CN109089907B - Non-caking cat litter and preparation method thereof - Google Patents

Non-caking cat litter and preparation method thereof Download PDF

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Publication number
CN109089907B
CN109089907B CN201810923950.XA CN201810923950A CN109089907B CN 109089907 B CN109089907 B CN 109089907B CN 201810923950 A CN201810923950 A CN 201810923950A CN 109089907 B CN109089907 B CN 109089907B
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parts
sieving
mesh sieve
cat litter
water
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CN109089907A (en
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董兆斌
乔志强
王根宪
王锐
陈新乐
张治有
郭安柱
王英宏
刘彬
董军社
吕晓莉
刘亚军
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Shangluo Shengda Industrial Co.,Ltd.
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Luonan Shengda Agricultural And Sideline Products Development Co ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01KANIMAL HUSBANDRY; CARE OF BIRDS, FISHES, INSECTS; FISHING; REARING OR BREEDING ANIMALS, NOT OTHERWISE PROVIDED FOR; NEW BREEDS OF ANIMALS
    • A01K1/00Housing animals; Equipment therefor
    • A01K1/015Floor coverings, e.g. bedding-down sheets ; Stable floors
    • A01K1/0152Litter
    • A01K1/0154Litter comprising inorganic material
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01KANIMAL HUSBANDRY; CARE OF BIRDS, FISHES, INSECTS; FISHING; REARING OR BREEDING ANIMALS, NOT OTHERWISE PROVIDED FOR; NEW BREEDS OF ANIMALS
    • A01K1/00Housing animals; Equipment therefor
    • A01K1/015Floor coverings, e.g. bedding-down sheets ; Stable floors
    • A01K1/0152Litter
    • A01K1/0155Litter comprising organic material

Abstract

The invention discloses non-caking cat litter and a preparation method thereof, wherein the non-caking cat litter is prepared from the following raw materials in parts by weight: 80-100 parts of walnut shell particles, 5-12 parts of diaphragma juglandis powder, 2-7 parts of citric acid, 3-8 parts of sodium bicarbonate, 4-9 parts of sodium carboxymethylcellulose and 4-10 parts of medical stone powder; wherein the water content of the walnut shell particles is 8-10%, and the split wood flour is obtained by the following pretreatment: mixing the core wood according to the material-liquid ratio of 1g: adding 0.3L of water, decocting at 100 deg.C for 30-50min, cooling to room temperature, adding Lentinus Edodes solution with the same volume as the water, soaking for 4-5 hr, ultrasonic treating for 15-25min, filtering, vacuum drying the residue to water content of 8-10%, and pulverizing. The cat litter provided by the invention has high water absorption speed, can quickly absorb water in cat litter, and is convenient to collect; the water saturation time is long, and the use time of the cat litter is long.

Description

Non-caking cat litter and preparation method thereof
Technical Field
The invention belongs to the technical field of cat litter, and particularly relates to non-caking cat litter and a preparation method thereof.
Background
With the improvement of the quality of life of people, the pet breeding is favored by more and more people, but the problem of environmental pollution caused by pet excrement in the process of breeding the pet is solved, and the great attention of people is paid.
The cat litter is a substance used for burying excrement and urine and controlling odor for cats kept by a feeder, has good water absorption and is a necessary product for families for keeping pet cats. The cat urine contains about 95% of water and about 5% of ammonia, and can generate serious odor and bacteria if not cleaned in time after the cat excretes.
The existing cat litter is basically divided into two types, one type is caking type cat litter, and the other type is non-caking type cat litter. The caking cat litter, particularly the cat litter prepared from sodium bentonite, can form cat urine into a mass after the cat urinates, so that the cat urine is convenient to clean, but the cat litter has large dust and poor deodorization capability; in the prior art, some environment-friendly caked cat litters prepared by using crop straws, light-density cellulose, pine trees and the like have good water absorption effect, can be directly thrown into a closestool, are easy to breed bacteria, have poor caked strength, and are easy to scatter by a cat after excretion, thus bringing inconvenience to the collection; the development of non-caking type cat litter is about to be earlier than caking type cat litter to clay cat litter that does not agglomerate is given first place to, and this kind of cat litter brings certain inconvenience for picking up owing to can not caking, however, this kind of cat litter water saturation time is long, can excrete the back at the cat and absorb cat urine rapidly, with cat litter moisture dry suction sclerosis, the water saturation time extension, then the live time of cat litter also prolongs, this can be for needing to use the cat litter for a long time and inconvenient in time the raiser who cleans up brings the convenience, saves the resource. However, the conventional non-caking cat litter has a short water saturation time and causes a serious odor when the cat litter is not cleaned in time after excretion. Therefore, the cat litter with short water absorption time, long water saturation time and long service time is of great significance for feeding cats.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides the non-caking cat litter which is long in water saturation time and long in service time.
The non-caking cat litter is prepared from the following raw materials in parts by weight:
80-100 parts of walnut shell particles, 5-12 parts of diaphragma juglandis powder, 2-7 parts of citric acid, 3-8 parts of sodium bicarbonate, 4-9 parts of sodium carboxymethylcellulose and 4-10 parts of medical stone powder;
wherein the water content of the walnut shell particles is 8-10%,
the split wood flour is obtained by the following pretreatment: mixing the core wood according to the material-liquid ratio of 1g: adding 0.3L of water, decocting at 100 deg.C for 30-50min, cooling to room temperature, adding Lentinus Edodes solution with the same volume as the water, soaking for 4-5 hr, ultrasonic treating for 15-25min, filtering, vacuum drying the residue to water content of 8-10%, and pulverizing.
Preferably, the walnut shell particles have a particle size distribution ratio of: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: (2-3).
Preferably, the particle size distribution ratio of the distraction wood flour is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: (2-3).
Preferably, the mushroom liquid is prepared by the following method: mixing dry shiitake mushrooms with water according to the mass ratio of 1:3000, soaking for 1h, decocting for 2h, filtering, keeping filter residues for later use, and cooling the obtained filtrate to room temperature to obtain the shiitake mushroom liquid.
Preferably, the conditions of the ultrasonic treatment are: the ultrasonic power is 400W, and the ultrasonic frequency is 40 KHz.
Preferably, the vacuum drying conditions are as follows: vacuum drying at 45-60 deg.C.
The preparation method of the non-caking cat litter comprises the following steps:
(1) pretreating the diaphragma juglandis to prepare diaphragma juglandis powder;
(2) crushing walnut shells, and screening to control the water content to be 8-10% to obtain walnut shell particles;
(3) mixing citric acid, sodium bicarbonate, sodium carboxymethylcellulose and Maifanitum powder, adding walnut shell particles and distraction wood powder, stirring and mixing;
(4) granulating at 300 deg.C under a compression ratio of 1:6, pulverizing the granules with a double-roll pulverizer, and sieving with 3-20 mesh sieve.
And a biomass granulator is adopted during granulation.
The 8-14-mesh sieve does not comprise a 14-mesh sieve, and specifically the 8-mesh sieve can pass through the sieve, and the 14-mesh sieve cannot pass through the sieve; sieving with 14-20 mesh sieve does not include sieving with 20 mesh sieve, specifically sieving with 14 mesh sieve and sieving with 20 mesh sieve; sieving with 20-100 mesh sieve, not including 100 mesh sieve, specifically passing through 20 mesh sieve, and not passing through 100 mesh sieve; the sieve with 3-20 meshes does not comprise the sieve with 20 meshes, and specifically means the sieve with 3 meshes and not with 20 meshes.
The water content is controlled to be 8-10%, the control is carried out by a method in the prior art, for example, when the water content is lower than 8-10%, a proper amount of water can be added into walnut shells, and then the walnut shells are kept stand for 24-48h in a closed environment or 24-48h in a certain humidity environment, so that the water content reaches 8-10%; when the water content is higher than 8-10%, drying to make the water content be 8-10%.
The core wood is a wood material sandwiched between walnut kernels, has a strong wood fragrance, is pretreated and crushed, and is added into cat litter, so that the adsorption capacity is strong.
The invention has the advantages that:
the cat litter provided by the invention is safe and pollution-free, can keep the natural costustoot flavor of walnut shells and diaphragma juglandis, has strong adsorption capacity and good deodorization capacity, can keep no residual ammonia in a cat litter basin for a long time, and has no peculiar smell; the water absorption speed is high, the water in the cat feces can be rapidly absorbed, so that the cat feces are hardened and are convenient to collect; the water saturation time is long, and the use time of the cat litter is long.
Detailed Description
The mushroom liquid used in the examples was prepared by the following method: mixing dry shiitake mushrooms with water according to the mass ratio of 1:3000, soaking for 1h, decocting for 2h, filtering, keeping filter residues for later use, and cooling the obtained filtrate to room temperature to obtain the shiitake mushroom liquid.
Example 1
1. The non-caking cat litter is prepared from the following raw materials in parts by weight:
80 parts of walnut shell particles, 5 parts of diaphragma juglandis powder, 2 parts of citric acid, 3 parts of sodium bicarbonate, 4 parts of sodium carboxymethylcellulose and 4 parts of medical stone powder;
wherein the split wood flour is obtained by the following pretreatment: adding diaphragma juglandis into water according to the material-liquid ratio of 1g:0.3L, decocting at 100 ℃ for 30min, cooling to room temperature, adding shiitake liquid with the same volume as the water, continuing to soak for 4h, then carrying out ultrasonic treatment for 25min under the conditions of ultrasonic power of 400W and ultrasonic frequency of 40KHz, filtering, carrying out vacuum drying on filter residue at 45 ℃ until the water content is 8%, and crushing;
the particle size distribution proportion of the walnut shell particles is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 2; the water content of the walnut shell particles is 8%;
the particle size distribution proportion of the distraction wood flour is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 2;
2. the preparation method of the non-caking cat litter comprises the following steps:
(1) pretreating the diaphragma juglandis to prepare the diaphragma juglandis wood powder, which specifically comprises the following steps: adding diaphragma juglandis into water according to the material-liquid ratio of 1g:0.3L, decocting at 100 ℃ for 30min, cooling to room temperature, then adding mushroom liquid with the same volume as the water, continuing to soak for 4h, then carrying out ultrasonic treatment for 25min under the conditions of ultrasonic power of 400W and ultrasonic frequency of 40KHz, filtering, carrying out vacuum drying on filter residue at 45 ℃ until the water content is 8%, crushing, and sieving to obtain the diaphragma juglandis powder with the particle size distribution ratio: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: the proportion of sieving by a 20-100 mesh sieve is 1:1: 2;
(2) crushing walnut shells, screening, controlling the water content to be 8% to obtain walnut shell particles, wherein the walnut shell particles are sieved by a 8-14-mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 2;
(3) mixing citric acid, sodium bicarbonate, sodium carboxymethylcellulose and Maifanitum powder, adding walnut shell particles and distraction wood powder, stirring and mixing;
(4) granulating by using a biomass granulator under the conditions of 300 ℃ and a compression ratio of 1:6, then crushing granules obtained by granulation by using a double-roll crusher, and sieving by using a 3-20-mesh sieve.
Example 2
1. The non-caking cat litter is prepared from the following raw materials in parts by weight:
100 parts of walnut shell particles, 12 parts of diaphragma juglandis wood powder, 7 parts of citric acid, 8 parts of sodium bicarbonate, 9 parts of sodium carboxymethylcellulose and 10 parts of medical stone powder;
wherein the split wood flour is obtained by the following pretreatment: adding diaphragma juglandis into water according to the material-liquid ratio of 1g:0.3L, decocting at 100 ℃ for 50min, cooling to room temperature, adding shiitake liquid with the same volume as the water, continuing to soak for 5h, then carrying out ultrasonic treatment for 15min under the conditions of ultrasonic power of 400W and ultrasonic frequency of 40KHz, filtering, carrying out vacuum drying on filter residue at 60 ℃ until the water content is 10%, and crushing;
the particle size distribution proportion of the walnut shell particles is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 3; the water content of the walnut shell particles is 10 percent;
the particle size distribution proportion of the distraction wood flour is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 3;
2. the preparation method of the non-caking cat litter comprises the following steps:
(1) pretreating the diaphragma juglandis to prepare the diaphragma juglandis wood powder, which specifically comprises the following steps: adding diaphragma juglandis into water according to the material-liquid ratio of 1g:0.3L, decocting for 50min at 100 ℃, cooling to room temperature, then adding mushroom liquid with the same volume as the water, continuing to soak for 5h, then carrying out ultrasonic treatment for 15min under the conditions of ultrasonic power of 400W and ultrasonic frequency of 40KHz, filtering, carrying out vacuum drying on filter residue at 60 ℃ until the water content is 10%, and crushing to obtain the diaphragma juglandis powder with the particle size distribution ratio: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: the proportion of sieving by a 20-100 mesh sieve is 1:1: 3;
(2) crushing walnut shells, screening, controlling the water content to be 10% to obtain walnut shell particles, wherein the walnut shell particles are sieved by a sieve with 8-14 meshes: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 3;
(3) mixing citric acid, sodium bicarbonate, sodium carboxymethylcellulose and Maifanitum powder, adding walnut shell particles and distraction wood powder, stirring and mixing;
(4) granulating by using a biomass granulator under the conditions of 300 ℃ and a compression ratio of 1:6, then crushing granules obtained by granulation by using a double-roll crusher, and sieving by using a 3-20-mesh sieve.
Example 3
1. The non-caking cat litter is prepared from the following raw materials in parts by weight:
90 parts of walnut shell particles, 7 parts of diaphragma juglandis powder, 3 parts of citric acid, 5 parts of sodium bicarbonate, 6 parts of sodium carboxymethylcellulose and 6 parts of medical stone powder;
wherein the split wood flour is obtained by the following pretreatment: adding diaphragma juglandis into water according to the material-liquid ratio of 1g:0.3L, decocting at 100 ℃ for 40min, cooling to room temperature, adding shiitake liquid with the same volume as the water, continuing to soak for 4.5h, then carrying out ultrasonic treatment for 20min under the conditions of ultrasonic power of 400W and ultrasonic frequency of 40KHz, filtering, carrying out vacuum drying on filter residue at 55 ℃ until the water content is 9%, and crushing;
the particle size distribution proportion of the walnut shell particles is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 3; the water content of the walnut shell particles is 8%;
the particle size distribution proportion of the distraction wood flour is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 2;
2. the preparation method of the non-caking cat litter comprises the following steps:
(1) pretreating the diaphragma juglandis to obtain diaphragma juglandis wood powder, which specifically comprises the following steps: adding diaphragma juglandis into water according to the material-liquid ratio of 1g:0.3L, decocting at 100 ℃ for 40min, cooling to room temperature, then adding mushroom liquid with the same volume as the water, continuing to soak for 4.5h, then carrying out ultrasonic treatment for 20min under the conditions of ultrasonic power of 400W and ultrasonic frequency of 40KHz, filtering, carrying out vacuum drying on filter residue at 55 ℃ until the water content is 9%, and crushing to obtain the diaphragma juglandis powder with the particle size distribution ratio of: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 2;
(2) crushing walnut shells, screening, controlling the water content to be 8% to obtain walnut shell particles, wherein the walnut shell particles are sieved by a 8-14-mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 3;
(3) mixing citric acid, sodium bicarbonate, sodium carboxymethylcellulose and Maifanitum powder, adding walnut shell particles and distraction wood powder, stirring and mixing;
(4) granulating by using a biomass granulator under the conditions of 300 ℃ and a compression ratio of 1:6, then crushing granules obtained by granulation by using a double-roll crusher, and sieving by using a 3-20-mesh sieve.
Example 4
1. The non-caking cat litter is prepared from the following raw materials in parts by weight:
95 parts of walnut shell particles, 10 parts of diaphragma juglandis wood powder, 6 parts of citric acid, 6 parts of sodium bicarbonate, 7 parts of sodium carboxymethylcellulose and 7 parts of medical stone powder;
wherein the split wood flour is obtained by the following pretreatment: adding diaphragma juglandis into water according to the material-liquid ratio of 1g:0.3L, decocting at 100 ℃ for 45min, cooling to room temperature, adding shiitake liquid with the same volume as the water, continuing to soak for 5h, then carrying out ultrasonic treatment for 20min under the conditions of ultrasonic power of 400W and ultrasonic frequency of 40KHz, filtering, carrying out vacuum drying on filter residue at 50 ℃ until the water content is 9%, and crushing;
the particle size distribution proportion of the walnut shell particles is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 2; the water content of the walnut shell particles is 9%;
the particle size distribution proportion of the distraction wood flour is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 3;
2. the preparation method of the non-caking cat litter comprises the following steps:
(1) pretreating the diaphragma juglandis to prepare the diaphragma juglandis wood powder, which specifically comprises the following steps: adding diaphragma juglandis into water according to the material-liquid ratio of 1g:0.3L, decocting for 45min at 100 ℃, cooling to room temperature, then adding mushroom liquid with the same volume as the water, continuing to soak for 5h, then carrying out ultrasonic treatment for 20min under the conditions of ultrasonic power of 400W and ultrasonic frequency of 40KHz, filtering, carrying out vacuum drying on filter residue at 50 ℃ until the water content is 9%, and crushing to obtain the diaphragma juglandis powder with the particle size distribution ratio: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 3;
(2) crushing walnut shells, screening, controlling the water content to be 9%, and obtaining walnut shell particles, wherein the particle size distribution ratio of the walnut shell particles is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 2;
(3) mixing citric acid, sodium bicarbonate, sodium carboxymethylcellulose and Maifanitum powder, adding walnut shell particles and distraction wood powder, stirring and mixing;
(4) granulating by using a biomass granulator under the conditions of 300 ℃ and a compression ratio of 1:6, then crushing granules obtained by granulation by using a double-roll crusher, and sieving by using a 3-20-mesh sieve.
Comparative example
The same as example 4, but without the addition of the distraction wood flour, is specified below:
1. the non-caking cat litter is prepared from the following raw materials in parts by weight:
95 parts of walnut shell particles, 6 parts of citric acid, 6 parts of sodium bicarbonate, 7 parts of sodium carboxymethyl cellulose and 7 parts of medical stone powder;
the particle size distribution proportion of the walnut shell particles is as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 2; the water content of the walnut shell particles is 9%;
2. the preparation method of the non-caking cat litter comprises the following steps:
(1) crushing walnut shells, screening, controlling the water content to be 9%, and obtaining walnut shell particles with the particle size distribution ratio as follows: sieving with 8-14 mesh sieve: sieving with a 14-20 mesh sieve: sieving with a 20-100 mesh sieve in a ratio of 1: 2;
(2) mixing citric acid, sodium bicarbonate, sodium carboxymethylcellulose and medical stone powder, adding the walnut shell particles obtained in the step (1), and stirring and mixing;
(3) granulating by using a biomass granulator under the conditions of 300 ℃ and a compression ratio of 1:6, then crushing granules obtained by granulation by using a double-roll crusher, and sieving by using a 3-20-mesh sieve.
Performance detection
Water absorption Performance test
1. Water absorption rate detection
The same mass of cat litter was taken, distilled water, normal saline, 1% mass concentration urea/normal saline solution, and fresh cat urine were taken to act on cat litter, and the time taken for the liquids to be sucked up was observed, and the results are shown in table 1, in which the volumes of the liquids were all 50mL, the masses of the cat litter were the same, and were all 100 g;
TABLE 1 Water absorption Rate test results (time: s)
Figure DEST_PATH_IMAGE001
2. Water absorption detection
The tapped product was measured to the scale using a 100mL straight measuring cylinder, poured into a 200 mesh standard sieve and weighed as M1, and after 15min of immersion, weighed as M2, the water absorption = (M2-M1) ÷ M1 (unit: g/g), the water absorption results are shown in table 2.
TABLE 2 Water absorption results (g/g)
Figure 779736DEST_PATH_IMAGE002
Second, the service time
3kg of cat litter provided by the invention is taken for 4 cats to normally use, after the cat litter is used for 10 days, the cat litter is saturated, after the cat litter is saturated, the cat litter is naturally dried, the cat litter can be repeatedly used for 9-10 times (10 days each time), 5-6g of the cat litter is lost each time, and in the using process, the cat litter has no odor and good deodorization capacity;
under the same condition, 3kg of cat litter of the comparative example is taken for 4 cats to normally use, the cat litter is saturated after being used for 2 days, and the cat litter is dried after being saturated and can be used for 2-3 times (2 days each time);
therefore, the cat litter provided by the invention is long in water saturation time, can be repeatedly used for many times, can save the cat litter, can be used for at least 3 months, is low in loss and has a good deodorization effect; when the core wood is not added, the water saturation time of the cat litter is obviously shortened, and the repeated use times are seriously reduced.

Claims (1)

1. A non-caking cat litter comprising: the composition is characterized by comprising the following raw materials in parts by weight:
80-100 parts of walnut shell particles, 5-12 parts of diaphragma juglandis powder, 2-7 parts of citric acid, 3-8 parts of sodium bicarbonate, 4-9 parts of sodium carboxymethylcellulose and 4-10 parts of medical stone powder;
wherein the water content of the walnut shell particles is 8-10%,
the split wood flour is obtained by the following pretreatment: mixing the core wood according to the material-liquid ratio of 1g: adding 0.3L of water, decocting at 100 deg.C for 30-50min, cooling to room temperature, adding Lentinus Edodes solution with the same volume as the water, soaking for 4-5 hr, ultrasonic treating for 15-25min, filtering, vacuum drying the residue to water content of 8-10%, and pulverizing;
the particle size distribution proportion of the walnut shell particles is as follows: sieving with 8-14 mesh sieve, sieving with 14-20 mesh sieve, sieving with 20-100 mesh sieve at ratio of 1:1 (2-3);
the particle size distribution proportion of the distraction wood flour is as follows: sieving with 8-14 mesh sieve, sieving with 14-20 mesh sieve, sieving with 20-100 mesh sieve at ratio of 1:1 (2-3);
the mushroom liquid is prepared by the following method: mixing dry shiitake mushrooms with water according to a mass ratio of 1:3000, soaking for 1h, decocting for 2h, filtering, keeping filter residues for later use, and cooling the obtained filtrate to room temperature to obtain shiitake mushroom liquid;
the ultrasonic treatment conditions are as follows: the ultrasonic power is 400W, and the ultrasonic frequency is 40 KHz;
the vacuum drying conditions are as follows: vacuum drying at 45-60 deg.C;
the preparation method of the non-caking cat litter is characterized by comprising the following steps: the method comprises the following steps:
(1) pretreating the diaphragma juglandis to prepare diaphragma juglandis powder;
(2) crushing walnut shells, and screening to control the water content to be 8-10% to obtain walnut shell particles;
(3) mixing citric acid, sodium bicarbonate, sodium carboxymethylcellulose and Maifanitum powder, adding walnut shell particles and distraction wood powder, stirring and mixing;
(4) granulating at 300 deg.C under a compression ratio of 1:6, pulverizing the granules with a double-roll pulverizer, and sieving with 3-20 mesh sieve.
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