CN109077985A - Skin care compositions and its application - Google Patents

Skin care compositions and its application Download PDF

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Publication number
CN109077985A
CN109077985A CN201811339124.7A CN201811339124A CN109077985A CN 109077985 A CN109077985 A CN 109077985A CN 201811339124 A CN201811339124 A CN 201811339124A CN 109077985 A CN109077985 A CN 109077985A
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Prior art keywords
extract
skin care
care compositions
facial mask
water
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CN109077985B (en
Inventor
丘卓秋
孙娟娟
赵美贺
谢水林
魏坤
王晓慧
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GUANGZHOU RUI SEN BIOTECHNOLOGY Co Ltd
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GUANGZHOU RUI SEN BIOTECHNOLOGY Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to a kind of skin care compositions and its applications.The skin care compositions includes each component of following weight content: 2%~4% kudzu root extract, 0.8%~1.2% osbeckia extract, 0.4%~1.2% Herba Agrimoniae extract, 0.3%~1.2% Rhizoma Smilacis Glabrae extract, 0.5%~1.5% wild marjoram grass extract, 3%~10% glycerol, 2%~8% butanediol, 0.2%~0.8% Sodium Hyaluronate, 0.01%~0.3% xanthan gum, 1%~3% glycerin polyether -26,0.4%~1.5% panthenol, 0.1%~0.3% allantoin, surplus are water.The skin care formula is as facial mask essence, it is not only safe and non-stimulating, there is good moisturizing, crease-resistant, white-skinned face function, it is important to, the skin care formula -10 DEG C and 42 DEG C at a temperature of can keep uniform, not stratified state for a long time, that is, there is extraordinary stability.

Description

Skin care compositions and its application
Technical field
The present invention relates to daily skin care fields, more particularly to a kind of skin care compositions and its application.
Background technique
In recent years, with the raising of the change of consumption idea and the level of consumption, people urgently thirst for being promoted the beauty of oneself Product consumption class pursues emphatically high-grade cosmetics to oneself bring " healthy beauty ".Therefore, day in the market So, green, safe and without side-effects functional cosmetics increasingly by the favor of consumers, and medicine skin care item with Its unique safety and non-sensitization, become the main force of natural cosmetics, therefore, the development of China's medicine skin care item industry " imperative ".Nowadays, China's medicine skin care item industry is gradually developed, and all kinds of medicine skin care item products are such as on the market It emerges rapidly in large numbersBamboo shoots after a spring rain, it is dripping to meet the eye on every side.But it cannot still come to a halt in the exploration of medicine skin care item industry.
Pueraria lobata is known as the good reputation of " asia ginseng ", and often feeding pueraria lobata, kudzu-vine root powder, Gegen tablets and Au nanoring balsam pear slice etc. are adjustable Function of human body is built up health, and body resistance against diseases, postpone aging and prolong life, vigor of remaining youthful forever are improved.Pueraria lobata removes carbon water rich in Except compound and the nutritional ingredients such as amino acid needed by human and mineral element, also containing isoflavone compound and less The Flavonoid substances of amount.Wherein, daidzein, daidzin, Puerarin are the main actives of pueraria lobata, especially with puerarin content Highest.Pueraria lobata has antitumor, improvement islet function, treatment cardiovascular disease, adjusts blood lipid metabolism, removes the function such as free radical Effect, nowadays pueraria lobata is widely applied in industries such as food, drug, health care products.
Although with kudzu root extract prepare facial mask liquid it has been reported that for example, prior art discloses facial mask use face Film liquid includes consisting of ingredient root of kudzu vine extract, snail extract, glycerol, snake oil, thermal water, pearl powder, grape pip extraction Liquid, fish-skin extracting solution, bird's nest extracting solution, honey, Yoghourt, cocounut oil, mulberry, extract solution from aloe, amino acid, AHA, black bearberry Element, vitamin E oil, vitamin B6, tremella extract, egg white and tea polyphenols.For another example pueraria lobata face disclosed in the prior art Film, the component of used facial mask liquid include kudzu root extract, composite vegetables extractive, propylene glycol, glycerol, polyethylene glycol- 400, dipotassium glycyrrhizinate, tertiary sodium phosphate, sodium alginate, Acritamer 940, Sodium Hyaluronate, glycine betaine and water.Although existing pueraria lobata The facial mask liquid of extract preparation whitening, moisturizing moisturizing, in terms of played certain effect, but with kudzu root extract It is temperature sensitive for the facial mask essence of effective component, it is particularly easy to be layered, influences very much the performance of skin effect.
It would therefore be highly desirable to provide a kind of heatproof, stable skin care compositions.
Summary of the invention
Based on this, the main object of the present invention is to provide a kind of heatproof, stable skin care compositions.The skin care compositions In use, it under -10 DEG C, 42 DEG C of environment temperatures, still can be good at keeping uniform state, it is existing not occur layering As.
The purpose of the present invention is what is be achieved through the following technical solutions:
A kind of skin care compositions, the skin care compositions include each component of following weight content: 2%~4% pueraria lobata extracts Object, 0.8%~1.2% osbeckia extract, 0.4%~1.2% Herba Agrimoniae extract, 0.3%~1.2% smilax extract Object, 0.5%~1.5% wild marjoram grass extract, 3%~10% glycerol, 2%~8% butanediol, 0.2%~0.8% hyaluronic acid Sodium, 0.01%~0.3% xanthan gum, 1%~3% glycerin polyether -26,0.4%~1.5% panthenol, 0.1%~0.3% allantois Element, surplus are water.
In wherein some embodiments, which includes each component of following weight content: 2%~4% pueraria lobata Extract, 0.8%~1.2% osbeckia extract, 0.4%~1.2% Herba Agrimoniae extract, 0.3%~1.2% smilax mention Take object, 0.5%~1.5% wild marjoram grass extract, 4%~8% glycerol, 5%~8% butanediol, 0.2%~0.5% hyalomitome Sour sodium, 0.01%~0.1% xanthan gum, 1%~2% glycerin polyether -26,1%~1.5% panthenol, 0.1%~0.3% allantois Element, surplus are water.
In wherein some embodiments, which includes each component of following weight content: 2.5%~4% Pueraria lobota Root extract, 0.8%~1.2% osbeckia extract, 1%~1.2% Herba Agrimoniae extract, 0.3%~1% smilax extract Object, 0.6%~1.2% wild marjoram grass extract, 4%~8% glycerol, 5%~8% butanediol, 0.2%~0.5% hyaluronic acid Sodium, 0.01%~0.1% xanthan gum, 1%~2% glycerin polyether -26,1%~1.5% panthenol, 0.1%~0.3% allantoin, Surplus is water.
In wherein some embodiments, which includes each component of following weight content: 3%~4% pueraria lobata Extract, 0.8%~1.2% osbeckia extract, 1%~1.2% Herba Agrimoniae extract, 0.8%~1% smilax extract Object, 0.8~1.2% wild marjoram grass extract, 4%~8% glycerol, 5%~8% butanediol, 0.2%~0.5% Sodium Hyaluronate, 0.01%~0.1% xanthan gum, 1%~2% glycerin polyether -26,1%~1.5% panthenol, 0.1%~0.3% allantoin are remaining Amount is water.
In wherein some embodiments, which includes each component of following weight content: 3% pueraria lobata extracts Object, 1% osbeckia extract, 1.2% Herba Agrimoniae extract, 1% Rhizoma Smilacis Glabrae extract, 0.8% wild marjoram grass extract, 5% is sweet Oil, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26,1.4% panthenol, 0.1% urine Bursin, surplus are water.
In wherein some embodiments, which includes each component of following weight content: 2%~2.5% Pueraria lobota Root extract, 0.8%~1% osbeckia extract, 0.8%~1% Herba Agrimoniae extract, 0.3%~1% smilax extract Object, 0.6%~1% wild marjoram grass extract, 4%~8% glycerol, 5%~8% butanediol, 0.2%~0.5% Sodium Hyaluronate, 0.01%~0.1% xanthan gum, 1%~2% glycerin polyether -26,1%~1.5% panthenol, 0.1%~0.3% allantoin are remaining Amount is water.
In wherein some embodiments, which includes each component of following weight content: 2% pueraria lobata extracts Object, 1% osbeckia extract, 1% Herba Agrimoniae extract, 1% Rhizoma Smilacis Glabrae extract, 1% wild marjoram grass extract, 5% glycerol, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26,1.4% panthenol, 0.1% allantois Element, surplus are water.
It is a further object of the present invention to provide a kind of above-mentioned skin care compositions to prepare the use in facial mask as Essence On the way.
A further object of the invention is to provide a kind of facial mask, and the Essence of the facial mask uses above-mentioned skin care compositions.
In wherein some embodiments, the facial mask cloth of the facial mask be by pueraria lobata fiber, silk fiber is blended forms.
Compared with prior art, the present invention have it is following the utility model has the advantages that
The present invention is by suitable kudzu root extract and osbeckia extract, Herba Agrimoniae extract, Rhizoma Smilacis Glabrae extract, wild marjoram The collocation of careless extract, then with glycerol, butanediol, Sodium Hyaluronate, xanthan gum, glycerin polyether -26, panthenol, allantoin, water one It rises and constitutes skin care formula.The skin care formula is not only safe and non-stimulating, has good moisturizing, crease-resistant, white-skinned face function, which matches Side also down to -10 DEG C and up to 42 DEG C at a temperature of can keep uniform, not stratified state for a long time, i.e., with extraordinary Stability.The skin care formula can be used as facial mask essence.
Detailed description of the invention
Fig. 1 is figure compared with 1 facial mask of embodiment is averaged white-skinned face function with bare substrate facial mask.
Specific embodiment
It to facilitate the understanding of the present invention, below will be to invention is more fully described.But the present invention can be to be permitted Mostly different form is realized, however it is not limited to embodiment described herein.On the contrary, purpose of providing these embodiments is makes It is more thorough and comprehensive to the understanding of the disclosure.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term as used herein "and/or" includes one or more phases Any and all combinations of the listed item of pass.
In skin care compositions provided by the invention:
(1) kudzu root extract contains the ultra-oxygen anion free radical (O that can remove skin surface2), hydroxyl free Base (OH), 1,1- diphenyl -2- phenyl radical (DPPH) etc. have very strong in vitro anti-oxidation.Kudzu root extract With the anti-ageing wrinkle-dispelling function of whitening.(2) contain agrimonine, agrimonolide containing herb in Herba Agrimoniae extract (Agrimonolide), tannin and volatile oil etc..The present invention mainly applies the tannin that condensed type tan shortcake can be generated in hairyvein agrimony, should Ingredient can make protein coagulating and the intracorporal plasmic solidification of microorganism in exudate after wound, therefore can form scab film, Reducing secretion can prevent infected with bacteriostasis again.The tannin has stronger reproducibility, and it is free can to remove the intracorporal super oxygen of biology Base delays senescence.(3) the full extract of smilax significantly inhibits effect to pseudomonad, staphylococcus aureus etc., can play It releives antiallergic and other effects.(4) wild marjoram grass extract can eliminate pruitus and oedema phenomenon.(5) it is separated in osbeckia To matter quercetin, Kaempferol and their three kinds of two compounds of sugar, have compared with strong anti-oxidation etc..
Extract of the invention is prepared by conventional Supercritical extraction process.Supercritical extraction (supercritical fluid exatration, SPE), with supercritical fluid replace conventional organic solvent to it is important effectively at Divide the new separation technology for extracting separation, wherein supercritical fluid refers to that temperature is more than critical-temperature, and pressure is more than critical The dense fluids of pressure.At this moment fluid with and liquid similar in density and there is very strong solvability, while also having Have and is similar to and the characteristics such as high diffusibility, low viscosity, low surface tension similar in gas.The principle of this method are as follows: air pump will Stored good carbon dioxide pressurization, making carbon dioxide, in a supercritical state (critical pressure 7.38MPa, critical-temperature are 31.05℃).Extraction kettle is added in liquid CO 2 after pressurization, extraction kettle is the tank that solvent occurs that extraction is reacted with plant Body, liquid carbon dioxide has the fatty acid of plant, vegetable soda, ethers, ketone, glyceride etc. molten well in extraction kettle Solution effect, carbon dioxide just extract these substances of plant in supercriticality.After extracting these substances, liquid Carbon dioxide has been transported to separating still together with extract, and carbon dioxide is separated with extract there, titanium dioxide Carbon is retracted huge profit use, and extract, which is left, to be come.Extraction process flow: a certain amount of plant → supercritical CO is accurately weighed2Extraction Take → nitrogen evaporator drying (up to extract) → weighing → addition chromatographic ethanol → ultrasonic dissolution → brown volumetric flask in constant volume it is close Envelope → -18 DEG C of placement refrigerator saves.Wherein, the extraction conditions of kudzu root extract are as follows: under 38 DEG C of temperature, 40MPa pressure, extraction Shi Changwei 3h;The extraction conditions of Herba Agrimoniae extract are as follows: pressure 45.2MPa, 65 DEG C of temperature, extraction time 1.5h;Smilax mentions Take the extraction conditions of object and wild marjoram grass extract are as follows: pressure 35MPa, temperature 45 C, extraction time 1-2h;Osbeckia extract extraction Take condition are as follows: pressure 21MPa, 37 DEG C of temperature, extraction time 2.5h;And CO used above2Flow is 13kg/h.
Embodiment 1
The present embodiment provides a kind of skin care compositions and preparation method thereof, application.
The skin care compositions includes each component of weight content shown in table 1.
The preparation method of the skin care compositions includes:
(1) it is stocked up according to the formula of table 1, then mixes A phase, B phase, C phase shown in table 2, D phase, E phase:
A phase component include 74.04% water, 5% glycerol, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26;B phase component includes 2% kudzu root extract, 0.8% panthenol;C phase component includes 2% water, 0.6% general Alcohol;D phase component includes 2% water, 0.1% allantoin;E phase component include 1% osbeckia extract, 1% Herba Agrimoniae extract, 1% Rhizoma Smilacis Glabrae extract, 1% wild marjoram grass extract.
(2) preparation of skin care compositions:
Emulsion pot is added in A phase component, is heated to 85 DEG C, stirring and dissolving is complete;B is mixed uniformly, is added in emulsion pot, Matter is to uniformly without particle;C phase low-grade fever is uniformly mixed, and is added in emulsion pot, and homogeneous is to uniformly without particle, reservation;45 DEG C are cooled to, Low-grade fever is added and dissolves the transparent D phase mixed, stirs evenly;E phase each component is added, stirring is complete to dissolving.
The skin care compositions can be used as facial mask essence.By facial mask essence and facial mask cloth under sterilising conditions vacuum seal Bag can form facial mask.
The preparation of facial mask cloth that the present embodiment uses includes:
(1) pueraria lobata fiber extracts in radix puerariae waste residue: first cleaning radix puerariae waste residue repeatedly, washes off the shallow lake in radix puerariae waste residue Powder, by the step for after, in radix puerariae waste residue content it is highest be pectin, lignin and cellulose.Obtain cellulose, Ying Zhe Pectin and lignin are removed again.
With reference to a method for such as congruence, i.e., the pectin and lignin in oxidation boiling-off method removal radix puerariae waste residue need to be used, specifically Method is as follows: clean radix puerariae waste residue is placed in natural air drying at cleaning;Air-dried radix puerariae waste residue is put into dense equipped with 17.5g/L In the beaker of the hydrogen peroxide of the NaOH solution and 12g/L concentration of degree, bath raio (bath raio liquor ratio is textile dyeing and finishing term, Refer to the ratio of dip dyeing mode fabric and dye liquor.) it is 1:40, the kiering 3h in 95 DEG C of thermostat water bath;By the pueraria lobata after boiling-off Waste residue is cleaned, and impurity is removed, and drying (can be opened as congruent, 2011).
(2) prepared by facial mask cloth: the pueraria lobata fiber prepared being carried out by weaving loom with silk fiber blended, then is cut into Facial mask print, remembers.
Embodiment 2
The present embodiment provides a kind of skin care compositions and preparation method thereof, application.
The skin care compositions includes each component of weight content shown in table 1.
The preparation method of the skin care compositions includes:
(1) it is stocked up according to the formula of table 1, then mixes A phase, B phase, C phase shown in table 2, D phase, E phase:
A phase component include 73.04% water, 5% glycerol, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26;B phase component includes 3% kudzu root extract, 0.8% panthenol;C phase component includes: 2% water, 0.6% general Alcohol;D phase component includes 2% water, 0.1% allantoin;E phase component include 1% osbeckia extract, 1.2% Herba Agrimoniae extract, 1% Rhizoma Smilacis Glabrae extract, 0.8% wild marjoram grass extract.
(2) preparation of skin care compositions:
Emulsion pot is added in A phase component, is heated to 85 DEG C, stirring and dissolving is complete;B is mixed uniformly, is added in emulsion pot, Matter is to uniformly without particle;C phase low-grade fever is uniformly mixed, and is added in emulsion pot, and homogeneous is to uniformly without particle, reservation;45 DEG C are cooled to, Low-grade fever is added and dissolves the transparent D phase mixed, stirs evenly;E phase each component is added, stirring is complete to dissolving.
The skin care compositions can be used as facial mask essence.By facial mask essence and facial mask cloth under sterilising conditions vacuum seal Bag can form facial mask.The preparation of facial mask cloth is the same as embodiment 1.
Embodiment 3
The present embodiment provides a kind of skin care compositions and preparation method thereof, application.
The skin care compositions includes each component of weight content shown in table 1.
The preparation method of the skin care compositions includes:
(1) it is stocked up according to the formula of table 1, then mixes A phase, B phase, C phase shown in table 2, D phase, E phase:
A phase component include 71.84% water, 5% glycerol, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26;B phase component includes 4% kudzu root extract, 0.8% panthenol;C phase component includes 2% water, 0.6% general Alcohol;D phase component includes 2% water, 0.1% allantoin;E phase component includes 1.2% osbeckia extract, the extraction of 1.2% hairyvein agrimony Object, 0.8% Rhizoma Smilacis Glabrae extract, 1% wild marjoram grass extract.
(2) preparation of skin care compositions:
Emulsion pot is added in A phase component, is heated to 85 DEG C, stirring and dissolving is complete;B is mixed uniformly, is added in emulsion pot, Matter is to uniformly without particle;C phase low-grade fever is uniformly mixed, and is added in emulsion pot, and homogeneous is to uniformly without particle, reservation;45 DEG C are cooled to, Low-grade fever is added and dissolves the transparent D phase mixed, stirs evenly;E phase each component is added, stirring is complete to dissolving.
The skin care compositions can be used as facial mask essence.By facial mask essence and facial mask cloth under sterilising conditions vacuum seal Bag can form facial mask.The preparation of facial mask cloth is the same as embodiment 1.
Embodiment 4
The present embodiment provides a kind of skin care compositions and preparation method thereof, application.
The skin care compositions includes each component of weight content shown in table 1.
The preparation method of the skin care compositions includes:
(1) it is stocked up according to the formula of table 1, then mixes A phase, B phase, C phase shown in table 2, D phase, E phase:
A phase component include 72.04% water, 5% glycerol, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26;B phase component includes 4% kudzu root extract, 0.8% panthenol;C phase component includes 2% water, 0.6% general Alcohol;D phase component includes 2% water, 0.1% allantoin;E phase component include 0.8% osbeckia extract, 1% Herba Agrimoniae extract, 1% Rhizoma Smilacis Glabrae extract, 1.2% wild marjoram grass extract.
(2) preparation of skin care compositions:
Emulsion pot is added in A phase component, is heated to 85 DEG C, stirring and dissolving is complete;B is mixed uniformly, is added in emulsion pot, Matter is to uniformly without particle;C phase low-grade fever is uniformly mixed, and is added in emulsion pot, and homogeneous is to uniformly without particle, reservation;45 DEG C are cooled to, Low-grade fever is added and dissolves the transparent D phase mixed, stirs evenly;E phase each component is added, stirring is complete to dissolving.
The skin care compositions can be used as facial mask essence.By facial mask essence and facial mask cloth under sterilising conditions vacuum seal Bag can form facial mask.The preparation of facial mask cloth is the same as embodiment 1.
Embodiment 5
The present embodiment provides a kind of skin care compositions and preparation method thereof, application.
The skin care compositions includes each component of weight content shown in table 1.
The preparation method of the skin care compositions includes:
(1) it is stocked up according to the formula of table 1, then mixes A phase, B phase, C phase shown in table 2, D phase, E phase:
A phase component include: 74.84% water, 5% glycerol, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26;B phase component includes: 2.5% kudzu root extract, 0.8% panthenol;C phase component include: 2% water, 0.6% panthenol;D phase component includes: 2% water, 0.1% allantoin;E phase component includes: 0.8% osbeckia extract, 1% red crowned crane Careless extract, 0.3% Rhizoma Smilacis Glabrae extract, 0.6% wild marjoram grass extract.
(2) preparation of skin care compositions:
Emulsion pot is added in A phase component, is heated to 85 DEG C, stirring and dissolving is complete;B is mixed uniformly, is added in emulsion pot, Matter is to uniformly without particle;C phase low-grade fever is uniformly mixed, and is added in emulsion pot, and homogeneous is to uniformly without particle, reservation;45 DEG C are cooled to, Low-grade fever is added and dissolves the transparent D phase mixed, stirs evenly;E phase each component is added, stirring is complete to dissolving.
The skin care compositions can be used as facial mask essence.By facial mask essence and facial mask cloth under sterilising conditions vacuum seal Bag can form facial mask.The preparation of facial mask cloth is the same as embodiment 1.
Embodiment 6
The present embodiment is the change case of embodiment 1, and variation place essentially consists in the formula of skin care compositions, the present embodiment shield The formula of skin composition is as follows: 2% kudzu root extract, 0.8% osbeckia extract, 0.4% Herba Agrimoniae extract, 0.3% soil Tuckahoe extracts, 0.5% wild marjoram grass extract, 3% glycerol, 2% butanediol, 0.2% Sodium Hyaluronate, 0.01% xanthan gum, 1% glycerin polyether -26,0.4% panthenol, 0.1% allantoin, surplus are water.
Embodiment 7
The present embodiment is the change case of embodiment 1, and variation place essentially consists in the formula of skin care compositions, the present embodiment shield The formula of skin composition is as follows: 4% kudzu root extract, 1.2% osbeckia extract, 1.2% Herba Agrimoniae extract, 1.2% soil Tuckahoe extracts, 1.5% wild marjoram grass extract, 10% glycerol, 8% butanediol, 0.8% Sodium Hyaluronate, 0.3% xanthan gum, 3% glycerin polyether -26,1.5% panthenol, 0.3% allantoin, surplus are water.
Comparative example 1
This comparative example provides a kind of skin care compositions and preparation method thereof, application.
The skin care compositions includes each component of weight content shown in table 1.This comparative formulation is main with embodiment 1 Difference is without containing kudzu root extract.
The preparation method of the skin care compositions includes:
(1) it is stocked up according to the formula of table 1, then mixes A phase, B phase, C phase shown in table 2, D phase, E phase:
A phase component include: 74.04% water, 5% glycerol, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26;B phase component includes: 2% water, 0.8% panthenol;C phase component includes: 2% water, 0.6% panthenol;D phase Component includes: 2% water, 0.1% allantoin;E phase component includes: 1% osbeckia extract, 1% Herba Agrimoniae extract, 1% soil Tuckahoe extracts, 1% wild marjoram grass extract.
(2) preparation of skin care compositions:
Emulsion pot is added in A phase component, is heated to 85 DEG C, stirring and dissolving is complete;B is mixed uniformly, is added in emulsion pot, Matter is to uniformly without particle;C phase low-grade fever is uniformly mixed, and is added in emulsion pot, and homogeneous is to uniformly without particle, reservation;45 DEG C are cooled to, Low-grade fever is added and dissolves the transparent D phase mixed, stirs evenly;E phase each component is added, stirring is complete to dissolving.
The skin care compositions can be used as facial mask essence.By facial mask essence and facial mask cloth under sterilising conditions vacuum seal Bag can form facial mask.The preparation of facial mask cloth is the same as embodiment 1.
Comparative example 2
This comparative example provides a kind of skin care compositions and preparation method thereof, application.
The skin care compositions includes each component of weight content shown in table 1.This comparative formulation is main with embodiment 1 Difference includes that the weight content of kudzu root extract is 5%, i.e. the content of kudzu root extract has exceeded the framework of the present definition.
The preparation method of the skin care compositions includes:
(1) it is stocked up according to the formula of table 1, then mixes A phase, B phase, C phase shown in table 2, D phase, E phase:
A phase component include: 71.04% water, 5% glycerol, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26;B phase component includes: 5% kudzu root extract, 0.8% panthenol;C phase component includes: 2% water, 0.6% Panthenol;D phase component includes: 2% water, 0.1% allantoin;E phase component includes: 1% osbeckia extract, the extraction of 1% hairyvein agrimony Object, 1% Rhizoma Smilacis Glabrae extract, 1% wild marjoram grass extract.
(2) preparation of skin care compositions:
Emulsion pot is added in A phase component, is heated to 85 DEG C, stirring and dissolving is complete;B is mixed uniformly, is added in emulsion pot, Matter is to uniformly without particle;C phase low-grade fever is uniformly mixed, and is added in emulsion pot, and homogeneous is to uniformly without particle, reservation;45 DEG C are cooled to, Low-grade fever is added and dissolves the transparent D phase mixed, stirs evenly;E phase each component is added, stirring is complete to dissolving.
The skin care compositions can be used as facial mask essence.By facial mask essence and facial mask cloth under sterilising conditions vacuum seal Bag can form facial mask.The preparation of facial mask cloth is the same as embodiment 1.
Comparative example 3
This comparative example is the comparative example of embodiment 1, compared with Example 1, the main distinction be do not add osbeckia extract, Herba Agrimoniae extract, Rhizoma Smilacis Glabrae extract, wild marjoram grass extract and contain 6% kudzu root extract.The preparation of facial mask cloth is the same as real Apply example 1.
Table 1
Table 2
Performance test
(1) stability test
Heat resistance test: 10 embodiments, 1 gained facial mask essence sample is taken, the test tube of 20mm × 120mm is respectively charged into It is interior, clean rubber plug beyond the Great Wall.5 test tubes are placed in and are pre-adjusted to 42 DEG C of constant incubator, in addition 5 are placed in room temperature (25 DEG C) compare, and irregularly observe, compare.Referring to the heat resistance test method of embodiment 1, testing example 2 to embodiment 7, the sample of comparative example 1 to 4.Count the processing and control not being layered.
Cold resistance test: 10 embodiments, 1 gained facial mask essence sample is taken, the examination of branch 20mm × 120mm is respectively charged into In pipe, clean rubber plug beyond the Great Wall.5 test tubes are placed in and are pre-adjusted to -10 DEG C of refrigerator, in addition 5 are placed in room temperature (25 DEG C), it irregularly observes, compare.Referring to the heat resistance test method of embodiment 1, testing example 2 to embodiment 7, comparative example 1 To 4 sample.
As a result referring to the following table 3.Table 3
According to table 3, the sample of embodiment 1 to 7, room temperature, heat, it is cold under the conditions of can keep uniform, no for a long time The system of layering.In the sample of embodiment 1 to 7, the overall effect of 2 sample of embodiment is better than 3,4,5 sample of embodiment, implements The stablizing effect of 3,4,5 sample of example is better than embodiment 1 and embodiment 6,7 samples.Therefore, skincare composition composition formula of the present invention is deposited In preferred scheme.For embodiment sample, the stability of 1 to 4 sample of comparative example is poor, with the propulsion of time, It is more and more to there are the sample quantities being layered.This explanation, kudzu root extract and its additive amount and kudzu root extract are mentioned with other Take the cooperation of object most important for stablizing for formula.
(2) moisture-keeping efficacy is tested
For every sample, select 50 female volunteers of the age bracket between 20 years old~50 years old as study subject, And the skin type of study subject is dry skin.Subject is divided into 5 groups, every group of 10 people.Test the previous day subject is not Any skin-protection product or cleaning product can be used in recipient site.
Test starts the inboard arm skin area progress that preceding 0.5 hour need to use moisture of skin tester to subject Moisture content of skin test, each region duplicate measurements 5 times, and corresponding data is recorded, as blank control.
Facial mask essence is applied to inboard arm, and test point region is 3 × 3cm, the amount for being coated with Essence is 25 μ L.By Examination person need to be 23 DEG C~25 DEG C in temperature, and humidity carries out under conditions of being 50%~60%.It is tested after coating using moisture of skin Instrument and the lost instrument of moisture of skin measure tested region, each region duplicate measurements 5 times, and record corresponding data.
The results are shown in Table 4, and 5 specific embodiments all have good moisture-keeping efficacy, and 1 moisture-keeping efficacy of specific embodiment Relatively preferably.
4 skin moisture content of table compares
(3) Product Safety is evaluated
Human skin pastes patch test: choosing volunteer's conduct without skin allergy history that 60 age brackets are 25 years old~50 years old Study subject.And subject is randomly divided into 6 groups, every group of 10 people.Everyone distributes 1 mask product of specific embodiment at random, in phase Patch patch test is carried out under the conditions of same closed environment, i.e., facial mask is pasted on to the side at the back of subject, then other side conduct Control zone removed facial mask, and carries out the cleaning of patch portion after 15 minutes, respectively at 0.5,1,3,5,10,24,48 hour observation skin Reaction, and recorded according to 5 dermoreaction grade of table.
5 patch test skin adverse reaction grading standard of table
Skin adverse reaction Grade
It is reactionless 0
Light red spot 1
Erythema, infiltration, papule 2
Erythema, oedema, papule, blister 3
Erythema, oedema, bleb 4
Test result: human skin paste spot the experimental results showed that, the patch spot that each group subject passes through different embodiment facial masks Test, embodiment and comparative example product is the adverse reaction for observing skin after 0.5,1,3,5,10,24,48 hour, is said Bright mask product of the present invention has safety and nonirritant.It is surveyed using facial mask of the same method to embodiment 2 to 7 Examination, it is as a result and safe, nonirritant.
(4) crease-resistant efficacy assessments
Temperature be 24 DEG C~26 DEG C, humidity be 50%~60% opposite stable environment under the conditions of, to 35 35 years old~ 50 years old female volunteers are tested.I.e. subject uses 1 mask product of embodiment in face side, and produces using facial mask After product, observation in 8 weeks by a definite date is carried out to subject using DermaTOP, (VISIOD-3D is quick without using mask product for the other side Imaging method: skin instant imaging analysis system DermaTOP uses fringe projection measuring technique, is passed by head and Liang Ge ear Sensor once positions, the secondary positioning of facial laser, camera intake image, three-dimensional cutaneous fast imaging and computer disposal image Obtain wrinkle index.) can be obtained by wrinkle index, it is average up to 50% using side face wrinkles' depth reduced rate of facial mask, and Other side face wrinkles' depth reduced rate average out to 28%.Therefore, which has effects that crease-resistant.After tested, embodiment 2 Similarly have effects that 7 sample of embodiment crease-resistant.
(5) white-skinned face function is evaluated
It selects the left and right arm of 80 subjects as tested region, Multi-functional skin test macro is used by technical staff And skin test probe MPA9 (German CK company) carries out initial value data acquisition.In the tested region cleaned by clear water, Respectively use bare substrate facial mask and 1 sample facial mask of embodiment primary in corresponding region sooner or later daily, it may be noted that dduring test not Other any products can be used in test zone.Continuous 8 weeks routine observations and test are carried out to subject, and record dependency number According to.Record data can be obtained by statistical analysis as shown in Figure 1, the mask product that can obtain specific embodiment 1 has preferable beauty Contour painting effect.After tested, embodiment 2 to 7 sample of embodiment similarly has white-skinned face function.
In conclusion the present invention mentions suitable kudzu root extract and osbeckia extract, Herba Agrimoniae extract, smilax Take object, wild marjoram grass extract collocation, then with glycerol, butanediol, Sodium Hyaluronate, xanthan gum, glycerin polyether -26, panthenol, urine Bursin, water constitute skin care formula together.The skin care formula is not only safe and non-stimulating, has good moisturizing, crease-resistant, whitening function Effect, the skin care formula also down to -10 DEG C and up to 42 DEG C at a temperature of can keep uniform, not stratified state for a long time, i.e., With extraordinary stability.The skin care formula can be used as facial mask essence.
Each technical characteristic of embodiment described above can be combined arbitrarily, for simplicity of description, not to above-mentioned reality It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited In contradiction, all should be considered as described in this specification.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.

Claims (10)

1. a kind of skin care compositions, which is characterized in that the skin care compositions includes each component of following weight content: 2%~4% Kudzu root extract, 0.8%~1.2% osbeckia extract, 0.4%~1.2% Herba Agrimoniae extract, 0.3%~1.2% soil Fu Siberian cocklebur extract, 0.5%~1.5% wild marjoram grass extract, 3%~10% glycerol, 2%~8% butanediol, 0.2%~0.8% thoroughly Bright matter acid sodium, 0.01%~0.3% xanthan gum, 1%~3% glycerin polyether -26,0.4%~1.5% panthenol, 0.1%~ 0.3% allantoin, surplus are water.
2. skin care compositions according to claim 1, which is characterized in that the skin care compositions includes following weight content Each component: 2%~4% kudzu root extract, 0.8%~1.2% osbeckia extract, 0.4%~1.2% Herba Agrimoniae extract, 0.3%~1.2% Rhizoma Smilacis Glabrae extract, 0.5%~1.5% wild marjoram grass extract, 4%~8% glycerol, 5%~8% fourth two Alcohol, 0.2%~0.5% Sodium Hyaluronate, 0.01%~0.1% xanthan gum, 1%~2% glycerin polyether -26,1%~1.5% Panthenol, 0.1%~0.3% allantoin, surplus are water.
3. skin care compositions according to claim 2, which is characterized in that the skin care compositions includes following weight content Each component: 2.5%~4% kudzu root extract, 0.8%~1.2% osbeckia extract, 1%~1.2% Herba Agrimoniae extract, 0.3%~1% Rhizoma Smilacis Glabrae extract, 0.6%~1.2% wild marjoram grass extract, 4%~8% glycerol, 5%~8% butanediol, 0.2%~0.5% Sodium Hyaluronate, 0.01%~0.1% xanthan gum, 1%~2% glycerin polyether -26,1%~1.5% are general Alcohol, 0.1%~0.3% allantoin, surplus are water.
4. skin care compositions according to claim 3, which is characterized in that the skin care compositions includes following weight content Each component: 3%~4% kudzu root extract, 0.8%~1.2% osbeckia extract, 1%~1.2% Herba Agrimoniae extract, 0.8%~1% Rhizoma Smilacis Glabrae extract, 0.8~1.2% wild marjoram grass extract, 4%~8% glycerol, 5%~8% butanediol, 0.2%~0.5% Sodium Hyaluronate, 0.01%~0.1% xanthan gum, 1%~2% glycerin polyether -26,1%~1.5% are general Alcohol, 0.1%~0.3% allantoin, surplus are water.
5. skin care compositions according to claim 4, which is characterized in that the skin care compositions includes following weight content Each component: 3% kudzu root extract, 1% osbeckia extract, 1.2% Herba Agrimoniae extract, 1% Rhizoma Smilacis Glabrae extract, 0.8% Wild marjoram grass extract, 5% glycerol, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26, 1.4% panthenol, 0.1% allantoin, surplus are water.
6. skin care compositions according to claim 1 or 2, which is characterized in that the skin care compositions includes that following weight contains The each component of amount: 2%~2.5% kudzu root extract, 0.8%~1% osbeckia extract, 0.8%~1% hairyvein agrimony are extracted Object, 0.3%~1% Rhizoma Smilacis Glabrae extract, 0.6%~1% wild marjoram grass extract, 4%~8% glycerol, 5%~8% butanediol, 0.2%~0.5% Sodium Hyaluronate, 0.01%~0.1% xanthan gum, 1%~2% glycerin polyether -26,1%~1.5% are general Alcohol, 0.1%~0.3% allantoin, surplus are water.
7. skin care compositions according to claim 6, which is characterized in that the skin care compositions includes following weight content Each component: 2% kudzu root extract, 1% osbeckia extract, 1% Herba Agrimoniae extract, 1% Rhizoma Smilacis Glabrae extract, 1% wild marjoram Careless extract, 5% glycerol, 8% butanediol, 0.2% Sodium Hyaluronate, 0.06% xanthan gum, 1.2% glycerin polyether -26, 1.4% panthenol, 0.1% allantoin, surplus are water.
8. the described in any item skin care compositions of claim 1 to 7 are preparing the purposes in facial mask as Essence.
9. a kind of facial mask, which is characterized in that the Essence of the facial mask uses the described in any item skin care groups of claim 1 to 7 Close object.
10. facial mask according to claim 9, which is characterized in that the facial mask cloth of the facial mask is by pueraria lobata fiber, silk fibroin Tie up blended form.
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CN113995701A (en) * 2021-11-06 2022-02-01 马丙生 Composition for removing acne and acne marks and preparation method and application thereof
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