CN105218067A - A kind of purple sand pug and preparation method thereof - Google Patents
A kind of purple sand pug and preparation method thereof Download PDFInfo
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- CN105218067A CN105218067A CN201510596050.5A CN201510596050A CN105218067A CN 105218067 A CN105218067 A CN 105218067A CN 201510596050 A CN201510596050 A CN 201510596050A CN 105218067 A CN105218067 A CN 105218067A
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- purple sand
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- red mud
- pug
- shale
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- 239000004576 sand Substances 0.000 title claims abstract description 91
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 89
- 230000032683 aging Effects 0.000 claims description 16
- 238000003825 pressing Methods 0.000 claims description 16
- 238000007789 sealing Methods 0.000 claims description 16
- 239000000126 substance Substances 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 10
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 9
- 238000000498 ball milling Methods 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 8
- 239000002002 slurry Substances 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- 239000010453 quartz Substances 0.000 claims description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 6
- 229910052681 coesite Inorganic materials 0.000 claims description 6
- 229910052593 corundum Inorganic materials 0.000 claims description 6
- 229910052906 cristobalite Inorganic materials 0.000 claims description 6
- 229910052595 hematite Inorganic materials 0.000 claims description 6
- 239000011019 hematite Substances 0.000 claims description 6
- 229910052900 illite Inorganic materials 0.000 claims description 6
- LIKBJVNGSGBSGK-UHFFFAOYSA-N iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Fe+3].[Fe+3] LIKBJVNGSGBSGK-UHFFFAOYSA-N 0.000 claims description 6
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 6
- VGIBGUSAECPPNB-UHFFFAOYSA-L nonaaluminum;magnesium;tripotassium;1,3-dioxido-2,4,5-trioxa-1,3-disilabicyclo[1.1.1]pentane;iron(2+);oxygen(2-);fluoride;hydroxide Chemical compound [OH-].[O-2].[O-2].[O-2].[O-2].[O-2].[F-].[Mg+2].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[K+].[K+].[K+].[Fe+2].O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2 VGIBGUSAECPPNB-UHFFFAOYSA-L 0.000 claims description 6
- 239000000377 silicon dioxide Substances 0.000 claims description 6
- 229910052682 stishovite Inorganic materials 0.000 claims description 6
- 229910052905 tridymite Inorganic materials 0.000 claims description 6
- 229910001845 yogo sapphire Inorganic materials 0.000 claims description 6
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Inorganic materials O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 claims description 5
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 4
- 229910021532 Calcite Inorganic materials 0.000 claims description 3
- MCMNRKCIXSYSNV-UHFFFAOYSA-N ZrO2 Inorganic materials O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 3
- 229910001919 chlorite Inorganic materials 0.000 claims description 3
- 229910052619 chlorite group Inorganic materials 0.000 claims description 3
- QBWCMBCROVPCKQ-UHFFFAOYSA-N chlorous acid Chemical compound OCl=O QBWCMBCROVPCKQ-UHFFFAOYSA-N 0.000 claims description 3
- 229910052622 kaolinite Inorganic materials 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims 2
- 239000002994 raw material Substances 0.000 abstract description 18
- 230000001737 promoting effect Effects 0.000 abstract description 2
- 239000004927 clay Substances 0.000 abstract 2
- 239000002689 soil Substances 0.000 abstract 2
- 239000003086 colorant Substances 0.000 abstract 1
- 239000000843 powder Substances 0.000 description 11
- 239000000049 pigment Substances 0.000 description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical group [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 5
- 239000011734 sodium Substances 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- 241001122767 Theaceae Species 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 238000010304 firing Methods 0.000 description 2
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- UPWOEMHINGJHOB-UHFFFAOYSA-N cobalt(III) oxide Inorganic materials O=[Co]O[Co]=O UPWOEMHINGJHOB-UHFFFAOYSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 239000010445 mica Substances 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 description 1
- 229910001950 potassium oxide Inorganic materials 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
- 229910001948 sodium oxide Inorganic materials 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 229910052572 stoneware Inorganic materials 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
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Abstract
The invention discloses a kind of purple sand pug, be made up of Boccaro shale and red soil, in mass ratio routine described Boccaro shale: red soil=1 ~ 3: 1 ~ 3.In addition, the preparation method of above-mentioned purple sand pug is also disclosed.The present invention without the need to adding other any industrial raw material and artificial colors, and obtains functional, superior in quality purple sand pug, fire the purple-clay product natural environmental-protective, the excellent performance that obtain; Meanwhile, preparation technology is simple, workable, the realization of easy to utilize and industrialization, is conducive to promoting the development of purple-clay product application and technology.
Description
Technical Field
The invention relates to the technical field of ceramic raw materials, in particular to a purple sand pug and a preparation method thereof.
Background
The purple sand pottery utensil is a stoneware, is a ceramic product between pottery and porcelain, has the characteristics of compact structure, higher strength, thermal shock resistance and good air permeability, and is a traditional culture which is popular among people in China when being brewed by the purple sand tea set. The purple placer used for firing the purple sand pottery is iron-containing argillaceous siltstone and consists of hydromica, kaolin, quartz, mica scraps, iron and other mineral components, and the main chemical components comprise silicon oxide, aluminum oxide, iron oxide, calcium oxide, magnesium oxide, manganese oxide, potassium oxide, sodium oxide and the like; the color is various, and the red purple sand, the white purple sand, the yellow purple sand, the green purple sand and the black purple sand are mainly classified. However, because the existing high-grade purple sand raw materials are few, particularly the exploitation of Yixing purple sand mineral resources is limited by the government since 2005, the purple sand products in the market at present are almost made of inferior purple sand raw materials or purple sand tailing raw materials and chemical raw materials (Fe)2O3、MnO2、Co2O3Etc.), seriously harms human health and is not beneficial to the application and development of purple sand products.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide the purple sand pug with excellent performance without adding any chemical raw materials so as to obtain a natural environment-friendly purple sand product with excellent performance. The invention also aims to provide a preparation method of the purple sand pug.
The purpose of the invention is realized by the following technical scheme:
the purple sand pug provided by the invention comprises purple sand shale and red mud, wherein the mass ratio of the purple sand shale to the red mud is 1-3: 1-3.
In the scheme, the granularity of the purple sand shale is 80-150 meshes, and the granularity of the red mud is more than 100 meshes.
Furthermore, the purple sand shale with rich reserves, excellent quality and low cost in Jingdezhen areas of Jiangxi province is adopted as the raw material, and the chemical composition of the purple sand shale is SiO257.01～64.5％、Al2O317.45～23.8％、Fe2O37.83～14.60％、TiO20.75～0.91％、MgO0.21～1.55％、K2O1.21～4.71％、Na20.01-0.92% of O, 0.02-1.34% of CaO0, and 4.22-6.94% of loss on ignition; the main phase composition of the material is quartz, illite, hematite and anatase.
Furthermore, the red mud in the zone of Leping of Jiangxi province is used as a raw material, and the chemical composition of the red mud is SiO258.06～62.25％、Al2O314.36～15.82％、Fe2O35.26～7.62％、TiO20.68～0.76％、MgO1.73～2.16％、K2O2.92～3.46％、Na2O0.06～0.24％、CaO3.07～3.85％、MnO20.01～0.05％、P2O50.08～0.18％、SO30.01～0.05％、BaO0.04～0.08％、ZnO0.01～0.03％、ZrO20.03-0.09%, 0.01-0.05% of PbO0.01-7.79% of loss on ignition; the main phase composition of the material is quartz, kaolinite, hematite, illite, chlorite and calcite.
The other purpose of the invention is realized by the following technical scheme:
the preparation method of the purple sand pug provided by the invention comprises the following steps: and mixing the purple sand shale and the red mud in proportion, performing ball milling, filtering, slurry sucking, vacuum pugging, pressing into mud strips, sealing and ageing for 3-5 times, and repeatedly performing vacuum pugging, pressing into mud strips and sealing and ageing to obtain the purple sand pug.
The invention has the following beneficial effects:
(1) the invention does not need to add any other industrial raw materials and artificial pigments, and can directly utilize the purple sand shale in Jingdezhen areas and the red mud in Leping areas to prepare the purple sand pug with good performance and quality. The fired purple sand product is natural and environment-friendly, and the product is not easy to crack, has good quality, more natural texture, delicate hand feeling, good light transmittance and water color and good color.
(2) The invention has rich raw material sources, simple preparation process and strong operability, is convenient for popularization and application and realization of industrialization, and is beneficial to promoting the application and technical development of the purple sand product.
The present invention will be described in further detail with reference to examples.
Detailed Description
The embodiment of the invention adopts purple sand shale with rich reserves, excellent quality and low cost in Jingdezhen areas of Jiangxi province and red mud in Leping areas of Jiangxi province as raw materials. Wherein,
the chemical composition of the purple sand shale is SiO257.01～64.5％、Al2O317.45～23.8％、Fe2O37.83～14.60％、TiO20.75～0.91％、MgO0.21～1.55％、K2O1.21～4.71％、Na20.01-0.92% of O, 0.02-1.34% of CaO0, and 4.22-6.94% of loss on ignition; the main phase composition of the material is quartz, illite, hematite and anatase.
The chemical composition of the red mud is SiO258.06～62.25％、Al2O314.36～15.82％、Fe2O35.26～7.62％、TiO20.68～0.76％、MgO1.73～2.16％、K2O2.92～3.46％、Na2O0.06～0.24％、CaO3.07～3.85％、MnO20.01～0.05％、P2O50.08～0.18％、SO30.01～0.05％、BaO0.04～0.08％、ZnO0.01～0.03％、ZrO20.03-0.09%, 0.01-0.05% of PbO0.01-7.79% of loss on ignition; the main phase composition of the material is quartz, kaolinite, hematite, illite, chlorite and calcite.
The first embodiment is as follows:
1. the purple sand pug comprises purple sand shale and red mud, wherein the mass ratio of the purple sand shale to the red mud is 2: 3.
2. The preparation method of the purple sand pug comprises the following steps: respectively crushing the purple sand shale and the red mud into 80-mesh and 100-mesh powder, mixing the powder according to the proportion without adding any other artificial pigment and chemical raw materials, performing ball milling, filtering, slurry sucking, vacuum pugging, pressing into mud strips, sealing and ageing, and repeating the vacuum pugging, pressing the mud strips and sealing and ageing for 3 times to obtain the purple sand mud material.
Example two:
1. the purple sand pug comprises purple sand shale and leping red mud, wherein the mass ratio of the purple sand shale to the red mud is 1: 1.
2. The preparation method of the purple sand pug comprises the following steps: the purple sand shale and the red mud are crushed into 120 meshes of powder and then mixed according to the proportion, no other artificial pigment and chemical raw materials are added, and the purple sand mud material is prepared by ball milling, filtering, slurry sucking, vacuum pugging, pressing into mud strips, sealing and ageing for 3 times, and repeated vacuum pugging, pressing into mud strips and sealing and ageing.
Example three:
1. the purple sand pug comprises purple sand shale and leping red mud, wherein the mass ratio of the purple sand shale to the red mud is 1: 1.
2. The preparation method of the purple sand pug comprises the following steps: respectively crushing the purple sand shale and the red mud into 150-mesh powder, mixing the powder according to a ratio, adding no other artificial pigment and chemical raw materials, performing ball milling, filtering, slurry sucking, vacuum pugging, pressing into mud strips, sealing and ageing for 3 times, and repeatedly performing vacuum pugging, pressing into mud strips and sealing and ageing to obtain the purple sand pug.
Example four:
1. the purple sand pug comprises purple sand shale and leping red mud, wherein the mass ratio of the purple sand shale to the red mud is 3: 2.
2. The preparation method of the purple sand pug comprises the following steps: respectively crushing the purple sand shale and the red mud into 150-mesh and 100-mesh powder, mixing the powder according to the proportion without adding any other artificial pigment and chemical raw materials, performing ball milling, filtering, slurry sucking, vacuum pugging, pressing into mud strips, sealing and ageing, and repeating the vacuum pugging, pressing the mud strips and sealing and ageing for 3 times to obtain the purple sand mud material.
Example five:
1. the purple sand pug comprises purple sand shale and leping red mud, wherein the mass ratio of the purple sand shale to the red mud is 3: 2.
2. The preparation method of the purple sand pug comprises the following steps: respectively crushing the purple sand shale and the red mud into 150-mesh and 100-mesh powder, mixing the powder according to the proportion without adding any other artificial pigment and chemical raw materials, performing ball milling, filtering, slurry sucking, vacuum pugging, pressing into mud strips, sealing and ageing, and repeating the vacuum pugging, pressing the mud strips and sealing and ageing for 5 times to obtain the purple sand mud material.
Example six:
1. the purple sand pug comprises purple sand shale and leping red mud, wherein the mass ratio of the purple sand shale to the red mud is 3: 2.
2. The preparation method of the purple sand pug comprises the following steps: respectively crushing the purple sand shale and the red mud into 150-mesh and 200-mesh powder, mixing the powder according to the proportion without adding any other artificial pigment and chemical raw materials, performing ball milling, filtering, slurry sucking, vacuum pugging, pressing into mud strips, sealing and ageing, and repeating the vacuum pugging, pressing the mud strips and sealing and ageing for 4 times to prepare the purple sand pug.
The purple sand pug prepared by the first to sixth embodiments of the invention is made into a purple sand teapot product, and the firing temperature is 1120 ℃. Adopting an extremely cold and extremely hot experiment to detect the purple sand teapot product: cooling the tea pot to-20 deg.C, and spraying the pot body with 100 deg.C boiling water for 3 times. The purple sand teapot product prepared by the embodiment of the invention does not crack, and the fired purple sand teapot has more natural texture, exquisite hand feeling, good light transmission and water color and good color.
Claims (5)
1. The purple sand pug is characterized in that: the purple sand shale red mud comprises purple sand shale and red mud, wherein the mass ratio of the purple sand shale to the red mud is 1-3: 1-3.
2. The purple sand pug of claim 1, which is characterized in that: the particle size of the purple sand shale is 80-150 meshes, and the particle size of the red mud is more than 100 meshes.
3. The purple sand of claim 1 or 2Pug, which is characterized in that: the chemical composition of the purple sand shale is SiO257.01～64.5％、Al2O317.45～23.8％、Fe2O37.83～14.60％、TiO20.75～0.91％、MgO0.21～1.55％、K2O1.21～4.71％、Na20.01-0.92% of O, 0.02-1.34% of CaO0, and 4.22-6.94% of loss on ignition; the main phase composition of the material is quartz, illite, hematite and anatase.
4. The purple sand pug of claim 1 or 2, which is characterized in that: the chemical composition of the red mud is SiO258.06～62.25％、Al2O314.36～15.82％、Fe2O35.26～7.62％、TiO20.68～0.76％、MgO1.73～2.16％、K2O2.92～3.46％、Na2O0.06～0.24％、CaO3.07～3.85％、MnO20.01～0.05％、P2O50.08～0.18％、SO30.01～0.05％、BaO0.04～0.08％、ZnO0.01～0.03％、ZrO20.03-0.09%, 0.01-0.05% of PbO0.01-7.79% of loss on ignition; the main phase composition of the material is quartz, kaolinite, hematite, illite, chlorite and calcite.
5. The preparation method of the purple sand pug as set forth in any one of claims 1 to 4, which is characterized in that: and mixing the purple sand shale and the red mud in proportion, performing ball milling, filtering, slurry sucking, vacuum pugging, pressing into mud strips, sealing and ageing for 3-5 times, and repeatedly performing vacuum pugging, pressing into mud strips and sealing and ageing to obtain the purple sand pug.
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| CN105837166A (en) * | 2016-03-22 | 2016-08-10 | 登封市天中邑文化产业发展有限责任公司 | Medical stone ware preparing method and ware prepared by method |
| CN105837167A (en) * | 2016-03-22 | 2016-08-10 | 登封市天中邑文化产业发展有限责任公司 | Medical stone blank material composition and preparation method thereof, ware preparation method and ware |
| CN106336191A (en) * | 2016-08-21 | 2017-01-18 | 宜兴爱宜艺术陶瓷有限公司 | Method for refining purple grit mud from blue algae |
| CN106431189A (en) * | 2016-08-30 | 2017-02-22 | 无锡能以信科技有限公司 | Vacuum firing process for purple clay teapots and purple clay teapots produced by vacuum firing process |
| CN106747356A (en) * | 2016-12-15 | 2017-05-31 | 宜兴市钰光紫砂研究所 | A kind of anti-corrosion boccaro material |
| CN107488025A (en) * | 2017-08-02 | 2017-12-19 | 景德镇陶源矿业有限公司 | A kind of large-scale boccaro wine vat pug and preparation method thereof |
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| CN108083762A (en) * | 2017-11-30 | 2018-05-29 | 喀左高品宝砂紫陶艺术研发有限公司 | A kind of preparation method of composite purple sand mud |
| CN108863308A (en) * | 2018-08-17 | 2018-11-23 | 德阳极光文创设计有限公司 | Ceramic material based on composite rock mineral |
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| CN109133861A (en) * | 2018-11-14 | 2019-01-04 | 齐齐哈尔市碾子山区民乐麦饭石工艺品厂 | A kind of production method of medical stone pottery |
| CN110105046A (en) * | 2019-06-04 | 2019-08-09 | 云南曲成水业科技有限公司 | Novel pottery pot and preparation method thereof |
| CN111807826A (en) * | 2020-04-26 | 2020-10-23 | 武钢集团昆明钢铁股份有限公司 | Green mud purple sand and preparation method thereof |
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