CN108948929B - Preparation method of cool wicker product - Google Patents
Preparation method of cool wicker product Download PDFInfo
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- CN108948929B CN108948929B CN201810586439.5A CN201810586439A CN108948929B CN 108948929 B CN108948929 B CN 108948929B CN 201810586439 A CN201810586439 A CN 201810586439A CN 108948929 B CN108948929 B CN 108948929B
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- wicker
- cool
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- powder
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
- C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09D133/10—Homopolymers or copolymers of methacrylic acid esters
- C09D133/12—Homopolymers or copolymers of methyl methacrylate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/38—Boron-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
- C08K9/06—Ingredients treated with organic substances with silicon-containing compounds
Abstract
The invention discloses a preparation method of an air-dried wicker product, which comprises the following operation steps: (1) uniformly mixing butyl methacrylate, methyl methacrylate, trifluoroethyl acrylate, deionized water, an emulsifier and an initiator, heating to 75-80 ℃, and carrying out polymerization treatment for 2-3 hours to prepare a polymerization emulsion; (2) adding andalusite powder, feldspar powder and tourmaline powder into the modification liquid to obtain a cool feeling additive; (3) uniformly mixing the cool additive, the polymerization emulsion, the dispersant and the defoaming agent to prepare the wicker cool coating; (4) and coating the wicker cool feeling coating on the surface of the wicker product after the wicker product is knitted and formed, and then putting the wicker product into an oven for drying treatment to obtain a finished product. The preparation method of the cool wicker product provided by the invention is simple to operate and low in cost, and the prepared wicker product has cool surface, so that wicker products used in summer, such as wicker chairs, and the like, have more excellent cooling effect.
Description
Technical Field
The invention belongs to the technical field of wicker weaving, and particularly relates to a preparation method of a cool wicker product.
Background
Wicker products are handcrafts widely distributed among China, "basket weaves, and families all have", because the raw material sources of the process are very wide. The wicker products are deeply favored by consumers because of unique and beautiful appearance and simple color, but no wicker products with cool feeling are sold in the market at present.
Disclosure of Invention
In order to further enrich wicker products, the invention provides a preparation method of a cool wicker product.
The invention is realized by the following technical scheme.
A preparation method of a cool wicker product comprises the following operation steps:
(1) according to the weight portion, after 17-22 portions of butyl methacrylate, 30-46 portions of methyl methacrylate, 5-9 portions of trifluoroethyl acrylate, 17-22 portions of deionized water, 0.4-0.8 portion of emulsifier and 0.1-0.3 portion of initiator are uniformly mixed, heated to 75-80 ℃, and polymerized for 2-3 hours to prepare polymerization emulsion;
(2) adding 18-25 parts by weight of andalusite powder, 10-15 parts by weight of feldspar powder and 16-20 parts by weight of tourmaline powder into a modification liquid, heating the modification liquid to 55-60 ℃, and carrying out heat preservation treatment for 2-3 hours to obtain the cool additive, wherein the modification liquid is prepared from the following components in parts by weight: 55-60 parts of ethanol, 3-6 parts of 4-aminopropylmethyldimethoxysilane and 8-10 parts of N-2-aminoethyl-3-aminopropyltrimethoxysilane;
(3) uniformly mixing 25-30 parts of cool additive, 70-80 parts of polymerized emulsion, 2-5 parts of dispersant and 1-2 parts of defoamer according to parts by weight to prepare the wicker cool coating;
(4) and coating the wicker cool feeling coating on the surface of the wicker product after the wicker product is knitted and formed, and then putting the wicker product into an oven for drying treatment to obtain a finished product.
Specifically, the emulsifier in the step (1) is any one of polyoxyethylene octylphenol ether or polyoxyethylene nonylphenol ether.
Specifically, the initiator is any one of di-tert-butyl peroxide and dicumyl peroxide.
Specifically, in the step (2), the average particle diameters of andalusite powder, feldspar powder and tourmaline powder are all 300 meshes.
Specifically, in the step (3), the dispersant is glyceryl tristearate, and the defoaming agent is emulsified silicone oil.
Specifically, in the step (4), the drying temperature is 55-60 ℃, and the drying time is 3-4 hours.
According to the technical scheme, the beneficial effects of the invention are as follows:
the preparation method of the cool wicker product provided by the invention is simple to operate and low in cost, and the prepared wicker product has cool surface, so that wicker products used in summer, such as wicker chairs, and the like, have more excellent cooling effect. The polymerized emulsion prepared in the step (1) has excellent film-forming property, strong adhesive force of a film layer and strong adhesive force to a cool additive, so that the phenomenon of separation of the cool additive is not easy to occur in the use process of the wicker product; according to the invention, the monaminosilane and the bisaminosilane are cooperatively used for processing the andalusite powder, the feldspar powder and the tourmaline powder, so that the dispersion effect of the andalusite powder, the feldspar powder and the tourmaline powder in the polymerized emulsion can be effectively improved, and the spatial distribution of the andalusite powder, the feldspar powder and the tourmaline powder can be more regular, so that the cool feeling effect of the wicker product is more obvious; after the andalusite powder, the feldspar powder and the tourmaline powder are synergistic, the cool feeling effect is obvious, the surface of the wicker product can be effectively made to have cool feeling for a long time, and the applicability of the wicker product is greatly improved.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the following examples further illustrate the present invention in detail. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Example 1
A preparation method of a cool wicker product comprises the following operation steps:
(1) according to the weight portion, after 17 portions of butyl methacrylate, 30 portions of methyl methacrylate, 5 portions of trifluoroethyl acrylate, 17 portions of deionized water, 0.4 portion of emulsifier and 0.1 portion of initiator are uniformly mixed, heating to 75 ℃, and carrying out polymerization treatment for 2 hours to prepare a polymerization emulsion;
(2) adding 18 parts by weight of andalusite powder, 10 parts by weight of feldspar powder and 16 parts by weight of tourmaline powder into a modification liquid, heating the modification liquid to 55 ℃, and carrying out heat preservation treatment for 2 hours to obtain the cool additive, wherein the modification liquid is prepared from the following components in parts by weight: 55 parts of ethanol, 3 parts of 4-aminopropylmethyldimethoxysilane and 8 parts of N-2-aminoethyl-3-aminopropyltrimethoxysilane;
(3) uniformly mixing 25 parts of cool additive, 70 parts of polymerized emulsion, 2 parts of dispersant and 1 part of defoamer according to parts by weight to prepare the wicker cool paint;
(4) and coating the wicker cool feeling coating on the surface of the wicker chair after the wicker chair is woven and formed, and then putting the wicker chair into an oven for drying treatment to obtain a finished product.
Specifically, the emulsifier in the step (1) is octylphenol polyoxyethylene ether.
Specifically, the initiator is di-tert-butyl peroxide.
Specifically, in the step (2), the average particle diameters of andalusite powder, feldspar powder and tourmaline powder are all 300 meshes.
Specifically, in the step (3), the dispersant is glyceryl tristearate, and the defoaming agent is emulsified silicone oil.
Specifically, in the step (4), the temperature of the drying treatment is 55 ℃, and the time of the drying treatment is 3 hours.
The wicker chair prepared by the embodiment has a remarkable cool surface effect.
Example 2
A preparation method of a cool wicker product comprises the following operation steps:
(1) uniformly mixing 20 parts of butyl methacrylate, 38 parts of methyl methacrylate, 7 parts of trifluoroethyl acrylate, 20 parts of deionized water, 0.6 part of emulsifier and 0.2 part of initiator according to parts by weight, heating to 78 ℃, and carrying out polymerization treatment for 2.5 hours to prepare a polymerization emulsion;
(2) adding 23 parts by weight of andalusite powder, 13 parts by weight of feldspar powder and 18 parts by weight of tourmaline powder into a modification liquid, heating the modification liquid to 58 ℃, and carrying out heat preservation treatment for 2.5 hours to obtain the cool additive, wherein the modification liquid is prepared from the following components in parts by weight: 58 parts of ethanol, 5 parts of 4-aminopropylmethyldimethoxysilane and 9 parts of N-2-aminoethyl-3-aminopropyltrimethoxysilane;
(3) uniformly mixing 28 parts of cool additive, 75 parts of polymerization emulsion, 3 parts of dispersant and 2 parts of defoamer according to parts by weight to prepare the wicker cool paint;
(4) and coating the wicker cool feeling coating on the surface of the wicker mat after the wicker mat is woven and formed, and then putting the wicker mat into an oven to be dried to obtain a finished product.
Specifically, the emulsifier in the step (1) is nonylphenol polyoxyethylene ether.
Specifically, the initiator is dicumyl peroxide.
Specifically, in the step (2), the average particle diameters of andalusite powder, feldspar powder and tourmaline powder are all 300 meshes.
Specifically, in the step (3), the dispersant is glyceryl tristearate, and the defoaming agent is emulsified silicone oil.
Specifically, in the step (4), the temperature of the drying treatment is 58 ℃, and the time of the drying treatment is 3.5 hours.
The wicker summer sleeping mat prepared by the embodiment has a remarkable surface cool feeling effect.
Example 3
A preparation method of a cool wicker product comprises the following operation steps:
(1) uniformly mixing 22 parts of butyl methacrylate, 46 parts of methyl methacrylate, 9 parts of trifluoroethyl acrylate, 22 parts of deionized water, 0.8 part of emulsifier and 0.3 part of initiator in parts by weight, heating to 80 ℃, and carrying out polymerization treatment for 3 hours to prepare a polymerization emulsion;
(2) adding 25 parts by weight of andalusite powder, 15 parts by weight of feldspar powder and 20 parts by weight of tourmaline powder into a modification liquid, heating the modification liquid to 60 ℃, and carrying out heat preservation treatment for 3 hours to obtain the cool feeling additive, wherein the modification liquid is prepared from the following components in parts by weight: 60 parts of ethanol, 6 parts of 4-aminopropylmethyldimethoxysilane and 10 parts of N-2-aminoethyl-3-aminopropyltrimethoxysilane;
(3) uniformly mixing 30 parts of cool additive, 80 parts of polymerized emulsion, 5 parts of dispersant and 2 parts of defoamer according to parts by weight to prepare the wicker cool paint;
(4) and brushing wicker cool feeling coating on the surface of the wicker kennel after the wicker kennel is woven and formed, and then putting the wicker kennel into an oven to be dried to obtain a finished product.
Specifically, the emulsifier in the step (1) is nonylphenol polyoxyethylene ether.
Specifically, the initiator is dicumyl peroxide.
Specifically, in the step (2), the average particle diameters of andalusite powder, feldspar powder and tourmaline powder are all 300 meshes.
Specifically, in the step (3), the dispersant is glyceryl tristearate, and the defoaming agent is emulsified silicone oil.
Specifically, in the step (4), the temperature of the drying treatment is 60 ℃, and the time of the drying treatment is 4 hours.
The wicker kennel prepared in the embodiment has a remarkable cool feeling effect on the surface, and can provide a cool inhabitation environment for pet dogs in summer.
Finally, the above embodiments are only for illustrating the technical solutions of the present invention and not for limiting, although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions may be made to the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention, and all of them should be covered in the claims of the present invention.
Claims (6)
1. The preparation method of the cool wicker product is characterized by comprising the following operation steps:
(1) according to the weight portion, after 17-22 portions of butyl methacrylate, 30-46 portions of methyl methacrylate, 5-9 portions of trifluoroethyl acrylate, 17-22 portions of deionized water, 0.4-0.8 portion of emulsifier and 0.1-0.3 portion of initiator are uniformly mixed, heated to 75-80 ℃, and polymerized for 2-3 hours to prepare polymerization emulsion;
(2) adding 18-25 parts by weight of andalusite powder, 10-15 parts by weight of feldspar powder and 16-20 parts by weight of tourmaline powder into a modification liquid, heating the modification liquid to 55-60 ℃, and carrying out heat preservation treatment for 2-3 hours to obtain the cool additive, wherein the modification liquid is prepared from the following components in parts by weight: 55-60 parts of ethanol, 3-6 parts of 4-aminopropylmethyldimethoxysilane and 8-10 parts of N-2-aminoethyl-3-aminopropyltrimethoxysilane;
(3) uniformly mixing 25-30 parts of cool additive, 70-80 parts of polymerized emulsion, 2-5 parts of dispersant and 1-2 parts of defoamer according to parts by weight to prepare the wicker cool coating;
(4) and coating the wicker cool feeling coating on the surface of the wicker product after the wicker product is knitted and formed, and then putting the wicker product into an oven for drying treatment to obtain a finished product.
2. The method for preparing a cool wicker product according to claim 1, wherein the emulsifier in step (1) is any one of octylphenol polyoxyethylene ether or nonylphenol polyoxyethylene ether.
3. The method for preparing a cool wicker product according to claim 1, wherein the initiator is any one of di-tert-butyl peroxide and dicumyl peroxide.
4. The method for preparing a cool wicker product according to claim 1, wherein in the step (2), the average particle sizes of the andalusite powder, the feldspar powder and the tourmaline powder are all 300 meshes.
5. The method for preparing a cool wicker product according to claim 1, wherein in the step (3), the dispersant is glyceryl tristearate and the defoaming agent is silicone emulsion.
6. The method for preparing a cool wicker product according to claim 1, wherein in the step (4), the temperature of the drying treatment is 55-60 ℃, and the time of the drying treatment is 3-4 hours.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810586439.5A CN108948929B (en) | 2018-06-08 | 2018-06-08 | Preparation method of cool wicker product |
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| CN201810586439.5A CN108948929B (en) | 2018-06-08 | 2018-06-08 | Preparation method of cool wicker product |
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| CN108948929A CN108948929A (en) | 2018-12-07 |
| CN108948929B true CN108948929B (en) | 2020-09-29 |
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| CN109938419B (en) * | 2019-03-27 | 2021-02-09 | 上海小蓝象服装有限公司 | Sweat-removing naked-feeling triple bacteriostatic underpants and preparation method thereof |
| CN112045812A (en) * | 2020-07-27 | 2020-12-08 | 安徽阜南县万家和工艺品有限公司 | Treatment process for improving cool contact feeling of wicker deck chair |
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