CN108905292A - A kind of alternating temperature oil water separator and volatile oil extracting system - Google Patents
A kind of alternating temperature oil water separator and volatile oil extracting system Download PDFInfo
- Publication number
- CN108905292A CN108905292A CN201811118267.5A CN201811118267A CN108905292A CN 108905292 A CN108905292 A CN 108905292A CN 201811118267 A CN201811118267 A CN 201811118267A CN 108905292 A CN108905292 A CN 108905292A
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- alternating temperature
- shell
- oil water
- water separator
- chamber
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
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Abstract
A kind of alternating temperature oil water separator, is related to field of pharmaceutical equipment, during heavy oil decline, can be cooled down again to oil water mixture after light oil separation, the density contrast of heavy oil and water is made to become larger, to be more easier to separate.The alternating temperature oil water separator is easy to operate, and separative efficiency is high, and being particularly suitable for, which has light oil again, the volatile oil of heavy oil.A kind of volatile oil extracting system comprising above-mentioned alternating temperature oil water separator, it is high for the separative efficiency of oil water mixture, the yield of volatile oil can be improved.
Description
Technical field
The present invention relates to field of pharmaceutical equipment, in particular to a kind of alternating temperature oil water separator and volatile oil extracting
System.
Background technique
Volatile oil is also referred to as essential oil, is that the one kind existed in plant has volatility, can be with steam distillation, not with water
Miscible oily liquids.Volatile oil has fragrant odor mostly, and has various bioactivity.Volatile oil is in plant
Boundary's distributed pole is wide, and the plant used as Chinese medicine just has hundreds of containing volatile oil.The composition of volatile oil is considerably complicated, basic
Group becomes terpenoid, aromatic compound, aliphatic compound etc., and the ratio that wherein terpene accounts for is maximum and mainly single
Terpene, sequiterpene and its containing oxygen derivative.The important substance that volatile oil is acted on as Chinese medicine generation, study its extract with separate for
Developing new drug and promotion TCM Modernization are of great significance.For a long time, domestic and foreign scholars mention traditional medicine volatile oil
It takes and has carried out a large amount of research and probe with separating, constantly improved although extracting with separation method, majority is still
In the laboratory research stage, industrial application can not be carried out.
Volatile oil collection separator collection matched with extract equipment, separative efficiency are not high enough at present, to part medicinal material
In mass production even can not be collected into volatile oil, cause medicinal material utilization rate low, energy consumption is high, it is at high cost the problems such as, volatile oil mentions
It takes, separate the quality for equipping the production and product that have seriously affected Chinese materia medica preparation.
In consideration of it, special propose the application.
Summary of the invention
The present invention provides a kind of oil water separators, it is intended to improve existing oil water separator to the recovery rate of volatile oil not
Enough high problems.
The present invention also provides a kind of volatile oil extracting systems, high to the extraction efficiency of volatile oil.
What the embodiment of the present invention was realized in：
A kind of alternating temperature oil water separator comprising shell and be located at the intracorporal separation chamber of shell, be provided at the top of shell light
Oil eliminator, bottom are provided with heavy fuel separator；Separation chamber includes the first separation chamber for being located at upper part of the housing, and is located at shell
Second separation chamber of lower part；Miscella feed pipe is extend into the first separation chamber through shell, and water phase outlet tube is stretched through shell
Enter into the second separation chamber；The position of corresponding second separation chamber of hull outside is arranged with condenser jacket, shape between condenser jacket and shell
At there is the condensation chamber passed through for condensate liquid.
Further, in the other preferred embodiments of the present invention, condensation chamber is provided with condensate inlet and condensate liquid goes out
Mouthful, condensate inlet is located at the bottom of condensation chamber, and condensate outlet is located at the top of condensation chamber.
Further, in the other preferred embodiments of the present invention, condensation chamber is arranged along the circumferential direction of shell, and around shell
One week.
Further, in the other preferred embodiments of the present invention, condenser jacket is made of heat-barrier material.
Further, in the other preferred embodiments of the present invention, alternating temperature oil water separator is additionally provided with condenser pipe, condensation
Pipe includes inlet tube, helix tube and outlet tube, and helix tube is located in the second separation chamber, and is arranged around water phase outlet tube, helix tube
Both ends be connected to respectively with inlet tube and outlet tube, inlet tube and outlet tube run through shell.
Further, it in the other preferred embodiments of the present invention, is provided at the top of shell in equilibrium separation room
The respirator of air pressure.
Further, in the other preferred embodiments of the present invention, alternating temperature oil water separator further includes cyclone separator, rotation
Stream separator is located in the first separation chamber, and the head piece that enters of cyclone separator is connected to miscella feed pipe, the top of cyclone separator
Portion is provided with overflow port, and bottom is provided with underflow opening.
Further, in the other preferred embodiments of the present invention, vortex chamber, vortex chamber packet are provided in cyclone separator
Include the cylindrical section vortex chamber being located above and underlying conical section vortex chamber, the opening's edge cylinder that becomes a mandarin of cyclone separator
The tangential direction setting of section vortex chamber.
Further, in the other preferred embodiments of the present invention, be provided with spoiler below underflow opening, spoiler with
Shell connection, and be arranged with the underflow opening interval of cyclone separator；Liquid gap was provided between spoiler and shell.
A kind of volatile oil extracting system comprising above-mentioned alternating temperature oil water separator.
The beneficial effect of the embodiment of the present invention is：
The embodiment of the invention provides a kind of alternating temperature oil water separators, can be after light oil separation, in heavy oil decline
In the process, cooled down again to oil water mixture, the density contrast of heavy oil and water is made to become larger, to be more easier to separate.The change
Warm oil water separator is easy to operate, and separative efficiency is high, and being particularly suitable for, which has light oil again, the volatile oil of heavy oil.
The embodiment of the invention also provides a kind of volatile oil extracting systems comprising above-mentioned alternating temperature oil water separator, it is right
It is high in the separative efficiency of oil water mixture, the yield of volatile oil can be improved.
Detailed description of the invention
In order to illustrate the technical solution of the embodiments of the present invention more clearly, below will be to needed in the embodiment attached
Figure is briefly described, it should be understood that the following drawings illustrates only certain embodiments of the present invention, therefore is not construed as pair
The restriction of range for those of ordinary skill in the art without creative efforts, can also be according to this
A little attached drawings obtain other relevant attached drawings.
Fig. 1 is a kind of schematic diagram of alternating temperature oil water separator provided by first embodiment of the invention；
Fig. 2 is a kind of schematic diagram of alternating temperature oil water separator provided by second embodiment of the invention；
Fig. 3 is a kind of cross-sectional view of the cyclone separator of alternating temperature oil water separator provided by second embodiment of the invention；
Fig. 4 is a kind of signal of the spoiler of alternating temperature oil water separator provided by second embodiment of the embodiment of the present invention
Figure.
Icon：100- alternating temperature oil water separator；110- shell；111- light oil separator；112- heavy fuel separator；113- is mixed
Close oily feed pipe；114- water phase outlet tube；115- respirator；The separation chamber 120-；The first separation chamber 121-；122- second is separated
Room；130- condenser jacket；131- condensation chamber；132- condensate inlet；133- condensate outlet；140- condenser pipe；141- inlet tube；
142- helix tube；143- outlet tube；150- cyclone separator；151- enters head piece；152- overflow port；153- underflow opening；154- rotation
Flow chamber；1541- cylindrical section vortex chamber；1542- conical section vortex chamber；160- spoiler；161- crosses liquid gap；200- alternating temperature grease
Separator.
Specific embodiment
To keep the purposes, technical schemes and advantages of embodiment of the present invention clearer, implement below in conjunction with the present invention
The technical solution in embodiment of the present invention is clearly and completely described in attached drawing in mode, it is clear that described reality
The mode of applying is some embodiments of the invention, rather than whole embodiments.Based on the embodiment in the present invention, ability
Domain those of ordinary skill every other embodiment obtained without creative efforts, belongs to the present invention
The range of protection.Therefore, the detailed description of the embodiments of the present invention provided in the accompanying drawings is not intended to limit below and is wanted
The scope of the present invention of protection is sought, but is merely representative of selected embodiment of the invention.Based on the embodiment in the present invention,
Every other embodiment obtained by those of ordinary skill in the art without making creative efforts belongs to this
Invent the range of protection.
In the description of the present invention, it is to be understood that, term " center ", " longitudinal direction ", " transverse direction ", " length ", " width ",
" thickness ", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outside", " up time
The orientation or positional relationship of the instructions such as needle ", " counterclockwise " is to be based on the orientation or positional relationship shown in the drawings, and is merely for convenience of
The description present invention and simplified description, rather than the equipment of indication or suggestion meaning or element must have a particular orientation, with spy
Fixed orientation construction and operation, therefore be not considered as limiting the invention.
In addition, term " first ", " second " are used for descriptive purposes only and cannot be understood as indicating or suggesting relative importance
Or implicitly indicate the quantity of indicated technical characteristic.Define " first " as a result, the feature of " second " can be expressed or
Implicitly include one or more of the features.In the description of the present invention, the meaning of " plurality " is two or more,
Unless otherwise specifically defined.
In the present invention unless specifically defined or limited otherwise, term " installation ", " connected ", " connection ", " fixation " etc.
Term shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or integral；It can be mechanical connect
It connects, is also possible to be electrically connected；It can be directly connected, can also can be in two elements indirectly connected through an intermediary
The interaction relationship of the connection in portion or two elements.It for the ordinary skill in the art, can be according to specific feelings
Condition understands the concrete meaning of above-mentioned term in the present invention.
In the present invention unless specifically defined or limited otherwise, fisrt feature second feature "upper" or "lower"
It may include that the first and second features directly contact, also may include that the first and second features are not direct contacts but pass through it
Between other characterisation contact.Moreover, fisrt feature includes the first spy above the second feature " above ", " above " and " above "
Sign is right above second feature and oblique upper, or is merely representative of first feature horizontal height higher than second feature.Fisrt feature exists
Second feature " under ", " lower section " and " following " include that fisrt feature is directly below and diagonally below the second feature, or is merely representative of
First feature horizontal height is less than second feature.
First embodiment
Present embodiments provide a kind of alternating temperature oil water separator 100, referring to Fig.1 shown in comprising shell 110 and be located at shell
Separation chamber 120 in body 110.
As shown in Figure 1, in the present embodiment, the generally cylindrical type of shell 110, the top of shell 110 is provided with light oil point
From device 111, bottom is provided with heavy fuel separator 112.Separation chamber 120 includes the first separation chamber 121 for being located at 110 top of shell,
And the second separation chamber 122 positioned at 110 lower part of shell.Miscella feed pipe extend into the first separation chamber 121 through shell 110
Interior, water phase outlet tube 114 is extend into the second separation chamber 122 through shell 110.Corresponding second separation chamber 122 on the outside of shell 110
Position be arranged with condenser jacket 130, the condensation chamber 131 passed through for condensate liquid is formed between condenser jacket 130 and shell 110.
The oil water mixture formed by volatile oil and condensed water is entered in the first separation chamber 121 by miscella feed pipe,
Light oil in oil water mixture rises, and the light oil separator 111 by being located at 121 top of the first separation chamber is collected.And it weighs
Oil and water then sink to entering the second separation chamber 122 together, and further separate in sinking watching, and the heavy oil after separation is by the
The heavy fuel separator 112 of two separation chambers, 122 bottom is collected, and condensed water is then discharged from water phase outlet tube 114.But heavy oil
It is close with the density of water, to realize that separation takes a long time.The present embodiment by heavy oil and it is underwater heavy during, then
It is secondary to cool down to it, to increase the density contrast of heavy oil and water, make it easier to separate.It is worth noting that, in this implementation
In example, it is not separated really between the first separation chamber 121 and the second separation chamber 122, the first separation chamber 121 and second
Separation chamber 122 is actually still one complete whole, and the second separation chamber 122 is only to have the effect to cool down again according to it
Fruit, and the differentiation functionally carried out.
Condensation chamber 131 is provided with condensate inlet 132 and condensate outlet 133, and condensate inlet 132 is located at condensation chamber
131 bottom, condensate outlet 133 are located at the top of condensation chamber 131.Condensate liquid moves from the bottom to top, mixed with heavy oil and water
It closes and forms adverse current between object, achieve the purpose that improve cooling effect.
Condensation chamber 131 allows condensate liquid from shell and around shell 110 1 weeks along the circumferential direction setting of shell 110
110 all directions uniformly cool down to the mixing liquid in the second separation chamber 122, increase the effect of separation.
Condenser jacket 130 is made of heat-barrier material.Condenser jacket 130 made of heat-barrier material can prevent the excessive of cold air, make
Heat transmitting can preferably occur between shell 110 for condensate liquid, improve the cooling to mixing liquid in the second separation chamber 122 and imitate
Rate.
The top of shell 110 is provided with respirator 115.Respirator 115 can be used for the air pressure in equilibrium separation room 120,
It avoids the occurrence of since separation caused by negative pressure is unsmooth, flows backwards, or by feelings such as hydrojet, the leakages of the excessive initiation of pressure
Condition.
Second embodiment
A kind of alternating temperature oil water separator 200 is present embodiments provided, referring to shown in Fig. 2, is provided with first embodiment
Alternating temperature oil water separator 100 it is essentially identical, distinguish it is as follows.
In order to further promote cooling efficiency, as shown in Fig. 2, the alternating temperature oil water separator 200 in the present embodiment is also set
It is equipped with condenser pipe 140, condenser pipe 140 includes inlet tube 141, helix tube 142 and outlet tube 143, and helix tube 142 is located at second point
It is arranged from room 122, and around water phase outlet tube 114, the both ends of helix tube 142 connect with inlet tube 141 and outlet tube 143 respectively
Logical, inlet tube 141 and outlet tube 143 run through shell 110.Condenser pipe 140 can be extend into the second separation chamber 122, to second
Mixing liquid inside separation chamber 122 cools down, and is used cooperatively with condensation chamber 131, can greatly increase cooling efficiency.
Further, as shown in Figures 2 and 3, in the present embodiment, alternating temperature oil water separator 200 further includes cyclonic separation
Device 150, cyclone separator 150 are located in the first separation chamber 121, and cyclone separator 150 enters head piece 151 and miscella feed pipe
113 connections, the top of cyclone separator 150 are provided with overflow port 152, and bottom is provided with underflow opening 153.Cyclone separator 150
Preliminary separation can be carried out to oil water mixture, under the effect of centrifugation, light oil is by the overflow port at the top of cyclone separator 150
152 outflows, and heavy oil and water are then flowed out by the underflow opening 153 of 150 bottom of cyclone separator.
Vortex chamber 154 is provided in cyclone separator 150, vortex chamber 154 includes the cylindrical section vortex chamber being located above
1541 and underlying conical section vortex chamber 1542, cyclone separator 150 enter head piece 151 along cylindrical section vortex chamber
1541 tangential direction setting.The oil water mixture tangentially entered helically gestalt movement is entering conical section vortex chamber
After 1542, with being gradually reduced for internal diameter, liquid in rotation speed is gradually accelerated.Since the bore of underflow opening 153 is smaller, so that liquid
Body can not all be discharged from underflow opening 153.Under such circumstances, heavy oil and water are flowed along the cavity wall of vortex chamber 154 by underflow opening 153
Out, and light oil is squeezed to upward at the lower center of pressure, flowed out by overflow port 152, realize the initial gross separation of light oil.
Further, as shown in Figure 2 and Figure 4, the lower section of underflow opening 153 is provided with spoiler 160, spoiler 160 and shell
Body 110 connects, and is spaced and is arranged with the underflow opening of cyclone separator 150 153；It was provided between spoiler 160 and shell 110
Liquid gap 161.The movement velocity of the heavy oil and water that flowed out by underflow opening 153 is very fast, after flowing into the second separation chamber 122, cannot do
Cooling is stopped to sufficient.The setting of spoiler 160 can then play preferable buffer function, heavy oil and water slug to spoiler
On 160, after being blocked deceleration, then by cross liquid gap 161 be flowed into the second separation chamber 122, adequately cooled down, Jin Erti
High score from effect.
The present embodiment additionally provides a kind of volatile oil extracting system comprising above-mentioned alternating temperature oil water separator 200.It includes
Above-mentioned alternating temperature oil water separator 200, it is high for the separative efficiency of oil water mixture, the yield of volatile oil can be improved.
In conclusion the embodiment of the invention provides a kind of alternating temperature oil water separator, it can be after light oil separation, Yu Chong
During oil decline, cooled down again to oil water mixture, the density contrast of heavy oil and water is made to become larger, to be more easier point
From.The alternating temperature oil water separator is easy to operate, and separative efficiency is high, and being particularly suitable for, which has light oil again, the volatile oil of heavy oil.
The embodiment of the invention also provides a kind of volatile oil extracting systems comprising above-mentioned alternating temperature oil water separator, it is right
It is high in the separative efficiency of oil water mixture, the yield of volatile oil can be improved.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, for the skill of this field
For art personnel, the invention may be variously modified and varied.All within the spirits and principles of the present invention, made any to repair
Change, equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of alternating temperature oil water separator, which is characterized in that including shell and be located at the intracorporal separation chamber of the shell, the shell
Top be provided with light oil separator, bottom is provided with heavy fuel separator；The separation chamber includes being located at the upper part of the housing
First separation chamber, and the second separation chamber positioned at the lower part of the housing；Miscella feed pipe extend into institute through the shell
It states in the first separation chamber, water phase outlet tube is extend into second separation chamber through the shell；The hull outside is corresponding
The position of second separation chamber is arranged with condenser jacket, is formed between the condenser jacket and the shell and passes through for condensate liquid
Condensation chamber.
2. alternating temperature oil water separator according to claim 1, which is characterized in that the condensation chamber is provided with condensate inlet
And condensate outlet, the condensate inlet are located at the bottom of the condensation chamber, the condensate outlet is located at the condensation chamber
Top.
3. alternating temperature oil water separator according to claim 2, which is characterized in that circumferential direction of the condensation chamber along the shell
Setting, and around the shell one week.
4. alternating temperature oil water separator according to claim 2, which is characterized in that the condenser jacket is made of heat-barrier material.
5. alternating temperature oil water separator according to claim 1, which is characterized in that the alternating temperature oil water separator is additionally provided with
Condenser pipe, the condenser pipe include inlet tube, helix tube and outlet tube, and the helix tube is located in second separation chamber, and
Be arranged around the water phase outlet tube, the both ends of the helix tube are connected to the inlet tube and the outlet tube respectively, it is described into
Liquid pipe and the outlet tube run through the shell.
6. alternating temperature oil water separator according to claim 1, which is characterized in that be provided at the top of the shell for putting down
Weigh the respirator for separating room pressure.
7. alternating temperature oil water separator according to claim 1, which is characterized in that the alternating temperature oil water separator further includes rotation
Stream separator, the cyclone separator are located in first separation chamber, and the head piece that enters of the cyclone separator is mixed with described
Oily feed pipe is connected to, and is provided with overflow port at the top of the cyclone separator, bottom is provided with underflow opening.
8. alternating temperature oil water separator according to claim 7, which is characterized in that be provided with eddy flow in the cyclone separator
Chamber, the vortex chamber include the cylindrical section vortex chamber being located above and underlying conical section vortex chamber, the eddy flow point
The tangential direction of the cylindrical section vortex chamber described in opening's edge that becomes a mandarin from device is arranged.
9. alternating temperature oil water separator according to claim 8, which is characterized in that be provided with flow-disturbing below the underflow opening
Plate, the spoiler are connect with the shell, and are arranged with the underflow opening interval of the cyclone separator；The spoiler and institute
It states and was provided with liquid gap between shell.
10. a kind of volatile oil extracting system, which is characterized in that including alternating temperature grease as described in any one of claims 1 to 9 point
From device.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811118267.5A CN108905292B (en) | 2018-09-25 | 2018-09-25 | Temperature-changing oil-water separator and volatile oil extraction system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811118267.5A CN108905292B (en) | 2018-09-25 | 2018-09-25 | Temperature-changing oil-water separator and volatile oil extraction system |
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| Publication Number | Publication Date |
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| CN108905292A true CN108905292A (en) | 2018-11-30 |
| CN108905292B CN108905292B (en) | 2023-09-26 |
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ID=64409972
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| Application Number | Title | Priority Date | Filing Date |
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| CN201811118267.5A Active CN108905292B (en) | 2018-09-25 | 2018-09-25 | Temperature-changing oil-water separator and volatile oil extraction system |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113845979A (en) * | 2021-11-10 | 2021-12-28 | 鲁南制药集团股份有限公司 | Novel volatile oil extraction equipment |
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