CN108967425B - Monochamus alternatus lure rod and preparation method and application thereof - Google Patents
Monochamus alternatus lure rod and preparation method and application thereof Download PDFInfo
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- CN108967425B CN108967425B CN201811009607.0A CN201811009607A CN108967425B CN 108967425 B CN108967425 B CN 108967425B CN 201811009607 A CN201811009607 A CN 201811009607A CN 108967425 B CN108967425 B CN 108967425B
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/06—Unsaturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/34—Shaped forms, e.g. sheets, not provided for in any other sub-group of this main group
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N27/00—Biocides, pest repellants or attractants, or plant growth regulators containing hydrocarbons
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
- A01N35/06—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing keto or thioketo groups as part of a ring, e.g. cyclohexanone, quinone; Derivatives thereof, e.g. ketals
Abstract
The invention relates to a monochamus alternatus attractant rod and a preparation method and application thereof, wherein the monochamus alternatus attractant rod comprises the following raw materials in parts by weight: 1-2 parts of (3R,6E) -2, 3-dihydro-methyl farnesyl ester, 1-3 parts of 3-hydroxycyclohexyl-2-ketone, 2-4 parts of alpha-pinene, 2-4 parts of beta-pinene, 5-10 parts of methyl abietate and 75-85 parts of diatomite. The monochamus alternatus attractant rod contains a sex attractant with a strong attraction effect on monochamus alternatus, and the odor emitted by alpha-pinene and beta-pinene can attract monochamus alternatus. Methyl abietate is mainly used for slowing down the release of the attractant. The monochamus alternatus attractant rod can be inserted into the trapping device, and continuously releases attractant smell for a long time to attract monochamus alternatus to enter the trapping device. The effect is very good, and the pine needle nematode control agent can be used for controlling the population density of monochamus alternatus forests and inhibiting the spread and spread of pine needle nematode diseases.
Description
Technical Field
The invention belongs to the field of forestry science, and particularly relates to a monochamus alternatus lure rod and a preparation method and application thereof.
Background
Monochamus alternatus hope is a trunk-boring pest which is seriously harmful in forestry, can cause pine wilt and death, and is also a main vector insect of pine wilt disease, namely pine nematode disease. The method controls the population quantity and the growth trend of monochamus alternatus, reduces the population density of monochamus alternatus in forests, is one of important ways for controlling the spread and the spread of pine nematode diseases, and has important effect on protecting economic forests and landscape forests.
The attractant is used for trapping Monochamus alternatus, is a pollution-free ecological prevention and control technology which is small in amount, efficient, environment-friendly and not easy to generate resistance, and has been widely applied to production. In order to protect forest resources, all levels of forestry departments trap monochamus alternatus annually, and a large amount of manpower and material resources are consumed in the process.
At present, a plurality of monochamus alternatus attractants exist in the market, but the monochamus alternatus attractants have the defects of complex components, high production cost, unsatisfactory attracting effect and the like. Therefore, how to obtain a safe, efficient, environment-friendly and simple-ingredient monochamus alternatus attractant is a technical problem to be solved urgently by technical personnel in the field.
Disclosure of Invention
One purpose of the invention is to provide a monochamus alternatus lure rod.
The monochamus alternatus attractant rod comprises the following raw materials in parts by weight: 1-2 parts of (3R,6E) -2, 3-dihydro-methyl farnesyl ester, 1-3 parts of 3-hydroxycyclohexyl-2-ketone, 2-4 parts of alpha-pinene, 2-4 parts of beta-pinene, 5-10 parts of methyl abietate and 75-85 parts of diatomite.
The Monochamus alternatus attractant rod comprises (3R,6E) -2, 3-dihydromethyl farnesyl ester and 3-hydroxycyclohexan-2-ketone, and has a sex attractant with strong attraction effect on Monochamus alternatus. Alpha-pinene and beta-pinene, both of which are mainly present in pine trees, emit odors that attract monochamus alternatus. Methyl abietate is mainly used for slowing down the release of the attractant. The monochamus alternatus attractant rod can be inserted into the trapping device, and continuously releases attractant smell for a long time to attract monochamus alternatus to enter the trapping device. The effect is very good, and the pine needle nematode control agent can be used for controlling the population density of monochamus alternatus forests and inhibiting the spread and spread of pine needle nematode diseases.
In addition, the monochamus alternatus lure rod can also have the following additional technical characteristics:
as a preferred embodiment of the invention, the monochamus alternatus lure rod comprises the following raw materials in parts by weight: 1 part of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 3 parts of 3-hydroxycyclohexan-2-one, 2 parts of alpha-pinene, 4 parts of beta-pinene, 5 parts of methyl abietate and 85 parts of diatomite.
As a preferred embodiment of the invention, the monochamus alternatus lure rod comprises the following raw materials in parts by weight: 2 parts of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 1 part of 3-hydroxycyclohexan-2-one, 4 parts of alpha-pinene, 2 parts of beta-pinene, 10 parts of methyl abietate and 75 parts of diatomite.
As a preferred embodiment of the invention, the monochamus alternatus lure rod comprises the following raw materials in parts by weight: 1.5 parts of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 2 parts of 3-hydroxycyclohexan-2-one, 3 parts of alpha-pinene, 3 parts of beta-pinene, 7 parts of methyl abietate and 80 parts of diatomite.
The invention also aims to provide a preparation method of the monochamus alternatus lure rod.
The preparation method of the monochamus alternatus lure rod comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring, and pressing into a rod shape by a machine to obtain the Monochamus alternatus attractant rod.
Further, when the diatomite and the water are added and stirred, the stirring time is 3min to 8 min.
The invention also aims to provide the application of the monochamus alternatus lure rod in the preparation of other products capable of luring monochamus alternatus.
Additional aspects and advantages of the invention will be set forth in part in the description which follows and, in part, will be obvious from the description, or may be learned by practice of the invention.
Detailed Description
The following detailed description of embodiments of the invention is intended to be illustrative, and not to be construed as limiting the invention.
Example 1
Embodiment 1 provides a monochamus alternatus lure rod, which comprises the following raw materials in parts by weight: 1 part of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 1 part of 3-hydroxycyclohexan-2-one, 3 parts of alpha-pinene, 3 parts of beta-pinene, 5 parts of methyl abietate and 85 parts of diatomite.
The preparation method of the monochamus alternatus lure rod in the embodiment 1 comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring for 3min, and pressing into a rod shape by using a machine to obtain the Monochamus alternatus attractant rod.
Example 2
Embodiment 2 provides a monochamus alternatus lure rod, which comprises the following raw materials in parts by weight: 1 part of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 2 parts of 3-hydroxycyclohexan-2-one, 2 parts of alpha-pinene, 4 parts of beta-pinene, 7 parts of methyl abietate and 82 parts of diatomite.
The preparation method of the monochamus alternatus lure rod in the embodiment 2 comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring for 8min, and pressing into a rod shape by using a machine to obtain the Monochamus alternatus attractant rod.
Example 3
Embodiment 3 provides a monochamus alternatus lure rod, which comprises the following raw materials in parts by weight: 1.5 parts of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 3 parts of 3-hydroxycyclohexan-2-one, 3 parts of alpha-pinene, 3 parts of beta-pinene, 10 parts of methyl abietate and 75 parts of diatomite.
The preparation method of the monochamus alternatus lure rod in the embodiment 3 comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring for 4min, and pressing into a rod shape by using a machine to obtain the Monochamus alternatus attractant rod.
Example 4
Embodiment 4 provides a monochamus alternatus lure rod, which comprises the following raw materials in parts by weight: 1.5 parts of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 2 parts of 3-hydroxycyclohexan-2-one, 4 parts of alpha-pinene, 2 parts of beta-pinene, 8 parts of methyl abietate and 80 parts of diatomite.
The preparation method of the monochamus alternatus lure rod in the embodiment 4 comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring for 5min, and pressing into a rod shape by using a machine to obtain the Monochamus alternatus attractant rod.
Example 5
Embodiment 5 provides a monochamus alternatus lure rod, which comprises the following raw materials in parts by weight: 2 parts of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 1 part of 3-hydroxycyclohexan-2-one, 3 parts of alpha-pinene, 3 parts of beta-pinene, 5 parts of methyl abietate and 85 parts of diatomite.
The preparation method of the monochamus alternatus lure rod in the embodiment 5 comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring for 6min, and pressing into a rod shape by using a machine to obtain the Monochamus alternatus attractant rod.
Example 6
Embodiment 6 provides a monochamus alternatus lure rod, which comprises the following raw materials in parts by weight: 2 parts of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 2 parts of 3-hydroxycyclohexan-2-one, 2 parts of alpha-pinene, 4 parts of beta-pinene, 7 parts of methyl abietate and 80 parts of diatomite.
The preparation method of the monochamus alternatus lure rod in the embodiment 6 comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring for 7min, and pressing into a rod shape by using a machine to obtain the Monochamus alternatus attractant rod.
Example 7
Embodiment 7 provides a monochamus alternatus lure rod, which comprises the following raw materials in parts by weight: 1.5 parts of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 3 parts of 3-hydroxycyclohexan-2-one, 3 parts of alpha-pinene, 3 parts of beta-pinene, 10 parts of methyl abietate and 78 parts of diatomite.
The preparation method of the monochamus alternatus lure rod in the embodiment 7 comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring for 8min, and pressing into a rod shape by using a machine to obtain the Monochamus alternatus attractant rod.
Example 8
Embodiment 8 provides a monochamus alternatus lure rod, which comprises the following raw materials in parts by weight: 1.5 parts of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 2 parts of 3-hydroxycyclohexan-2-one, 4 parts of alpha-pinene, 2 parts of beta-pinene, 8 parts of methyl abietate and 82 parts of diatomite.
The preparation method of the monochamus alternatus lure rod in the embodiment 8 comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring for 3min, and pressing into a rod shape by using a machine to obtain the Monochamus alternatus attractant rod.
Example 9
Embodiment 9 provides a monochamus alternatus lure rod, which comprises the following raw materials in parts by weight: 1 part of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 1 part of 3-hydroxycyclohexan-2-one, 3 parts of alpha-pinene, 3 parts of beta-pinene, 5 parts of methyl abietate and 85 parts of diatomite.
The preparation method of the monochamus alternatus lure rod in the embodiment 9 comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring for 5min, and pressing into a rod shape by using a machine to obtain the Monochamus alternatus attractant rod.
Example 10
Embodiment 10 provides a monochamus alternatus lure rod, which comprises the following raw materials in parts by weight: 1 part of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 2 parts of 3-hydroxycyclohexan-2-one, 2 parts of alpha-pinene, 4 parts of beta-pinene, 10 parts of methyl abietate and 79 parts of diatomite.
The preparation method of the monochamus alternatus lure rod in the embodiment 10 comprises the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring for 6min, and pressing into a rod shape by using a machine to obtain the Monochamus alternatus attractant rod.
The Monochamus alternatus lure rods prepared in examples 1-10 were placed in traps, while a blank group and a commercial product were set as a control group, 6 specimens per group, with a spacing of about 30 meters between adjacent traps. The trapping results are checked once a week, and the number of longicorn is recorded in detail, and the time of one month is taken as a limit. The test results are shown in Table 1.
Table 1: examples and control group Experimental results on the number of attracted longicorn
Attractant | Total number of heads | Mean number of |
Example 1 | 897 | 149.5 |
Example 2 | 881 | 146.8 |
Example 3 | 906 | 151.0 |
Example 4 | 877 | 146.2 |
Example 5 | 906 | 151.0 |
Example 6 | 1012 | 168.7 |
Example 7 | 903 | 150.5 |
Example 8 | 928 | 154.7 |
Example 9 | 914 | 152.3 |
Example 10 | 889 | 148.2 |
Control group | 684 | 114.0 |
Blank group | 0 | 0.0 |
As can be seen from table 1: compared with a control group, the monochamus alternatus attractant rod prepared by the invention has a more remarkable attracting effect, and the trapping amount is obviously superior to that of the other side, so that the advancement of the monochamus alternatus attractant rod in the technology is proved, and the monochamus alternatus attractant rod can be used for controlling the population density of monochamus alternatus woodland and inhibiting the spread and the spread of pine wilt diseases.
In conclusion, the monochamus alternatus attractant rod disclosed by the invention contains (3R,6E) -2, 3-dihydromethyl farnesyl ester and 3-hydroxycyclohexan-2-ketone, and is a sex attractant with strong attraction effect on monochamus alternatus. Alpha-pinene and beta-pinene, both of which are mainly present in pine trees, emit odors that attract monochamus alternatus. Methyl abietate is mainly used for slowing down the release of the attractant. The monochamus alternatus attractant rod can be inserted into the trapping device, and continuously releases attractant smell for a long time to attract monochamus alternatus to enter the trapping device. The effect is very good, and the pine needle nematode control agent can be used for controlling the population density of monochamus alternatus forests and inhibiting the spread and spread of pine needle nematode diseases.
In the description herein, references to the description of the term "one embodiment," "some embodiments," "an example," "a specific example," or "some examples," etc., mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above are not necessarily intended to refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples. Furthermore, various embodiments or examples and features of different embodiments or examples described in this specification can be combined and combined by one skilled in the art without contradiction.
Although embodiments of the present invention have been shown and described above, it is understood that the above embodiments are exemplary and should not be construed as limiting the present invention, and that variations, modifications, substitutions and alterations can be made to the above embodiments by those of ordinary skill in the art within the scope of the present invention.
Claims (4)
1. The monochamus alternatus lure rod is characterized by being prepared from the following raw materials in parts by weight: 2 parts of (3R,6E) -2, 3-dihydromethyl farnesyl ester, 2 parts of 3-hydroxycyclohexan-2-one, 2 parts of alpha-pinene, 4 parts of beta-pinene, 7 parts of methyl abietate and 80 parts of diatomite.
2. The method for preparing the monochamus alternatus lure rod according to claim 1, which is characterized by comprising the following steps: firstly, mixing the (3R,6E) -2, 3-dihydromethyl farnesyl ester, the 3-hydroxycyclohexyl-2-one, the alpha-pinene, the beta-pinene and the methyl abietate, then adding the diatomite and the water, stirring, and pressing into a rod shape by a machine to obtain the Monochamus alternatus attractant rod.
3. The method for preparing the Monochamus alternatus lure rod according to claim 2, wherein stirring time is 3-8 min when the diatomite and the water are added and stirred.
4. Use of the Monochamus alternatus attractant rod of claim 1 or the Monochamus alternatus attractant rod prepared by the preparation method of any one of claims 2 to 3 in preparation of other products capable of attracting Monochamus alternatus.
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