CN102731065B - Heat-insulation ceramic tile and its manufacturing method - Google Patents
Heat-insulation ceramic tile and its manufacturing method Download PDFInfo
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- CN102731065B CN102731065B CN201210225172.XA CN201210225172A CN102731065B CN 102731065 B CN102731065 B CN 102731065B CN 201210225172 A CN201210225172 A CN 201210225172A CN 102731065 B CN102731065 B CN 102731065B
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Abstract
The invention relates to a ceramic tile and its manufacturing method. According to the heat-insulation ceramic tile, ceramic tile blank materials including 35-45 wt% of kaolin, 20-25 wt% of feldspar, 20-40% of diatomite, 5-10% of quartzite and water are compacted into a base substrate; the inside of the base substrate is a hollow chamber which is filled with asbestos; the base substrate is glazed; glaze slip is composed of 40-60 wt% of a diatomite powder, 15-25 wt% of a quartzite powder, 15-20 wt% of a wollastonite powder, 5-10 wt% of hollow beads, 3-6 wt% of a silicone resin micropowder, 0-3 wt% of a color powder and water, and is prepared by sintering at high temperature in a combustion kiln. The ratio of the above materials except water is the mass ratio. The method for manufacturing the heat-insulation ceramic tile comprises the following steps of: a, preparing the ceramic tile blank materials according to the above ratio; b, compacting the ceramic tile base substrate through a mold; c, preparing the ceramic tile blank materials and the glaze slip according to the above ratio; d, glazing; and e, sintering the heat-insulation ceramic tile at high temperature. The heat-insulation ceramic tile provided by the invention is used for surface laying of building space.
Description
Technical field
The present invention relates to ceramic tile and manufacture method thereof.
Background technology
Heat insulating ceramic tile is a kind of novel ceramic tile that is applied in recent years building field, and adopting adiabatic material of construction is to be conducive to the way that reduces energy expenditure, be beneficial to environmental protection.
A kind of implementation of heat insulating ceramic tile is directly at ceramic tile, to form heat insulation air chamber structure, and the way of formation heat-insulation chamber structure has multiple, and the patent of invention as 200710124041.1 discloses a kind of cellular vacuum hole heat insulating ceramic tile and production technique thereof.The raw material of the heat insulating ceramic tile adobe of this invention forms: 1. kaolin 60%-70%, 2. plastic foam particle 1%-5%, 3. water 20%-30%; The raw material of described reflective white glaze forms: 1. silicon oxide 50%-65%, 2. aluminum oxide 13%-18%, 2. calcium oxide 12%-17%, 4. magnesium oxide 0.5%-1.5%, 5. sodium oxide 3%-4%, 6. potassium oxide 1%-1.5%, above content is weight percentage, described porous plastics includes but not limited to urethane plastic foam beads, and the diameter of its particle is at 6MM-7MM.Its production technique is the various raw materials of heat insulating ceramic tile to be mixed to the adobe that is pressed into specification naturally parch, spray after reflective white glaze dries and fire and form.Ceramic tile plastic foam particle when firing can melt, and the brick body inside being therefore fired into after finished product there will be some cellular vacuum holes, and this vacuum hole is not connected mutually, keeps constant temperature, has effect of heat insulation.
The another kind of implementation of heat insulating ceramic tile is to adopt in ceramic tile, directly to add the mode of lagging material, as Chinese patent 200610060281.5 discloses a kind of heat-insulating energy-saving temperature-constant ceramic brick and production technique thereof.The ceramic tile of this invention is by work in-process heat insulating ceramic tile and be coated in its lip-deep heat-insulation constant temperature paint and form; the raw material of work in-process heat insulating ceramic tile forms (weight): (1) kaolin 30%-40%; (2) calcite in powder 20%-30%; (3) talcum powder 5%-10%; (4) cenosphere 10%-15%, (5) water 20%-25%; The raw material of heat-insulation constant temperature paint forms (weight), (1) titanium dioxide 25%-35%, (2) cenosphere 8%-13%, (3) talcum powder 3%-5%, fluorine silicon resin 35%-42%, (5) solvent 15%-25%, (6) pigment 0.3%-1%, (7) auxiliary agent 1-3%.Production technique is to make respectively work in-process heat insulating ceramic tile and heat-insulation constant temperature paint, then divides on the brick face that is sprayed on work in-process heat insulating ceramic tile for two to three times, parch qualitative after and get final product.
The physical strength of the heat insulating ceramic tile of the first implementation is not high.The second implementation is mainly to realize insulation effect by cenosphere.Cenosphere main component is the powder body material of a kind of loose, the good fluidity that forms through 1400 ℃ of high-temperature firing sortings of silicon-dioxide and aluminium sesquioxide.The diameter of cenosphere is larger, and hollow rate is higher, and effect of heat insulation is better.Conventionally in order to reach good insulation effect, need to adopt the cenosphere of larger particles, so production cost is higher.
Summary of the invention
The present invention proposes a kind ofly can meet better physical strength and suitable heat insulating ceramic tile and the manufacture method thereof of cost cost.
Technical scheme of the present invention is:
Heat insulating ceramic tile, by the kaolin of 35-45%, the diatomite of the feldspar of 20-25%, 20-40%, the ceramic tile blank compacting of the quartzite of 5-10% and water forms base substrate, base substrate Nei Wei hollow chamber, in hollow chamber, be filled with asbestos, glazing on base substrate, the quartzite powder of the diatomite powder that glaze slip is 40-60% by mass percent, 15-25%, 15-20% wollastonite powder, the cenosphere of 5-10%, color powder and the water of the silicone resin micro mist of 3-6%, 0-3% form, and make via burning kiln high-temperature firing; The proportioning of above various materials is the outer mass percent that dewaters.
Further, the preferred mass per-cent of described ceramic tile blank is: kaolin accounts for 37%, and feldspar accounts for 22%, and diatomite accounts for 35%, and quartzite accounts for 6%.
Further, the preferred mass per-cent of described glaze slip is: diatomite powder accounts for 50%, quartzite powder accounts for 18%, wollastonite powder accounts for 18%, cenosphere accounts for 8%, silicone resin micro mist accounts for 4%, color powder accounts for 2%.
The manufacture method of heat insulating ceramic tile, comprises the steps:
(a) kaolin that is 35-45% by mass percent, the feldspar of 20-25%, the diatomite of 20-40%, the quartzite of 5-10% is through fragmentation, and adds water and mix and make ceramic tile blank;
(b) some ceramic tile blanks that step (a) made are poured in mold, at mold bottom surface uniform fold one deck ceramic tile blank, then on the ceramic tile blank thin layer of bottom surface, put into asbestos, the asbestos layer area of putting into is less than the floorage of ceramic tile blank, then on asbestos layer, pour again some ceramic tile blanks into, and the space between mold bottom surface and end face also fills ceramic tile blank, asbestos are wrapped in ceramic tile blank, scrape the ceramic tile blank of flat top surface;
(c) the quartzite powder of the diatomite powder that is 40-60% by mass percent, 15-25%, 15-20% wollastonite powder, the cenosphere of 5-10%,, the color powder of the silicone resin micro mist of 3-6%, 0-3% adds water is uniformly mixed, make glaze slip;
(d) ceramic tile blank that the glaze slip making by step (c) makes step (b) carries out glazing;
(e) ceramic tile blank is put into burning kiln, high-temperature firing is made heat insulating ceramic tile.
Further, the preferred mass per-cent of the ceramic tile blank in described step (a) is: kaolin accounts for 37%, and feldspar accounts for 22%, and diatomite accounts for 35%, and quartzite accounts for 6%.
Further, the preferred mass per-cent of the glaze slip in described step (c) is: diatomite powder accounts for 50%, quartzite powder accounts for 18%, wollastonite powder accounts for 18%, cenosphere accounts for 8%, silicone resin micro mist accounts for 4%, color powder accounts for 2%.
The present invention fills asbestos in the middle of ceramic tile blank, has radiating effect well and low cost, and only in glaze slip, uses a small amount of cenosphere and silicone resin micro mist.Therefore, can replace the relatively large higher lagging material of cost of existing heat insulating ceramic tile needs, thereby greatly reduce material cost.And adopt kaolin, feldspar, diatomite, quartzite as ceramic tile blank, than traditional ceramic tile blank, can form more microporous structure, be conducive to insulation effect, the physical strength that makes ceramic tile is not poor yet; And in the glaze of ceramic tile, also adopted relatively large diatomite, manufacturing cost is lower, has good effect of heat insulation.
Embodiment
Now in conjunction with embodiment, the present invention is further described.
Heat insulating ceramic tile, by the kaolin of 35-45%, the diatomite of the feldspar of 20-25%, 20-40%, the ceramic tile blank compacting of the quartzite of 5-10% and water forms base substrate, base substrate Nei Wei hollow chamber, in hollow chamber, be filled with asbestos, glazing on base substrate, the quartzite powder of the diatomite powder that glaze slip is 40-60% by mass percent, 15-25%, 15-20% wollastonite powder, the cenosphere of 5-10%, color powder and the water of the silicone resin micro mist of 3-6%, 0-3% form, and make via burning kiln high-temperature firing; The proportioning of above various materials is the outer mass percent that dewaters.
The manufacture method of heat insulating ceramic tile, comprises the steps:
(a) kaolin that is 35-45% by mass percent, the feldspar of 20-25%, the diatomite of 20-40%, the quartzite of 5-10% is through fragmentation, and adds water and mix and make ceramic tile blank;
(b) some ceramic tile blanks that step (a) made are poured in mold, at mold bottom surface uniform fold one deck ceramic tile blank, then on the ceramic tile blank thin layer of bottom surface, put into asbestos, the asbestos layer area of putting into is less than the floorage of ceramic tile blank, then on asbestos layer, pour again some ceramic tile blanks into, and the space between mold bottom surface and end face also fills ceramic tile blank, asbestos are wrapped in ceramic tile blank, scrape the ceramic tile blank of flat top surface;
(c) the quartzite powder of the diatomite powder that is 40-60% by mass percent, 15-25%, 15-20% wollastonite powder, the cenosphere of 5-10%,, the color powder of the silicone resin micro mist of 3-6%, 0-3% adds water is uniformly mixed, make glaze slip;
(d) ceramic tile blank that the glaze slip making by step (c) makes step (b) carries out glazing;
(e) ceramic tile blank is put into burning kiln, high-temperature firing is made heat insulating ceramic tile.
Above-mentioned ceramic tile blank can be by following table 1 the proportioning (mass percent) of several embodiment implement:
Table 1:
 |
Kaolin | Feldspar | Diatomite | Quartzite |
| Embodiment 1 | 35% | 20% | 40% | 5% |
| Embodiment 2 | 37% | 22% | 35% | 6% |
| Embodiment 3 | 38% | 20% | 34% | 8% |
| Embodiment 4 | 40% | 23% | 28% | 9% |
| Embodiment 5 | 45% | 25% | 20% | 10% |
Above-mentioned glaze slip can be by following table 2 the proportioning (mass percent) of several embodiment implement:
Table 2:
| Diatomite powder | Quartzite powder | Wollastonite powder | Cenosphere | Silicone resin micro mist | Color powder | |
| Embodiment 1 | 40% | 25% | 18% | 8% | 6% | 3% |
| Embodiment 2 | 45% | 18% | 20% | 9% | 6% | 2% |
| Embodiment 3 | 50% | 18% | 18% | 8% | 4% | 2% |
| Embodiment 4 | 55% | 15% | 17% | 10% | 3% | 0 |
| Embodiment 5 | 60% | 15% | 15% | 5% | 5% | 0 |
Although specifically show and introduced the present invention in conjunction with preferred embodiment; but those skilled in the art should be understood that; within not departing from the spirit and scope of the present invention that appended claims limits; can make a variety of changes the present invention in the form and details, be protection scope of the present invention.
Claims (6)
1. heat insulating ceramic tile, it is characterized in that: by the kaolin of 35-45%, the diatomite of the feldspar of 20-25%, 20-40%, the ceramic tile blank compacting of the quartzite of 5-10% and water forms base substrate, base substrate Nei Wei hollow chamber, in hollow chamber, be filled with asbestos, glazing on base substrate, the quartzite powder of the diatomite powder that glaze slip is 40-60% by mass percent, 15-25%, 15-20% wollastonite powder, the cenosphere of 5-10%, color powder and the water of the silicone resin micro mist of 3-6%, 0-3% form, and make via burning kiln high-temperature firing; The proportioning of above various materials is the outer mass percent that dewaters.
2. heat insulating ceramic tile according to claim 1, is characterized in that: the preferred mass per-cent of described ceramic tile blank is: kaolin accounts for 37%, and feldspar accounts for 22%, and diatomite accounts for 35%, and quartzite accounts for 6%.
3. heat insulating ceramic tile according to claim 1, is characterized in that: the preferred mass per-cent of described glaze slip is: diatomite powder accounts for 50%, quartzite powder accounts for 18%, wollastonite powder accounts for 18%, cenosphere accounts for 8%, silicone resin micro mist accounts for 4%, color powder accounts for 2%.
4. the manufacture method of heat insulating ceramic tile, is characterized in that, comprises the steps:
(a) kaolin that is 35-45% by mass percent, the feldspar of 20-25%, the diatomite of 20-40%, the quartzite of 5-10% is through fragmentation, and adds water and mix and make ceramic tile blank;
(b) some ceramic tile blanks that step (a) made are poured in mold, at mold bottom surface uniform fold one deck ceramic tile blank, then on the ceramic tile blank thin layer of bottom surface, put into asbestos, the asbestos layer area of putting into is less than the floorage of ceramic tile blank, then on asbestos layer, pour again some ceramic tile blanks into, and the space between mold bottom surface and end face also fills ceramic tile blank, asbestos are wrapped in ceramic tile blank, scrape the ceramic tile blank of flat top surface;
(c) the quartzite powder of the diatomite powder that is 40-60% by mass percent, 15-25%, 15-20% wollastonite powder, the cenosphere of 5-10%,, the color powder of the silicone resin micro mist of 3-6%, 0-3% adds water is uniformly mixed, make glaze slip;
(d) ceramic tile blank that the glaze slip making by step (c) makes step (b) carries out glazing;
(e) ceramic tile blank is put into burning kiln, high-temperature firing is made heat insulating ceramic tile.
5. the manufacture method of heat insulating ceramic tile according to claim 4, is characterized in that: the preferred mass per-cent of the ceramic tile blank in described step (a) is: kaolin accounts for 37%, and feldspar accounts for 22%, and diatomite accounts for 35%, and quartzite accounts for 6%.
6. the manufacture method of heat insulating ceramic tile according to claim 4, is characterized in that: the preferred mass per-cent of the glaze slip in described step (c) is: diatomite powder accounts for 50%, quartzite powder accounts for 18%, wollastonite powder accounts for 18%, cenosphere accounts for 8%, silicone resin micro mist accounts for 4%, color powder accounts for 2%.
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| CN201210225172.XA CN102731065B (en) | 2012-07-03 | 2012-07-03 | Heat-insulation ceramic tile and its manufacturing method |
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| CN201210225172.XA CN102731065B (en) | 2012-07-03 | 2012-07-03 | Heat-insulation ceramic tile and its manufacturing method |
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| CN102731065B true CN102731065B (en) | 2014-02-12 |
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| CN103880397B (en) * | 2014-02-18 | 2015-03-18 | 青岛泉佳美硅藻泥科技有限公司 | Diatomite ceramic and preparation method thereof |
| CN104761236B (en) * | 2015-04-28 | 2016-09-07 | 福建省南安市荣达建材有限公司 | A kind of sound insulation negative ion ceramic ceramic tile |
| CN104987046A (en) * | 2015-07-15 | 2015-10-21 | 江苏振宇环保科技有限公司 | Building thermal insulation material |
| CN105732067A (en) * | 2016-01-21 | 2016-07-06 | 广西大学 | Thermal-insulation ceramic tile and preparation method thereof |
| CN114477954A (en) * | 2022-03-02 | 2022-05-13 | 阳城福龙陶瓷有限公司 | Heat-insulating constant-temperature energy-saving ceramic tile and production process thereof |
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| JP2005200244A (en) * | 2004-01-13 | 2005-07-28 | Inax Corp | Tile and its producing method |
| CN101875556B (en) * | 2009-10-16 | 2012-07-04 | 北京工业大学 | Light ceramic tiles and manufacturing process thereof |
| CN102173761B (en) * | 2011-01-01 | 2013-04-24 | 蔡锋盛 | Ceramic clay used for powder paint decoration and production method of powder paint decorative ceramic prepared from same |
| CN102503565B (en) * | 2011-09-29 | 2013-05-22 | 陈维鹏 | Manufacturing method of ceramic product with crack glaze |
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