CN109020478A - A kind of preparation method of lightweight Over-summer cultivation carcass and its injecting paste material and the injecting paste material - Google Patents
A kind of preparation method of lightweight Over-summer cultivation carcass and its injecting paste material and the injecting paste material Download PDFInfo
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- CN109020478A CN109020478A CN201810883917.9A CN201810883917A CN109020478A CN 109020478 A CN109020478 A CN 109020478A CN 201810883917 A CN201810883917 A CN 201810883917A CN 109020478 A CN109020478 A CN 109020478A
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/131—Inorganic additives
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/1305—Organic additives
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/28—Slip casting
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/77—Density
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
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Abstract
The invention discloses the preparation methods of a kind of lightweight Over-summer cultivation carcass and its injecting paste material and the injecting paste material.According to parts by weight, which is made of 40-60 parts of Over-summer cultivation carcass blanks, 4-16 parts of hard hollow spheres, 0.2-0.5 parts of sodium humates and 30-35 parts of water.Since hard hollow sphere is suitable with the density of injecting paste material, the viscosity of injecting paste material is larger simultaneously, even if the density of hard hollow sphere and injecting paste material is deviated, floating or sinking tendency of the hard hollow sphere in injecting paste material are also very slow, therefore the hard hollow sphere at the different depth in injecting paste material can keep the suspended state of relative quiescent, guarantee that hard hollow sphere is dispersed in injecting paste material, the density and intensity for ensuring each position of Over-summer cultivation carcass of subsequent preparation are all consistent, to reduce carcass density on the basis of guaranteeing traditional aesthetic and using effect to Over-summer cultivation, guarantee carcass strength simultaneously.
Description
Technical field
The invention belongs to Over-summer cultivation manufacture technology fields, and in particular to a kind of lightweight Over-summer cultivation carcass and its slip casting material
The preparation method of material and the injecting paste material.
Background technique
Over-summer cultivation is various in style, and moulding is lively, and glaze colours is dark green, and decoration is abundant, there is very high practical and artistic value,
Occupy highly important status on China's ceramic history.It is that one kind contains that the kiln place of production one is got in history with used main celadon raw material
Rock forming mineral after the giant granite weathering of quartz-kaolinite-sericite type, the content of iron is relatively high, and content exists
1.5% or more, up to 3% or so, therefore cinerous is also presented in carcass in some areas.It is now recognized that ancients are not make to raw material
In the case where any processing, gossamery more kiln light carcass has been burnt out with reducing flame, has made one of Over-summer cultivation
Important feature.In the Tang Dynasty, poet Pi Xiu just says that " visitor Xing and more people, can all make hereby device in its " tea bowl " poem.Circle lunar soul
It falls, light as cloud soul rises ", " light such as cloud soul " what is said is exactly the central characteristics of Over-summer cultivation.
However the generally existing very big problem of Over-summer cultivation imitated using modern crafts and raw material at present, after firing
Porcelain otherwise carcass it is heavy, it is difficult to achieve the effect that ancient Over-summer cultivation " light as cloud soul ", can only accomplish to be similar to;It is light but
Intensity is insufficient, is easy breakage, and light from ancients and strong, refreshing shape has both there are also with a distance from.
Summary of the invention
Present invention purpose is to provide a kind of light and high intensity lightweight Over-summer cultivation carcass and its injecting paste material
With the preparation method of the injecting paste material.
For achieving the above object, the technical solution of the application is as follows:
A kind of lightweight Over-summer cultivation carcass injecting paste material, according to parts by weight, the lightweight Over-summer cultivation carcass injecting paste material
It is made of following raw material: 40-60 parts of Over-summer cultivation carcass blanks, 4-16 parts of hard hollow spheres, 0.2-0.5 parts of sodium humates, 30-
35 parts of water;
The density of the hard hollow sphere is suitable with the density of the lightweight Over-summer cultivation carcass injecting paste material.
The present invention adds hard hollow sphere in Over-summer cultivation carcass blank, and the density of hard hollow sphere and the lightweight get over kiln
The density of celadon carcass injecting paste material is suitable, therefore hard hollow sphere can be presented in lightweight Over-summer cultivation carcass injecting paste material
Suspended state, simultaneously because the viscosity of injecting paste material is larger, even if the density of hard hollow sphere and injecting paste material is deviated,
The floating or sinking tendency of the even hard hollow sphere being dispersed in injecting paste material are also very slow, therefore not in injecting paste material
The suspended state of relative quiescent can be kept with the hard hollow sphere of depth, guarantee that hard hollow sphere is dispersed in slip casting
In material, it is ensured that the density and intensity at each position of Over-summer cultivation carcass of subsequent preparation are all consistent.Since hard is hollow
The density of ball and the density of injecting paste material are suitable, after inserting in injecting paste material, can guarantee traditional to examine Over-summer cultivation
Carcass density is reduced on the basis of beauty and using effect, while guaranteeing carcass strength.
Diluent and plasticizer of the sodium humate as injecting paste material, can improve the rheological property of injecting paste material.
Preferably, the density of the hard hollow sphere is in above-mentioned lightweight Over-summer cultivation carcass injecting paste material
1.6-1.8g/cm3, the density of the lightweight Over-summer cultivation carcass injecting paste material is 1.67-1.69g/cm3。
Preferably, the partial size of the hard hollow sphere is in above-mentioned lightweight Over-summer cultivation carcass injecting paste material
0.2-2mm, bulk density 0.2-0.8g/cm3.Bulk density, which refers to, is freely filled in a certain container dust or powder
In, measured mass per volume after the completion of rigid filling.
Preferably, the hard hollow sphere is mullite in above-mentioned lightweight Over-summer cultivation carcass injecting paste material
Hollow sphere or alumina hollow ball.
The viscosity of the lightweight Over-summer cultivation carcass injecting paste material of the application are as follows: in mud viscosimeter, flow out described in 100mL
Lightweight Over-summer cultivation carcass injecting paste material needed for the time be 59-63 seconds.Under the viscosity, the stable dispersion of hard hollow sphere
Both time and injecting paste material mobility obtain preferable balance, have both guaranteed injecting paste material good fluidity, also ensure that hard sky
Bulbus cordis can be stably dispersed in injecting paste material.
Over-summer cultivation carcass blank can use Over-summer cultivation carcass blank common in the art.Preferably,
In above-mentioned lightweight Over-summer cultivation carcass injecting paste material, according to parts by weight, the Over-summer cultivation carcass blank is by following original
Material is made: 38 parts of Shangyu china clay, 39 parts of Shaoxing Hua Jie porcelain stone, and 14 parts of the profound china clay of Huangshi, 2 parts of soil of dragon's fountain Zijin, alumina powder 5
Part, 2 parts of silica flour.
The preparation method of the lightweight Over-summer cultivation carcass injecting paste material the following steps are included:
(1) all raw materials for taking the Over-summer cultivation carcass blank, according to raw material: ballstone: water=1:2:0.75 ratio
Example carries out high speed ball milling 20min, after crossing 200 meshes, is placed at 110 DEG C and dries, and obtains the Over-summer cultivation carcass blank;
The Over-summer cultivation carcass blank of acquisition is in powdery, convenient for saving and taking at any time.
(2) Over-summer cultivation carcass blank is uniformly mixed with sodium humate, water, hard hollow sphere is added, is dispersed with stirring 2h,
Obtain the lightweight Over-summer cultivation carcass injecting paste material.
Present invention also provides using Over-summer cultivation carcass made of the lightweight Over-summer cultivation carcass injecting paste material and
Over-summer cultivation.By the lightweight Over-summer cultivation carcass injecting paste material after aged, injection forming, biscuiting, that is, obtains and get over kiln blueness
Porcelain body body;Over-summer cultivation is obtained after the glazing of Over-summer cultivation carcass, glaze firing.The ageing, injection forming, biscuiting, glazing, glaze
Firing technique is technology mature in the prior art, and the application repeats no more.
Compared with prior art, the invention has the benefit that
The present invention adds hard hollow sphere in Over-summer cultivation carcass blank, and the density of hard hollow sphere and the lightweight get over kiln
The density of celadon carcass injecting paste material is suitable, therefore hard hollow sphere can be presented in lightweight Over-summer cultivation carcass injecting paste material
Suspended state, simultaneously because the viscosity of injecting paste material is larger, even if the density of hard hollow sphere and injecting paste material is deviated,
The floating or sinking tendency of the even hard hollow sphere being dispersed in injecting paste material are also very slow, therefore not in injecting paste material
The suspended state of relative quiescent can be kept with the hard hollow sphere of depth, guarantee that hard hollow sphere is dispersed in slip casting
In material, it is ensured that the density and intensity at each position of Over-summer cultivation carcass of subsequent preparation are all consistent.Since hard is hollow
The density of ball and the density of injecting paste material are suitable, after inserting in injecting paste material, can guarantee traditional to examine Over-summer cultivation
Carcass density is reduced on the basis of beauty and using effect, while guaranteeing carcass strength.
Specific embodiment
Specific embodiment is set forth below, and further details of the technical solution of the present invention.
Embodiment 1
A kind of lightweight Over-summer cultivation carcass injecting paste material of the present embodiment, preparation method include:
(1) 38 parts of Shangyu china clay are taken, 39 parts of Shaoxing Hua Jie porcelain stone, 14 parts of the profound china clay of Huangshi, aoxidizes by 2 parts of soil of dragon's fountain Zijin
5 parts of aluminium powder, 2 parts of silica flour, according to raw material: ballstone: water=1:2:0.75 ratio carries out high speed ball milling 20min, crosses 200 meshes
Afterwards, it is placed at 110 DEG C and dries, obtain Over-summer cultivation carcass blank;
(2) the Over-summer cultivation carcass blank, 0.2 part of sodium humate and 30 parts of water of 40 parts of dry powder-shapeds are taken, is uniformly mixed, is added
(density of alumina hollow ball is 1.6g/cm to 4 parts of alumina hollow balls3, partial size 0.2-2mm, bulk density 0.2g/
cm3), dispersion 2h is mixed, obtains the lightweight Over-summer cultivation carcass injecting paste material of the present embodiment;
The density of the lightweight Over-summer cultivation carcass injecting paste material of acquisition is 1.67g/cm3, viscosity are as follows: in mud viscosimeter
In, the time needed for flowing out 100mL lightweight Over-summer cultivation carcass injecting paste material is 59 seconds.
Embodiment 2
A kind of lightweight Over-summer cultivation carcass injecting paste material of the present embodiment, preparation method include:
(1) 38 parts of Shangyu china clay are taken, 39 parts of Shaoxing Hua Jie porcelain stone, 14 parts of the profound china clay of Huangshi, aoxidizes by 2 parts of soil of dragon's fountain Zijin
5 parts of aluminium powder, 2 parts of silica flour, according to raw material: ballstone: water=1:2:0.75 ratio carries out high speed ball milling 20min, crosses 200 meshes
Afterwards, it is placed at 110 DEG C and dries, obtain Over-summer cultivation carcass blank;
(2) the Over-summer cultivation carcass blank, 0.5 part of sodium humate and 35 parts of water of 50 parts of dry powder-shapeds are taken, is uniformly mixed, is added
(density of alumina hollow ball is 1.8g/cm to 12 parts of alumina hollow balls3, partial size 0.2-2mm, bulk density 0.6g/
cm3), dispersion 2h is mixed, obtains the lightweight Over-summer cultivation carcass injecting paste material of the present embodiment;
The density of the lightweight Over-summer cultivation carcass injecting paste material of acquisition is 1.69g/cm3, viscosity are as follows: in mud viscosimeter
In, the time needed for flowing out 100mL lightweight Over-summer cultivation carcass injecting paste material is 61 seconds.
Embodiment 3
A kind of lightweight Over-summer cultivation carcass injecting paste material of the present embodiment, preparation method include:
(1) 38 parts of Shangyu china clay are taken, 39 parts of Shaoxing Hua Jie porcelain stone, 14 parts of the profound china clay of Huangshi, aoxidizes by 2 parts of soil of dragon's fountain Zijin
5 parts of aluminium powder, 2 parts of silica flour, according to raw material: ballstone: water=1:2:0.75 ratio carries out high speed ball milling 20min, crosses 200 meshes
Afterwards, it is placed at 110 DEG C and dries, obtain Over-summer cultivation carcass blank;
(2) the Over-summer cultivation carcass blank, 0.5 part of sodium humate and 35 parts of water of 60 parts of dry powder-shapeds are taken, is uniformly mixed, is added
(density of mullite hollow spheres is 1.6g/cm to 8 parts of mullite hollow spheres3, partial size 0.2-2mm, bulk density 0.4g/
cm3), dispersion 2h is mixed, obtains the lightweight Over-summer cultivation carcass injecting paste material of the present embodiment;
The density of the lightweight Over-summer cultivation carcass injecting paste material of acquisition is 1.69g/cm3, viscosity are as follows: in mud viscosimeter
In, the time needed for flowing out 100mL lightweight Over-summer cultivation carcass injecting paste material is 63 seconds.
Embodiment 4
A kind of lightweight Over-summer cultivation carcass injecting paste material of the present embodiment, preparation method include:
(1) 38 parts of Shangyu china clay are taken, 39 parts of Shaoxing Hua Jie porcelain stone, 14 parts of the profound china clay of Huangshi, aoxidizes by 2 parts of soil of dragon's fountain Zijin
5 parts of aluminium powder, 2 parts of silica flour, according to raw material: ballstone: water=1:2:0.75 ratio carries out high speed ball milling 20min, crosses 200 meshes
Afterwards, it is placed at 110 DEG C and dries, obtain Over-summer cultivation carcass blank;
(2) the Over-summer cultivation carcass blank, 0.5 part of sodium humate and 35 parts of water of 50 parts of dry powder-shapeds are taken, is uniformly mixed, is added
(density of mullite hollow spheres is 1.7g/cm to 16 parts of mullite hollow spheres3, partial size 0.2-2mm, bulk density 0.8g/
cm3), dispersion 2h is mixed, obtains the lightweight Over-summer cultivation carcass injecting paste material of the present embodiment;
The density of the lightweight Over-summer cultivation carcass injecting paste material of acquisition is 1.69g/cm3, viscosity are as follows: in mud viscosimeter
In, the time needed for flowing out 100mL lightweight Over-summer cultivation carcass injecting paste material is 63 seconds.
Aged, injection forming, biscuiting by the lightweight Over-summer cultivation carcass injecting paste material obtained in embodiment 1-4 respectively
Afterwards, Over-summer cultivation carcass is made;Over-summer cultivation is made in Over-summer cultivation carcass after glazing, glaze firing.Above-mentioned ageing, slip casting at
Type, biscuiting, glazing, glaze firing technique are technologies mature in the prior art, and the application repeats no more.It is green to compare more kiln obtained
The density and bending strength of porcelain body body, such as table 1.
Table 1
Over-summer cultivation | Density (g/cm3) | Bending strength (MPa) |
Embodiment 1 | 2.35 | 72 |
Embodiment 2 | 2.26 | 60 |
Embodiment 3 | 2.32 | 66 |
Embodiment 4 | 2.23 | 55 |
Imitative Over-summer cultivation sample (slip casting) | 2.35 | 30 |
Imitative Over-summer cultivation sample (throwing) | 2.45 | 40 |
Eastern Han Dynasty's Over-summer cultivation | 2.3 | 70 |
Seen from table 1, compared with Eastern Han Dynasty's Over-summer cultivation, imitated Over-summer cultivation sample (either slip casting in the prior art
Technique production or billet withdrawing technology production) density it is all larger so that celadon sample carcass is heavy;And bending strength is only
There is the half or so of Eastern Han Dynasty's Over-summer cultivation, carcass is excessively crisp, and intensity is inadequate.
And use the lightweight Over-summer cultivation carcass injecting paste material of embodiment 1-4 through Over-summer cultivation carcass made from grouting process
Density and bending strength it is close with Eastern Han Dynasty's Over-summer cultivation, when carcass density is down to 2.23g/cm3When still have 55MPa's
Bending strength.
Claims (9)
1. a kind of lightweight Over-summer cultivation carcass injecting paste material, which is characterized in that according to parts by weight, be made of following raw material: 40-
60 parts of Over-summer cultivation carcass blanks, 4-16 parts of hard hollow spheres, 0.2-0.5 parts of sodium humates, 30-35 parts of water;
The density of the hard hollow sphere is suitable with the density of the lightweight Over-summer cultivation carcass injecting paste material.
2. lightweight Over-summer cultivation carcass injecting paste material as described in claim 1, which is characterized in that the hard hollow sphere
Density is 1.6-1.8g/cm3, the density of the lightweight Over-summer cultivation carcass injecting paste material is 1.67-1.69g/cm3。
3. lightweight Over-summer cultivation carcass injecting paste material as described in claim 1, which is characterized in that the hard hollow sphere
Partial size is 0.2-2mm, bulk density 0.2-0.8g/cm3。
4. lightweight Over-summer cultivation carcass injecting paste material as described in claim 1, which is characterized in that the hard hollow sphere is
Mullite hollow spheres or alumina hollow ball.
5. lightweight Over-summer cultivation carcass injecting paste material as described in claim 1, which is characterized in that in mud viscosimeter, stream
The time needed for lightweight Over-summer cultivation carcass injecting paste material described in 100mL is 59-63 seconds out.
6. lightweight Over-summer cultivation carcass injecting paste material as described in claim 1, which is characterized in that according to parts by weight, described
Over-summer cultivation carcass blank be prepared from the following raw materials: 38 parts of Shangyu china clay, 39 parts of Shaoxing Hua Jie porcelain stone, the profound china clay 14 of Huangshi
Part, 2 parts, 5 parts of alumina powder, 2 parts of silica flour of soil of dragon's fountain Zijin.
7. the preparation method of the lightweight Over-summer cultivation carcass injecting paste material as described in any one of claim 1-6, feature
It is, comprising the following steps:
(1) all raw materials for taking the Over-summer cultivation carcass blank, according to raw material: ballstone: water=1:2:0.75 ratio into
Row high speed ball milling 20min is placed at 110 DEG C and dries after crossing 200 meshes, obtains the Over-summer cultivation carcass blank;
(2) Over-summer cultivation carcass blank is uniformly mixed with sodium humate, water, hard hollow sphere is added, is dispersed with stirring 2h, obtained
The lightweight Over-summer cultivation carcass injecting paste material.
8. getting over kiln using lightweight made of the lightweight Over-summer cultivation carcass injecting paste material as described in any one of claim 1-6
Celadon carcass.
9. getting over kiln using lightweight made of the lightweight Over-summer cultivation carcass injecting paste material as described in any one of claim 1-6
Celadon.
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Application publication date: 20181218 |