CN104983656B - A kind of CC frost and preparation method thereof - Google Patents
A kind of CC frost and preparation method thereof Download PDFInfo
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- CN104983656B CN104983656B CN201510347142.XA CN201510347142A CN104983656B CN 104983656 B CN104983656 B CN 104983656B CN 201510347142 A CN201510347142 A CN 201510347142A CN 104983656 B CN104983656 B CN 104983656B
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Abstract
The present invention provides a kind of CC frost and preparation method thereof, it includes following components: water, isononyl isononanoate, glycerol, butanediol, PEG/PPG 20/15 polydimethylsiloxane, polydimethylsiloxane, titanium dioxide, Muscovitum, silica flour, cetyl PEG/PPG 10/1 polydimethylsiloxane, magnesium sulfate, polymethyl methacrylate, distearyl dimethylammonium Strese Hofmann's hectorite., Limax secretions, leaf of Herb Gynostemmae Pentaphylli extract, dulse elite, Herba Centellae extract, ivory white toner, PEG 10 polydimethylsiloxane, methyl hydroxybenzoate, propyl hydroxybenzoate, EDETATE SODIUM and essence.The right safety of CC cold weather of the present invention, clearly pastes skin after using, repair skin comprehensively, revise the colour of skin, whitening skin and preserving moisture, sun-proof isolation resultant effect good.
Description
Technical field
The invention belongs to cosmetic technical field, be specifically related to a kind of CC frost and preparation method thereof.
Background technology
CC frost (CC.CREAM) is the abbreviation of English COLOR.CONTROL.CREAM, and Chinese is the full effects of color regulation and control
Repair Rong Shuan.Be initially by first big skin care item Co., Ltd. of Japan be after revision skin uneven designed by, especially carry out
The people of skin surface injury and laser surgery uses, therefore is referred to as " color regulation and control frost ", is provided that impaired more serious skin is protected
Protect and maintenance effect, and have the feature visually aligning the colour of skin concurrently.From the beginning of day this area, enter the medical cosmetology of Korea S afterwards
With makeups market cause blockbuster, rapidly become, at the short frost of CC in two years, single product that Korea S's girl's staff is indispensable, its
Product, while revising the colour of skin, also gives skin whitening skin and preserving moisture and isolates the injury that skin is caused by outside contamination, relative to
Screening flaw effect that BB frost is pursued is compared, and CC frost more payes attention to sensitivity skin, the care maintenance of subhealth state skin, the safest
Gentleness, therefore CC frost is increasingly pursued by people and is become fashion trend.
Chinese patent application CN 103735444A discloses a kind of Multifunctional CC cream, and this CC frost includes silicone oil emulsification agent, prevents
Shine agent, polyalcohols wetting agent, EDETATE SODIUM, phenoxyethanol, Herba portulacae extract, aminoacids complex, fermented soybean extract,
Deionized water, oils and fats, hydrophobic pigment, electrolyte, pentanediol, essence, Flos Narcissi chinensis extract, hamamelis extract and collagen egg
White anti-wrinkle agent.Though this CC frost is salubrious without greasy feeling, use, hide the flaw effective, but the effects such as its moisturizing, bright color, persistency
It need to improve.
Chinese patent application CN 103655234A discloses a kind of moisture type CC cream composition, and this CC cream composition includes
Oils and fats, emulsifying agent, opaque, stabilizer, polyhydric alcohol, colloid raw material and deionized water.The water outlet of this CC cream composition, moistening effect
Good, but it hides the effect such as the flaw, whitening and need to improve.
Chinese patent application CN 104434719A discloses a kind of Limax secretions filtrate and is promoting color make-up series products patch skin
Application in performance.This patent research finds that adding Limax secretions filtrate in color make-up series products is remarkably improved color make-up class product
The patch skin effect of product.Pharmacology and clinical research show, Herb Gynostemmae Pentaphylli is almost non-toxic, have no side effect, and have anticancer, blood fat reducing, anti-ageing
Always acting on, can strengthen body immune function, the side effect etc. of preventing and treating glucocorticoid, therefore Herb Gynostemmae Pentaphylli extract is generally as medicine
Product, health product use.Chinese patent application CN 103191172A discloses Herb Gynostemmae Pentaphylli extract and is preparing skin anti-light aging
Application in cosmetics.Chinese patent application CN 102871924A discloses the Herb Gynostemmae Pentaphylli extract application as wetting agent.In
State patent application CN 104523536A discloses a kind of whitening skin and preserving moisture cosmetics containing Herba Centellae extract.But not yet send out
Existing Limax secretions, Herb Gynostemmae Pentaphylli extract, Herba Centellae extract and the compositions of dulse elite and said composition are at CC frost
In application.
It is intended to just can solve the problem of all skin with a bottle product for current most people, and the most existing
The CC frost correction colour of skin, whitening skin and preserving moisture, sun-proof isolation resultant effect poor, accordingly, it would be desirable to a kind of CC frost solves these problems
And reach good using effect.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of CC frost, its natural safety, clearly pastes skin, Quan Mianxiu after using
Multiple skin, revise the colour of skin, whitening skin and preserving moisture, sun-proof isolation resultant effect good.
For solving above-mentioned technical problem, technical scheme is as follows:
A kind of CC frost, including following components: the poly-diformazan of water, isononyl isononanoate, glycerol, butanediol, PEG/PPG-20/15
Radical siloxane, polydimethylsiloxane, titanium dioxide, Muscovitum, silica flour, cetyl PEG/PPG-10/1 polydimethylsiloxane,
Magnesium sulfate, polymethyl methacrylate, distearyl dimethylammonium Strese Hofmann's hectorite., Limax secretions, leaf of Herb Gynostemmae Pentaphylli extract, dulse
Elite, Herba Centellae extract, ivory white toner, KF6017, methyl hydroxybenzoate, propyl hydroxybenzoate, EDETATE SODIUM
And essence.
Further, described CC frost includes the component of following percentage by weight meter: water 50 ~ 65%, isononyl isononanoate 5 ~
8%, glycerol 5 ~ 8%, butanediol 5 ~ 8%, PEG/PPG-20/15 polydimethylsiloxane 3 ~ 6%, polydimethylsiloxane 2 ~ 5%, two
Titanium oxide 2 ~ 4%, Muscovitum 2 ~ 5%, silica flour 1 ~ 3%, cetyl PEG/PPG-10/1 polydimethylsiloxane 0.5 ~ 2%, magnesium sulfate 0.8
~ 2%, polymethyl methacrylate 0.5 ~ 2%, distearyl dimethylammonium Strese Hofmann's hectorite. 0.5 ~ 2%, Limax secretions 0.3 ~ 1%, Herb Gynostemmae Pentaphylli
Leaf extract 0.3 ~ 1%, dulse elite 0.3 ~ 1%, Herba Centellae extract 0.3 ~ 1%, ivory white toner 0.3 ~ 1%, PEG-10 are poly-
Dimethyl siloxane 0.3 ~ 1%, methyl hydroxybenzoate 0.1 ~ 0.5%, propyl hydroxybenzoate 0.1 ~ 0.5%, EDETATE SODIUM 0.01 ~ 0.03% and essence
0.01~0.1%。
As the preferred embodiment of the present invention, described CC frost is made up of the component of following percentage by weight meter: water
59.42%, isononyl isononanoate 6%, glycerol 6%, butanediol 6%, PEG/PPG-20/15 polydimethylsiloxane 4%, poly dimethyl
Siloxanes 3%, titanium dioxide 3%, Muscovitum 3%, silica flour 2%, cetyl PEG/PPG-10/1 polydimethylsiloxane 1%, magnesium sulfate
1.2%, polymethyl methacrylate 1%, distearyl dimethylammonium Strese Hofmann's hectorite. 1%, Limax secretions 0.5%, leaf of Herb Gynostemmae Pentaphylli extract
0.6%, dulse elite 0.5%, Herba Centellae extract 0.5%, ivory white toner 0.4%, KF6017 0.5%,
Methyl hydroxybenzoate 0.2%, propyl hydroxybenzoate 0.1%, EDETATE SODIUM 0.02% and essence 0.06%.
PEG/PPG-20/15 polydimethylsiloxane described in technical solution of the present invention, polydimethylsiloxane, cetyl
PEG/PPG-10/1 polydimethylsiloxane, distearyl dimethylammonium Strese Hofmann's hectorite. and KF6017 are as emulsifying
Agent；Described isononyl isononanoate and magnesium sulfate are as stabilizer；Described glycerol and butanediol are as wetting agent；Described methyl hydroxybenzoate
With propyl hydroxybenzoate as anticorrosion and bactericidal agent；Described polymethyl methacrylate is more moist by product, spreadability, pro-skin sense
More preferably, scribble effect is the most docile；Described ivory white toner is more stable by product colour, makeup is more natural.
Described titanium dioxide is the titanium dioxide after silicon processes, radius 100 nanometer, good dispersion；Can more preferable uniform skin
Color, easy to apply, do not take off adornment, covering facial defect more at ease, light and enlarged pores, more can intelligence mix colours, allows skin as the most ceramic
As moist；Effective Modifying Capability, the light source that refraction is extraneous, reach soft brilliant white light sensation, overall bright color.
Described silica flour can the painting of improving product and the sliding skinfeel of dry and comfortable silk, increase matt effect, strengthen light scattering
And soft focus (atomization) effect, make dressing the brightest.
Described Limax secretions is containing natural collagen protein, elastin, allantoin, Portugal (grape) alduronic acid, the life of multiple dimension
Element etc..Skin deep layer is brought in nutrition contained by these compositions into, has and can repair skin, increases the nutrition of skin, locks water moisturizing, tender
Skin whitening, print of dispelling reparation, anti-ageing multi-efficiency of waiting for a long time.
Described Herb Gynostemmae Pentaphylli extract can improve the function of the aquaporin in Skin Cell, promotes to produce aquaporin egg
In vain, import moisture to cell interior, bring skin water profit from cell interior.Cell is moistened, and skin also can become water therewith
Profit.
Described dulse elite rich in sargassum thunbergii polyphenol, carotenoid, tocopherol, polysaccharide, polysaccharide class, required and non-must
Need gal4 amino acid, skin renewal, collagen protein synthesis can be promoted, there is the effect such as whitening, moisturizing.
Described Herba Centellae extract can promote collagen protein synthesis, promotes the secretion of mucopolysaccharide, increases the water conservation degree of skin,
Activation updates Skin Cell, makes skin releive, promotes and have reflecting feel；It also has the activation of fibroblast gene simultaneously
Effect, can strengthen the vigor of skin basal cell, keeps elasticity of skin and consolidation sense, smooth face fine wrinkles.
Described Limax secretions, Herb Gynostemmae Pentaphylli extract, dulse elite and Herba Centellae extract are compounding, in conjunction with emulsifying agent
(PEG/PPG-20/15 polydimethylsiloxane etc.), stabilizer (isononyl isononanoate etc.), wetting agent (glycerol and butanediol),
The basic materials such as opaque (titanium dioxide, Muscovitum and silica flour etc.) obtain CC of the present invention frost, and each component is worked in coordination with, and reach CC of the present invention frost
Clearly paste skin after using, there is no a greasy feeling, waterproof antiperspirant, persistently fix, and it is effective to hide the flaw, bright color, the tender profit of skin beauty water
Pool, life-time service can whitening, revise the colour of skin, repair the purposes such as face microgroove.
Present invention also offers the preparation method of above-mentioned CC frost, have and comprise the following steps:
(1) by polydimethylsiloxane, isononyl isononanoate, titanium dioxide, Muscovitum, silica flour, polymethyl methacrylate,
Distearyl dimethylammonium Strese Hofmann's hectorite. and ivory white toner add in agitated kettle, and stirring homogenizing, to without granule, obtains material one；
(2) by material one and PEG/PPG-20/15 polydimethylsiloxane, KF6017, oxybenzene first
Ester, propyl hydroxybenzoate and the mixing of cetyl PEG/PPG-10/1 polydimethylsiloxane add in oil phase pot, are heated to 75 ~ 85 DEG C,
Make it dissolve completely, obtain material two, be incubated standby；
(3) water, glycerol, butanediol, magnesium sulfate and EDETATE SODIUM are added in aqueous phase pot, be heated to 80 ~ 90 DEG C, be incubated 25
~ 35 minutes, obtain material three, be incubated standby；
(4) it is transferred to be pre-heated in the agitated kettle of 80 ~ 85 DEG C by material two and material three, stirs 10 ~ 15 minutes, homogenizing
Start cooling after 5 ~ 10 minutes, when temperature is down to 45 DEG C, adds Limax secretions, leaf of Herb Gynostemmae Pentaphylli extract, dulse elite, amass
Snow grass extract and essence, stir and i.e. obtain CC frost.
Further, the mixing speed of described stirring is 40 ~ 50 revs/min.
Therefore, relative with prior art, present invention have an advantage that
(1) CC frost quality of the present invention is frivolous ventilative, and one brush i.e. combines together with skin, clearly pastes skin, does not has greasy feeling, anti-
Water antiperspirant, persistently fixing, and it is effective to hide the flaw, bright color, skin beauty water is tender moist, and sun-proof isolation has moistening effect simultaneously；
(2) CC frost of the present invention contains Limax secretions, leaf of Herb Gynostemmae Pentaphylli extract, dulse elite and Herba Centellae extract etc.
Natural animal-plant elite, works in coordination with and gos deep at the bottom of flesh while immediately hiding the flaw, bright color, reaches to desalinate mottle melanin, whitening, repaiies
The positive colour of skin, repairs the purposes such as face's microgroove；
(3) each component of CC of the present invention frost is worked in coordination with, and revises the resultant effects such as the colour of skin, whitening skin and preserving moisture, sun-proof isolation good, and safety
Non-stimulated, the preparation technology of CC the most of the present invention frost is simple, and condition is easily-controllable, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following example.?
In the scope of the present invention or without departing from present disclosure, spirit and scope, CC frost of the present invention is carried out suitably
Improve, replace the component that effect is identical, will become apparent to those skilled in the art that they are considered as being included in
Within the scope of the present invention.
In the embodiment of the present invention 1 ~ 3 and comparative example 1 ~ 3, producer and the article No. of constituent part are as follows:
Embodiment 1, CC of the present invention frost and preparation thereof
Formula: by weight percentage, water 59.42%, isononyl isononanoate 6%, glycerol 6%, butanediol 6%, PEG/PPG-
20/15 polydimethylsiloxane 4%, polydimethylsiloxane 3%, titanium dioxide 3%, Muscovitum 3%, silica flour 2%, cetyl PEG/
PPG-10/1 polydimethylsiloxane 1%, magnesium sulfate 1.2%, polymethyl methacrylate 1%, distearyl dimethylammonium Strese Hofmann's hectorite.
1%, Limax secretions 0.5%, leaf of Herb Gynostemmae Pentaphylli extract 0.6%, dulse elite 0.5%, Herba Centellae extract 0.5%, ivory buff
Powder 0.4%, KF6017 0.5%, methyl hydroxybenzoate 0.2%, propyl hydroxybenzoate 0.1%, EDETATE SODIUM 0.02% and essence
0.06%。
Preparation: (1) is by polydimethylsiloxane, isononyl isononanoate, titanium dioxide, Muscovitum, silica flour, polymethylacrylic acid
Methyl ester, distearyl dimethylammonium Strese Hofmann's hectorite. and ivory white toner add in agitated kettle, and stirring homogenizing, to without granule, obtains material
One；
(2) by material one and PEG/PPG-20/15 polydimethylsiloxane, KF6017, oxybenzene first
Ester, propyl hydroxybenzoate and the mixing of cetyl PEG/PPG-10/1 polydimethylsiloxane add in oil phase pot, are heated to 80 DEG C so that it is
Dissolve completely, obtain material two, be incubated standby；
(3) water, glycerol, butanediol, magnesium sulfate and EDETATE SODIUM are added in aqueous phase pot, be heated to 85 DEG C, be incubated 30 points
Clock, obtains material three, is incubated standby；
(4) it is transferred to be pre-heated in the agitated kettle of 85 DEG C by material two and material three, stirs 10 minutes, homogenizing 8 minutes
After start cooling, when temperature is down to 45 DEG C, add Limax secretions, leaf of Herb Gynostemmae Pentaphylli extract, dulse elite, Herba Centellae extract
Thing and essence, stir and i.e. obtain CC frost.
The mixing speed of above-mentioned stirring is 45 revs/min.
Embodiment 2, CC of the present invention frost and preparation thereof
Formula: by weight percentage, water 54.89%, isononyl isononanoate 5%, glycerol 8%, butanediol 5%, PEG/PPG-
20/15 polydimethylsiloxane 3%, polydimethylsiloxane 5%, titanium dioxide 2%, Muscovitum 5%, silica flour 1%, cetyl PEG/
PPG-10/1 polydimethylsiloxane 2%, magnesium sulfate 2%, polymethyl methacrylate 0.5%, distearyl dimethylammonium Strese Hofmann's hectorite.
2%, Limax secretions 1%, leaf of Herb Gynostemmae Pentaphylli extract 0.3%, dulse elite 1%, Herba Centellae extract 0.3%, ivory white toner
0.3%, KF6017 1%, methyl hydroxybenzoate 0.1%, propyl hydroxybenzoate 0.5%, EDETATE SODIUM 0.01% and essence
0.1%。
Preparation: (1) is by polydimethylsiloxane, isononyl isononanoate, titanium dioxide, Muscovitum, silica flour, polymethylacrylic acid
Methyl ester, distearyl dimethylammonium Strese Hofmann's hectorite. and ivory white toner add in agitated kettle, and stirring homogenizing, to without granule, obtains material
One；
(2) by material one and PEG/PPG-20/15 polydimethylsiloxane, KF6017, oxybenzene first
Ester, propyl hydroxybenzoate and the mixing of cetyl PEG/PPG-10/1 polydimethylsiloxane add in oil phase pot, are heated to 75 DEG C so that it is
Dissolve completely, obtain material two, be incubated standby；
(3) water, glycerol, butanediol, magnesium sulfate and EDETATE SODIUM are added in aqueous phase pot, be heated to 80 DEG C, be incubated 35 points
Clock, obtains material three, is incubated standby；
(4) it is transferred to be pre-heated in the agitated kettle of 80 DEG C by material two and material three, stirs 15 minutes, homogenizing 5 minutes
After start cooling, when temperature is down to 45 DEG C, add Limax secretions, leaf of Herb Gynostemmae Pentaphylli extract, dulse elite, Herba Centellae extract
Thing and essence, stir and i.e. obtain CC frost.
The mixing speed of above-mentioned stirring is 40 revs/min.
Embodiment 3, CC of the present invention frost and preparation thereof
Formula: by weight percentage, water 53.64%, isononyl isononanoate 8%, glycerol 5%, butanediol 8%, PEG/PPG-
20/15 polydimethylsiloxane 6%, polydimethylsiloxane 2%, titanium dioxide 4%, Muscovitum 2%, silica flour 3%, cetyl PEG/
PPG-10/1 polydimethylsiloxane 0.5%, magnesium sulfate 0.8%, polymethyl methacrylate 2%, distearyl dimethylammonium Strese Hofmann's hectorite.
0.5%, Limax secretions 0.3%, leaf of Herb Gynostemmae Pentaphylli extract 1%, dulse elite 0.3%, Herba Centellae extract 1%, ivory white toner
1%, KF6017 0.3%, methyl hydroxybenzoate 0.5%, propyl hydroxybenzoate 0.1%, EDETATE SODIUM 0.03% and essence
0.03%。
Preparation: (1) is by polydimethylsiloxane, isononyl isononanoate, titanium dioxide, Muscovitum, silica flour, polymethylacrylic acid
Methyl ester, distearyl dimethylammonium Strese Hofmann's hectorite. and ivory white toner add in agitated kettle, and stirring homogenizing, to without granule, obtains material
One；
(2) by material one and PEG/PPG-20/15 polydimethylsiloxane, KF6017, oxybenzene first
Ester, propyl hydroxybenzoate and the mixing of cetyl PEG/PPG-10/1 polydimethylsiloxane add in oil phase pot, are heated to 85 DEG C so that it is
Dissolve completely, obtain material two, be incubated standby；
(3) water, glycerol, butanediol, magnesium sulfate and EDETATE SODIUM are added in aqueous phase pot, be heated to 90 DEG C, be incubated 25 ~ 35
Minute, obtain material three, be incubated standby；
(4) it is transferred to be pre-heated in the agitated kettle of 85 DEG C by material two and material three, stirs 10 minutes, homogenizing 10 minutes
After start cooling, when temperature is down to 45 DEG C, add Limax secretions, leaf of Herb Gynostemmae Pentaphylli extract, dulse elite, Herba Centellae extract
Thing and essence, stir and i.e. obtain CC frost.
The mixing speed of above-mentioned stirring is 50 revs/min.
The CC frost of embodiment 1 ~ 3 is done testing performance index, and its test result is as follows:
1, outward appearance: slightly flowing, band opaque light sensation mastic；
2, color and luster: ivory white；
3, heat-resistant stability investigates (45 DEG C × 24h): qualified；
4, cold-resistant study on the stability (-15 DEG C × 24h): qualified.
Comparative example 1,
Formula: by weight percentage, water 59.42%, isononyl isononanoate 6%, glycerol 6%, butanediol 6%, PEG/PPG-
20/15 polydimethylsiloxane 5%, polydimethylsiloxane 3%, titanium dioxide 3%, Muscovitum 3%, silica flour 3.1%, cetyl PEG/
PPG-10/1 polydimethylsiloxane 1%, magnesium sulfate 1.2%, polymethyl methacrylate 1%, distearyl dimethylammonium Strese Hofmann's hectorite.
1%, ivory white toner 0.4%, KF6017 0.5%, methyl hydroxybenzoate 0.2%, propyl hydroxybenzoate 0.1%, EDETATE SODIUM
0.02% and essence 0.06%.
Preparation method is with reference to embodiment 1.
Comparative example 2,
Formula: by weight percentage, water 59.42%, isononyl isononanoate 6%, glycerol 6%, butanediol 6%, PEG/PPG-
20/15 polydimethylsiloxane 4%, polydimethylsiloxane 3%, titanium dioxide 3%, Muscovitum 3%, silica flour 2%, cetyl PEG/
PPG-10/1 polydimethylsiloxane 1%, magnesium sulfate 1.2%, polymethyl methacrylate 1%, distearyl dimethylammonium Strese Hofmann's hectorite.
1%, Limax secretions 2.1%, ivory white toner 0.4%, KF6017 0.5%, methyl hydroxybenzoate 0.2%, oxybenzene third
Ester 0.1%, EDETATE SODIUM 0.02% and essence 0.06%.
Preparation method is with reference to embodiment 1.
Comparative example 3,
Formula: by weight percentage, water 59.42%, isononyl isononanoate 6%, glycerol 12%, PEG/PPG-20/15 poly-two
Methylsiloxane 5%, polydimethylsiloxane 3%, Muscovitum 6%, magnesium sulfate 1.2%, polymethyl methacrylate 1%, distearyl diformazan
Ammonium Strese Hofmann's hectorite. 1%, Limax secretions 0.5%, leaf of Herb Gynostemmae Pentaphylli extract 0.6%, dulse elite 0.5%, Herba Centellae extract
0.5%, ivory white toner 2.4%, KF6017 0.5%, methyl hydroxybenzoate 0.2%, propyl hydroxybenzoate 0.1%, EDTA bis-
Sodium 0.02% and essence 0.06%.
Preparation method is with reference to embodiment 1.
Test example one, Product Safety evaluation (experiment of human body skin patch)
One, trial target: the CC frost that embodiment 1 ~ 3, comparative example 1 ~ 3 prepare
Tested crowd's number: 60 people, women
Age: between 20 ~ 50 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Packet: 6 groups, often organize 10 people, 28 ± 2 years old mean age.
Two, patch method: select qualified speckle examination device, with closed patch experiment method, by tested material about 0.020g ~
0.025g drips in speckle examination device, and external special adhesive tape is covered on experimenter back, removes tested material, after removing respectively after 24 hours
0.5, within 6,12,24,48 hours, observe dermoreaction, record its knot according to dermoreaction grade scale in " cosmetics health specification "
Really.
Three, experimental result: human skin patch result shows: each group experimenter by embodiment 1 ~ 3, comparative example 1 ~
The patch test of the CC frost of 2, observed dermoreaction at 0.5,6,12,24,48 hours, and wherein skin adverse reaction occurs in 0 example, says
Bright described CC frost uses safety.
Test example two, product effect assessment
Part I: CC frost moisture retention is evaluated
One, trial target: the CC frost that embodiment 1 ~ 3 prepares
Two, tested crowd
Sex number: female, 30 people
Age: between 20 ~ 40 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Packet: be divided into 3 groups, often organize 10 people.
Method of testing: test environment temperature is constant temperature 25 ± 1 DEG C, relative humidity is 60 ± 5%, before test, experimenter is left
Right forearm uses alkalescence fancy soap to dry after cleaning, expose, rest half an hour in such circumstances.On the forearm of experimenter left and right each stroke
Going out the tested region of square of 4cm × 4cm, left arm is the tested region being coated with CC frost, and the symmetrical region of right arm is that blank is subject to
Examination district.Use Corneometer CM 825 PC tester probe, in tested region, choose 10 points measure (single
Measure), and record mean values as benchmark.Use Corneometer CM 825 PC tester probe, in tested region
Measure 70 seconds (measuring continuously) continuously, and record mean values as benchmark.Take 1gCC frost and be applied to tested district, on skin uniformly
Smear 2min.At 10min, 40min, 60min, 120min, 180min, probe is used to carry out single respectively at recipient site and connect
Continuous measurement, and record test result.Calculate moisture of skin percentage change in different time points.Concrete outcome sees table 1 below
With table 2.
The table 1 CC of the present invention single test result of frost moisture retention
Table 2 CC of the present invention frost moisture retention follow-on test result
From upper Tables 1 and 2, the embodiment of the present invention 1 ~ 3 CC frost can improve the moisture retention of skin, and persistently moisturizing effect
The best, wherein moisturizing and lasting moistening effect with embodiment 1 are optimal, illustrate that the embodiment of the present invention 1 CC each component of frost is worked in coordination with.
Part II: CC frost resultant effect is evaluated
One, trial target: the CC frost that embodiment 1 ~ 3, comparative example 1 ~ 3 prepare
Two, tested crowd
Sex number: female, 120 people
Age: between 25 ~ 50 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Packet: be divided into 6 groups, often organizes 20 people, often 29 ± 2 years old mean age of group.
Three, method of testing: after experimenter cleans face, takes the addition of C C frost and is applied in face, observe and experience using effect.
Test assessment result is as follows:
The feedback conclusive table on probation of table 3 embodiment 1 CC frost
The feedback conclusive table on probation of table 4 embodiment 2 CC frost
The feedback conclusive table on probation of table 5 embodiment 3 CC frost
The feedback conclusive table on probation of table 6 comparative example 1 CC frost
The feedback conclusive table on probation of table 7 comparative example 2 CC frost
The feedback conclusive table on probation of table 8 comparative example 3 CC frost
From upper table 3 ~ 8, often organizing 20 bit test persons, the CC frost of embodiment 1 ~ 3 is obtained for the accreditation of tester, simultaneously
The degree of recognition of the CC frost of embodiment 1 ~ 3 is also significantly greater than comparative example 1 ~ 3, and wherein the degree of recognition with embodiment 1 is the highest, and this is described
The bright each component of embodiment 1 is worked in coordination with, and resultant effect is optimal.Tester all represents, CC frost emulsion form of the present invention gently saturating quality, one brush is i.e.
Combine together with skin, after using, clearly paste skin, there is no a greasy feeling, waterproof antiperspirant, persistently fix, and it is effective to hide the flaw, also may be used
Desalination mottle melanin, bright color, replenishing water and preserving moisture, skin beauty water is tender moist, life-time service can whitening, revise the colour of skin, repair face
Portion's microgroove.The questionnaire of user there is not people allergic phenomena occur simultaneously.
Compared with Example 1, comparative example 1 formula without Limax secretions, leaf of Herb Gynostemmae Pentaphylli extract, dulse elite and amasss
Snow grass extract；Containing Limax secretions in comparative example 2 formula, but it is free from leaf of Herb Gynostemmae Pentaphylli extract, dulse elite and amasss
Snow grass extract；Lacking the component such as titanium dioxide, silica flour in comparative example 3 formula, the effect of comparative example 1 ~ 3 CC frost is all not as good as real
Execute example 1 ~ 3, illustrate that each component of the present invention exists synergism.
The principle of above-described embodiment only illustrative present invention and effect thereof, not for limiting the present invention.Any ripe
Above-described embodiment all can be modified under the spirit and the scope of the present invention or change by the personage knowing this technology.Cause
This, have usually intellectual such as complete with institute under technological thought without departing from disclosed spirit in art
All equivalences become are modified or change, and must be contained by the claim of the present invention.
Claims (5)
1. a CC frost, it is characterised in that include following components: water, isononyl isononanoate, glycerol, butanediol, PEG/PPG-
20/15 polydimethylsiloxane, polydimethylsiloxane, titanium dioxide, Muscovitum, silica flour, cetyl PEG/PPG-10/1 poly-two
Methylsiloxane, magnesium sulfate, polymethyl methacrylate, distearyl dimethylammonium Strese Hofmann's hectorite., Limax secretions, leaf of Herb Gynostemmae Pentaphylli carry
Take that thing, dulse elite, Herba Centellae extract, toner be ivory white, KF6017, methyl hydroxybenzoate, oxybenzene third
Ester, EDETATE SODIUM and essence.
2. CC frost as claimed in claim 1, it is characterised in that include the component of following percentage by weight meter: water 50 ~ 65%, different
N-nonanoic acid different nonyl ester 5 ~ 8%, glycerol 5 ~ 8%, butanediol 5 ~ 8%, PEG/PPG-20/15 polydimethylsiloxane 3 ~ 6%, poly dimethyl silicon
Oxygen alkane 2 ~ 5%, titanium dioxide 2 ~ 4%, Muscovitum 2 ~ 5%, silica flour 1 ~ 3%, cetyl PEG/PPG-10/1 polydimethylsiloxane 0.5 ~
2%, magnesium sulfate 0.8 ~ 2%, polymethyl methacrylate 0.5 ~ 2%, distearyl dimethylammonium Strese Hofmann's hectorite. 0.5 ~ 2%, Limax secretions
0.3 ~ 1%, leaf of Herb Gynostemmae Pentaphylli extract 0.3 ~ 1%, dulse elite 0.3 ~ 1%, Herba Centellae extract 0.3 ~ 1%, toner ivory white 0.3
~ 1%, KF6017 0.3 ~ 1%, methyl hydroxybenzoate 0.1 ~ 0.5%, propyl hydroxybenzoate 0.1 ~ 0.5%, EDETATE SODIUM 0.01
~ 0.03% and essence 0.01 ~ 0.1%.
3. CC frost as claimed in claim 2, it is characterised in that be made up of the component of following percentage by weight meter: water 59.42%,
Isononyl isononanoate 6%, glycerol 6%, butanediol 6%, PEG/PPG-20/15 polydimethylsiloxane 4%, polydimethylsiloxane
3%, titanium dioxide 3%, Muscovitum 3%, silica flour 2%, cetyl PEG/PPG-10/1 polydimethylsiloxane 1%, magnesium sulfate 1.2%, poly-
Methyl methacrylate 1%, distearyl dimethylammonium Strese Hofmann's hectorite. 1%, Limax secretions 0.5%, leaf of Herb Gynostemmae Pentaphylli extract 0.6%, red
Skin algae elite 0.5%, Herba Centellae extract 0.5%, toner are ivory white 0.4%, KF6017 0.5%, oxybenzene first
Ester 0.2%, propyl hydroxybenzoate 0.1%, EDETATE SODIUM 0.02% and essence 0.06%.
4. according to the preparation method of the CC frost described in claim 1 ~ 3 any one, it is characterised in that comprise the following steps:
(1) by polydimethylsiloxane, isononyl isononanoate, titanium dioxide, Muscovitum, silica flour, polymethyl methacrylate, two hard
In fat dimethylammonium Strese Hofmann's hectorite. and toner ivory white addition agitated kettle, stirring homogenizing, to without granule, obtains material one；
(2) by material one and PEG/PPG-20/15 polydimethylsiloxane, KF6017, methyl hydroxybenzoate, hydroxyl
Phenylpropyl alcohol ester and the mixing of cetyl PEG/PPG-10/1 polydimethylsiloxane add in oil phase pot, are heated to 75 ~ 85 DEG C so that it is molten
Solve completely, obtain material two, be incubated standby；
(3) water, glycerol, butanediol, magnesium sulfate and EDETATE SODIUM are added in aqueous phase pot, be heated to 80 ~ 90 DEG C, be incubated 25 ~ 35
Minute, obtain material three, be incubated standby；
(4) it is transferred to be pre-heated in the agitated kettle of 80 ~ 85 DEG C by material two and material three, stirs 10 ~ 15 minutes, homogenizing 5 ~ 10
Start cooling after minute, when temperature is down to 45 DEG C, add Limax secretions, leaf of Herb Gynostemmae Pentaphylli extract, dulse elite, Herba Centellae
Extract and essence, stir and i.e. obtain CC frost.
5. the preparation method of CC frost as claimed in claim 4, it is characterised in that the mixing speed of described stirring is 40 ~ 50 turns/
Minute.
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Address after: Huadu District, Guangdong city of Guangzhou province 510880 Flower Town Qiyuan Road No. 28 Patentee after: Guangzhou Kema biotechnology Polytron Technologies Inc Address before: Hua Town, Huadu District, Guangdong Province, 510880 Avenue, Guangzhou City Patentee before: Kerma (unit of kinetic energy) bio tech ltd, Guangzhou |