CN109089907A - A kind of non-agglomerated type cat litter and preparation method thereof - Google Patents
A kind of non-agglomerated type cat litter and preparation method thereof Download PDFInfo
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- CN109089907A CN109089907A CN201810923950.XA CN201810923950A CN109089907A CN 109089907 A CN109089907 A CN 109089907A CN 201810923950 A CN201810923950 A CN 201810923950A CN 109089907 A CN109089907 A CN 109089907A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01K—ANIMAL HUSBANDRY; CARE OF BIRDS, FISHES, INSECTS; FISHING; REARING OR BREEDING ANIMALS, NOT OTHERWISE PROVIDED FOR; NEW BREEDS OF ANIMALS
- A01K1/00—Housing animals; Equipment therefor
- A01K1/015—Floor coverings, e.g. bedding-down sheets ; Stable floors
- A01K1/0152—Litter
- A01K1/0154—Litter comprising inorganic material
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01K—ANIMAL HUSBANDRY; CARE OF BIRDS, FISHES, INSECTS; FISHING; REARING OR BREEDING ANIMALS, NOT OTHERWISE PROVIDED FOR; NEW BREEDS OF ANIMALS
- A01K1/00—Housing animals; Equipment therefor
- A01K1/015—Floor coverings, e.g. bedding-down sheets ; Stable floors
- A01K1/0152—Litter
- A01K1/0155—Litter comprising organic material
Abstract
The present invention discloses a kind of non-agglomerated type cat litter and preparation method thereof, and the non-agglomerated type cat litter is made of the raw material of following parts by weight: 80-100 parts of walnut shell particle, 5-12 parts of wood powder of diverting one's attention, 2-7 parts of citric acid, 3-8 parts of sodium bicarbonate, 4-9 parts of sodium carboxymethylcellulose, 4-10 parts of medical stone powder；Wherein, the water content of the walnut shell particle is 8-10%, the wood powder of diverting one's attention is obtained by following pretreatment: Diaphragma juglandis being added to the water according to solid-liquid ratio 1g:0.3L, 30-50min is decocted at 100 DEG C, is cooled to room temperature, then the mushroom liquor with the water phase same volume is added, continue to impregnate 4-5h, be then ultrasonically treated 15-25min, filters, it is 8-10% that filter residue, which is dried under vacuum to water content, is crushed.Cat litter provided by the invention, absorption speed is fast, can conveniently tidy up rapidly by the moisture absorption in cat dung；The water saturation time is long, and cat litter is long using the time.
Description
Technical field
The invention belongs to cat litter technical fields, and in particular to a kind of non-agglomerated type cat litter and preparation method thereof.
Background technique
With the improvement of people's life quality, raising pet is liked still, how solving to raise by more and more people
During pet, the great attention of people is had been obtained in problem of environmental pollution caused by pet excrement.
Cat litter is to raise the main cat for its raising to be used to bury substance used in excrement and urine, control smell, is had preferable
Water imbibition is the common necessary article for raising pet cat family.Ammonia containing 95% or so moisture and 5% or so in cat urine, in cat
After excretion, if clearing up not in time, serious stink can be generated, while can also non-self bacterial.
Existing cat litter is divided into two classes substantially, and one kind is phyma type cat litter, and another kind of is non-phyma type cat litter.Phyma type
Cat litter made from cat litter, especially sodium bentonite can urinate cat to form a group after cat urination, convenient for cleaning, but this
A kind of cat litter dust is big, and deodorizing capability is poor；In the prior art, there are also use agricultural crop straw, the cellulose of light density, pine
The environment-friendly type of the preparations such as tree is agglomerated cat litter, and soaking effect is good, can directly throw into closestool, but bacterium easy to breed, and is agglomerated
Intensity difference, cat are easy to oneself to be done after excretion to dissipate, to tidying up and bring some inconvenience；The development of non-agglomerated type cat litter
Will be earlier than phyma type cat litter, based on the clay cat litter of not conglomeration, this kind of cat litters brings one due to that cannot agglomerate, to tidying up
Fixed inconvenience, still, this kind of cat litter water saturation time are long, rapidly can urinate cat after cat drains and absorb, cat liquid dung point is inhaled
Stiffization, water saturation time extends, then cat litter was also extended using the time, this can be to needing for a long time using cat litter and not side
Just the feeding swept in time is main to be brought convenience, and resource is saved.But existing non-agglomerated type cat litter, the water saturation time is short, in cat
Cleaning will generate serious stink not in time after excretion.So providing, a kind of absorbent time is short, the water saturation time is long, uses
The cat litter of time length is for raising cat important in inhibiting.
Summary of the invention
In view of the drawbacks of the prior art, the present invention provides a kind of non-agglomerated type cat litter, and the water saturation time is long, uses the time
It is long.
A kind of non-agglomerated type cat litter, is made of the raw material of following parts by weight:
80-100 parts of walnut shell particle, 5-12 parts of wood powder of diverting one's attention, 2-7 parts of citric acid, 3-8 parts of sodium bicarbonate, carboxymethyl cellulose
4-9 parts of sodium, 4-10 parts of medical stone powder；
Wherein, the water content of the walnut shell particle is 8-10%,
The wood powder of diverting one's attention is obtained by following pretreatment: Diaphragma juglandis is added to the water according to solid-liquid ratio 1g:0.3L,
30-50min is decocted at 100 DEG C, is cooled to room temperature, the mushroom liquor with the water phase same volume is then added, continues to impregnate 4-5h,
Then it is ultrasonically treated 15-25min, is filtered, it is 8-10% that filter residue, which is dried under vacuum to water content, is crushed.
Preferably, it the particle diameter distribution ratio of the walnut shell particle are as follows: cross 8-14 mesh: crosses 14-20 mesh: crossing 20-100
Mesh is 1:1:(2-3).
Preferably, it the particle diameter distribution ratio of the wood powder of diverting one's attention are as follows: cross 8-14 mesh: crosses 14-20 mesh: crossing 20-100 mesh
Sieve is 1:1:(2-3).
Preferably, the mushroom liquor is prepared by the following method to obtain: by dried thin mushroom according to mass ratio 1:3000 with
Water mixing after impregnating 1h, decocts 2h, then filters, filter residue is spare, and gained filtrate is cooled to room temperature, as mushroom liquor.
Preferably, the condition of the ultrasonic treatment are as follows: ultrasonic power 400W, supersonic frequency 40KHz.
Preferably, the vacuum drying condition are as follows: be dried in vacuo at 45-60 DEG C.
The preparation method of above-mentioned non-agglomerated type cat litter, comprising the following steps:
(1) Diaphragma juglandis is pre-processed, wood powder of diverting one's attention is prepared；
(2) walnut shell is crushed, is sieved, controlling its water content is 8-10%, obtains walnut shell particle；
(3) it by citric acid, sodium bicarbonate, sodium carboxymethylcellulose, medical stone powder, mixing, adds walnut shell particle and diverts one's attention
Wood powder is stirred；
(4) 300 DEG C, compression ratio be 1:6 under conditions of pelletize, then with pair roller pulverizer by the obtained particle of granulation
It is crushed, crosses 3-20 mesh.
Biomass granulation machine is used when granulation.
Heretofore described 8-14 mesh of crossing does not include 14 meshes, in particular to can pass through 8 meshes, while cannot pass through 14
Mesh；It crosses 14-20 mesh not and includes 20 meshes, in particular to can be by 14 meshes, while 20 meshes cannot be passed through；It crosses
20-100 mesh does not include 100 meshes, in particular to can be by 20 mesh, while cannot lead to and sieve with 100 mesh sieve；Cross 3-20 mesh
Do not include 20 meshes, in particular to can be by 3 meshes, while 20 meshes cannot be passed through.
Heretofore described control water content is 8-10%, is controlled by method in the prior art, for example, when containing
When water is lower than 8-10%, suitable water can be added into walnut shell, 24-48h is then stood under closed environment, or one
Determine to stand 24-48h under humidity environment, its water content is made to reach 8-10%；When water content is higher than 8-10%, by drying drying,
Make its moisture content in 8-10%.
Diaphragma juglandis is the wood materials being clipped between walnut kernel, there is strong radix aucklandiae taste, after pretreatment crushes, is added
In cat litter, adsorption capacity is strong.
Advantages of the present invention:
Cat litter provided by the invention, safety non-pollution are able to maintain walnut shell and the natural radix aucklandiae taste of Diaphragma juglandis, and adsorption capacity is strong,
Deodorizing capability is good, can keep the ammonia of noresidue in cat litter box, free from extraneous odour for a long time；Absorption speed is fast, can be rapidly by the water in cat dung
Divide and absorb, hardens cat dung, conveniently tidy up；The water saturation time is long, and cat litter is long using the time.
Specific embodiment
Mushroom liquor used in embodiment is prepared using following methods: by dried thin mushroom according to mass ratio 1:3000
It is mixed with water, after impregnating 1h, decocts 2h, then filter, filter residue is spare, and gained filtrate is cooled to room temperature, as mushroom liquor.
Embodiment 1
1. a kind of non-agglomerated type cat litter, is made of the raw material of following parts by weight:
80 parts of walnut shell particle, 5 parts of wood powder of diverting one's attention, 2 parts of citric acid, 3 parts of sodium bicarbonate, 4 parts of sodium carboxymethylcellulose, medical stone
4 parts of powder；
Wherein, described to divert one's attention what wood powder was obtained by following pretreatment: water is added according to solid-liquid ratio 1g:0.3L in Diaphragma juglandis
In, 30min is decocted at 100 DEG C, after being cooled to room temperature, the mushroom liquor with the water phase same volume is then added, continues to impregnate
Then 4h is ultrasonically treated 25min under conditions of ultrasonic power 400W, supersonic frequency 40KHz, filtering, by filter residue at 45 DEG C
Being dried under vacuum to water content is 8%, is crushed；
The particle diameter distribution ratio of the walnut shell particle are as follows: cross 8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:
2；The water content of the walnut shell particle is 8%；
The particle diameter distribution ratio of the wood powder of diverting one's attention are as follows: cross 8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:2；
2. the preparation method of above-mentioned non-agglomerated type cat litter, comprising the following steps:
(1) Diaphragma juglandis is pre-processed, wood powder of diverting one's attention is prepared, it is specific as follows: Diaphragma juglandis is added according to solid-liquid ratio 1g:0.3L
In water, 30min is decocted at 100 DEG C, after being cooled to room temperature, the mushroom liquor with the water phase same volume is then added, continues to soak
4h is steeped, is then ultrasonically treated 25min under conditions of ultrasonic power 400W, supersonic frequency 40KHz, is filtered, by filter residue at 45 DEG C
Under be dried under vacuum to water content be 8%, crush, sieving, the particle diameter distribution ratio of obtained wood powder of diverting one's attention are as follows: cross 8-14 mesh: mistake
14-20 mesh: the ratio for crossing 20-100 mesh is 1:1:2；
(2) walnut shell is crushed, is sieved, controlling its water content is 8%, obtains walnut shell particle, wherein cross 8-14 mesh: mistake
14-20 mesh: crossing 20-100 mesh is 1:1:2；
(3) it by citric acid, sodium bicarbonate, sodium carboxymethylcellulose, medical stone powder, mixing, adds walnut shell particle and diverts one's attention
Wood powder is stirred；
(4) 300 DEG C, compression ratio be 1:6 under conditions of, pelletized using biomass granulation machine, then crushed with pair roller type
Machine crushes the particle that granulation obtains, and crosses 3-20 mesh.
Embodiment 2
1. a kind of non-agglomerated type cat litter, is made of the raw material of following parts by weight:
100 parts of walnut shell particle, 12 parts of wood powder of diverting one's attention, 7 parts of citric acid, 8 parts of sodium bicarbonate, 9 parts of sodium carboxymethylcellulose, wheat meal
10 parts of mountain flour；
Wherein, described to divert one's attention what wood powder was obtained by following pretreatment: water is added according to solid-liquid ratio 1g:0.3L in Diaphragma juglandis
In, 50min is decocted at 100 DEG C, after being cooled to room temperature, the mushroom liquor with the water phase same volume is then added, continues to impregnate
Then 5h is ultrasonically treated 15min under conditions of ultrasonic power 400W, supersonic frequency 40KHz, filtering, by filter residue at 60 DEG C
Being dried under vacuum to water content is 10%, is crushed；
The particle diameter distribution ratio of the walnut shell particle are as follows: cross 8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:
3；The water content of the walnut shell particle is 10%；
The particle diameter distribution ratio of the wood powder of diverting one's attention are as follows: cross 8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:3；
2. the preparation method of above-mentioned non-agglomerated type cat litter, comprising the following steps:
(1) Diaphragma juglandis is pre-processed, wood powder of diverting one's attention is prepared, it is specific as follows: Diaphragma juglandis is added according to solid-liquid ratio 1g:0.3L
In water, 50min is decocted at 100 DEG C, after being cooled to room temperature, the mushroom liquor with the water phase same volume is then added, continues to soak
5h is steeped, is then ultrasonically treated 15min under conditions of ultrasonic power 400W, supersonic frequency 40KHz, is filtered, by filter residue at 60 DEG C
Under be dried under vacuum to water content be 10%, crush, the particle diameter distribution ratio of obtained wood powder of diverting one's attention are as follows: cross 8-14 mesh: cross 14-
20 meshes: the ratio for crossing 20-100 mesh is 1:1:3；
(2) walnut shell is crushed, is sieved, controlling its water content is 10%, obtains walnut shell particle, wherein cross 8-14 mesh: mistake
14-20 mesh: crossing 20-100 mesh is 1:1:3；
(3) citric acid, sodium bicarbonate, sodium carboxymethylcellulose, medical stone powder are mixed, adds walnut shell particle and Diaphragma juglandis
Powder is stirred；
(4) 300 DEG C, compression ratio be 1:6 under conditions of, pelletized using biomass granulation machine, then crushed with pair roller type
Machine crushes the particle that granulation obtains, and crosses 3-20 mesh.
Embodiment 3
1. a kind of non-agglomerated type cat litter, is made of the raw material of following parts by weight:
90 parts of walnut shell particle, 7 parts of wood powder of diverting one's attention, 3 parts of citric acid, 5 parts of sodium bicarbonate, 6 parts of sodium carboxymethylcellulose, medical stone
6 parts of powder；
Wherein, described to divert one's attention what wood powder was obtained by following pretreatment: water is added according to solid-liquid ratio 1g:0.3L in Diaphragma juglandis
In, 40min is decocted at 100 DEG C, after being cooled to room temperature, the mushroom liquor with the water phase same volume is then added, continues to impregnate
Then 4.5h is ultrasonically treated 20min under conditions of ultrasonic power 400W, supersonic frequency 40KHz, filtering, by filter residue at 55 DEG C
Under be dried under vacuum to water content be 9%, crush；
The particle diameter distribution ratio of the walnut shell particle are as follows: cross 8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:
3；The water content of the walnut shell particle is 8%；
The particle diameter distribution ratio of the wood powder of diverting one's attention are as follows: cross 8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:2；
2. the preparation method of above-mentioned non-agglomerated type cat litter, comprising the following steps:
(1) Diaphragma juglandis is pre-processed, obtains wood powder of diverting one's attention, it is specific as follows: water is added according to solid-liquid ratio 1g:0.3L in Diaphragma juglandis
In, 40min is decocted at 100 DEG C, after being cooled to room temperature, the mushroom liquor with the water phase same volume is then added, continues to impregnate
Then 4.5h is ultrasonically treated 20min under conditions of ultrasonic power 400W, supersonic frequency 40KHz, filtering, by filter residue at 55 DEG C
Under to be dried under vacuum to water content be 9%, crush, the particle diameter distribution ratio for the wood powder that obtains diverting one's attention are as follows: cross 8-14 mesh: crossing 14-20 mesh
Sieve: crossing 20-100 mesh is 1:1:2；
(2) walnut shell is crushed, is sieved, controlling its water content is 8%, obtains walnut shell particle, wherein cross 8-14 mesh: mistake
14-20 mesh: crossing 20-100 mesh is 1:1:3；
(3) citric acid, sodium bicarbonate, sodium carboxymethylcellulose, medical stone powder are mixed, adds walnut shell particle and Diaphragma juglandis
Powder is stirred；
(4) 300 DEG C, compression ratio be 1:6 under conditions of, pelletized using biomass granulation machine, then crushed with pair roller type
Machine crushes the particle that granulation obtains, and crosses 3-20 mesh.
Embodiment 4
1. a kind of non-agglomerated type cat litter, is made of the raw material of following parts by weight:
95 parts of walnut shell particle, 10 parts of wood powder of diverting one's attention, 6 parts of citric acid, 6 parts of sodium bicarbonate, 7 parts of sodium carboxymethylcellulose, wheat meal
7 parts of mountain flour；
Wherein, described to divert one's attention what wood powder was obtained by following pretreatment: water is added according to solid-liquid ratio 1g:0.3L in Diaphragma juglandis
In, 45min is decocted at 100 DEG C, after being cooled to room temperature, the mushroom liquor with the water phase same volume is then added, continues to impregnate
Then 5h is ultrasonically treated 20min under conditions of ultrasonic power 400W, supersonic frequency 40KHz, filtering, by filter residue at 50 DEG C
Being dried under vacuum to water content is 9%, is crushed；
The particle diameter distribution ratio of the walnut shell particle are as follows: cross 8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:
2；The water content of the walnut shell particle is 9%；
The particle diameter distribution ratio of the wood powder of diverting one's attention are as follows: cross 8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:3；
2. the preparation method of above-mentioned non-agglomerated type cat litter, comprising the following steps:
(1) Diaphragma juglandis is pre-processed, wood powder of diverting one's attention is prepared, it is specific as follows: Diaphragma juglandis is added according to solid-liquid ratio 1g:0.3L
In water, 45min is decocted at 100 DEG C, after being cooled to room temperature, the mushroom liquor with the water phase same volume is then added, continues to soak
5h is steeped, is then ultrasonically treated 20min under conditions of ultrasonic power 400W, supersonic frequency 40KHz, is filtered, by filter residue at 50 DEG C
Under be dried under vacuum to water content be 9%, crush, the particle diameter distribution ratio of obtained wood powder of diverting one's attention are as follows: cross 8-14 mesh: cross 14-20
Mesh: crossing 20-100 mesh is 1:1:3；
(2) walnut shell is crushed, is sieved, controlling its water content is 9%, obtains walnut shell particle, wherein the grain of walnut shell particle
Diameter distribution proportion are as follows: cross 8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:2；
(3) citric acid, sodium bicarbonate, sodium carboxymethylcellulose, medical stone powder are mixed, adds walnut shell particle and Diaphragma juglandis
Powder is stirred；
(4) 300 DEG C, compression ratio be 1:6 under conditions of, pelletized using biomass granulation machine, then crushed with pair roller type
Machine crushes the particle that granulation obtains, and crosses 3-20 mesh.
Comparative example
With embodiment 4, but it is added without wood powder of diverting one's attention, specific as follows:
1. a kind of non-agglomerated type cat litter, is made of the raw material of following parts by weight:
95 parts of walnut shell particle, 6 parts of citric acid, 6 parts of sodium bicarbonate, 7 parts of sodium carboxymethylcellulose, 7 parts of medical stone powder；
The particle diameter distribution ratio of the walnut shell particle are as follows: cross 8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:
2；The water content of the walnut shell particle is 9%；
2. the preparation method of above-mentioned non-agglomerated type cat litter, comprising the following steps:
(1) walnut shell is crushed, is sieved, controlling its water content is 9%, the particle diameter distribution ratio of obtained walnut shell particle are as follows: mistake
8-14 mesh: cross 14-20 mesh: crossing 20-100 mesh is 1:1:2；
(2) citric acid, sodium bicarbonate, sodium carboxymethylcellulose, medical stone powder are mixed, adds the walnut that step (1) obtains
Shell particle, is stirred；
(3) 300 DEG C, compression ratio be 1:6 under conditions of, pelletized using biomass granulation machine, then crushed with pair roller type
Machine crushes the particle that granulation obtains, and crosses 3-20 mesh.
Performance detection
The detection of one, water absorbing properties
1. absorption speed detects
The cat litter for taking phase homogenous quantities takes distilled water, physiological saline, urea/normal saline solution of 1% mass concentration, fresh cat urine
Cat litter is acted on, observation liquid blots the time used, the results are shown in Table 1, wherein the volume of each liquid is all 50mL, cat litter matter
It measures identical, is all 100g；
1 absorption speed test result of table (time: s)
2. water absorption rate detects
Jolt ramming product is measured to scale with 100mL straight graduated cylinder, is poured into 200 the polished standard screens, is weighed as M1, soak 15min
Afterwards, it is weighed as M2, then, water absorption rate=(M2-M1) ÷ M1(unit: g/g), water absorption rate the results are shown in Table 2.
2 water absorption rate result (g/g) of table
Two, use the time
3kg cat litter provided by the invention is taken, for 4 cat normal uses, after 10 days, cat litter reaches saturation, after saturation, by cat
Sand naturally dry, moreover it is possible to Reusability 9-10 times (every time 10 days), lose 5-6g every time, and in use process, odorless removes
Smelly ability is good；
Under similarity condition, the 3kg cat litter of comparative example is taken, for 4 cat normal uses, after 2 days, cat litter reaches saturation, satisfies
With it is rear, cat litter is dried, moreover it is possible to continue to use 2-3 times (every time 2 days)；
It can be seen that cat litter provided by the invention, the water saturation time is long, it is reusable often, cat litter can be saved, at least can
Using 3 months, loss was few, and good deodorization effect；When without adding Diaphragma juglandis, the water saturation time of cat litter is obviously shortened, weight
Multiple access times degradation.
Claims (7)
1. a kind of non-agglomerated type cat litter, it is characterised in that: be made of the raw material of following parts by weight:
80-100 parts of walnut shell particle, 5-12 parts of wood powder of diverting one's attention, 2-7 parts of citric acid, 3-8 parts of sodium bicarbonate, carboxymethyl cellulose
4-9 parts of sodium, 4-10 parts of medical stone powder；
Wherein, the water content of the walnut shell particle is 8-10%,
The wood powder of diverting one's attention is obtained by following pretreatment: Diaphragma juglandis is added to the water according to solid-liquid ratio 1g:0.3L,
30-50min is decocted at 100 DEG C, is cooled to room temperature, the mushroom liquor with the water phase same volume is then added, continues to impregnate 4-5h,
Then it is ultrasonically treated 15-25min, is filtered, it is 8-10% that filter residue, which is dried under vacuum to water content, is crushed.
2. non-agglomerated type cat litter according to claim 1, it is characterised in that: the particle diameter distribution ratio of the walnut shell particle
Are as follows: cross 8-14 mesh: crossing 14-20 mesh: crossing 20-100 mesh is 1:1:(2-3).
3. non-agglomerated type cat litter according to claim 1, it is characterised in that: the particle diameter distribution ratio of the wood powder of diverting one's attention are as follows:
Cross 8-14 mesh: crossing 14-20 mesh: crossing 20-100 mesh is 1:1:(2-3).
4. non-agglomerated type cat litter according to claim 1, it is characterised in that: the mushroom liquor is to be prepared by the following method
It arrives: dried thin mushroom is mixed according to mass ratio 1:3000 with water, after impregnating 1h, decoct 2h, then filter, filter residue is spare, gained
Filtrate is cooled to room temperature, as mushroom liquor.
5. non-agglomerated type cat litter according to claim 1, it is characterised in that: the condition of the ultrasonic treatment are as follows: ultrasonic power
400W, supersonic frequency 40KHz.
6. non-agglomerated type cat litter according to claim 1, it is characterised in that: the vacuum drying condition are as follows: at 45-60 DEG C
Lower vacuum drying.
7. the preparation method of non-agglomerated type cat litter described in claim 1, it is characterised in that: the following steps are included:
(1) Diaphragma juglandis is pre-processed, wood powder of diverting one's attention is prepared；
(2) walnut shell is crushed, is sieved, controlling its water content is 8-10%, obtains walnut shell particle；
(3) citric acid, sodium bicarbonate, sodium carboxymethylcellulose, medical stone powder are mixed, adds walnut shell particle and Diaphragma juglandis
Powder is stirred；
(4) 300 DEG C, compression ratio be 1:6 under conditions of pelletize, then with pair roller pulverizer by the obtained particle of granulation
It is crushed, crosses 3-20 mesh.
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