CN103588449A - Method for preparing steam-pressing bricks from multiple raw mineral materials - Google Patents

Method for preparing steam-pressing bricks from multiple raw mineral materials Download PDF

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Publication number
CN103588449A
CN103588449A CN201310555801.XA CN201310555801A CN103588449A CN 103588449 A CN103588449 A CN 103588449A CN 201310555801 A CN201310555801 A CN 201310555801A CN 103588449 A CN103588449 A CN 103588449A
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China
Prior art keywords
raw material
mineral
preparation
raw
autoclaved brick
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CN201310555801.XA
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CN103588449B (en
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王长富
毛东超
王玉童
刘伟
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ANHUI FUYANG FULONG BUILDING MATERIALS Co Ltd
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ANHUI FUYANG FULONG BUILDING MATERIALS Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/91Use of waste materials as fillers for mortars or concrete

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  • Curing Cements, Concrete, And Artificial Stone (AREA)
  • Press-Shaping Or Shaping Using Conveyers (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

The invention discloses a method for preparing steam-pressing bricks from multiple raw mineral materials. The steam-pressing bricks which are prepared from the multiple raw mineral materials are prepared from the following raw materials in parts by weight: 45-50 parts of coal ash, 10-15 parts of tailing, 13-16 parts of electrolytic rock ballast, 12-16 parts of lime and 2-4 parts of composite modified mineral powder. According to the invention, a plurality of mineral substances are compounded and modified, the obtained powder can be well compatible with other raw materials, and the steam-pressing bricks are non-cracking, high in strength, environment-friendly and simple in preparation process.

Description

The preparation method of the autoclaved brick that one kind of multiple raw mineral materialss make
Technical field
The present invention relates to autoclaved brick field, is exactly the preparation method of the autoclaved brick that makes of one kind of multiple raw mineral materialss.
Background technology
Utilize (one or several of above raw material) such as flyash, cinder, coal gangue, mine tailings, residue of chemical industry or natural sand, tidal land mud as main raw material, it is non-burning brick that a kind of novel wall material of manufacturing without high-temperature calcination is referred to as, and claims again autoclaved brick.
Summary of the invention
The object of the present invention is to provide the preparation method of the autoclaved brick that one kind of multiple raw mineral materialss make.
Above-mentioned purpose realizes by following scheme:
The preparation method of the autoclaved brick that one kind of multiple raw mineral materialss make, is characterized in that:
Comprise the following steps:
(1) attapulgite, wilkinite, ground granulated blast furnace slag, oyster shell whiting, volcano rock dust are added in clear water after mixing, stir, soak after 5-8 hour, centrifugal treating 9-15min, after centrifugal, after filtering, being dried, at the temperature of 900-950 ℃, in dodging firing, dodge burning 7-9 second, take out, add in suitable quantity of water and grind together with all the other raw materials, adding 10-15% hydrochloric acid soln tune PH is 4-5 again, and ground slurry is to 400-500 order, and repeated hydrogenation sodium oxide is adjusted to neutrality, after dry, obtain composite modified mineral powder standby;
Described composite modified mineral powder is made by the raw material of following weight parts:
Attapulgite 3-5, wilkinite 10-12, ground granulated blast furnace slag 13-17, oyster shell whiting 5-8, volcano rock dust 1-2, Radix Angelicae Sinensis oil 1-2, silane coupling agent KH530 1.4-2.3, urea 0.1-0.2, Trisodium Citrate 0.1-0.3, polyoxyethylene octylphenol ether 1-2;
(2) batching: the autoclaved brick that described multi mineral raw material makes is that the raw material by following weight parts makes: flyash 45-50, mine tailing 10-15, electrolysis rock ballast 13-16, lime 12-16, composite modified mineral powder 2-4;
(3) after each raw material blending preparation being taken, add suitable quantity of water and mix, obtain compound;
(4) compound is poured into the mold standing 2-3h after moulding;
(5) carry out, again steam press maintenance, curing temperature is 180 ℃-190 ℃, and curing time is 7-8h, and pressure is 1.2-1.3MPa, after and get final product.  
The preparation method of the autoclaved brick that one kind of multiple described raw mineral materialss make, is characterized in that: the rotating speed of described whizzer is 1500-1800r/min.
The preparation method of the autoclaved brick that one kind of multiple described raw mineral materialss make, is characterized in that: the weight of the water described in step (3) and the ratio of each raw material gross weight are 0.2-0.3: 1.
Beneficial effect of the present invention is: the present invention has utilized multi mineral composite modified, and gained powder can be compatible with other raw materials well, and gained autoclaved brick does not ftracture, and intensity is high, environmental protection, and preparation technology is simple.
Embodiment
The preparation method of the autoclaved brick that one kind of multiple raw mineral materialss make, comprises the following steps:
(1) attapulgite, wilkinite, ground granulated blast furnace slag, oyster shell whiting, volcano rock dust are added in clear water after mixing, stir, soak after 6 hours, centrifugal treating 12min, the rotating speed of whizzer is 1800r/min, after centrifugal, after filtering, being dried, at the temperature of 950 ℃, in dodging firing, dodge burning 9 seconds, take out, add in suitable quantity of water and grind together with all the other raw materials, then adding 15% hydrochloric acid soln, to adjust PH be 5, after ground slurry to 500 order, repeated hydrogenation sodium oxide is adjusted to neutrality, after being dried, obtains composite modified mineral powder standby;
Described composite modified mineral powder is made by the raw material of following weight kg:
Attapulgite 5, wilkinite 10, ground granulated blast furnace slag 15, oyster shell whiting 8, volcano rock dust 1, Radix Angelicae Sinensis oil 1, silane coupling agent KH530 1.8, urea 0.1, Trisodium Citrate 0.3, polyoxyethylene octylphenol ether 1;
(2) batching: the autoclaved brick that described multi mineral raw material makes is that the raw material by following weight kg makes: flyash 50, mine tailing 10, electrolysis rock ballast 14, lime 16, composite modified mineral powder 2;
(3) after each raw material blending preparation being taken, add water and mix, the ratio of the weight of described water and each raw material gross weight is 0.3: 1, obtains compound;
(4) compound is poured into the mold standing 3h after moulding;
(5) carry out, again steam press maintenance, curing temperature is 190 ℃, and curing time is 8h, and pressure is 1.2MPa, after and get final product.  
Its properties of autoclaved brick that the present embodiment is produced after testing all can meet JC239-2001 < < flyash brick > > MU10 class requirement, its ultimate compression strength is 14.4MPa, folding strength is 4.2MPa, and dry shrinkage, carbonation coefficient, frost resistance experiment are qualified.

Claims (3)

1. the preparation method of the autoclaved brick that one kind of multiple raw mineral materialss make, is characterized in that:
Comprise the following steps:
(1) attapulgite, wilkinite, ground granulated blast furnace slag, oyster shell whiting, volcano rock dust are added in clear water after mixing, stir, soak after 5-8 hour, centrifugal treating 9-15min, after centrifugal, after filtering, being dried, at the temperature of 900-950 ℃, in dodging firing, dodge burning 7-9 second, take out, add in suitable quantity of water and grind together with all the other raw materials, adding 10-15% hydrochloric acid soln tune PH is 4-5 again, and ground slurry is to 400-500 order, and repeated hydrogenation sodium oxide is adjusted to neutrality, after dry, obtain composite modified mineral powder standby;
Described composite modified mineral powder is made by the raw material of following weight parts:
Attapulgite 3-5, wilkinite 10-12, ground granulated blast furnace slag 13-17, oyster shell whiting 5-8, volcano rock dust 1-2, Radix Angelicae Sinensis oil 1-2, silane coupling agent KH530 1.4-2.3, urea 0.1-0.2, Trisodium Citrate 0.1-0.3, polyoxyethylene octylphenol ether 1-2;
(2) batching: the autoclaved brick that described multi mineral raw material makes is that the raw material by following weight parts makes: flyash 45-50, mine tailing 10-15, electrolysis rock ballast 13-16, lime 12-16, composite modified mineral powder 2-4;
(3) after each raw material blending preparation being taken, add suitable quantity of water and mix, obtain compound;
(4) compound is poured into the mold standing 2-3h after moulding;
(5) carry out, again steam press maintenance, curing temperature is 180 ℃-190 ℃, and curing time is 7-8h, and pressure is 1.2-1.3MPa, after and get final product.
2. the preparation method of the autoclaved brick that one kind of multiple raw mineral materialss according to claim 1 make, is characterized in that: the rotating speed of described whizzer is 1500-1800r/min.
3. the preparation method of the autoclaved brick that one kind of multiple raw mineral materialss according to claim 1 make, is characterized in that: the weight of the water described in step (3) and the ratio of each raw material gross weight are 0.2-0.3: 1.
CN201310555801.XA 2013-11-11 2013-11-11 The preparation method of the autoclaved brick that one kind of multiple raw mineral materialss obtain Active CN103588449B (en)

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Cited By (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104774028A (en) * 2015-04-25 2015-07-15 安徽阜阳富龙建筑材料有限责任公司 Insulating autoclaved brick
CN104817300A (en) * 2015-04-25 2015-08-05 安徽阜阳富龙建筑材料有限责任公司 Steam-pressing brick containing sludge
CN104844087A (en) * 2015-04-25 2015-08-19 安徽阜阳富龙建筑材料有限责任公司 Environmentally-friendly tourmaline autoclaved brick
CN105693206A (en) * 2016-03-18 2016-06-22 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with mango aromatic smell
CN105712699A (en) * 2016-03-18 2016-06-29 安徽绿风环保节能材料有限公司 Environmentally-friendly decorative bricks having aromatic odor of tangerines
CN105776954A (en) * 2016-03-18 2016-07-20 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with Hami melon fragrance
CN105773788A (en) * 2016-03-18 2016-07-20 安徽绿风环保节能材料有限公司 Environment-friendly decoration brick with apple aromatic odor
CN105776955A (en) * 2016-03-18 2016-07-20 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with lily fragrance
CN105801028A (en) * 2016-03-18 2016-07-27 安徽绿风环保节能材料有限公司 Environment-friendly decorating brick with orange-fragrant-and-sweet smell
CN105819804A (en) * 2016-03-18 2016-08-03 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with jasmine flower fragrance
CN105819807A (en) * 2016-03-18 2016-08-03 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with pineapple fragrance
CN105819803A (en) * 2016-03-18 2016-08-03 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with lemon fragrance
CN105819806A (en) * 2016-03-18 2016-08-03 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with strawberry fragrance
CN105819805A (en) * 2016-03-18 2016-08-03 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with rose flower fragrance
CN105837146A (en) * 2016-03-18 2016-08-10 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick block with cool and refreshing mint smell
CN105837145A (en) * 2016-03-18 2016-08-10 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick block with banana aromatic smell
CN105837164A (en) * 2016-03-18 2016-08-10 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick block with juicy peach aromatic smell
CN105837165A (en) * 2016-03-18 2016-08-10 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick block with grape sour and sweet smell

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102161577A (en) * 2010-12-22 2011-08-24 广东惠和硅制品有限公司 Building brick manufactured by using silicon-containing waste residue and manufacturing method of building brick
CN102875066A (en) * 2012-08-25 2013-01-16 马鞍山豹龙新型建材有限公司 Chromic slag aerated brick and preparation method thereof
CN102875067A (en) * 2012-08-25 2013-01-16 马鞍山豹龙新型建材有限公司 Modified nano mineral powder-containing aerated brick
CN102875183A (en) * 2012-08-25 2013-01-16 马鞍山豹龙新型建材有限公司 Preparation process for autoclaved curing aerated brick

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102161577A (en) * 2010-12-22 2011-08-24 广东惠和硅制品有限公司 Building brick manufactured by using silicon-containing waste residue and manufacturing method of building brick
CN102875066A (en) * 2012-08-25 2013-01-16 马鞍山豹龙新型建材有限公司 Chromic slag aerated brick and preparation method thereof
CN102875067A (en) * 2012-08-25 2013-01-16 马鞍山豹龙新型建材有限公司 Modified nano mineral powder-containing aerated brick
CN102875183A (en) * 2012-08-25 2013-01-16 马鞍山豹龙新型建材有限公司 Preparation process for autoclaved curing aerated brick

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
缪正坤等: "建筑垃圾作骨料生产保温砌块的研究", 《新型建筑材料》, no. 3, 31 December 2010 (2010-12-31), pages 26 - 29 *

Cited By (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104774028A (en) * 2015-04-25 2015-07-15 安徽阜阳富龙建筑材料有限责任公司 Insulating autoclaved brick
CN104817300A (en) * 2015-04-25 2015-08-05 安徽阜阳富龙建筑材料有限责任公司 Steam-pressing brick containing sludge
CN104844087A (en) * 2015-04-25 2015-08-19 安徽阜阳富龙建筑材料有限责任公司 Environmentally-friendly tourmaline autoclaved brick
CN105693206A (en) * 2016-03-18 2016-06-22 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with mango aromatic smell
CN105712699A (en) * 2016-03-18 2016-06-29 安徽绿风环保节能材料有限公司 Environmentally-friendly decorative bricks having aromatic odor of tangerines
CN105776954A (en) * 2016-03-18 2016-07-20 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with Hami melon fragrance
CN105773788A (en) * 2016-03-18 2016-07-20 安徽绿风环保节能材料有限公司 Environment-friendly decoration brick with apple aromatic odor
CN105776955A (en) * 2016-03-18 2016-07-20 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with lily fragrance
CN105801028A (en) * 2016-03-18 2016-07-27 安徽绿风环保节能材料有限公司 Environment-friendly decorating brick with orange-fragrant-and-sweet smell
CN105819804A (en) * 2016-03-18 2016-08-03 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with jasmine flower fragrance
CN105819807A (en) * 2016-03-18 2016-08-03 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with pineapple fragrance
CN105819803A (en) * 2016-03-18 2016-08-03 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with lemon fragrance
CN105819806A (en) * 2016-03-18 2016-08-03 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with strawberry fragrance
CN105819805A (en) * 2016-03-18 2016-08-03 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick with rose flower fragrance
CN105837146A (en) * 2016-03-18 2016-08-10 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick block with cool and refreshing mint smell
CN105837145A (en) * 2016-03-18 2016-08-10 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick block with banana aromatic smell
CN105837164A (en) * 2016-03-18 2016-08-10 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick block with juicy peach aromatic smell
CN105837165A (en) * 2016-03-18 2016-08-10 安徽绿风环保节能材料有限公司 Environment-friendly decorative brick block with grape sour and sweet smell

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