CN108905267A - A kind of volatile oil crystallization extraction system and essential oil production line - Google Patents
A kind of volatile oil crystallization extraction system and essential oil production line Download PDFInfo
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- CN108905267A CN108905267A CN201811118060.8A CN201811118060A CN108905267A CN 108905267 A CN108905267 A CN 108905267A CN 201811118060 A CN201811118060 A CN 201811118060A CN 108905267 A CN108905267 A CN 108905267A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0009—Crystallisation cooling by heat exchange by direct heat exchange with added cooling fluid
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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Abstract
A kind of volatile oil crystallization extraction system, it is related to field of pharmaceutical equipment, it uses alternating temperature crystallization oil water separator to separate product, the alternating temperature crystallizes oil water separator can be during oil water mixture declines, it is cooling that depth is carried out to it, oil-phase component therein is promoted to condense to form crystallization, crystallization enters in filter device with water phase to be separated.Volatile oil crystallization extraction system is suitable under low temperature to be formed the collection of the material of crystallization, and simple to operate, separative efficiency is high, can be realized the online collection of material, saves human and material resources.A kind of essential oil production line comprising above-mentioned volatile oil crystallizes extraction system, high for the extraction efficiency of essential oil, is able to achieve the efficient production of essential oil product.
Description
Technical field
The present invention relates to field of pharmaceutical equipment, crystallize extraction system in particular to a kind of volatile oil and essential oil is raw
Produce assembly line.
Background technique
Volatile oil is also referred to as essential oil, is that the one kind existed in plant has volatility, can be with steam distillation, not with water
Miscible oily liquids.Volatile oil has fragrant odor mostly, and has various bioactivity.Volatile oil is in plant
Boundary's distributed pole is wide, and the plant used as Chinese medicine just has hundreds of containing volatile oil.The composition of volatile oil is considerably complicated, basic
Group becomes terpenoid, aromatic compound, aliphatic compound etc., and the ratio that wherein terpene accounts for is maximum and mainly single
Terpene, sequiterpene and its containing oxygen derivative.The important substance that volatile oil is acted on as Chinese medicine generation, study its extract with separate for
Developing new drug and promotion TCM Modernization are of great significance.For a long time, domestic and foreign scholars mention traditional medicine volatile oil
It takes and has carried out a large amount of research and probe with separating, constantly improved although extracting with separation method, majority is still
In the laboratory research stage, industrial application can not be carried out.
Volatile oil collection separator collection matched with extract equipment, separative efficiency are not high enough at present, to part medicinal material
In mass production even can not be collected into volatile oil, cause medicinal material utilization rate low, energy consumption is high, it is at high cost the problems such as, volatile oil mentions
It takes, separate the quality for equipping the production and product that have seriously affected Chinese materia medica preparation.
In consideration of it, special propose the application.
Summary of the invention
The present invention provides a kind of volatile oil to crystallize extraction system, it is intended to improve existing oil water separator to volatile oil
The not high enough problem of recovery rate.
The present invention also provides a kind of essential oil production lines, and the efficient production of essential oil may be implemented.
What the embodiment of the present invention was realized in：
A kind of volatile oil crystallization extraction system comprising steam generator, extractor, condenser, filter device and change
Temperature crystallization oil water separator, steam generator with extract pot bottom steam inlet be connected to, the gaseous phase outlet at the top of extractor and
The feed end of condenser is connected to, and the discharge end of condenser is connected to the feed end of alternating temperature crystallization oil water separator, alternating temperature crystal oil
The discharge end of separator passes through filter device and is connected to steam generation facility；
The alternating temperature crystallizes oil water separator comprising shell and is located at the intracorporal separation chamber of shell, is provided at the top of shell
For the respirator of equilibrium separation room pressure, bottom is provided with the bubbler for ventilating into separation chamber；Separation chamber includes
Positioned at the first separation chamber of upper part of the housing, and positioned at the second separation chamber of lower part of the housing；Feed pipe extend into the through shell
In one separation chamber, one end of discharge nozzle is extend into the second separation chamber through shell, and the other end is connect with filter device；Outside shell
The position of corresponding second separation chamber in side is arranged with main condenser set, is formed with the master passed through for condensate liquid between main condenser set and shell
Condensation chamber.
Further, in preferred embodiments of the present invention, the bottom of extractor is provided with for leading to steam generator
Enter to the equally distributed steam uniform device of steam of extractor.
Further, in preferred embodiments of the present invention, which further includes surge tank, surge tank
Feed end is connected to the discharge end of filter device, and the discharge end of surge tank is connected to steam generator.
Further, in the other preferred embodiments of the present invention, main condenser chamber is provided with main condenser liquid entrance and master is cold
Condensate outlet, main condenser liquid entrance are located at the bottom of main condenser chamber, and the outlet of main condenser liquid is located at the top of main condenser chamber.
Further, in the other preferred embodiments of the present invention, main condenser chamber is arranged along the circumferential direction of shell, and around shell
Body one week.
Further, in the other preferred embodiments of the present invention, the position of corresponding first separation chamber of hull outside is arranged
There is secondary condenser jacket, the secondary condensation chamber passed through for condensate liquid is formed between secondary condenser jacket and shell.
Further, in the other preferred embodiments of the present invention, secondary condensation chamber is provided with secondary condensate inlet and pair is cold
Condensate outlet, secondary condensate inlet are located at the bottom of secondary condensation chamber, and secondary condensate outlet is located at the top of secondary condensation chamber.
Further, in the other preferred embodiments of the present invention, condensation chamber is arranged along the circumferential direction of shell, and around shell
One week.
Further, in the other preferred embodiments of the present invention, alternating temperature crystallization oil water separator is additionally provided with condenser pipe,
Condenser pipe includes inlet tube, helix tube and outlet tube, and helix tube is located in the second separation chamber, and is arranged around discharge nozzle, helix tube
Both ends be connected to respectively with inlet tube and outlet tube, inlet tube and outlet tube run through shell.
Further, in the other preferred embodiments of the present invention, it further includes cyclonic separation that alternating temperature, which crystallizes oil water separator,
Device, cyclone separator are located in the first separation chamber, and the head piece that enters of cyclone separator is connected to feed pipe, the top of cyclone separator
It is provided with overflow port, bottom is provided with underflow opening.
Further, in the other preferred embodiments of the present invention, vortex chamber, vortex chamber packet are provided in cyclone separator
Include the cylindrical section vortex chamber being located above and underlying conical section vortex chamber, the opening's edge cylinder that becomes a mandarin of cyclone separator
The tangential direction setting of section vortex chamber.
Further, in the other preferred embodiments of the present invention, be provided with spoiler below underflow opening, spoiler with
Shell connection, and be arranged with the underflow opening interval of cyclone separator；Liquid gap was provided between spoiler and shell.
A kind of volatile oil extracting system comprising above-mentioned alternating temperature crystallizes oil water separator.
The beneficial effect of the embodiment of the present invention is：
The embodiment of the invention provides a kind of volatile oil to crystallize extraction system, uses alternating temperature crystallization oil water separator to production
Product are separated, which, which crystallizes oil water separator, can carry out depth cooling to it during oil water mixture declines,
Oil-phase component therein is promoted to condense to form crystallization, crystallization enters in filter device with water phase to be separated.The volatile oil knot
Brilliant extraction system is suitable under low temperature to be formed the collection of the material of crystallization, and simple to operate, separative efficiency is high, Neng Goushi
The online collection of existing material, saves human and material resources.
The embodiment of the invention also provides a kind of essential oil production lines comprising and above-mentioned volatile oil crystallizes extraction system,
It is high for the extraction efficiency of essential oil, is able to achieve the efficient production of essential oil product.
Detailed description of the invention
In order to illustrate the technical solution of the embodiments of the present invention more clearly, below will be to needed in the embodiment attached
Figure is briefly described, it should be understood that the following drawings illustrates only certain embodiments of the present invention, therefore is not construed as pair
The restriction of range for those of ordinary skill in the art without creative efforts, can also be according to this
A little attached drawings obtain other relevant attached drawings.
Fig. 1 is a kind of schematic diagram of volatile oil crystallization extraction system provided by first embodiment of the invention；
Fig. 2 is a kind of alternating temperature crystallization water-oil separating of volatile oil crystallization extraction system provided by first embodiment of the invention
The schematic diagram of device；
Fig. 3 is a kind of alternating temperature crystallization water-oil separating of volatile oil crystallization extraction system provided by second embodiment of the invention
The schematic diagram of device；
Fig. 4 is a kind of section view of the cyclone separator of volatile oil crystallization extraction system provided by second embodiment of the invention
Figure；
Fig. 5 is a kind of showing for spoiler of volatile oil crystallization extraction system provided by second embodiment of the embodiment of the present invention
It is intended to.
Icon：10- volatile oil crystallizes extraction system；11- steam generator；12- extractor；12a- steam uniform device；13-
Condenser；14- filter device；15- surge tank；100- alternating temperature crystallizes oil water separator；110- shell；111- respirator；112-
Bubbler；113- feed pipe；114- discharge nozzle；The separation chamber 120-；The first separation chamber 121-；The second separation chamber 122-；130- mistake
Filter device；140- main condenser set；141- main condenser chamber；142- main condenser liquid entrance；The outlet of 143- main condenser liquid；The condensation of 150- pair
Set；151- pair condensation chamber；152- pair condensate inlet；153- pair condensate outlet；160- condenser pipe；161- inlet tube；162-
Helix tube；163- outlet tube；170- cyclone separator；171- enters head piece；172- overflow port；173- underflow opening；174- vortex chamber；
1741- cylindrical section vortex chamber；1742- conical section vortex chamber；180- spoiler；181- crosses liquid gap；200- alternating temperature crystallizes grease
Separator.
Specific embodiment
To keep the purposes, technical schemes and advantages of embodiment of the present invention clearer, implement below in conjunction with the present invention
The technical solution in embodiment of the present invention is clearly and completely described in attached drawing in mode, it is clear that described reality
The mode of applying is some embodiments of the invention, rather than whole embodiments.Based on the embodiment in the present invention, ability
Domain those of ordinary skill every other embodiment obtained without creative efforts, belongs to the present invention
The range of protection.Therefore, the detailed description of the embodiments of the present invention provided in the accompanying drawings is not intended to limit below and is wanted
The scope of the present invention of protection is sought, but is merely representative of selected embodiment of the invention.Based on the embodiment in the present invention,
Every other embodiment obtained by those of ordinary skill in the art without making creative efforts belongs to this
Invent the range of protection.
In the description of the present invention, it is to be understood that, term " center ", " longitudinal direction ", " transverse direction ", " length ", " width ",
" thickness ", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outside", " up time
The orientation or positional relationship of the instructions such as needle ", " counterclockwise " is to be based on the orientation or positional relationship shown in the drawings, and is merely for convenience of
The description present invention and simplified description, rather than the equipment of indication or suggestion meaning or element must have a particular orientation, with spy
Fixed orientation construction and operation, therefore be not considered as limiting the invention.
In addition, term " first ", " second " are used for descriptive purposes only and cannot be understood as indicating or suggesting relative importance
Or implicitly indicate the quantity of indicated technical characteristic.Define " first " as a result, the feature of " second " can be expressed or
Implicitly include one or more of the features.In the description of the present invention, the meaning of " plurality " is two or more,
Unless otherwise specifically defined.
In the present invention unless specifically defined or limited otherwise, term " installation ", " connected ", " connection ", " fixation " etc.
Term shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or integral；It can be mechanical connect
It connects, is also possible to be electrically connected；It can be directly connected, can also can be in two elements indirectly connected through an intermediary
The interaction relationship of the connection in portion or two elements.It for the ordinary skill in the art, can be according to specific feelings
Condition understands the concrete meaning of above-mentioned term in the present invention.
In the present invention unless specifically defined or limited otherwise, fisrt feature second feature "upper" or "lower"
It may include that the first and second features directly contact, also may include that the first and second features are not direct contacts but pass through it
Between other characterisation contact.Moreover, fisrt feature includes the first spy above the second feature " above ", " above " and " above "
Sign is right above second feature and oblique upper, or is merely representative of first feature horizontal height higher than second feature.Fisrt feature exists
Second feature " under ", " lower section " and " following " include that fisrt feature is directly below and diagonally below the second feature, or is merely representative of
First feature horizontal height is less than second feature.
First embodiment
A kind of volatile oil crystallization extraction system 10 is present embodiments provided, it is shown referring to Fig.1 comprising steam generator
11, extractor 12, condenser 13, filter device 14 and alternating temperature crystallize oil water separator 100.Wherein, steam generator 11 with
The steam inlet of 12 bottom of extractor is connected to, and the gaseous phase outlet at 12 top of extractor is connected to the feed end of condenser 13, is condensed
The discharge end of device 13 is connected to the feed end of alternating temperature crystallization oil water separator 100, and alternating temperature crystallizes the discharge end of oil water separator 100
It is connected to by filter device 14 and with steam generator 11.The bottom of extractor 12 is provided with for steam generator 11 to be passed through
To the equally distributed steam uniform device 12a of steam of extractor 12.
Further, volatile oil crystallization extraction system 10 further includes surge tank 15, the feed end of surge tank 15 and filtering
The discharge end of device 14 is connected to, and the discharge end of surge tank 15 is connected to steam generator 11.
As shown in Fig. 2, the crystallization oil water separator 100 of alternating temperature used by the present embodiment is including shell 110 and is located at shell
Separation chamber 120 in 110.The generally cylindrical type of shell 110, the top of shell 110 are provided with respirator 111, and bottom is provided with
Bubbler 112.Separation chamber 120 includes the first separation chamber 121 positioned at 110 top of shell, and positioned at the of 110 lower part of shell
Two separation chambers 122.Feed pipe 113 is extend into the first separation chamber 121 through shell 110, and shell is run through in one end of discharge nozzle 114
110 extend into the second separation chamber 122, and the other end is connect with filter device 130.Corresponding second separation chamber 122 on the outside of shell 110
Position be arranged with main condenser set 140, main condenser set 140 and shell 110 between is formed with the main condenser chamber passed through for condensate liquid
141。
The oil water mixture formed by volatile oil and condensed water is entered in the first separation chamber 121 by feed pipe 113.Volatilization
It include target product and other impurity compositions in oil, the light component impurity in oil water mixture rises, carries out just with product
Step separation.And product and water then sink to entering the second separation chamber 122 together, during sinking, pass through main condenser chamber 141
In condensate liquid cool down to the product in the second separation chamber 122, form it into crystallization, crystallization is with water by discharge nozzle
114 are discharged in filter device 130, are separated by solid-liquid separation.In crystallization process, the bubbler 112 of 110 bottom of shell can be roused
Outlet bubble plays the role of stirring, and promotes the rapid crystallization of product.The respirator 111 of shell 110 can be used for equilibrium separation room
Air pressure in 120 is avoided the occurrence of since separation caused by negative pressure is unsmooth, flows backwards, or by the spray of the excessive initiation of pressure
Situations such as liquid, leakage.It is worth noting that, in the present embodiment, between the first separation chamber 121 and the second separation chamber 122 not
Having and is really separated, the first separation chamber 121 and the second separation chamber 122 are actually still one complete whole, and second
Separation chamber 122 is only the differentiation functionally for having the effect to cool down again according to it, and carrying out.Preferably, main condenser chamber
Condensate temperature in 141 is controlled at -20~0 DEG C, to guarantee that sufficient condensation-crystallization can be carried out to product.
Main condenser chamber 141 is provided with main condenser liquid entrance 142 and main condenser liquid outlet 143, and main condenser liquid entrance 142 is located at
The bottom of main condenser chamber 141, main condenser liquid outlet 143 are located at the top of main condenser chamber 141.Condensate liquid moves from the bottom to top, with
Adverse current is formed between product and the mixture of water, achievees the purpose that improve cooling effect.
Main condenser chamber 141 allows condensate liquid from shell and around shell 110 1 weeks along the circumferential direction setting of shell 110
110 all directions uniformly cool down to the mixing liquid in the second separation chamber 122, increase the effect of separation.
Main condenser set 140 is made of heat-barrier material.The set of main condenser made of heat-barrier material 140 can prevent the outer of cold air
It overflows, allows condensate liquid that heat transmitting preferably to occur between shell 110, improve to mixing liquid in the second separation chamber 122
Cool down efficiency.
Further, the position of corresponding first separation chamber 121 is arranged with secondary condenser jacket 150, secondary condenser jacket on the outside of shell 110
The secondary condensation chamber 151 passed through for condensate liquid is formed between 150 and shell 110.Preferably, the condensate liquid in secondary condensation chamber 151
Temperature is 5~20 DEG C, can be precooled to the mixing liquid entered in the first separation chamber 121.It is cooled down in product
During crystallization, temperature change is too fast, and it is too fast to will cause crystalline rate, and being easy to cause to sandwich in crystallization has impurity, influences to produce
Product purity.And can then slow down the variation of temperature by precooling, keep the process of crystallization more gentle, improves the pure of product
Degree.
Similarly, secondary condensation chamber 151 is provided with secondary condensate inlet 152 and secondary condensate outlet 153, secondary condensate inlet
152 are located at the bottom of secondary condensation chamber 151, and secondary condensate outlet 153 is located at the top of secondary condensation chamber 151.Condensate liquid is from the bottom to top
Movement forms adverse current between product and the mixture of water, achievees the purpose that improve cooling effect.
Secondary condensation chamber 151 allows condensate liquid from shell and around shell 110 1 weeks along the circumferential direction setting of shell 110
110 all directions uniformly cool down to the mixing liquid in the second separation chamber 122, increase the effect of separation.
Secondary condenser jacket 150 is made of heat-barrier material.Pair condenser jacket 150 made of heat-barrier material can prevent the outer of cold air
It overflows, allows condensate liquid that heat transmitting preferably to occur between shell 110, improve to mixing liquid in the second separation chamber 122
Cool down efficiency.
Second embodiment
A kind of volatile oil crystallization extraction system (not shown) is present embodiments provided, is become with provided by first embodiment
The difference of temperature crystallization oil water separator 100 is which employs alternating temperatures to crystallize oil water separator 200.Alternating temperature crystallizes water-oil separating
Device 200 is to improve to obtain on the basis of alternating temperature crystallizes oil water separator 100, with alternating temperature crystallization oil water separator 100
It distinguishes as follows.
In order to further promote cooling efficiency, as shown in figure 3, the alternating temperature in the present embodiment crystallizes oil water separator 200
It is additionally provided with condenser pipe 160, condenser pipe 160 includes inlet tube 161, helix tube 162 and outlet tube 163, and helix tube 162 is located at the
In two separation chambers 122, and it is arranged around discharge nozzle 114, the both ends of helix tube 162 connect with inlet tube 161 and outlet tube 163 respectively
Logical, inlet tube 161 and outlet tube 163 run through shell 110.Condenser pipe 160 can be extend into the second separation chamber 122, to second
Mixing liquid inside separation chamber 122 cools down, and is used cooperatively with main condenser chamber 141, can greatly increase cooling efficiency.
Further, as shown in Figure 3 and Figure 4, in the present embodiment, alternating temperature crystallization oil water separator 200 further includes eddy flow
Separator 170, cyclone separator 170 are located in the first separation chamber 121, and cyclone separator 170 enters head piece 171 and feed pipe
113 connections, the top of cyclone separator 170 are provided with overflow port 172, and bottom is provided with underflow opening 173.Cyclone separator 170
Preliminary separation can be carried out to oil water mixture, under the effect of centrifugation, light component impurity is by 170 top of cyclone separator
Overflow port 172 flows out, and product and water are then flowed out by the underflow opening 173 of 170 bottom of cyclone separator.
Vortex chamber 174 is provided in cyclone separator 170, vortex chamber 174 includes the cylindrical section vortex chamber being located above
1741 and underlying conical section vortex chamber 1742, cyclone separator 170 enter head piece 171 along cylindrical section vortex chamber
1741 tangential direction setting.The oil water mixture tangentially entered helically gestalt movement is entering conical section vortex chamber
After 1742, with being gradually reduced for internal diameter, liquid in rotation speed is gradually accelerated.Since the bore of underflow opening 173 is smaller, so that liquid
Body can not all be discharged from underflow opening 173.Under such circumstances, product and water are flowed along the cavity wall of vortex chamber 174 by underflow opening 173
Out, and squeeze light component impurity to upward at the lower center of pressure, flowed out by overflow port 172, realize light component impurity just
Step separation.
Further, as shown in Figure 3 and Figure 5, the lower section of underflow opening 173 is provided with spoiler 180, spoiler 180 and shell
Body 110 connects, and is spaced and is arranged with the underflow opening of cyclone separator 170 173；It was provided between spoiler 180 and shell 110
Liquid gap 181.The movement velocity of the product and water that flowed out by underflow opening 173 is very fast, after flowing into the second separation chamber 122, cannot do
Cooling is stopped to sufficient.The setting of spoiler 180 can then play preferable buffer function, product and water slug to spoiler
On 180, after being blocked deceleration, then by cross liquid gap 181 be flowed into the second separation chamber 122, adequately cooled down, Jin Erti
High score from effect.
The present embodiment additionally provides a kind of volatile oil extracting system comprising above-mentioned alternating temperature crystallizes oil water separator 200.Its
Oil water separator 200 is crystallized including above-mentioned alternating temperature, it is high for the separative efficiency of oil water mixture, the receipts of volatile oil can be improved
Rate.
In conclusion the embodiment of the invention provides a kind of volatile oil to crystallize extraction system, alternating temperature is used to crystallize grease
Separator separates product, the alternating temperature crystallize oil water separator can oil water mixture decline during, to its into
Row depth is cooling, and oil-phase component therein is promoted to condense to form crystallization, and crystallization enters in filter device with water phase to be separated.
Volatile oil crystallization extraction system is suitable under low temperature to be formed the collection of the material of crystallization, simple to operate, separation effect
Rate is high, can be realized the online collection of material, saves human and material resources.
The embodiment of the invention also provides a kind of essential oil production lines comprising and above-mentioned volatile oil crystallizes extraction system,
It is high for the extraction efficiency of essential oil, and are produced from be able to achieve essential oil product efficient raw 5.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, for the skill of this field
For art personnel, the invention may be variously modified and varied.All within the spirits and principles of the present invention, made any to repair
Change, equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of volatile oil crystallizes extraction system, which is characterized in that including steam generator, extractor, condenser, filter device
And alternating temperature crystallizes oil water separator, the steam generator is connected to the steam inlet for extracting pot bottom, the extraction
The gaseous phase outlet of tank top is connected to the feed end of the condenser, and the discharge end of the condenser and the alternating temperature crystallize grease
The feed end of separator is connected to, the discharge end of the alternating temperature crystallization oil water separator by the filter device and with the steam
Generating device connection；
The alternating temperature crystallization oil water separator includes shell and is located at the intracorporal separation chamber of the shell, and the top of the shell is arranged
There is the respirator for balancing the separation room pressure, bottom is provided with the bubbler for ventilating into the separation chamber；
The separation chamber includes positioned at the first separation chamber of the upper part of the housing, and the second separation chamber positioned at the lower part of the housing；
One end of feed pipe is extend into first separation chamber through the shell, and the discharge end of the other end and the condenser connects
It is logical；One end of discharge nozzle is extend into second separation chamber through the shell, and the other end is connect with the filter device；Institute
It states hull outside and corresponds to the position of second separation chamber and be arranged with main condenser set, shape between the main condenser set and the shell
At there is the main condenser chamber passed through for condensate liquid.
2. volatile oil according to claim 1 crystallizes extraction system, which is characterized in that it is cold that the main condenser chamber is provided with master
Lime set entrance and the outlet of main condenser liquid, the main condenser liquid entrance are located at the bottom of the main condenser chamber, and the main condenser liquid goes out
Mouth is located at the top of the main condenser chamber.
3. volatile oil according to claim 2 crystallizes extraction system, which is characterized in that the main condenser chamber is along the shell
Circumferential setting, and around the shell one week.
4. volatile oil according to claim 1 crystallizes extraction system, which is characterized in that the hull outside corresponds to described the
The position of one separation chamber is arranged with secondary condenser jacket, is formed with the pair passed through for condensate liquid between the pair condenser jacket and the shell
Condensation chamber.
5. volatile oil according to claim 4 crystallizes extraction system, which is characterized in that the pair condensation chamber is provided with secondary cold
Lime set entrance and secondary condensate outlet, the pair condensate inlet are located at the bottom of the secondary condensation chamber, and the pair condensate liquid goes out
Mouth is located at the top of the secondary condensation chamber.
6. volatile oil according to claim 5 crystallizes extraction system, which is characterized in that the condensation chamber is along the shell
Circumferential setting, and around the shell one week.
7. volatile oil according to claim 1 crystallizes extraction system, which is characterized in that the alternating temperature crystallizes oil water separator
It is additionally provided with condenser pipe, the condenser pipe includes inlet tube, helix tube and outlet tube, and the helix tube is located at second separation
Interior, and be arranged around the discharge nozzle, the both ends of the helix tube are connected to the inlet tube and the outlet tube respectively, described
Inlet tube and the outlet tube run through the shell.
8. volatile oil according to claim 1 crystallizes extraction system, which is characterized in that the alternating temperature crystallizes oil water separator
Further include cyclone separator, the cyclone separator is located in first separation chamber, the cyclone separator enter head piece with
The feed pipe is connected to, and is provided with overflow port at the top of the cyclone separator, bottom is provided with underflow opening.
9. volatile oil according to claim 8 crystallizes extraction system, which is characterized in that be provided in the cyclone separator
Vortex chamber, the vortex chamber include the cylindrical section vortex chamber being located above and underlying conical section vortex chamber, the rotation
The tangential direction of the cylindrical section vortex chamber described in opening's edge that becomes a mandarin of stream separator is arranged.
10. a kind of essential oil production line, which is characterized in that crystallized including volatile oil as described in any one of claims 1 to 9
Extraction system.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110280041A (en) * | 2019-07-01 | 2019-09-27 | 苏州乔发环保科技股份有限公司 | A kind of thickener |
| CN114561248A (en) * | 2022-03-02 | 2022-05-31 | 华润三九（雅安）药业有限公司 | Preparation method and device of volatile oil, inclusion compound and preparation method of pharmaceutical composition |
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| WO2013154419A1 (en) * | 2012-04-09 | 2013-10-17 | Oiltek Sdn Bhd | An apparatus for dry fractionation of oils and fats |
| CN203999038U (en) * | 2014-04-03 | 2014-12-10 | 扬州天源环保工程有限公司 | Cyclone-type water-and-oil separator |
| CN204952333U (en) * | 2015-09-22 | 2016-01-13 | 杭州森香科技有限公司 | Instantaneous overheated steam distillation equipment |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110280041A (en) * | 2019-07-01 | 2019-09-27 | 苏州乔发环保科技股份有限公司 | A kind of thickener |
| CN114561248A (en) * | 2022-03-02 | 2022-05-31 | 华润三九（雅安）药业有限公司 | Preparation method and device of volatile oil, inclusion compound and preparation method of pharmaceutical composition |
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