CN108978201B - 一种提高黄麻纤维品质的加工方法 - Google Patents
一种提高黄麻纤维品质的加工方法 Download PDFInfo
- Publication number
- CN108978201B CN108978201B CN201810773039.5A CN201810773039A CN108978201B CN 108978201 B CN108978201 B CN 108978201B CN 201810773039 A CN201810773039 A CN 201810773039A CN 108978201 B CN108978201 B CN 108978201B
- Authority
- CN
- China
- Prior art keywords
- parts
- fiber
- jute
- ethanol
- potassium acetate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000835 fiber Substances 0.000 title claims abstract description 93
- 235000011777 Corchorus aestuans Nutrition 0.000 title claims abstract description 63
- 235000010862 Corchorus capsularis Nutrition 0.000 title claims abstract description 63
- 240000000491 Corchorus aestuans Species 0.000 title claims abstract description 62
- 238000003672 processing method Methods 0.000 title claims abstract description 14
- 239000012046 mixed solvent Substances 0.000 claims abstract description 23
- 239000003607 modifier Substances 0.000 claims abstract description 18
- KARAZZXOSOLPBZ-UHFFFAOYSA-M potassium;ethanol;acetate Chemical compound [K+].CCO.CC([O-])=O KARAZZXOSOLPBZ-UHFFFAOYSA-M 0.000 claims abstract description 18
- 239000000463 material Substances 0.000 claims abstract description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 32
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 15
- 239000013530 defoamer Substances 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 10
- SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Chemical compound [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 claims description 6
- 229910021538 borax Inorganic materials 0.000 claims description 6
- LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 claims description 6
- QUBQYFYWUJJAAK-UHFFFAOYSA-N oxymethurea Chemical compound OCNC(=O)NCO QUBQYFYWUJJAAK-UHFFFAOYSA-N 0.000 claims description 6
- 229950005308 oxymethurea Drugs 0.000 claims description 6
- 239000000344 soap Substances 0.000 claims description 6
- 239000004328 sodium tetraborate Substances 0.000 claims description 6
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 6
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 6
- ITCAUAYQCALGGV-XTICBAGASA-M sodium;(1r,4ar,4br,10ar)-1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylate Chemical compound [Na+].C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C([O-])=O ITCAUAYQCALGGV-XTICBAGASA-M 0.000 claims description 6
- 239000004246 zinc acetate Substances 0.000 claims description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 5
- 241000779819 Syncarpia glomulifera Species 0.000 claims description 5
- WOWHHFRSBJGXCM-UHFFFAOYSA-M cetyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)C WOWHHFRSBJGXCM-UHFFFAOYSA-M 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 5
- 238000000576 coating method Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000001739 pinus spp. Substances 0.000 claims description 5
- 235000011056 potassium acetate Nutrition 0.000 claims description 5
- 238000003892 spreading Methods 0.000 claims description 5
- 238000000967 suction filtration Methods 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 5
- 229940036248 turpentine Drugs 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 4
- 239000004753 textile Substances 0.000 abstract description 7
- 238000011282 treatment Methods 0.000 abstract description 5
- 238000012986 modification Methods 0.000 abstract description 3
- 230000004048 modification Effects 0.000 abstract description 3
- 238000012545 processing Methods 0.000 abstract description 3
- 238000009987 spinning Methods 0.000 abstract description 3
- 238000009960 carding Methods 0.000 abstract description 2
- 239000006185 dispersion Substances 0.000 abstract description 2
- 238000011418 maintenance treatment Methods 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000003921 oil Substances 0.000 description 8
- 235000019198 oils Nutrition 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 6
- 244000025254 Cannabis sativa Species 0.000 description 3
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 description 3
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 description 3
- 235000009120 camo Nutrition 0.000 description 3
- 235000005607 chanvre indien Nutrition 0.000 description 3
- 239000011487 hemp Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 244000227473 Corchorus olitorius Species 0.000 description 2
- 235000010206 Corchorus olitorius Nutrition 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 230000006837 decompression Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 240000008564 Boehmeria nivea Species 0.000 description 1
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- 235000010203 Corchorus Nutrition 0.000 description 1
- 241000332384 Corchorus Species 0.000 description 1
- 240000004792 Corchorus capsularis Species 0.000 description 1
- 240000000797 Hibiscus cannabinus Species 0.000 description 1
- 240000006240 Linum usitatissimum Species 0.000 description 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 1
- 241000219071 Malvaceae Species 0.000 description 1
- 244000124853 Perilla frutescens Species 0.000 description 1
- 235000004348 Perilla frutescens Nutrition 0.000 description 1
- 241001521901 Tribulus lanuginosus Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000003211 malignant effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
- D06M11/66—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with sulfamic acid or its salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
- D06M11/71—Salts of phosphoric acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
- D06M11/82—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides with boron oxides; with boric, meta- or perboric acids or their salts, e.g. with borax
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/432—Urea, thiourea or derivatives thereof, e.g. biurets; Urea-inclusion compounds; Dicyanamides; Carbodiimides; Guanidines, e.g. dicyandiamides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
本发明涉及纺织品材料加工制作技术领域,公开了一种提高黄麻纤维品质的加工方法,对黄麻纤维进行改性处理,首先将漂洗处理后的黄麻纤维置于醋酸钾‑乙醇混合溶剂中分散开,然后加入纤维改性剂,改性处理后的黄麻纤维各项性能都会发生改变,进一步进行养护处理稳定性能,便于梳理,最终制备得到的黄麻纤维在强度、细度、长度、纺织性方面均得到显著提高,本发明显著提高了黄麻纤维的市场前景和经济价值,能够实现加深对黄麻纤维性能特点的研究以及对纺织品优质原料的扩充的现实意义,是一种极为值得推广使用的技术方案。
Description
技术领域
本发明属于纺织品材料加工制作技术领域,具体涉及一种提高黄麻纤维品质的加工方法。
背景技术
黄麻,属椴树科黄麻属,韧皮纤维作物,一年生草本植物,喜温暖湿润的气候,短日照作物,别名火麻、绿麻、络麻、水络麻、野洋麻、圆果黄麻、圆蒴黄麻、苦麻叶、牛泥茨、三珠草、天紫苏、麻骨头等,是一种长而柔软的、有光泽的植物纤维,可以织成高强度的粗糙的细丝。黄麻纤维是最廉价的天然纤维之一,种植量和用途的广泛都仅次于棉花,具有吸湿性能好、散失水分快等特点,主要用于纺织麻袋、粗麻布等。纤维的颜色从白色到褐色,长1-4米。
黄麻纤维是一种廉价而又性能优异的天然纤维素纤维,特有的纤维性能展现了产品良好的实用性和外观风格,受到消费者的青睐。但是由于黄麻纤维在提取加工中仍然受传统工艺的限制,导致黄麻纤维的品质得不到提高,与棉花、亚麻等天然纤维相比,依然存在许多不足,导致黄麻纤维纺织品在低层次产品上恶性竞争,制约着产品性能的开发利用。
发明内容
本发明的目的是针对现有的问题,提供了一种提高黄麻纤维品质的加工方法,最终制备得到的黄麻纤维在强度、细度、长度、纺织性方面均得到显著提高。
本发明是通过以下技术方案实现的:
一种提高黄麻纤维品质的加工方法,包括以下步骤:
(1)将漂洗处理后的黄麻纤维置于醋酸钾-乙醇混合溶剂中,在300-350转/分钟下搅拌混合15-20分钟,加入纤维改性剂,用量为混合溶剂质量的5.0-5.5%,该纤维改性剂按照重量份计由以下成分制成:醋酸锌13-16份、硼砂6.0-7.0份、氨基磺酸5.0-6.0份、松香酸钠皂4.0-4.5份、十六烷基三甲基氯化铵2.3-2.5份、二羟甲基脲占1.4-1.6份、氢氧化钠占1.0-1.4份、三聚磷酸钠占1.0-1.2份、水600-700份;
(2)将步骤(1)混合物料加热至40-45℃,滴加松节油-乙醇混合消泡剂,并保温低速搅拌1-2小时,搅拌速度为80-100转/分钟,然后置于离心机中在1500-1800转/分钟下离心处理10-12分钟,倒去上层液,使用质量浓度为0.12-0.14%的苏打水继续离心洗涤2-3次,减压抽滤后在50-55℃下干燥4-5小时得到改性黄麻纤维;
(3)在步骤(2)制备得到的改性黄麻纤维表面涂抹椰油,椰油用量为改性黄麻纤维质量的2.2-2.4%,然后至于恒温恒湿箱中铺展开,静止养护5-6小时,养护后经过60-70℃恒温干燥即可。
作为对上述方案的进一步描述,步骤(1)中所述醋酸钾-乙醇混合溶剂中醋酸钾与乙醇的混合质量比为1:14-16。
作为对上述方案的进一步描述,步骤(1)中所述醋酸钾-乙醇混合溶剂用量为纤维体积的3.0-3.5倍。
作为对上述方案的进一步描述,步骤(2)中所述松节油-乙醇混合消泡剂用量为混合物料质量的0.02-0.04%,其中松节油与乙醇的质量比为1:2.0-2.4。
作为对上述方案的进一步描述,步骤(3)中所述恒温恒湿箱中温度设置为18-20℃,相对湿度为65-68%。
本发明相比现有技术具有以下优点:为了提高现有黄麻纤维的品质性能,本发明提供了一种提高黄麻纤维品质的加工方法,对黄麻纤维进行改性处理,首先将漂洗处理后的黄麻纤维置于醋酸钾-乙醇混合溶剂中分散开,然后加入纤维改性剂,改性处理后的黄麻纤维各项性能都会发生改变,进一步进行养护处理稳定性能,便于梳理,最终制备得到的黄麻纤维在强度、细度、长度、纺织性方面均得到显著提高,本发明显著提高了黄麻纤维的市场前景和经济价值,能够实现加深对黄麻纤维性能特点的研究以及对纺织品优质原料的扩充的现实意义,是一种极为值得推广使用的技术方案。
具体实施方式
为使本发明的目的、技术方案及效果更加清楚、明确,下面结合具体实施例对本发明作进一步说明,应当理解,此处所描述的具体实施例仅仅用以解释本发明,并不用于限定本发明所提供的技术方案。
实施例1
一种提高黄麻纤维品质的加工方法,包括以下步骤:
(1)将漂洗处理后的黄麻纤维置于醋酸钾-乙醇混合溶剂中,在300转/分钟下搅拌混合15分钟,加入纤维改性剂,用量为混合溶剂质量的5.0%,该纤维改性剂按照重量份计由以下成分制成:醋酸锌13份、硼砂6.0份、氨基磺酸5.0份、松香酸钠皂4.0份、十六烷基三甲基氯化铵2.3份、二羟甲基脲占1.4份、氢氧化钠占1.0份、三聚磷酸钠占1.0份、水600份;
(2)将步骤(1)混合物料加热至40℃,滴加松节油-乙醇混合消泡剂,并保温低速搅拌1小时,搅拌速度为80转/分钟,然后置于离心机中在1500转/分钟下离心处理10分钟,倒去上层液,使用质量浓度为0.12%的苏打水继续离心洗涤2次,减压抽滤后在50℃下干燥4小时得到改性黄麻纤维;
(3)在步骤(2)制备得到的改性黄麻纤维表面涂抹椰油,椰油用量为改性黄麻纤维质量的2.2%,然后至于恒温恒湿箱中铺展开,静止养护5小时,养护后经过60℃恒温干燥即可。
作为对上述方案的进一步描述,步骤(1)中所述醋酸钾-乙醇混合溶剂中醋酸钾与乙醇的混合质量比为1:14。
作为对上述方案的进一步描述,步骤(1)中所述醋酸钾-乙醇混合溶剂用量为纤维体积的3.0倍。
作为对上述方案的进一步描述,步骤(2)中所述松节油-乙醇混合消泡剂用量为混合物料质量的0.02%,其中松节油与乙醇的质量比为1:2.0。
作为对上述方案的进一步描述,步骤(3)中所述恒温恒湿箱中温度设置为18℃,相对湿度为65%。
实施例2
一种提高黄麻纤维品质的加工方法,包括以下步骤:
(1)将漂洗处理后的黄麻纤维置于醋酸钾-乙醇混合溶剂中,在330转/分钟下搅拌混合18分钟,加入纤维改性剂,用量为混合溶剂质量的5.3%,该纤维改性剂按照重量份计由以下成分制成:醋酸锌14份、硼砂6.5份、氨基磺酸5.5份、松香酸钠皂4.2份、十六烷基三甲基氯化铵2.4份、二羟甲基脲占1.5份、氢氧化钠占1.2份、三聚磷酸钠占1.1份、水650份;
(2)将步骤(1)混合物料加热至42℃,滴加松节油-乙醇混合消泡剂,并保温低速搅拌1.5小时,搅拌速度为90转/分钟,然后置于离心机中在1600转/分钟下离心处理11分钟,倒去上层液,使用质量浓度为0.13%的苏打水继续离心洗涤2次,减压抽滤后在52℃下干燥4.5小时得到改性黄麻纤维;
(3)在步骤(2)制备得到的改性黄麻纤维表面涂抹椰油,椰油用量为改性黄麻纤维质量的2.3%,然后至于恒温恒湿箱中铺展开,静止养护5.5小时,养护后经过65℃恒温干燥即可。
作为对上述方案的进一步描述,步骤(1)中所述醋酸钾-乙醇混合溶剂中醋酸钾与乙醇的混合质量比为1:15。
作为对上述方案的进一步描述,步骤(1)中所述醋酸钾-乙醇混合溶剂用量为纤维体积的3.3倍。
作为对上述方案的进一步描述,步骤(2)中所述松节油-乙醇混合消泡剂用量为混合物料质量的0.03%,其中松节油与乙醇的质量比为1:2.2。
作为对上述方案的进一步描述,步骤(3)中所述恒温恒湿箱中温度设置为19℃,相对湿度为66%。
实施例3
一种提高黄麻纤维品质的加工方法,包括以下步骤:
(1)将漂洗处理后的黄麻纤维置于醋酸钾-乙醇混合溶剂中,在350转/分钟下搅拌混合20分钟,加入纤维改性剂,用量为混合溶剂质量的5.5%,该纤维改性剂按照重量份计由以下成分制成:醋酸锌16份、硼砂7.0份、氨基磺酸6.0份、松香酸钠皂4.5份、十六烷基三甲基氯化铵2.5份、二羟甲基脲占1.6份、氢氧化钠占1.4份、三聚磷酸钠占1.2份、水700份;
(2)将步骤(1)混合物料加热至45℃,滴加松节油-乙醇混合消泡剂,并保温低速搅拌2小时,搅拌速度为100转/分钟,然后置于离心机中在1800转/分钟下离心处理12分钟,倒去上层液,使用质量浓度为0.14%的苏打水继续离心洗涤3次,减压抽滤后在55℃下干燥5小时得到改性黄麻纤维;
(3)在步骤(2)制备得到的改性黄麻纤维表面涂抹椰油,椰油用量为改性黄麻纤维质量的2.4%,然后至于恒温恒湿箱中铺展开,静止养护6小时,养护后经过70℃恒温干燥即可。
作为对上述方案的进一步描述,步骤(1)中所述醋酸钾-乙醇混合溶剂中醋酸钾与乙醇的混合质量比为1:16。
作为对上述方案的进一步描述,步骤(1)中所述醋酸钾-乙醇混合溶剂用量为纤维体积的3.5倍。
作为对上述方案的进一步描述,步骤(2)中所述松节油-乙醇混合消泡剂用量为混合物料质量的0.04%,其中松节油与乙醇的质量比为1:2.4。
作为对上述方案的进一步描述,步骤(3)中所述恒温恒湿箱中温度设置为18-20℃,相对湿度为65-68%。
对比例1
与实施例1的区别仅在于,使用乙醇溶液代替步骤(1)中醋酸钾-乙醇混合溶剂,其余保持一致。
对比例2
与实施例2的区别仅在于,所述纤维改性剂中省略醋酸锌、硼砂、氨基磺酸的添加,其余保持一致。
对比例3
与实施例3的区别仅在于,所述纤维改性剂中省略松香酸钠皂、二羟甲基脲、三聚磷酸钠的添加其余保持一致。
对比例4
与实施例3的区别仅在于,省略步骤(3)中采用椰油养护处理过程,其余保持一致。
对比实验
分别使用实施例1-3和对比例1-4的方法提高黄麻纤维品质,并以专利公开号为CN102517650A公开的一种精细化黄麻纤维的加工方法作为对照,制备得到黄麻纺织纤维,保持无关变量一致,进行纤维性能评估的试验,对结果进行统计,结果如下表所示:
本发明显著提高了黄麻纤维的市场前景和经济价值,能够实现加深对黄麻纤维性能特点的研究以及对纺织品优质原料的扩充的现实意义,是一种极为值得推广使用的技术方案。
Claims (3)
1.一种提高黄麻纤维品质的加工方法,其特征在于,包括以下步骤:
(1)将漂洗处理后的黄麻纤维置于醋酸钾-乙醇混合溶剂中,在300-350转/分钟下搅拌混合15-20分钟,加入纤维改性剂,用量为混合溶剂质量的5.0-5.5%,该纤维改性剂按照重量份计由以下成分制成:醋酸锌13-16份、硼砂6.0-7.0份、氨基磺酸5.0-6.0份、松香酸钠皂4.0-4.5份、十六烷基三甲基氯化铵2.3-2.5份、二羟甲基脲占1.4-1.6份、氢氧化钠占1.0-1.4份、三聚磷酸钠占1.0-1.2份、水600-700份,所述醋酸钾-乙醇混合溶剂中醋酸钾与乙醇的混合质量比为1:14-16,醋酸钾-乙醇混合溶剂用量为纤维体积的3.0-3.5倍;
(2)将步骤(1)混合物料加热至40-45℃,滴加松节油-乙醇混合消泡剂,并保温低速搅拌1-2小时,搅拌速度为80-100转/分钟,然后置于离心机中在1500-1800转/分钟下离心处理10-12分钟,倒去上层液,使用质量浓度为0.12-0.14%的苏打水继续离心洗涤2-3次,减压抽滤后在50-55℃下干燥4-5小时得到改性黄麻纤维;
(3)在步骤(2)制备得到的改性黄麻纤维表面涂抹椰油,椰油用量为改性黄麻纤维质量的2.2-2.4%,然后置于恒温恒湿箱中铺展开,静置养护5-6小时,养护后经过60-70℃恒温干燥即可。
2.如权利要求1所述一种提高黄麻纤维品质的加工方法,其特征在于,步骤(2)中所述松节油-乙醇混合消泡剂用量为混合物料质量的0.02-0.04%,其中松节油与乙醇的质量比为1:2.0-2.4。
3.如权利要求1所述一种提高黄麻纤维品质的加工方法,其特征在于,步骤(3)中所述恒温恒湿箱中温度设置为18-20℃,相对湿度为65-68%。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810773039.5A CN108978201B (zh) | 2018-07-14 | 2018-07-14 | 一种提高黄麻纤维品质的加工方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810773039.5A CN108978201B (zh) | 2018-07-14 | 2018-07-14 | 一种提高黄麻纤维品质的加工方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN108978201A CN108978201A (zh) | 2018-12-11 |
CN108978201B true CN108978201B (zh) | 2023-06-13 |
Family
ID=64549033
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201810773039.5A Active CN108978201B (zh) | 2018-07-14 | 2018-07-14 | 一种提高黄麻纤维品质的加工方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN108978201B (zh) |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2334035B (en) * | 1998-02-09 | 2000-01-12 | Indian Jute Ind Res | Synergistic jute and/or allied fibre lubricating composition for improvement in productivity in jute industry |
AU2005224051B2 (en) * | 2004-03-23 | 2010-10-14 | Basf Se | Fungicidal detergent compositions |
JP5147252B2 (ja) * | 2007-02-02 | 2013-02-20 | 小松精練株式会社 | 透湿性防水布帛 |
CN102517650A (zh) * | 2011-11-28 | 2012-06-27 | 江苏紫荆花纺织科技股份有限公司 | 一种精细化黄麻纤维的加工方法 |
BR112014029306A2 (pt) * | 2012-05-24 | 2017-06-27 | Momentive Performance Mat Inc | composição e método para tratar têxteis |
CN107476049A (zh) * | 2017-08-30 | 2017-12-15 | 常州豫春化工有限公司 | 一种改性亚麻纤维的制备方法 |
CN107435238A (zh) * | 2017-08-31 | 2017-12-05 | 太仓雄鹰皮具有限公司 | 一种服装面料用环保耐久抗静电剂及其制备方法 |
CN107675270B (zh) * | 2017-09-29 | 2018-10-02 | 中国农业科学院麻类研究所 | 一种梯次利用麻类韧皮原料的方法 |
CN107630359A (zh) * | 2017-09-29 | 2018-01-26 | 界首市恒吉服饰有限责任公司 | 一种提高亚麻纤维布舒适性的方法 |
-
2018
- 2018-07-14 CN CN201810773039.5A patent/CN108978201B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN108978201A (zh) | 2018-12-11 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN1208505C (zh) | 竹纤维及其制造方法 | |
CN104997206B (zh) | 一种具有抑菌作用的竹纤维服装面料 | |
CN106978716B (zh) | 夏季清凉女装及其制备方法 | |
CN105442059B (zh) | 一种抗菌性能好的织造用龙须草纤维 | |
CN102230296B (zh) | 一种非织造材料用染色木浆纸的制备方法 | |
CN104195650A (zh) | 一种可纺性柔软椰壳细纤维生产工艺及其制品应用 | |
CN101353824B (zh) | 二次加溶剂物理溶解草植物纤维的方法 | |
CN103835005A (zh) | 一种罗布麻闪爆和超临界二氧化碳流体联合脱胶方法 | |
CN105133135B (zh) | 一种竹纤维与麻纤维混纺布料 | |
CN105297149A (zh) | 一种竹纤维及其制备方法 | |
CN108978201B (zh) | 一种提高黄麻纤维品质的加工方法 | |
CN103276597B (zh) | 一种山羊绒两型纤维的染色工艺 | |
CN101210350B (zh) | 一种竹纤维有机加工工艺 | |
CN104963219B (zh) | 提高活性染料在木棉纤维上的上染率及固色率的方法 | |
CN103850036B (zh) | 床单面料 | |
CN109914124A (zh) | 一种植物提取物改性制备的麻纤维及其制备方法 | |
CN105506805A (zh) | 一种玄武岩纤维增强改性苘麻纤维复合材料的制备方法 | |
CN105231502A (zh) | 一种新型内衣用抗菌面料 | |
CN101130887A (zh) | 应用复合酶对黄麻进行脱胶的方法 | |
CN109913966B (zh) | 一种利用植物纤维素制备高强度人造纤维丝的方法 | |
CN105220242A (zh) | 一种柔软的织造用龙须草纤维 | |
CN110230111A (zh) | 一种以白杨木为原料制备莱赛尔纤维的方法 | |
CN108978269A (zh) | 一种提高涤纶织物染色牢度的处理方法 | |
CN105671957B (zh) | 用于高支纯棉纱线上浆的复合浆料制备、应用及退浆方法 | |
CN113774659A (zh) | 一种积雪草纤维的制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant |