirred 6min obtains material B
III: taking the natural botanical extraction liquid of surplus, be added in closed agitator tank, be heated to 43 DEG C, simultaneously first
Compound surfactant and material B high-speed stirred 6min is added, adds material A and is sufficiently mixed stirring, after heat preservation stands 5min
Pour into the mixing of RO water.
Comparative example 1
This comparative example is related to a kind of disinfection sanitizer, relative to embodiment 1, only eliminates adding for natural botanical extraction liquid
Add, other raw material compositions, content and preparation method are same as Example 1.
Comparative example 2
This comparative example is related to a kind of disinfection sanitizer, and relative to embodiment 2, there is only producing into for natural botanical extraction liquid
Part is different；
What this comparative example natural botanical extraction liquid used produces composition as Patrinia villosa Juss.
Comparative example 3
This comparative example is related to a kind of disinfection sanitizer, and relative to embodiment 3, there is only producing into for natural botanical extraction liquid
Part is different；
What this comparative example natural botanical extraction liquid used produces composition as olive leaf.
Comparative example 4
This comparative example is related to a kind of disinfection sanitizer, and relative to embodiment 4, there is only producing into for natural botanical extraction liquid
Part is different；
What this comparative example natural botanical extraction liquid used produces composition as folium artemisiae argyi: garlic=4:1.5 (mass ratio).
Comparative example 5
This comparative example is related to a kind of disinfection sanitizer, and relative to embodiment 5, there is only the composition of surfactant differences；
The composition that this comparative example surfactant uses is sorbitan fatty acid ester.
Comparative example 6
This comparative example is related to a kind of disinfection sanitizer, and relative to embodiment 5, there is only the differences of preparation method；
This comparative example the preparation method is as follows:
1,2-PD is first taken, after being warming up to 42 DEG C, allyl sulfides, snail mucus, avocado oil is added and is sufficiently mixed stirring,
It is then warming up to 48 DEG C again, remaining other all raw materials are added, are mixed in the agitator tank that revolving speed is 250r/min
45min.
Comparative example 7
This comparative example is related to a kind of commercially available common disinfection sanitizer, including following raw material by weight:
6 parts of eucalyptus oil；
8 parts of caryophyllus oil；
2 parts of odium stearate；
1.5 parts of aliphatic acid polyethenoxy ether；
10 parts of ethyl alcohol；
60 parts of deionized water.
Implementation result
For the beneficial effect for verifying the present invention, disinfection sanitizer made from above-described embodiment 1-5 and comparative example 1-7 is carried out
The test of following index.
One: air-borne bacteria content detection
12 20m of preparation2Closed room, carry out disinfection in unmanned situation effect observation indoors.Before disinfection, with six
Grade sieve pore air impact formula sampler carries out natural bacteria sampling, as sample before sterilizing.Example 1-5 and comparative example
The disinfection sanitizer of 1-7 preparation, closed room carries out sterilizing between 12 respectively, and spray amount is 3ml/m3.Effect
It after 18min, samples respectively, as sample after disinfection, and sampling plate is directly placed into 37 DEG C of incubators and cultivates 48h, counts life
Long clump count is as shown in table 6 below.
Table 6
| Group | Sample bacterium number cfu/m before sterilizing3 | Sample bacterium number cfu/m after disinfection3 | Disinfection efficiency % |
| Embodiment 1 | 22146 | 68 | 99.69 |
| Embodiment 2 | 20571 | 72 | 99.35 |
| Embodiment 3 | 21683 | 43 | 99.80 |
| Embodiment 4 | 23571 | 66 | 99.72 |
| Embodiment 5 | 20495 | 141 | 99.31 |
| Comparative example 1 | 22341 | 4819 | 78.43 |
| Comparative example 2 | 21643 | 3337 | 84.58 |
| Comparative example 3 | 20874 | 3032 | 85.47 |
| Comparative example 4 | 23615 | 4685 | 80.16 |
| Comparative example 5 | 22030 | 3767 | 82.90 |
| Comparative example 6 | 22796 | 3296 | 85.54 |
| Comparative example 7 | 21367 | 5423 | 74.62 |
Among the above: disinfection efficiency=(sample bacterium number after sample bacterium number-disinfection before sterilizing)/sample bacterium number before sterilizing ×
100%；
By upper table 6 it is found that the disinfection sanitizer of the present embodiment improves 13.77- compared to comparative example on disinfection efficiency
25.18 percentage points, Disinfection Effect is more preferable, has on antiseptic property and is obviously improved and improves.
Two, bacteriostasis property detects
Respectively by three kinds of staphylococcus aureus, staphylococcus albus, Escherichia coli microbionations in agar plate nutrition
On fluid level, when inoculation, uniformly gathers.The sterile circular filter paper piece of tweezer sprays prepare in embodiment 1-5 and comparative example 1-7 respectively
Disinfection sanitizer to complete wetting, be attached on the agar plate nutrition fluid level of inoculated bacteria.Agar plate is placed in 37
DEG C incubator culture 3h.The diameter of duplicate measurements antibacterial ring size three times, takes its average value, is recorded in the following table 7, table 8 and table 9.
Table 7 (staphylococcus aureus)
Table 8 (staphylococcus albus)
| Group | Inhibition zone diameter mm | Relatively antibacterial efficiency % |
| Embodiment 1 | 23.8 | 97.14 |
| Embodiment 2 | 23.1 | 94.29 |
| Embodiment 3 | 24.5 | 100 |
| Embodiment 4 | 24.2 | 98.78 |
| Embodiment 5 | 23.3 | 95.10 |
| Comparative example 1 | 13.8 | 56.33 |
| Comparative example 2 | 15.2 | 62.04 |
| Comparative example 3 | 14.9 | 60.82 |
| Comparative example 4 | 15.4 | 62.86 |
| Comparative example 5 | 14.6 | 59.59 |
| Comparative example 6 | 15.5 | 63.27 |
| Comparative example 7 | 12.7 | 51.84 |
Table 9 (Escherichia coli)
Among the above: inhibition zone diameter is bigger, illustrates that fungistatic effect is better；
By upper table 7 it is found that the disinfection sanitizer of the present embodiment compared to comparative example in bacteriostasis property effect more preferable, bacteriostasis property
Above have and is obviously improved and improves and (analyze the equal < 0.05 of P value using SAS system software variance statistic).
Three: product toxicity detection
Experiment detection process see the table below described in 10:
Table 10
In conjunction with the excellent effect of the present invention, applicant is illustrated constituent part and preparation method of the invention:
(1) snail mucus: in preparation system of the invention, the ingenious addition of snail mucus can play thick stabilization
Effect, not only have certain bactericidal effect, moreover it is possible to resist the destruction by aoxidizing and causing skin naturally, effectively maintain
Human skin it is tender with it is elastic, reach the effect of helping skin, tender skin, and can be good at the synergistic effect of the other compositions of the present invention
Its effectiveness is played, there is unobviousness.
(2) compound surfactant: surfactant as common one of the outer adding assistant of chemical-biological formulation art,
Its type mainly includes cationic, anionic, double property ionics, non-ionic, functional, has emulsification, solubilising, hair
The effects of bubble；Therefore, the influence of different types of surfactant and its content for different preparations is completely different, mainly
It is form, state and the difference of requirement because of medium, some surfactants, for the cationic, anionic, double singly matched
Property ionic, the surfactant that compounds in non-ionic middle a kind of such as the application, may certain preparation preferably
Performance, improve the functionality of preparation, but this kind of surfactant, it is also possible to be not suitable for being added in another preparation,
It plays a role to the functionality of formulation products and helps very little, and the too low or excessively high of surface-active contents can all influence finally to make
The performance of agent product；Applicant is largely tested in the case where above-mentioned a variety of factors are contemplated, and is obtained suitable the application sterilization and is disappeared
The compound surfactant of toxic agent, and this novel compound surfactant is only used, of the invention kill could be made
The state and performance of bacterium disinfectant performance are preferably promoted, and during development, why applicant uses sorbose
Alcohol acid anhydride aliphatic ester, lauryl glucoside, imidazoline surfactant, these four compositions of Cocoamidopropyl betaine are as this
The outer adding assistant of invention, the reason is as follows that: 1. green safe not poison, the rapid thorough 2. four kinds of compositions of biodegrade, which dissolve each other, cooperates with effect
Fruit is good；3. the stability of disinfection sanitizer, suspended dispersed, antistatic property, sterilizing etc. can be substantially improved, significantly mention
The performance of high product, and applicant also used the surfactant of other types, such as amino acid pattern class, quaternized species
Etc. said effect is not achieved；In addition, in this kind of compound surfactant the missing of composition, addition and the reduction of content or
Improve the realization that can all influence beneficial effect of the present invention.
(3) natural botanical extraction liquid: in existing disinfection sanitizer, it much all joined natural Chinese medicine draft and plant
Object composition, such as: aloe, folium artemisiae argyi, garlic, tealeaves etc., but Patrinia villosa Juss, olive leaf compound that the present invention uses are made
Natural botanical extraction liquid through applicant's lot of experiment validation, the beneficial effect that collaboration generates will more be suitable for more preferably this hair
Bright reaction system obtains unexpected effect；Be described further again below: 1. why applicant selects white-flowered
Field pennycress has reason: experiment discovery Patrinia villosa Juss extracting solution has very strong inhibiting effect to staphylococcus aureus, and
And there is apparent suppression toxic effect fruit, in addition, it in vitro all has staphylococcus albus, Escherichia coli, diphtheroid etc.
Good inhibiting effect, and these effectiveness patrinia scabiosaefolia Fiscs grass do not have；2. applicant is so selection olive leaf is because of it
Extracting solution has broad-spectrum antibacterial action, is able to suppress the live virus pathogen transmission growth that disappears, and olive leaf extract can also be effective
Maintain human skin it is tender with it is elastic, reach the effect of helping skin, tender skin；3. in addition, applicant further found that only according to the present invention
Operation the natural botanical extraction liquid that Patrinia villosa Juss, olive leaf compound are made is only optimal case of the invention, produce
The change of technique, composition and content will lead to the missing of beneficial effect of the present invention.
Certainly, because of the requirement of the mentality of designing and goal of the invention of disinfection sanitizer of the present invention, remaining group sorting of the present invention
It selects and content selection is obviously also non-obvious, those skilled in the art combine the prior art that can readily occur in absolutely not.
This has further embodiment in the preparation method of disinfection sanitizer of the present invention, in conjunction with the embodiment of the present invention it can be seen that, this
Raw material is added using I-III three step design in the preparation method of invention by several times in batches, and step is simple and orderly, rather than uses existing
There is technology is conventional to be added at one time, this technique is mutually fitted with the special proportion of disinfection sanitizer raw materials for production component of the present invention
It answers, only uses this technique, just can guarantee that the smooth sequential of disinfection sanitizer preparation reaction system carries out, ensure last system
The excellent characteristics of standby disinfection sanitizer out.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although referring to aforementioned reality
Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features.It is all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of air sterilizing composition, which is characterized in that including following raw material by weight:
3-5 parts of hypericin；
4.5-5.5 parts of allyl sulfides；
2-3 parts of snail mucus；
1.5-2.5 parts of avocado oil；
3-4 parts of glycyrrhizic acid；
6-8 parts of 1,2- propylene glycol；
16-20 parts of natural botanical extraction liquid；
1-2 parts of compound surfactant；
40-50 parts of RO water；
The compound surfactant is made of nonionic surfactant and double property ionic surface active agents.
2. a kind of air sterilizing composition according to claim 1, which is characterized in that by it is following by weight
Raw material composition:
3 parts of hypericin；
4.5 parts of allyl sulfides；
2 parts of snail mucus；
1.5 parts of avocado oil；
3 parts of glycyrrhizic acid；
6 parts of 1,2- propylene glycol；
16 parts of natural botanical extraction liquid；
1 part of compound surfactant；
40 parts of RO water；
The compound surfactant is to be filled by nonionic surfactant, double property ionic surface active agents according to mass ratio 1:2
It point is blended.
3. a kind of air sterilizing composition according to claim 1, which is characterized in that by it is following by weight
Raw material composition:
5 parts of hypericin；
5.5 parts of allyl sulfides；
3 parts of snail mucus；
2.5 parts of avocado oil；
4 parts of glycyrrhizic acid；
8 parts of 1,2- propylene glycol；
20 parts of natural botanical extraction liquid；
2 parts of compound surfactant；
50 parts of RO water；
The compound surfactant is to be filled by nonionic surfactant, double property ionic surface active agents according to mass ratio 2:3
Divide and is blended to obtain.
4. a kind of air sterilizing composition according to claim 1, which is characterized in that the sterilizing composition
The preparation method is as follows:
I: take the natural botanical extraction liquid of parts by weight 34%, be heated to 41 DEG C, under stirring condition, first be added hypericin and
Glycyrrhizic acid is sufficiently mixed stirring, after standing 22min, is heated to 49 DEG C again, is then poured slowly into the mixing of snail mucus, obtains
Material A；
II: taking 1,2-PD, be added in closed agitator tank, first pour into allyl sulfides, high-speed stirred 12min then falls again
Enter avocado oil, again high-speed stirred 9min, is heated to 45 DEG C later, insulated and stirred 7.5min obtains material B；
III: taking the natural botanical extraction liquid of surplus, be added in closed agitator tank, be heated to 41 DEG C, be first added simultaneously
Compound surfactant and material B high-speed stirred 7.5min add material A and are sufficiently mixed stirring, after heat preservation stands 3.5min
Pour into the mixing of RO water.
5. a kind of air sterilizing composition according to claim 1, which is characterized in that the natural botanical extraction liquid
Be made by following steps: by weight (3-5): (1-2) takes fresh Patrinia villosa Juss, olive leaf, is added after being smashed to pieces
The water of 4-6 times of its weight decocts 65-75min, ultrasonic extraction 10-15min, and 4-6 times of filter residue is added after centrifugal filtration into filter residue
The water of weight decocts 75-85min, ultrasonic extraction 10-15min, after centrifugal filtration, merges filtrate twice, is concentrated into original volume
1/5 to obtain the final product.
6. a kind of air sterilizing composition according to claim 1, which is characterized in that the natural botanical extraction liquid
It is made by following steps: taking fresh Patrinia villosa Juss, olive leaf by weight 3:1,4 times of its weight is added after being smashed to pieces
Water decoct 65min, ultrasonic extraction 10min, the water that 4 times of filter residue weight are added after centrifugal filtration into filter residue decocts 75min, surpasses
Sound extracts 10min, after centrifugal filtration, merges filtrate twice, is concentrated into the 1/5 of original volume to obtain the final product.
7. a kind of air sterilizing composition according to claim 1, which is characterized in that the natural botanical extraction liquid
It is made by following steps: taking fresh Patrinia villosa Juss, olive leaf by weight 5:2,6 times of its weight is added after being smashed to pieces
Water decoct 75min, ultrasonic extraction 15min, the water that 6 times of filter residue weight are added after centrifugal filtration into filter residue decocts 85min, surpasses
Sound extracts 15min, after centrifugal filtration, merges filtrate twice, is concentrated into the 1/5 of original volume to obtain the final product.
8. a kind of air sterilizing composition according to claim 1, which is characterized in that the non-ionic surface active
Agent is sorbitan fatty acid ester, lauryl glucoside according to mass ratio (1-3): (3-5) is sufficiently blended；It is described double
Property ionic surface active agent be imidazoline surfactant, Cocoamidopropyl betaine is according to mass ratio (3-4): (1-2) fills
It point is blended.
9. a kind of air sterilizing composition according to claim 1, which is characterized in that the non-ionic surface active
Agent is sorbitan fatty acid ester, lauryl glucoside is sufficiently blended according to mass ratio 1:3；Double property ion tables
Face activating agent is imidazoline surfactant, Cocoamidopropyl betaine is sufficiently blended according to mass ratio 3:1.
10. a kind of air sterilizing composition according to claim 1, which is characterized in that the non-ionic surface is living
Property agent be that sorbitan fatty acid ester, lauryl glucoside are sufficiently blended according to mass ratio 3:5；Double property ions
Surfactant is imidazoline surfactant, Cocoamidopropyl betaine is sufficiently blended according to mass ratio 2:1.
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| CN105219543A (en) * | 2015-11-16 | 2016-01-06 | 太仓东能环保设备有限公司 | A kind of natural bacteriostatic sanitising agent and preparation method |
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