CN109231836A - Imitative engraving noctilucent glaze material and its manufacture craft - Google Patents
Imitative engraving noctilucent glaze material and its manufacture craft Download PDFInfo
- Publication number
- CN109231836A CN109231836A CN201811230157.8A CN201811230157A CN109231836A CN 109231836 A CN109231836 A CN 109231836A CN 201811230157 A CN201811230157 A CN 201811230157A CN 109231836 A CN109231836 A CN 109231836A
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- CN
- China
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- ingredient
- noctilucence
- raw material
- noctilucent
- powder
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/04—Frit compositions, i.e. in a powdered or comminuted form containing zinc
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses the imitative engraving noctilucent glaze material of one kind and its manufacture crafts, wherein anti-engraving noctilucent glaze material includes raw material and noctilucence ingredient, it is characterized in that, the noctilucence ingredient includes yellow noctilucence ingredient, red noctilucence ingredient and green noctilucence ingredient, the weight percent that the group of the raw material is grouped as are as follows: silica 65%-70%, potassium oxide 2%-4%, aluminium oxide 20%-26%, zinc oxide 5%-6%, calcium oxide 2%-4%；The weight percent of the yellow noctilucence ingredient are as follows: barium sulphide 50%, magnesium sulfide 45%, aluminum phosphate 2%, potassium nitrate 3%, the weight percent of the red noctilucence ingredient are as follows: barium sulphide 50%, magnesium sulfide 45%, copper nitrate 3%, potassium phosphate 2%, the weight percent of the green noctilucence ingredient are as follows: calcium sulfide 50%, nitric acid 5%, barium sulfate 15%, sodium sulphate 15%, potassium nitrate 15%；The present invention is intended to provide a kind of with the smooth of porcelain facing, and can also self luminous imitative engraving noctilucent glaze material and its manufacture craft at night.
Description
Technical field
The present invention relates to luminous glaze fields, particularly say, especially a kind of imitative engraving noctilucent glaze material and its manufacture craft.
Background technique
With the development of society, people increasingly pay attention to construction material at one's side, especially imitative engraving building decoration product,
Since imitative engraving building decoration product shape is three-dimensional, glaze more beautiful after glazing but common is ordinary, and is unable to self-luminous,
It the characteristics of imitative engraving building decoration product cannot be protruded, has a greatly reduced quality so as to cause the ornamental value of product.
Summary of the invention
It is an object of the invention to be directed to above-mentioned situation, it is further provided the imitative engraving noctilucent glaze material of one kind and its production work
Skill.
The technical scheme of the present invention is realized as follows: a kind of anti-engraving noctilucent glaze material, including raw material and noctilucence are matched
Material, the noctilucence ingredient include yellow noctilucence ingredient, red noctilucence ingredient and green noctilucence ingredient, the component of the raw material
The weight percent of composition are as follows: silica 65%-70%, potassium oxide 2%-4%, aluminium oxide 20%-26%, zinc oxide 5%-
6%, calcium oxide 2%-4%；The weight percent of the yellow noctilucence ingredient are as follows: barium sulphide 50%, magnesium sulfide 45%, aluminum phosphate
2%, potassium nitrate 3%, the weight percent of the red noctilucence ingredient are as follows: barium sulphide 50%, magnesium sulfide 45%, copper nitrate 3%,
Potassium phosphate 2%, the weight percent of the green noctilucence ingredient are as follows: calcium sulfide 50%, nitric acid 5%, barium sulfate 15%, sodium sulphate
15%, potassium nitrate 15%.
A kind of manufacture craft of anti-engraving noctilucent glaze material, comprising the following steps:
S1: it raw material screening: with by the weight percent that the group of raw material is grouped as: silica
65%-70%, potassium oxide 2%-4%, aluminium oxide 20%-26%, zinc oxide 5%-6%, calcium oxide 2%-4%, while basis
The color needed carries out the screening of noctilucence ingredient；
S2, graininess ingredient will be made with the raw material got ready: ready raw material is put into stirred autoclave
In, temperature is warming up to 1150-1250 DEG C and is kept the temperature to molten condition, water is then carried out and extracts obtained graininess raw material；
S3: production luminescent powder will be carried out with the noctilucence ingredient got ready: corresponding yellow night is prepared according to required color
Light powder, red noctilucent powder and green noctilucent powder；
S4: grinding: graininess raw material obtained in S2 is ground, and screens the graininess raw material of 250 mesh
It is spare to make；
S5: it is mixed: the luminescent powder that S3 is obtained and the graininess raw material that S4 is obtained being put into agitating device, added
Enter water to be mixed, dries and get product.
Yellow noctilucent powder, red noctilucent powder in the manufacture craft of above-mentioned anti-engraving noctilucent glaze material, in the step S3
With green noctilucent powder production method are as follows: be first put into raw material after being mixed evenly in high-temperature resistant container, in 150 DEG C of environment of temperature
Under calcined, soaking time be 60 minutes, calcined raw material is put into ball mill later and carries out being ground into fine powder, finally will
Fine powder is impregnated with clear water to be precipitated, and precipitating powder is dried after removing clear water.
In the manufacture craft of above-mentioned anti-engraving noctilucent glaze material, water, luminescent powder in the step S5, graininess basis are matched
Material weight ratio is 1:4:10.
The beneficial effects of the present invention are the raw material and noctilucence ingredient are mixed, and guarantee to use the glaze
Material rear surface still has the smooth of porcelain facing, and can also self-luminous at night, the characteristics of capable of more protruding imitative carved product, and
Preferably the imitative carved product inside protection, ornamental value greatly improve.
Specific embodiment
Embodiment one
Present embodiment discloses a kind of anti-engraving noctilucent glaze material, including raw material and noctilucence ingredient, the noctilucence ingredients
Including yellow noctilucence ingredient, red noctilucence ingredient and green noctilucence ingredient, the weight percent that the group of the raw material is grouped as
Than are as follows: silica 65%, potassium oxide 3%, aluminium oxide 20%, zinc oxide 5%, calcium oxide 2%；The yellow noctilucence ingredient
Weight percent are as follows: barium sulphide 50%, magnesium sulfide 45%, aluminum phosphate 2%, potassium nitrate 3%, the weight of the red noctilucence ingredient
Percentage are as follows: barium sulphide 50%, magnesium sulfide 45%, copper nitrate 3%, potassium phosphate 2%, the weight percent of the green noctilucence ingredient
Than are as follows: calcium sulfide 50%, nitric acid 5%, barium sulfate 15%, sodium sulphate 15%, potassium nitrate 15%.
A kind of manufacture craft of anti-engraving noctilucent glaze material, comprising the following steps:
S1: it raw material screening: with by the weight percent that the group of raw material is grouped as: silica
65%, potassium oxide 3%, aluminium oxide 20%, zinc oxide 5%, calcium oxide 2%, while color as needed carries out noctilucence ingredient
Screening；
S2, graininess ingredient will be made with the raw material got ready: ready raw material is put into stirred autoclave
In, temperature is warming up to 1150 DEG C and is kept the temperature to molten condition, water is then carried out and extracts obtained graininess raw material；
S3: production luminescent powder will be carried out with the noctilucence ingredient got ready: corresponding yellow night is prepared according to required color
Light powder, red noctilucent powder and green noctilucent powder；
S4: grinding: graininess raw material obtained in S2 is ground, and screens the graininess raw material of 250 mesh
It is spare to make；
S5: it is mixed: the luminescent powder that S3 is obtained and the graininess raw material that S4 is obtained being put into agitating device, added
Enter water to be mixed, dry and get product, the water, luminescent powder, graininess raw material weight ratio are 1:4:10.
Yellow noctilucent powder, red noctilucent powder and green noctilucent powder production method in the step S3 are as follows: first put raw material
Enter after being mixed evenly in high-temperature resistant container, calcined under 150 DEG C of environment of temperature, soaking time is 60 minutes, later
Calcined raw material is put into ball mill to carry out being ground into fine powder, fine powder is impregnated with clear water finally and is precipitated, is incited somebody to action after removing clear water
Precipitating powder is dried.
The raw material and noctilucence ingredient are mixed, and guarantee still there is porcelain facing using the glaze rear surface
It is smooth, and can also self-luminous at night, the characteristics of capable of more protruding imitative carved product, and preferably protect internal imitative engraving
Product, ornamental value greatly improve.
Embodiment two
The embodiment two and the difference of embodiment one be, the weight percent that the group of the raw material is grouped as are as follows:
Silica 70%, potassium oxide 2%, aluminium oxide 20%, zinc oxide 5%, calcium oxide 3%.
When by making graininess ingredient with the raw material got ready, ready raw material is put into stirred autoclave
In, temperature is warming up to 1250 DEG C and is kept the temperature to molten condition, water is then carried out and extracts obtained graininess raw material.
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, it is all in spirit of the invention and
Within principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (4)
1. a kind of anti-engraving noctilucent glaze material, including raw material and noctilucence ingredient, which is characterized in that the noctilucence ingredient includes Huang
Color noctilucence ingredient, red noctilucence ingredient and green noctilucence ingredient, the weight percent that the group of the raw material is grouped as are as follows: two
Silica 65%-70%, potassium oxide 2%-4%, aluminium oxide 20%-26%, zinc oxide 5%-6%, calcium oxide 2%-4%；Institute
State the weight percent of yellow noctilucence ingredient are as follows: barium sulphide 50%, magnesium sulfide 45%, aluminum phosphate 2%, potassium nitrate 3%, it is described red
The weight percent of color noctilucence ingredient are as follows: barium sulphide 50%, magnesium sulfide 45%, copper nitrate 3%, potassium phosphate 2%, the green night
The weight percent of light ingredient are as follows: calcium sulfide 50%, nitric acid 5%, barium sulfate 15%, sodium sulphate 15%, potassium nitrate 15%.
2. a kind of manufacture craft of anti-engraving noctilucent glaze material, which comprises the following steps:
S1: it raw material screening: with by the weight percent that the group of raw material is grouped as: silica 65%-
70%, potassium oxide 2%-4%, aluminium oxide 20%-26%, zinc oxide 5%-6%, calcium oxide 2%-4%, while as needed
The screening of color progress noctilucence ingredient；
S2, graininess ingredient will be made with the raw material got ready: ready raw material is put into stirred autoclave, it will
Temperature, which heats up 1150-1250 DEG C, to be kept the temperature to molten condition, is then carried out water and is extracted obtained graininess raw material；
S3: production luminescent powder will be carried out with the noctilucence ingredient got ready: according to required color prepare corresponding yellow noctilucent powder,
Red noctilucent powder and green noctilucent powder；
S4: grinding: graininess raw material obtained in S2 is ground, and screens the graininess raw material of 250 mesh to make
It is spare；
S5: it is mixed: the luminescent powder that S3 is obtained and the graininess raw material that S4 is obtained being put into agitating device, water is added
It is mixed, dries and get product.
3. the manufacture craft of anti-engraving noctilucent glaze material according to claim 2, which is characterized in that the Huang in the step S3
Color luminescent powder, red noctilucent powder and green noctilucent powder production method are as follows: first raw material is put into high-temperature resistant container and is mixed
It after even, is calcined under 150 DEG C of environment of temperature, soaking time is 60 minutes, and calcined raw material is put into ball mill later
It carries out being ground into fine powder, fine powder is impregnated with clear water finally and is precipitated, precipitating powder is dried after removing clear water.
4. the manufacture craft of anti-engraving noctilucent glaze material according to claim 2, which is characterized in that in the step S5
Water, luminescent powder, graininess raw material weight ratio are 1:4:10.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811230157.8A CN109231836A (en) | 2018-10-22 | 2018-10-22 | Imitative engraving noctilucent glaze material and its manufacture craft |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811230157.8A CN109231836A (en) | 2018-10-22 | 2018-10-22 | Imitative engraving noctilucent glaze material and its manufacture craft |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109231836A true CN109231836A (en) | 2019-01-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811230157.8A Pending CN109231836A (en) | 2018-10-22 | 2018-10-22 | Imitative engraving noctilucent glaze material and its manufacture craft |
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| CN (1) | CN109231836A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114031420A (en) * | 2021-12-06 | 2022-02-11 | 亚细亚建筑材料股份有限公司 | Fluorescent glaze |
| CN114315137A (en) * | 2021-12-20 | 2022-04-12 | 浙江开尔新材料股份有限公司 | Noctilucent glaze material for enamel, noctilucent enamel plate and manufacturing method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105948502A (en) * | 2016-07-20 | 2016-09-21 | 詹良富 | Formula and preparation method of high-temperature noctilucent glaze |
| CN107651949A (en) * | 2017-09-30 | 2018-02-02 | 佛山欧神诺陶瓷股份有限公司 | A kind of luminescent ceramic glazed tile and preparation method thereof |
| CN107955428A (en) * | 2017-12-21 | 2018-04-24 | 温州维特利颜料科技有限公司 | A kind of formula and manufacturing process of color luminous pigment |
-
2018
- 2018-10-22 CN CN201811230157.8A patent/CN109231836A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105948502A (en) * | 2016-07-20 | 2016-09-21 | 詹良富 | Formula and preparation method of high-temperature noctilucent glaze |
| CN107651949A (en) * | 2017-09-30 | 2018-02-02 | 佛山欧神诺陶瓷股份有限公司 | A kind of luminescent ceramic glazed tile and preparation method thereof |
| CN107955428A (en) * | 2017-12-21 | 2018-04-24 | 温州维特利颜料科技有限公司 | A kind of formula and manufacturing process of color luminous pigment |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114031420A (en) * | 2021-12-06 | 2022-02-11 | 亚细亚建筑材料股份有限公司 | Fluorescent glaze |
| CN114315137A (en) * | 2021-12-20 | 2022-04-12 | 浙江开尔新材料股份有限公司 | Noctilucent glaze material for enamel, noctilucent enamel plate and manufacturing method thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190118 |