CN109276513A - A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end - Google Patents
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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Abstract
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, by deionized water, EDETATE SODIUM, glycerol, 1, 3-propanediol, niacinamide, parahydroxyacet-ophenone, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate, hydroxypropyl-trimethyl ammonium chloride hyaluronic acid, Xylitol-based glucoside/anhydro xylitol/xylitol/glucose/water, hydrolyze phycocolloid, grape seed extract, Yin Du le culm powder, leaf of Mentha piperita extract, wing seed Moringa seed extract, Chondrus crispus extract/tool is away from helictite algae extract, sodium chloride, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 composition.The present invention is prepared by certain technique and is realized; utilize the extra sebum of natural Yin Du le culm powder physical absorption; salubrious skin; it is succinct to add a variety of natural plants, is formed skin " protective film ", barrier pollutes micronic dust; chelate harmful heavy metal; it is anti-oxidant to nourish tender skin with allergy-relieving, purify skin nocuousness absurd creature;It maintains and wakes up cell viability, promote skin to rebuild, enhancing skin maintenance strength;Keep Skin Cell vitality and cohesiveness.
Description
Technical field
The present invention relates to a kind of composite plant oil-control bilayer surfactant articles at Han You le bamboo powder end.
Background technique
Common single layer surfactant only has the function of moisturizing, and marketed bilayer surfactant adds the mineral such as kaolin or Cab-O-sil
Source powder is used for a long time and is easy blocking pore, and skin water oil is unbalance, and skin is easily dark yellow.As PM2.5 value is exceeded, in air
Pollution micronic dust be readily adsorbed in skin surface, cause skin metabolism circulation be affected, blackhead, pore can be made coarse and allergy
Equal skin problems are more obvious.A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, interior-addition are a variety of natural
Plant is succinct, soothes the skin allergic symptom, nourishes tender skin, purifies skin nocuousness absurd creature;Outside-hydrolysis phycocolloid and wing seed are peppery
The wooden seed extract forms " protective film " in skin surface, using natural Zhi object Lai the oil of Yuan le bamboo fine powder physical absorption skin surface
Rouge reduces the infringement of pollutant.Inside and outside dual protection, effectively resists air pollution, and pure and fresh skin enhances skin maintenance barrier.
Summary of the invention
The object of the present invention is to provide a kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, it has day
Ran le bamboo powder physical absorption sebum;Various plants extract is added, energy allergy-relieving nourishes tender skin, purifies skin
Harmful absurd creature;And form skin " protective film ", barrier pollute micronic dust the characteristics of.
The present invention is implemented as follows: a kind of its parts by weight of the composite plant oil-control bilayer surfactant at Han You le bamboo powder end
Than are as follows:
A phase:
Deionized water 70.97-90.29, EDETATE SODIUM 0.03~0.1,
Glycerol 2~5,1,3-PD 5~8,
Niacinamide 0.5~3,
Parahydroxyacet-ophenone 0.2~0.3, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate 0.1~0.3,
Hydroxypropyl-trimethyl ammonium chloride hyaluronic acid 0.001~0.004,
Xylitol-based glucoside/anhydro xylitol/xylitol/glucose/water 0.3~0.7;
B phase
Hydrolysis phycocolloid 0.1~2, grape seed extract 0.1~0.5,
Yin Du le culm powder 0.5~1, leaf of Mentha piperita extract 0.5~1,
Wing seed Moringa seed extract 0.03~3,
Chondrus crispus extract/tool away from helictite algae extract 0.1~0.5,
Sodium chloride 0.3~0.6,
Boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide 0.02~0.05,
Phenoxyethanol 0.15~0.25, Sensiva SC50 0.1~0.2.
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, preparation method according to the following steps:
1. deionized water is added in water phase jacketed pan, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate, mixing speed control are added
At 20-25 revs/min, 20-30min is stirred, EDETATE SODIUM, Xylitol-based glucoside/dehydration wood are sequentially added under stirring
Sugar alcohol/xylitol/glucose/water, parahydroxyacet-ophenone and niacinamide simultaneously dissolves in deionized water;It is sufficiently stirred at room temperature,
It is passed through steam in the collet of jacketed pan, 80-85 DEG C is heated under stirring, maintains 10min sterilizing, is vapored away when being supplementary heating
Moisture, the going from water of 2%-3% can be added by formula;
2. Aqueous Phase Raw Material is added in emulsion pot by filter, stirring is opened, mixing speed is controlled at 20-25 revs/min
Temperature is warming up to 85 DEG C or so while stirring by clock.Under the conditions of 80-85 DEG C, glycerol and Hydroxyproyl Trimethyl chlorine are sequentially added
Change ammonium hyaluronic acid, being sufficiently stirred, which is swollen it uniformly, prevents conglomeration, can carry out homogeneous, homogeneous speed control is at 1500 revs/min
Clock or so homogeneous 3-5 minutes, keeps the temperature 20 minutes, opens cooling system and is cooled down;
3. be cooled to 35-40 DEG C, be added Chondrus crispus extract/tool away from helictite algae extract, leaf of Mentha piperita extract,
Hydrolyze phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, sodium chloride, borosilicic acid
Aluminium calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 carries out homogeneous 3-5 minutes, homogeneous speed
1500-2000 revs/min;Mixing speed is controlled at 20-25 revs/min, is stirred 10 minutes, is mixed them thoroughly;
The type of cooling is that chilled water is passed through in the collet of emulsion pot, and side stirring, side is cooling, and the speed of homogeneous and time answer
It is subject to strict control, in order to avoid excessive shear;At a lower temperature be added Chondrus crispus extract/tool away from helictite algae extract,
Leaf of Mentha piperita extract, hydrolysis phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- the third two
Alcohol, sodium chloride, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50, control stirring
It 20-35 revs/min of speed, stirs 10-15 minutes, to ensure its activity;
4. being aged and filling: it is filling with bottle placer after storage 1 day or 2 days, it needs to carry out performance rating, matter to product before filling
It is carried out after amount is qualified filling;It is needed when filling filling while stirring.
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder of the invention end, main component contain Yin Du le culm
Powder, leaf of Mentha piperita extract, wing seed Moringa seed extract and hydrolysis phycocolloid;It must be shaken up before, Tian Ran le bamboo oil suction fine powder
The extra grease of physical absorption skin keeps salubrious and increases the sliding feeling of skin silk simultaneously;Leaf of Mentha piperita extract is rich in simultaneously
Dried peppermint leaf flavanones soothes the skin allergic symptom inside skin;Wing seed Moringa seed extract has lotus-effect, reduces dirty
Object attachment is contaminated, cell is protected, preventing from heavy metal is encroached on, protects skin;Skin " protection can be formed in skin surface by hydrolyzing phycocolloid
Film ", shielding isolation pollution particle, polyphenoils protect skin cell to encroach on from pollution sources to purify skin.
In conclusion the present invention has unique appearance characteristics, it is double-deck surfactant when standing, upper layer is faint yellow
Bright aqua, lower layer are uniform powder, are shaken up before use as uniform pigment mixture, natural Yin Du le culm powder physics is utilized to inhale
Attached extra sebum, salubrious skin add a variety of natural plants essences, have allergy-relieving, nourish tender skin, purify flesh
Skin nocuousness absurd creature;Wing seed Moringa seed extract and hydrolysis phycocolloid form skin " protective film ", and barrier pollutes micronic dust, chelate harmful weight
Metal purification skin maintains and wakes up cell viability, anti-oxidant to promote skin to rebuild, enhance skin maintenance strength;Keep skin
Skin cell viability and cohesiveness.
Detailed description of the invention
Fig. 1 is the mean value that 30 subjects of the invention put forehead skin oil and fat content in different times.
Fig. 2 is that 30 subjects of the invention put forehead skin oil and fat changes of contents in different times.
Specific embodiment
The invention will be further described With reference to embodiment:
Embodiment 1
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, ingredients by weight portion rate:
A phase:
Deionized water 73.496, EDETATE SODIUM 0.1,
Glycerol 5,
1,3-PD 8,
Niacinamide 3,
Parahydroxyacet-ophenone 0.3,
Sodium metasilicate magnesium lithium/tetrasodium pyrophosphate 0.3,
Hydroxypropyl-trimethyl ammonium chloride hyaluronic acid 0.004,
Xylitol-based glucoside/anhydro xylitol/xylitol/glucose/water 0.7;
B phase
Phycocolloid 2 is hydrolyzed,
Grape seed extract 0.5,
Yin Du le culm powder 1,
Leaf of Mentha piperita extract 1,
Wing seed Moringa seed extract 3,
Chondrus crispus extract/tool away from helictite algae extract 0.5,
Sodium chloride 0.6,
Boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide 0.05,
Phenoxyethanol 0.25,
Sensiva SC50 0.2;
Preparation method is according to the following steps:
1. deionized water is added in water phase jacketed pan, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate, mixing speed control are added
At 20-25 revs/min, 20-30min is stirred, EDETATE SODIUM, Xylitol-based glucoside/dehydration wood are sequentially added under stirring
Sugar alcohol/xylitol/glucose/water, parahydroxyacet-ophenone and niacinamide simultaneously dissolves in deionized water;It is sufficiently stirred at room temperature,
It is passed through steam in the collet of jacketed pan, 80-85 DEG C is heated under stirring, maintains 10min sterilizing, is vapored away when being supplementary heating
Moisture, the going from water of 2%-3% can be added by formula;
2. Aqueous Phase Raw Material is added in emulsion pot by filter, stirring is opened, mixing speed is controlled at 20-25 revs/min
Temperature is warming up to 85 DEG C or so while stirring by clock.Under the conditions of 80-85 DEG C, glycerol and Hydroxyproyl Trimethyl chlorine are sequentially added
Change ammonium hyaluronic acid, being sufficiently stirred, which is swollen it uniformly, prevents conglomeration, can carry out homogeneous, homogeneous speed control is at 1500 revs/min
Clock or so homogeneous 3-5 minutes, keeps the temperature 20 minutes, opens cooling system and is cooled down;
3. be cooled to 35-40 DEG C, be added Chondrus crispus extract/tool away from helictite algae extract, leaf of Mentha piperita extract,
Hydrolyze phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, sodium chloride, borosilicic acid
Aluminium calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 carries out homogeneous 3-5 minutes, homogeneous speed
1500-2000 revs/min;Mixing speed is controlled at 20-25 revs/min, is stirred 10 minutes, is mixed them thoroughly;
The type of cooling is that chilled water is passed through in the collet of emulsion pot, and side stirring, side is cooling, and the speed of homogeneous and time answer
It is subject to strict control, in order to avoid excessive shear;At a lower temperature be added Chondrus crispus extract/tool away from helictite algae extract,
Leaf of Mentha piperita extract, hydrolysis phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- the third two
Alcohol, sodium chloride, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50, control stirring
It 20-35 revs/min of speed, stirs 10-15 minutes, to ensure its activity;
4. being aged and filling: it is filling with bottle placer after storage 1 day or 2 days, it needs to carry out performance rating, matter to product before filling
It is carried out after amount is qualified filling;It is needed when filling filling while stirring.
Embodiment 2
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, ingredients by weight portion rate:
A phase:
Deionized water 88.968,
EDETATE SODIUM 0.03,
Glycerol 3,
1,3-PD 5,
Niacinamide 0.5,
Parahydroxyacet-ophenone 0.2,
Sodium metasilicate magnesium lithium/tetrasodium pyrophosphate 0.1,
Hydroxypropyl-trimethyl ammonium chloride hyaluronic acid 0.002,
Xylitol-based glucoside/anhydro xylitol/xylitol/glucose/water 0.3;
B phase:
Phycocolloid 0.1 is hydrolyzed,
Grape seed extract 0.1,
Yin Du le culm powder 0.5,
Leaf of Mentha piperita extract 0.5,
Wing seed Moringa seed extract 0.03,
Chondrus crispus extract/tool away from helictite algae extract 0.1,
Sodium chloride 0.3,
Boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide 0.02
Phenoxyethanol 0.15,
Sensiva SC50 0.1;
Preparation method is according to the following steps:
1. deionized water is added in water phase jacketed pan, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate, mixing speed control are added
At 20-25 revs/min, 20-30min is stirred, EDETATE SODIUM, Xylitol-based glucoside/dehydration wood are sequentially added under stirring
Sugar alcohol/xylitol/glucose/water, parahydroxyacet-ophenone and niacinamide simultaneously dissolves in deionized water;It is sufficiently stirred at room temperature,
It is passed through steam in the collet of jacketed pan, 80-85 DEG C is heated under stirring, maintains 10min sterilizing, is vapored away when being supplementary heating
Moisture, the going from water of 2%-3% can be added by formula;
2. Aqueous Phase Raw Material is added in emulsion pot by filter, stirring is opened, mixing speed is controlled at 20-25 revs/min
Temperature is warming up to 85 DEG C or so while stirring by clock.Under the conditions of 80-85 DEG C, glycerol and Hydroxyproyl Trimethyl chlorine are sequentially added
Change ammonium hyaluronic acid, being sufficiently stirred, which is swollen it uniformly, prevents conglomeration, can carry out homogeneous, homogeneous speed control is at 1500 revs/min
Clock or so homogeneous 3-5 minutes, keeps the temperature 20 minutes, opens cooling system and is cooled down;
3. be cooled to 35-40 DEG C, be added Chondrus crispus extract/tool away from helictite algae extract, leaf of Mentha piperita extract,
Hydrolyze phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, sodium chloride, borosilicic acid
Aluminium calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 carries out homogeneous 3-5 minutes, homogeneous speed
1500-2000 revs/min;Mixing speed is controlled at 20-25 revs/min, is stirred 10 minutes, is mixed them thoroughly;
The type of cooling is that chilled water is passed through in the collet of emulsion pot, and side stirring, side is cooling, and the speed of homogeneous and time answer
It is subject to strict control, in order to avoid excessive shear;At a lower temperature be added Chondrus crispus extract/tool away from helictite algae extract,
Leaf of Mentha piperita extract, hydrolysis phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- the third two
Alcohol, sodium chloride, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50, control stirring
It 20-35 revs/min of speed, stirs 10-15 minutes, to ensure its activity;
4. being aged and filling: it is filling with bottle placer after storage 1 day or 2 days, it needs to carry out performance rating, matter to product before filling
It is carried out after amount is qualified filling;It is needed when filling filling while stirring.
Embodiment 3
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, ingredients by weight portion rate:
A phase:
Deionized water 82.307,
EDETATE SODIUM 0.05,
Glycerol 4,
1,3-PD 7,
Niacinamide 2,
Parahydroxyacet-ophenone 0.25,
Sodium metasilicate magnesium lithium/tetrasodium pyrophosphate 0.3,
Hydroxypropyl-trimethyl ammonium chloride hyaluronic acid 0.003,
Xylitol-based glucoside/anhydro xylitol/xylitol/glucose/water 0.4;
B phase:
Phycocolloid 0.3 is hydrolyzed,
Grape seed extract 0.3,
Yin Du le culm powder 0.8,
Leaf of Mentha piperita extract 0.8,
Wing seed Moringa seed extract 0.5,
Chondrus crispus extract/tool away from helictite algae extract 0.2,
Sodium chloride 0.4,
Boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide 0.04,
Phenoxyethanol 0.2,
Sensiva SC50 0.15;
Preparation method is according to the following steps:
1. deionized water is added in water phase jacketed pan, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate, mixing speed control are added
At 20-25 revs/min, 20-30min is stirred, EDETATE SODIUM, Xylitol-based glucoside/dehydration wood are sequentially added under stirring
Sugar alcohol/xylitol/glucose/water, parahydroxyacet-ophenone and niacinamide simultaneously dissolves in deionized water;It is sufficiently stirred at room temperature,
It is passed through steam in the collet of jacketed pan, 80-85 DEG C is heated under stirring, maintains 10min sterilizing, is vapored away when being supplementary heating
Moisture, the going from water of 2%-3% can be added by formula;
2. Aqueous Phase Raw Material is added in emulsion pot by filter, stirring is opened, mixing speed is controlled at 20-25 revs/min
Temperature is warming up to 85 DEG C or so while stirring by clock.Under the conditions of 80-85 DEG C, glycerol and Hydroxyproyl Trimethyl chlorine are sequentially added
Change ammonium hyaluronic acid, being sufficiently stirred, which is swollen it uniformly, prevents conglomeration, can carry out homogeneous, homogeneous speed control is at 1500 revs/min
Clock or so homogeneous 3-5 minutes, keeps the temperature 20 minutes, opens cooling system and is cooled down;
3. be cooled to 35-40 DEG C, be added Chondrus crispus extract/tool away from helictite algae extract, leaf of Mentha piperita extract,
Hydrolyze phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, sodium chloride, borosilicic acid
Aluminium calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 carries out homogeneous 3-5 minutes, homogeneous speed
1500-2000 revs/min;Mixing speed is controlled at 20-25 revs/min, is stirred 10 minutes, is mixed them thoroughly;
The type of cooling is that chilled water is passed through in the collet of emulsion pot, and side stirring, side is cooling, and the speed of homogeneous and time answer
It is subject to strict control, in order to avoid excessive shear;At a lower temperature be added Chondrus crispus extract/tool away from helictite algae extract,
Leaf of Mentha piperita extract, hydrolysis phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- the third two
Alcohol, sodium chloride, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50, control stirring
It 20-35 revs/min of speed, stirs 10-15 minutes, to ensure its activity;
4. being aged and filling: it is filling with bottle placer after storage 1 day or 2 days, it needs to carry out performance rating, matter to product before filling
It is carried out after amount is qualified filling;It is needed when filling filling while stirring.
Long-acting oil control effect scheme of this product implements and data statistics:
(1) 1. test purpose
By 30 people a set product is used in conjunction 4 weeks in open trial, the method for instrument test, cross-reference, and verifying product is long-acting
The effect of oil-control.
2. test sample and application method
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, first shakes up this product using preceding, takes appropriate refreshing
Skin water wipes face.
3. subject
3.1 all subjects receive oral and papery informed consent according to local statues, regulation.Informed consent solution
The property, purpose and the potential risk for participating in research of research have been released, and has emphasized to participate in the voluntary of test, subject can be at any time
It withdraws from the study in any reason.All informed consent signatures must be carried out before the study began.
3.2 inclusion criteria
1. Chinese women,
2. the age 20-55 years old;
3. oiliness or semi-oily skin;
4. subject copes with common cosmetics not allergy, other clinical researches are not participated within nearly three months;
5. during test, forbidding using other skin-protection products or other products for influencing test, daily necessities and reality in test
What is used before testing is consistent, forbids replacing.
3.3 target number of cases
Selected 35 people of Eligible subjects, it is ensured that be finally completed 30 people.
4. test equipment
4.1 skin oil and fat tester Sebumeter (Courage&Khazaka, Germany).
4.2 balances, sensibility reciprocal 0.01g (English weighing apparatus).
5. testing environment
Environmental requirement: temperature: 21.0 DEG C ± 1.0 DEG C;Humidity: 50% ± 5%.
6. experiment process
Period: 4 weeks are long-acting:
1. being screened to the subject for participating in test according to test requirements document, screened altogether into group 35, it is final to guarantee to complete
It is more than 30 people.
2. subject visits for the first time, test explanation is carried out to subject, and sign informed consent form.
3. subject, which tests morning on the same day, cannot use skin care item.After having cleaned face with clear water, between constant temperature and humidity
Rest 30 minutes.After 30 minutes, forehead fat content is tested with Sebumeter.
4. carrying out operation instruction to subject after the completion of test, after subject listens to explanation, product is provided, subject is in
Use test specimen within continuous 4 weeks.Period, subject is according to the instruction of test after product is used in conjunction 2 weeks, 4 weeks laggard guilds time
It visits, 3. step carries out facial test according to step.
5. confirming at the end of to the usage amount of product when test starts.
(1) service life of test specimen
It is used in conjunction within 4 weeks and (still, allows the 2 days errors in front and back)
(2) test position is observed
Forehead
(3) test result statistical method
The effective example of subject
Whether table 1 uses example classification chart
2 sample usage amount of table decides whether using example classification chart
7. data statistical analysis method
Data statistics: data are counted using SPSS, normal distribution-test are carried out to test data, if test data is
Normal distribution, then it is for statistical analysis using the t method of inspection;If test data is Non-Gaussian Distribution, rank sum test side is used
Method statistical method for statistical analysis level of significance α < 0.050.
8. test result
Skin oil and fat
Compared with before use, after 2 weeks (14 days), skin oil and fat content has dropped 56, there is significant difference.
Compared with before use, after 4 weeks (28 days), skin oil and fat content has dropped 57, there is significant difference.
8.1 skin oil and fat contents
The situation of change of skin oil and fat is assessed, the increase of measured value means the increase of skin oil and fat content.
In Fig. 1: compared with * is indicated before use, there is the difference (p < 0.050) of conspicuousness.
The following table 1 indicates that 30 subjects put the descriptive statistic of forehead skin oil and fat content measurement value in different times
1 measured value descriptive statistic of table
Illustrate: test of normality progressive conspicuousness (bilateral) numerical value > 0.050, then the series data Normal Distribution
The following table 2 indicates that 30 subjects put the difference analysis knot of forehead skin oil and fat content measurement value in different times
Fruit
2 test statistics of table (rank sum test)
Significant difference: p < 0.050
There was no significant difference: p >=0.050
Skin adverse reaction:
During using sample, the skin that local erythema, papule, wheal, oedema or whole body occurs in 0 subject is bad anti-
It answers.
In conclusion a kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder of the invention end, contains natural India
The extra grease of le culm powder physical absorption skin, keeps skin refreshing, and long-time service can improve sebum secretion surplus, reach
Oil-control efficacy effect;The effect of three kinds of plant extraction essence of unique addition can reinforce product in product effect: (1) leaf of Mentha piperita
Extract is rich in dried peppermint leaf flavanones, can inhibit the release of inflammation transmitting molecule, soothes the skin allergic symptom (2) wing seed moringa seeds
The unique film forming of extract has lotus-effect, reduces pollutant attachment, protects cell, encroach on preventing from heavy metal, protects flesh
Skin;(3) hydrolysis phycocolloid can skin surface formed skin " protective film ", shielding isolation pollution particle, protect skin cell from
Pollution sources infringement;Free radical is removed, anti-inflammatory repairing effect is reached.The present invention is not only outer as a surfactant used in everyday
It is unique to see, and has effects that plant skin care oil-control, is protected using " bimodulus ", effectively obstructs harmful substance infringement, soothes the skin allergy
Symptom maintains and wakes up cell viability, promotes skin to rebuild, enhancing skin maintenance strength;It keeps Skin Cell vitality and coagulates
Poly- power.
Above-described is only preferred embodiments of the invention.It should be pointed out that for the ordinary skill of this field
For personnel, without departing from the principles of the present invention, it can also make several improvements and modification, this is also considered as of the invention
Protection scope.
Primary raw material table
Claims (2)
1. a kind of its weight fraction ratio of the composite plant oil-control bilayer surfactant at Han You le bamboo powder end are as follows:
A phase:
B phase
2. the composite plant oil-control bilayer surfactant at a kind of Han You le bamboo powder end according to claim 1, which is characterized in that its
Preparation method is according to the following steps:
1. deionized water is added in water phase jacketed pan, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate is added, mixing speed control exists
20-25 revs/min, 20-30min is stirred, sequentially adds EDETATE SODIUM, Xylitol-based glucoside/dehydration xylose under stirring
Alcohol/xylitol/glucose/water, parahydroxyacet-ophenone and niacinamide simultaneously dissolves in deionized water;It is sufficiently stirred at room temperature,
It is passed through steam in the collet of jacketed pan, 80-85 DEG C is heated under stirring, maintains 10min sterilizing, is to be vapored away when supplementary heating
Moisture can be added going from water for 2%-3% by formula;
2. Aqueous Phase Raw Material is added in emulsion pot by filter, stirring is opened, mixing speed control is at 20-25 revs/min, side
It stirs side and temperature is warming up to 85 DEG C or so.Under the conditions of 80-85 DEG C, sequentially adds glycerol and hydroxypropyl-trimethyl ammonium chloride is saturating
Bright matter acid, being sufficiently stirred, which is swollen it uniformly, prevents conglomeration, can carry out homogeneous, homogeneous speed control at 1500 revs/min or so,
Homogeneous 3-5 minutes, 20 minutes are kept the temperature, cooling system is opened and is cooled down;
3. being cooled to 35-40 DEG C, Chondrus crispus extract/tool is added away from helictite algae extract, leaf of Mentha piperita extract, hydrolysis
Phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, sodium chloride, boron sikicate aluminum calcium/
Earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 carry out homogeneous 3-5 minutes, homogeneous speed 1500-
2000 revs/min,;Mixing speed is controlled at 20-25 revs/min, is stirred 10 minutes, is mixed them thoroughly;
The type of cooling is that chilled water is passed through in the collet of emulsion pot, and side stirring, side is cooling, and the speed of homogeneous and time should be subject to
Strict control, in order to avoid excessive shear;Chondrus crispus extract/tool is added at a lower temperature away from helictite algae extract, peppery thin
Lotus Leafextract, hydrolysis phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, chlorine
Change sodium, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50, controls mixing speed
It 20-35 revs/min, stirs 10-15 minutes, to ensure its activity;
4. being aged and filling: it is filling with bottle placer after storage 1 day or 2 days, it needs to carry out product performance rating before filling, quality conjunction
It is carried out after lattice filling;It is needed when filling filling while stirring.
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