CN109276513A - A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end - Google Patents

A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end Download PDF

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Publication number
CN109276513A
CN109276513A CN201811189154.4A CN201811189154A CN109276513A CN 109276513 A CN109276513 A CN 109276513A CN 201811189154 A CN201811189154 A CN 201811189154A CN 109276513 A CN109276513 A CN 109276513A
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extract
skin
revs
added
filling
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辛建雄
林颖娴
陈军
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Nox Bellcow Cosmetics Co Ltd
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Nox Bellcow Cosmetics Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/03Liquid compositions with two or more distinct layers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/20Halogens; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25Silicon; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/29Titanium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/673Vitamin B group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9717Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

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Abstract

A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, by deionized water, EDETATE SODIUM, glycerol, 1, 3-propanediol, niacinamide, parahydroxyacet-ophenone, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate, hydroxypropyl-trimethyl ammonium chloride hyaluronic acid, Xylitol-based glucoside/anhydro xylitol/xylitol/glucose/water, hydrolyze phycocolloid, grape seed extract, Yin Du le culm powder, leaf of Mentha piperita extract, wing seed Moringa seed extract, Chondrus crispus extract/tool is away from helictite algae extract, sodium chloride, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 composition.The present invention is prepared by certain technique and is realized; utilize the extra sebum of natural Yin Du le culm powder physical absorption; salubrious skin; it is succinct to add a variety of natural plants, is formed skin " protective film ", barrier pollutes micronic dust; chelate harmful heavy metal; it is anti-oxidant to nourish tender skin with allergy-relieving, purify skin nocuousness absurd creature;It maintains and wakes up cell viability, promote skin to rebuild, enhancing skin maintenance strength;Keep Skin Cell vitality and cohesiveness.

Description

A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end
Technical field
The present invention relates to a kind of composite plant oil-control bilayer surfactant articles at Han You le bamboo powder end.
Background technique
Common single layer surfactant only has the function of moisturizing, and marketed bilayer surfactant adds the mineral such as kaolin or Cab-O-sil Source powder is used for a long time and is easy blocking pore, and skin water oil is unbalance, and skin is easily dark yellow.As PM2.5 value is exceeded, in air Pollution micronic dust be readily adsorbed in skin surface, cause skin metabolism circulation be affected, blackhead, pore can be made coarse and allergy Equal skin problems are more obvious.A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, interior-addition are a variety of natural Plant is succinct, soothes the skin allergic symptom, nourishes tender skin, purifies skin nocuousness absurd creature;Outside-hydrolysis phycocolloid and wing seed are peppery The wooden seed extract forms " protective film " in skin surface, using natural Zhi object Lai the oil of Yuan le bamboo fine powder physical absorption skin surface Rouge reduces the infringement of pollutant.Inside and outside dual protection, effectively resists air pollution, and pure and fresh skin enhances skin maintenance barrier.
Summary of the invention
The object of the present invention is to provide a kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, it has day Ran le bamboo powder physical absorption sebum;Various plants extract is added, energy allergy-relieving nourishes tender skin, purifies skin Harmful absurd creature;And form skin " protective film ", barrier pollute micronic dust the characteristics of.
The present invention is implemented as follows: a kind of its parts by weight of the composite plant oil-control bilayer surfactant at Han You le bamboo powder end Than are as follows:
A phase:
Deionized water 70.97-90.29, EDETATE SODIUM 0.03~0.1,
Glycerol 2~5,1,3-PD 5~8,
Niacinamide 0.5~3,
Parahydroxyacet-ophenone 0.2~0.3, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate 0.1~0.3,
Hydroxypropyl-trimethyl ammonium chloride hyaluronic acid 0.001~0.004,
Xylitol-based glucoside/anhydro xylitol/xylitol/glucose/water 0.3~0.7;
B phase
Hydrolysis phycocolloid 0.1~2, grape seed extract 0.1~0.5,
Yin Du le culm powder 0.5~1, leaf of Mentha piperita extract 0.5~1,
Wing seed Moringa seed extract 0.03~3,
Chondrus crispus extract/tool away from helictite algae extract 0.1~0.5,
Sodium chloride 0.3~0.6,
Boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide 0.02~0.05,
Phenoxyethanol 0.15~0.25, Sensiva SC50 0.1~0.2.
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, preparation method according to the following steps:
1. deionized water is added in water phase jacketed pan, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate, mixing speed control are added At 20-25 revs/min, 20-30min is stirred, EDETATE SODIUM, Xylitol-based glucoside/dehydration wood are sequentially added under stirring Sugar alcohol/xylitol/glucose/water, parahydroxyacet-ophenone and niacinamide simultaneously dissolves in deionized water;It is sufficiently stirred at room temperature, It is passed through steam in the collet of jacketed pan, 80-85 DEG C is heated under stirring, maintains 10min sterilizing, is vapored away when being supplementary heating Moisture, the going from water of 2%-3% can be added by formula;
2. Aqueous Phase Raw Material is added in emulsion pot by filter, stirring is opened, mixing speed is controlled at 20-25 revs/min Temperature is warming up to 85 DEG C or so while stirring by clock.Under the conditions of 80-85 DEG C, glycerol and Hydroxyproyl Trimethyl chlorine are sequentially added Change ammonium hyaluronic acid, being sufficiently stirred, which is swollen it uniformly, prevents conglomeration, can carry out homogeneous, homogeneous speed control is at 1500 revs/min Clock or so homogeneous 3-5 minutes, keeps the temperature 20 minutes, opens cooling system and is cooled down;
3. be cooled to 35-40 DEG C, be added Chondrus crispus extract/tool away from helictite algae extract, leaf of Mentha piperita extract, Hydrolyze phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, sodium chloride, borosilicic acid Aluminium calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 carries out homogeneous 3-5 minutes, homogeneous speed 1500-2000 revs/min;Mixing speed is controlled at 20-25 revs/min, is stirred 10 minutes, is mixed them thoroughly;
The type of cooling is that chilled water is passed through in the collet of emulsion pot, and side stirring, side is cooling, and the speed of homogeneous and time answer It is subject to strict control, in order to avoid excessive shear;At a lower temperature be added Chondrus crispus extract/tool away from helictite algae extract, Leaf of Mentha piperita extract, hydrolysis phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- the third two Alcohol, sodium chloride, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50, control stirring It 20-35 revs/min of speed, stirs 10-15 minutes, to ensure its activity;
4. being aged and filling: it is filling with bottle placer after storage 1 day or 2 days, it needs to carry out performance rating, matter to product before filling It is carried out after amount is qualified filling;It is needed when filling filling while stirring.
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder of the invention end, main component contain Yin Du le culm Powder, leaf of Mentha piperita extract, wing seed Moringa seed extract and hydrolysis phycocolloid;It must be shaken up before, Tian Ran le bamboo oil suction fine powder The extra grease of physical absorption skin keeps salubrious and increases the sliding feeling of skin silk simultaneously;Leaf of Mentha piperita extract is rich in simultaneously Dried peppermint leaf flavanones soothes the skin allergic symptom inside skin;Wing seed Moringa seed extract has lotus-effect, reduces dirty Object attachment is contaminated, cell is protected, preventing from heavy metal is encroached on, protects skin;Skin " protection can be formed in skin surface by hydrolyzing phycocolloid Film ", shielding isolation pollution particle, polyphenoils protect skin cell to encroach on from pollution sources to purify skin.
In conclusion the present invention has unique appearance characteristics, it is double-deck surfactant when standing, upper layer is faint yellow Bright aqua, lower layer are uniform powder, are shaken up before use as uniform pigment mixture, natural Yin Du le culm powder physics is utilized to inhale Attached extra sebum, salubrious skin add a variety of natural plants essences, have allergy-relieving, nourish tender skin, purify flesh Skin nocuousness absurd creature;Wing seed Moringa seed extract and hydrolysis phycocolloid form skin " protective film ", and barrier pollutes micronic dust, chelate harmful weight Metal purification skin maintains and wakes up cell viability, anti-oxidant to promote skin to rebuild, enhance skin maintenance strength;Keep skin Skin cell viability and cohesiveness.
Detailed description of the invention
Fig. 1 is the mean value that 30 subjects of the invention put forehead skin oil and fat content in different times.
Fig. 2 is that 30 subjects of the invention put forehead skin oil and fat changes of contents in different times.
Specific embodiment
The invention will be further described With reference to embodiment:
Embodiment 1
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, ingredients by weight portion rate:
A phase:
Deionized water 73.496, EDETATE SODIUM 0.1,
Glycerol 5,
1,3-PD 8,
Niacinamide 3,
Parahydroxyacet-ophenone 0.3,
Sodium metasilicate magnesium lithium/tetrasodium pyrophosphate 0.3,
Hydroxypropyl-trimethyl ammonium chloride hyaluronic acid 0.004,
Xylitol-based glucoside/anhydro xylitol/xylitol/glucose/water 0.7;
B phase
Phycocolloid 2 is hydrolyzed,
Grape seed extract 0.5,
Yin Du le culm powder 1,
Leaf of Mentha piperita extract 1,
Wing seed Moringa seed extract 3,
Chondrus crispus extract/tool away from helictite algae extract 0.5,
Sodium chloride 0.6,
Boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide 0.05,
Phenoxyethanol 0.25,
Sensiva SC50 0.2;
Preparation method is according to the following steps:
1. deionized water is added in water phase jacketed pan, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate, mixing speed control are added At 20-25 revs/min, 20-30min is stirred, EDETATE SODIUM, Xylitol-based glucoside/dehydration wood are sequentially added under stirring Sugar alcohol/xylitol/glucose/water, parahydroxyacet-ophenone and niacinamide simultaneously dissolves in deionized water;It is sufficiently stirred at room temperature, It is passed through steam in the collet of jacketed pan, 80-85 DEG C is heated under stirring, maintains 10min sterilizing, is vapored away when being supplementary heating Moisture, the going from water of 2%-3% can be added by formula;
2. Aqueous Phase Raw Material is added in emulsion pot by filter, stirring is opened, mixing speed is controlled at 20-25 revs/min Temperature is warming up to 85 DEG C or so while stirring by clock.Under the conditions of 80-85 DEG C, glycerol and Hydroxyproyl Trimethyl chlorine are sequentially added Change ammonium hyaluronic acid, being sufficiently stirred, which is swollen it uniformly, prevents conglomeration, can carry out homogeneous, homogeneous speed control is at 1500 revs/min Clock or so homogeneous 3-5 minutes, keeps the temperature 20 minutes, opens cooling system and is cooled down;
3. be cooled to 35-40 DEG C, be added Chondrus crispus extract/tool away from helictite algae extract, leaf of Mentha piperita extract, Hydrolyze phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, sodium chloride, borosilicic acid Aluminium calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 carries out homogeneous 3-5 minutes, homogeneous speed 1500-2000 revs/min;Mixing speed is controlled at 20-25 revs/min, is stirred 10 minutes, is mixed them thoroughly;
The type of cooling is that chilled water is passed through in the collet of emulsion pot, and side stirring, side is cooling, and the speed of homogeneous and time answer It is subject to strict control, in order to avoid excessive shear;At a lower temperature be added Chondrus crispus extract/tool away from helictite algae extract, Leaf of Mentha piperita extract, hydrolysis phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- the third two Alcohol, sodium chloride, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50, control stirring It 20-35 revs/min of speed, stirs 10-15 minutes, to ensure its activity;
4. being aged and filling: it is filling with bottle placer after storage 1 day or 2 days, it needs to carry out performance rating, matter to product before filling It is carried out after amount is qualified filling;It is needed when filling filling while stirring.
Embodiment 2
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, ingredients by weight portion rate:
A phase:
Deionized water 88.968,
EDETATE SODIUM 0.03,
Glycerol 3,
1,3-PD 5,
Niacinamide 0.5,
Parahydroxyacet-ophenone 0.2,
Sodium metasilicate magnesium lithium/tetrasodium pyrophosphate 0.1,
Hydroxypropyl-trimethyl ammonium chloride hyaluronic acid 0.002,
Xylitol-based glucoside/anhydro xylitol/xylitol/glucose/water 0.3;
B phase:
Phycocolloid 0.1 is hydrolyzed,
Grape seed extract 0.1,
Yin Du le culm powder 0.5,
Leaf of Mentha piperita extract 0.5,
Wing seed Moringa seed extract 0.03,
Chondrus crispus extract/tool away from helictite algae extract 0.1,
Sodium chloride 0.3,
Boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide 0.02
Phenoxyethanol 0.15,
Sensiva SC50 0.1;
Preparation method is according to the following steps:
1. deionized water is added in water phase jacketed pan, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate, mixing speed control are added At 20-25 revs/min, 20-30min is stirred, EDETATE SODIUM, Xylitol-based glucoside/dehydration wood are sequentially added under stirring Sugar alcohol/xylitol/glucose/water, parahydroxyacet-ophenone and niacinamide simultaneously dissolves in deionized water;It is sufficiently stirred at room temperature, It is passed through steam in the collet of jacketed pan, 80-85 DEG C is heated under stirring, maintains 10min sterilizing, is vapored away when being supplementary heating Moisture, the going from water of 2%-3% can be added by formula;
2. Aqueous Phase Raw Material is added in emulsion pot by filter, stirring is opened, mixing speed is controlled at 20-25 revs/min Temperature is warming up to 85 DEG C or so while stirring by clock.Under the conditions of 80-85 DEG C, glycerol and Hydroxyproyl Trimethyl chlorine are sequentially added Change ammonium hyaluronic acid, being sufficiently stirred, which is swollen it uniformly, prevents conglomeration, can carry out homogeneous, homogeneous speed control is at 1500 revs/min Clock or so homogeneous 3-5 minutes, keeps the temperature 20 minutes, opens cooling system and is cooled down;
3. be cooled to 35-40 DEG C, be added Chondrus crispus extract/tool away from helictite algae extract, leaf of Mentha piperita extract, Hydrolyze phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, sodium chloride, borosilicic acid Aluminium calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 carries out homogeneous 3-5 minutes, homogeneous speed 1500-2000 revs/min;Mixing speed is controlled at 20-25 revs/min, is stirred 10 minutes, is mixed them thoroughly;
The type of cooling is that chilled water is passed through in the collet of emulsion pot, and side stirring, side is cooling, and the speed of homogeneous and time answer It is subject to strict control, in order to avoid excessive shear;At a lower temperature be added Chondrus crispus extract/tool away from helictite algae extract, Leaf of Mentha piperita extract, hydrolysis phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- the third two Alcohol, sodium chloride, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50, control stirring It 20-35 revs/min of speed, stirs 10-15 minutes, to ensure its activity;
4. being aged and filling: it is filling with bottle placer after storage 1 day or 2 days, it needs to carry out performance rating, matter to product before filling It is carried out after amount is qualified filling;It is needed when filling filling while stirring.
Embodiment 3
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, ingredients by weight portion rate:
A phase:
Deionized water 82.307,
EDETATE SODIUM 0.05,
Glycerol 4,
1,3-PD 7,
Niacinamide 2,
Parahydroxyacet-ophenone 0.25,
Sodium metasilicate magnesium lithium/tetrasodium pyrophosphate 0.3,
Hydroxypropyl-trimethyl ammonium chloride hyaluronic acid 0.003,
Xylitol-based glucoside/anhydro xylitol/xylitol/glucose/water 0.4;
B phase:
Phycocolloid 0.3 is hydrolyzed,
Grape seed extract 0.3,
Yin Du le culm powder 0.8,
Leaf of Mentha piperita extract 0.8,
Wing seed Moringa seed extract 0.5,
Chondrus crispus extract/tool away from helictite algae extract 0.2,
Sodium chloride 0.4,
Boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide 0.04,
Phenoxyethanol 0.2,
Sensiva SC50 0.15;
Preparation method is according to the following steps:
1. deionized water is added in water phase jacketed pan, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate, mixing speed control are added At 20-25 revs/min, 20-30min is stirred, EDETATE SODIUM, Xylitol-based glucoside/dehydration wood are sequentially added under stirring Sugar alcohol/xylitol/glucose/water, parahydroxyacet-ophenone and niacinamide simultaneously dissolves in deionized water;It is sufficiently stirred at room temperature, It is passed through steam in the collet of jacketed pan, 80-85 DEG C is heated under stirring, maintains 10min sterilizing, is vapored away when being supplementary heating Moisture, the going from water of 2%-3% can be added by formula;
2. Aqueous Phase Raw Material is added in emulsion pot by filter, stirring is opened, mixing speed is controlled at 20-25 revs/min Temperature is warming up to 85 DEG C or so while stirring by clock.Under the conditions of 80-85 DEG C, glycerol and Hydroxyproyl Trimethyl chlorine are sequentially added Change ammonium hyaluronic acid, being sufficiently stirred, which is swollen it uniformly, prevents conglomeration, can carry out homogeneous, homogeneous speed control is at 1500 revs/min Clock or so homogeneous 3-5 minutes, keeps the temperature 20 minutes, opens cooling system and is cooled down;
3. be cooled to 35-40 DEG C, be added Chondrus crispus extract/tool away from helictite algae extract, leaf of Mentha piperita extract, Hydrolyze phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, sodium chloride, borosilicic acid Aluminium calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 carries out homogeneous 3-5 minutes, homogeneous speed 1500-2000 revs/min;Mixing speed is controlled at 20-25 revs/min, is stirred 10 minutes, is mixed them thoroughly;
The type of cooling is that chilled water is passed through in the collet of emulsion pot, and side stirring, side is cooling, and the speed of homogeneous and time answer It is subject to strict control, in order to avoid excessive shear;At a lower temperature be added Chondrus crispus extract/tool away from helictite algae extract, Leaf of Mentha piperita extract, hydrolysis phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- the third two Alcohol, sodium chloride, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50, control stirring It 20-35 revs/min of speed, stirs 10-15 minutes, to ensure its activity;
4. being aged and filling: it is filling with bottle placer after storage 1 day or 2 days, it needs to carry out performance rating, matter to product before filling It is carried out after amount is qualified filling;It is needed when filling filling while stirring.
Long-acting oil control effect scheme of this product implements and data statistics:
(1) 1. test purpose
By 30 people a set product is used in conjunction 4 weeks in open trial, the method for instrument test, cross-reference, and verifying product is long-acting The effect of oil-control.
2. test sample and application method
A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end, first shakes up this product using preceding, takes appropriate refreshing Skin water wipes face.
3. subject
3.1 all subjects receive oral and papery informed consent according to local statues, regulation.Informed consent solution The property, purpose and the potential risk for participating in research of research have been released, and has emphasized to participate in the voluntary of test, subject can be at any time It withdraws from the study in any reason.All informed consent signatures must be carried out before the study began.
3.2 inclusion criteria
1. Chinese women,
2. the age 20-55 years old;
3. oiliness or semi-oily skin;
4. subject copes with common cosmetics not allergy, other clinical researches are not participated within nearly three months;
5. during test, forbidding using other skin-protection products or other products for influencing test, daily necessities and reality in test What is used before testing is consistent, forbids replacing.
3.3 target number of cases
Selected 35 people of Eligible subjects, it is ensured that be finally completed 30 people.
4. test equipment
4.1 skin oil and fat tester Sebumeter (Courage&Khazaka, Germany).
4.2 balances, sensibility reciprocal 0.01g (English weighing apparatus).
5. testing environment
Environmental requirement: temperature: 21.0 DEG C ± 1.0 DEG C;Humidity: 50% ± 5%.
6. experiment process
Period: 4 weeks are long-acting:
1. being screened to the subject for participating in test according to test requirements document, screened altogether into group 35, it is final to guarantee to complete It is more than 30 people.
2. subject visits for the first time, test explanation is carried out to subject, and sign informed consent form.
3. subject, which tests morning on the same day, cannot use skin care item.After having cleaned face with clear water, between constant temperature and humidity Rest 30 minutes.After 30 minutes, forehead fat content is tested with Sebumeter.
4. carrying out operation instruction to subject after the completion of test, after subject listens to explanation, product is provided, subject is in Use test specimen within continuous 4 weeks.Period, subject is according to the instruction of test after product is used in conjunction 2 weeks, 4 weeks laggard guilds time It visits, 3. step carries out facial test according to step.
5. confirming at the end of to the usage amount of product when test starts.
(1) service life of test specimen
It is used in conjunction within 4 weeks and (still, allows the 2 days errors in front and back)
(2) test position is observed
Forehead
(3) test result statistical method
The effective example of subject
Whether table 1 uses example classification chart
2 sample usage amount of table decides whether using example classification chart
7. data statistical analysis method
Data statistics: data are counted using SPSS, normal distribution-test are carried out to test data, if test data is Normal distribution, then it is for statistical analysis using the t method of inspection;If test data is Non-Gaussian Distribution, rank sum test side is used Method statistical method for statistical analysis level of significance α < 0.050.
8. test result
Skin oil and fat
Compared with before use, after 2 weeks (14 days), skin oil and fat content has dropped 56, there is significant difference.
Compared with before use, after 4 weeks (28 days), skin oil and fat content has dropped 57, there is significant difference.
8.1 skin oil and fat contents
The situation of change of skin oil and fat is assessed, the increase of measured value means the increase of skin oil and fat content.
In Fig. 1: compared with * is indicated before use, there is the difference (p < 0.050) of conspicuousness.
The following table 1 indicates that 30 subjects put the descriptive statistic of forehead skin oil and fat content measurement value in different times
1 measured value descriptive statistic of table
Illustrate: test of normality progressive conspicuousness (bilateral) numerical value > 0.050, then the series data Normal Distribution
The following table 2 indicates that 30 subjects put the difference analysis knot of forehead skin oil and fat content measurement value in different times Fruit
2 test statistics of table (rank sum test)
Significant difference: p < 0.050
There was no significant difference: p >=0.050
Skin adverse reaction:
During using sample, the skin that local erythema, papule, wheal, oedema or whole body occurs in 0 subject is bad anti- It answers.
In conclusion a kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder of the invention end, contains natural India The extra grease of le culm powder physical absorption skin, keeps skin refreshing, and long-time service can improve sebum secretion surplus, reach Oil-control efficacy effect;The effect of three kinds of plant extraction essence of unique addition can reinforce product in product effect: (1) leaf of Mentha piperita Extract is rich in dried peppermint leaf flavanones, can inhibit the release of inflammation transmitting molecule, soothes the skin allergic symptom (2) wing seed moringa seeds The unique film forming of extract has lotus-effect, reduces pollutant attachment, protects cell, encroach on preventing from heavy metal, protects flesh Skin;(3) hydrolysis phycocolloid can skin surface formed skin " protective film ", shielding isolation pollution particle, protect skin cell from Pollution sources infringement;Free radical is removed, anti-inflammatory repairing effect is reached.The present invention is not only outer as a surfactant used in everyday It is unique to see, and has effects that plant skin care oil-control, is protected using " bimodulus ", effectively obstructs harmful substance infringement, soothes the skin allergy Symptom maintains and wakes up cell viability, promotes skin to rebuild, enhancing skin maintenance strength;It keeps Skin Cell vitality and coagulates Poly- power.
Above-described is only preferred embodiments of the invention.It should be pointed out that for the ordinary skill of this field For personnel, without departing from the principles of the present invention, it can also make several improvements and modification, this is also considered as of the invention Protection scope.
Primary raw material table

Claims (2)

1. a kind of its weight fraction ratio of the composite plant oil-control bilayer surfactant at Han You le bamboo powder end are as follows:
A phase:
B phase
2. the composite plant oil-control bilayer surfactant at a kind of Han You le bamboo powder end according to claim 1, which is characterized in that its Preparation method is according to the following steps:
1. deionized water is added in water phase jacketed pan, sodium metasilicate magnesium lithium/tetrasodium pyrophosphate is added, mixing speed control exists 20-25 revs/min, 20-30min is stirred, sequentially adds EDETATE SODIUM, Xylitol-based glucoside/dehydration xylose under stirring Alcohol/xylitol/glucose/water, parahydroxyacet-ophenone and niacinamide simultaneously dissolves in deionized water;It is sufficiently stirred at room temperature, It is passed through steam in the collet of jacketed pan, 80-85 DEG C is heated under stirring, maintains 10min sterilizing, is to be vapored away when supplementary heating Moisture can be added going from water for 2%-3% by formula;
2. Aqueous Phase Raw Material is added in emulsion pot by filter, stirring is opened, mixing speed control is at 20-25 revs/min, side It stirs side and temperature is warming up to 85 DEG C or so.Under the conditions of 80-85 DEG C, sequentially adds glycerol and hydroxypropyl-trimethyl ammonium chloride is saturating Bright matter acid, being sufficiently stirred, which is swollen it uniformly, prevents conglomeration, can carry out homogeneous, homogeneous speed control at 1500 revs/min or so, Homogeneous 3-5 minutes, 20 minutes are kept the temperature, cooling system is opened and is cooled down;
3. being cooled to 35-40 DEG C, Chondrus crispus extract/tool is added away from helictite algae extract, leaf of Mentha piperita extract, hydrolysis Phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, sodium chloride, boron sikicate aluminum calcium/ Earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50 carry out homogeneous 3-5 minutes, homogeneous speed 1500- 2000 revs/min,;Mixing speed is controlled at 20-25 revs/min, is stirred 10 minutes, is mixed them thoroughly;
The type of cooling is that chilled water is passed through in the collet of emulsion pot, and side stirring, side is cooling, and the speed of homogeneous and time should be subject to Strict control, in order to avoid excessive shear;Chondrus crispus extract/tool is added at a lower temperature away from helictite algae extract, peppery thin Lotus Leafextract, hydrolysis phycocolloid, grape seed extract, wing seed Moringa seed extract, print degree le culm powder, 1,3- propylene glycol, chlorine Change sodium, boron sikicate aluminum calcium/earth silicon/titanic oxide/tin oxide, Phenoxyethanol and Sensiva SC50, controls mixing speed It 20-35 revs/min, stirs 10-15 minutes, to ensure its activity;
4. being aged and filling: it is filling with bottle placer after storage 1 day or 2 days, it needs to carry out product performance rating before filling, quality conjunction It is carried out after lattice filling;It is needed when filling filling while stirring.
CN201811189154.4A 2018-10-12 2018-10-12 A kind of composite plant oil-control bilayer surfactant at Han You le bamboo powder end Pending CN109276513A (en)

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CN112156038A (en) * 2020-11-10 2021-01-01 广州环亚化妆品科技有限公司 Composition with instant and long-acting oil control and moisture retention functions and preparation method and application thereof
CN112842922A (en) * 2021-02-05 2021-05-28 东晟源研究院(广州)有限公司 Formula and preparation method of water-powder double-layer oil control astringent for sensitive muscles
CN113350204A (en) * 2021-06-08 2021-09-07 诺斯贝尔化妆品股份有限公司 Physical and chemical combined oil-controlling and soothing shaking toner and preparation method thereof
CN114364362A (en) * 2019-09-11 2022-04-15 马扬化学产品工业有限公司 Natural composition of organosilicon substitute, preparation method and application thereof
CN115245478A (en) * 2021-04-28 2022-10-28 广州市索柔生物科技有限公司 Oil-control lasting BB cream
CN115634185A (en) * 2022-10-31 2023-01-24 苏州安特化妆品股份有限公司 Long-acting make-up-holding oil-controlling plant powder and preparation process thereof
CN115645338A (en) * 2022-10-10 2023-01-31 广州诗妃生物科技有限公司 Double-layer nano-gold negative ion oil control water and preparation method thereof
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CN110051587A (en) * 2019-05-04 2019-07-26 广州市爱百伊生物技术有限公司 A kind of preparation method and application of the anti-apolexis composition containing a variety of sodium hyaluronates
CN114364362A (en) * 2019-09-11 2022-04-15 马扬化学产品工业有限公司 Natural composition of organosilicon substitute, preparation method and application thereof
CN112156038A (en) * 2020-11-10 2021-01-01 广州环亚化妆品科技有限公司 Composition with instant and long-acting oil control and moisture retention functions and preparation method and application thereof
CN112842922A (en) * 2021-02-05 2021-05-28 东晟源研究院(广州)有限公司 Formula and preparation method of water-powder double-layer oil control astringent for sensitive muscles
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CN115634185A (en) * 2022-10-31 2023-01-24 苏州安特化妆品股份有限公司 Long-acting make-up-holding oil-controlling plant powder and preparation process thereof
CN116139064A (en) * 2023-04-17 2023-05-23 广州集妍化妆品科技有限公司 Sun-proof synergistic composition, application thereof and cosmetics
CN116139064B (en) * 2023-04-17 2023-07-14 广州集妍化妆品科技有限公司 Sun-proof synergistic composition, application thereof and cosmetics

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