CN108911699A - The preparation method of ceramics based on composite rock mineral - Google Patents

The preparation method of ceramics based on composite rock mineral Download PDF

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Publication number
CN108911699A
CN108911699A CN201810937497.8A CN201810937497A CN108911699A CN 108911699 A CN108911699 A CN 108911699A CN 201810937497 A CN201810937497 A CN 201810937497A CN 108911699 A CN108911699 A CN 108911699A
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China
Prior art keywords
parts
mud
preparation
filtering
mixed
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CN201810937497.8A
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Chinese (zh)
Inventor
赖国全
赖国光
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Deyang Aurora Creative Design Co Ltd
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Deyang Aurora Creative Design Co Ltd
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Priority to CN201810937497.8A priority Critical patent/CN108911699A/en
Publication of CN108911699A publication Critical patent/CN108911699A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/13Compounding ingredients
    • C04B33/131Inorganic additives
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/13Compounding ingredients
    • C04B33/16Lean materials, e.g. grog, quartz
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3208Calcium oxide or oxide-forming salts thereof, e.g. lime
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3232Titanium oxides or titanates, e.g. rutile or anatase
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/327Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3272Iron oxides or oxide forming salts thereof, e.g. hematite, magnetite

Abstract

The invention discloses the preparation methods of the ceramics based on composite rock mineral, laterite, porcelain sand, smart mud, porcelain mud, quartz are mixed in proportion, through ball milling, filtering, then in 1034~1123 DEG C of 2~3h of stirring;Boccaro shale, bloodstone, anatase, kaolinite, illite, chlorite, calcite are mixed in proportion, through ball milling, filtering, then in 982~1080 DEG C of 2~3h of stirring;Mixed at 800~900 DEG C, filtering, midge, vacuum pugging, be pressed into mud item and sealing it is aging, and repeatedly vacuum pugging, compacting mud item and seal it is aging 3~5 times, be made pug.Preparation method of the present invention is easy, convenient for operating with.

Description

The preparation method of ceramics based on composite rock mineral
Technical field
The present invention relates to ceramic fields, and in particular to the preparation method of the ceramics based on composite rock mineral.
Background technique
Shale is a kind of sedimentary rock, complicated component, but all joints with thin laminated or thin slice stratiform, mainly by clay The rock formed through pressure and temperature is deposited, but is wherein contaminated with quartz, the clast of feldspar and other chemical substances, according to The ingredient of its tramp material can be divided into:Calcareous shale, irony shale, siliceous shale, carbonaceous shale, black shale, oil shale It is likely to become iron ore Deng wherein irony shale, oil shale can run oil, and black shale can be used as the instruction of petroleum Stratum.
Shale is formed in the environment of hydrostatic, and silt is by prolonged deposition, so being frequently present in lake, river three The area Jiao Zhou also has the formation of shale in the continental shelf of ocean, the fossil of ancient times animals and plants is also usually comprised in shale.Have When also have the ichnofossil of animal or even the trace of ancient times raindrop that may all preserve in shale.
The general name of ceramics, pottery and porcelain.The traditional concept of ceramics refers to all is with Inorganic nonmetal minerals such as clays The artificial industrial products of raw material.It includes that the mixture by clay or containing clay is kneaded, forming, calcining and it is manufactured each Kind product.Its range is belonged to most fine fine pottery and porcelain by most coarse earthenware.Primary raw material for it is to take The silicate mineral (such as clay, feldspar, quartz) in nature, therefore with the works such as glass, cement, enamel, refractory material Industry belongs to the scope of " silicate industry ".
However between the ceramic material of existing shale minerals in firing, efficiency is lower, and yield rate is relatively low, obtains The consistency of the finished product arrived is also poor.
Summary of the invention
The technical problem to be solved by the present invention is to, and it is an object of the present invention to provide based on shale minerals ceramics preparation method, It solves the problems, such as.
The present invention is achieved through the following technical solutions:
The preparation method of ceramics based on shale minerals, which is characterized in that include the following steps:
(1) laterite, porcelain sand, smart mud, porcelain mud, quartz are mixed in proportion, through ball milling, filtering, then 1034~1123 DEG C stirring 2~3h;
(2) Boccaro shale, bloodstone, anatase, kaolinite, illite, chlorite, calcite are mixed in proportion, is passed through Ball milling, filtering, then in 982~1080 DEG C of 2~3h of stirring;
(3) object that step (1) and step (3) obtain is mixed at 800~900 DEG C, filtering, midge, vacuum pugging, It is pressed into mud item and sealing is aging, and vacuum pugging, compacting mud item and sealing aging 3~5 times repeatedly, pug is made.
The preparation method of ceramics based on shale minerals, in 1100 DEG C of stirring 2.5h in the step (1).
In 989 DEG C of stirring 2.5h in the step (2).
The present invention includes the component of following parts by weight:10~16 parts of laterite, 23~36 parts of porcelain sand, smart 10~17 parts of mud, 24~39 parts of porcelain mud, quartzy 11~21 parts, 10~18 parts of Boccaro shale, 14~26 parts of bloodstone, 8~19 parts of anatase, kaolinite 13~26 parts of stone, 8~19 parts of illite, 5~16 parts of chlorite, 4~16 parts of calcite.
Component including following parts by weight:12~15 parts of laterite, 28~33 parts of porcelain sand, smart 13~16 parts of mud, porcelain mud 29 ~34 parts, quartzy 15~20 parts, 14~17 parts of Boccaro shale, 17~24 parts of bloodstone, 11~18 parts of anatase, kaolinite 18 ~22 parts, 11~17 parts of illite, 9~13 parts of chlorite, 8~14 parts of calcite.
Component including following parts by weight:13 parts of laterite, 32 parts of porcelain sand, smart 15 parts of mud, 32 parts of porcelain mud, 18 parts of quartz, 16 parts of Boccaro shale, 23 parts of bloodstone, 16 parts of anatase, 21 parts of kaolinite, 15 parts of illite, 12 parts of chlorite, calcite 11 Part.
Compared with prior art, the present invention having the following advantages and benefits:
1, the present invention is based on the preparation method of the ceramics of shale minerals, ceramic material of the invention can preferably be burnt At, and it is burnt into the better quality of high-efficient, to obtain finished product;
2, the present invention is based on the preparation method of the ceramics of shale minerals, the component of ceramic material of the invention complements each other, The compactness of obtained finished product is more preferably;
3, the present invention is based on the preparation method of the ceramics of shale minerals, preparation method of the present invention is easy, convenient for operating with.
Specific embodiment
To make the objectives, technical solutions, and advantages of the present invention clearer, below with reference to embodiment, the present invention is made Further to be described in detail, exemplary embodiment of the invention and its explanation for explaining only the invention, are not intended as to this The restriction of invention.
Embodiment 1
The present invention is based on the preparation methods of the ceramics of shale minerals, include the following steps:
(1) laterite, porcelain sand, smart mud, porcelain mud, quartz are mixed in proportion, through ball milling, filtering, then 1034~1123 DEG C stirring 2~3h;
(2) Boccaro shale, bloodstone, anatase, kaolinite, illite, chlorite, calcite are mixed in proportion, is passed through Ball milling, filtering, then in 982~1080 DEG C of 2~3h of stirring;
(3) object that step (1) and step (3) obtain is mixed at 800~900 DEG C, filtering, midge, vacuum pugging, It is pressed into mud item and sealing is aging, and vacuum pugging, compacting mud item and sealing aging 3~5 times repeatedly, pug is made.
In 1100 DEG C of stirring 2.5h in the step (1).
In 989 DEG C of stirring 2.5h in the step (2).
Component including following parts by weight:13 parts of laterite, 32 parts of porcelain sand, smart 15 parts of mud, 32 parts of porcelain mud, 18 parts of quartz, 16 parts of Boccaro shale, 23 parts of bloodstone, 16 parts of anatase, 21 parts of kaolinite, 15 parts of illite, 12 parts of chlorite, calcite 11 Part.
Above-described specific embodiment has carried out further the purpose of the present invention, technical scheme and beneficial effects It is described in detail, it should be understood that being not used to limit this hair the foregoing is merely a specific embodiment of the invention Bright protection scope, all within the spirits and principles of the present invention, any modification, equivalent substitution, improvement and etc. done should all It is included within protection scope of the present invention.

Claims (3)

1. the preparation method of the ceramics based on composite rock mineral, which is characterized in that include the following steps:
(1) laterite, porcelain sand, smart mud, porcelain mud, quartz are mixed in proportion, through ball milling, filtering, is then stirred at 1034~1123 DEG C Mix 2~3h;
(2) Boccaro shale, bloodstone, anatase, kaolinite, illite, chlorite, calcite are mixed in proportion, through ball milling, Filtering, then in 982~1080 DEG C of 2~3h of stirring;
(3) object that step (1) and step (3) obtain is mixed at 800~900 DEG C, filtering, vacuum pugging, is pressed into midge Mud item and sealing are aging, and vacuum pugging, compacting mud item and sealing aging 3~5 times repeatedly, and pug is made.
2. the preparation method of the ceramics according to claim 1 based on composite rock mineral, which is characterized in that the step (1) in 1100 DEG C of stirring 2.5h in.
3. the preparation method of the ceramics according to claim 1 based on composite rock mineral, which is characterized in that the step (2) in 989 DEG C of stirring 2.5h in.
CN201810937497.8A 2018-08-17 2018-08-17 The preparation method of ceramics based on composite rock mineral Pending CN108911699A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110526679A (en) * 2019-09-20 2019-12-03 孟津青城古建制品有限公司 A kind of city wall process for producing bricks modelled after an antique

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105218067A (en) * 2015-09-16 2016-01-06 景德镇陶瓷学院 A kind of purple sand pug and preparation method thereof
CN107935554A (en) * 2017-11-30 2018-04-20 喀左高品宝砂紫陶艺术研发有限公司 A kind of production method of green grass or young crops section purple sand pug
CN108046751A (en) * 2017-12-20 2018-05-18 湖南华联瓷业股份有限公司 A kind of ceramic material and its ceramic

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105218067A (en) * 2015-09-16 2016-01-06 景德镇陶瓷学院 A kind of purple sand pug and preparation method thereof
CN107935554A (en) * 2017-11-30 2018-04-20 喀左高品宝砂紫陶艺术研发有限公司 A kind of production method of green grass or young crops section purple sand pug
CN108046751A (en) * 2017-12-20 2018-05-18 湖南华联瓷业股份有限公司 A kind of ceramic material and its ceramic

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
刘银等: "《无机非金属材料工艺学》", 30 September 2015, 中国科学技术大学出版社 *
沈鸿才: "《结构陶瓷及应用》", 30 April 1988, 国防工业出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110526679A (en) * 2019-09-20 2019-12-03 孟津青城古建制品有限公司 A kind of city wall process for producing bricks modelled after an antique

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Application publication date: 20181130

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