CN106902550A - A kind of fir essential oil production oily-water seperating equipment of optimization design - Google Patents
A kind of fir essential oil production oily-water seperating equipment of optimization design Download PDFInfo
- Publication number
- CN106902550A CN106902550A CN201710286827.7A CN201710286827A CN106902550A CN 106902550 A CN106902550 A CN 106902550A CN 201710286827 A CN201710286827 A CN 201710286827A CN 106902550 A CN106902550 A CN 106902550A
- Authority
- CN
- China
- Prior art keywords
- separation container
- dividing plate
- collecting pipe
- feed tube
- pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000341 volatile oil Substances 0.000 title claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 19
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 14
- 238000005457 optimization Methods 0.000 title claims abstract description 11
- 238000000926 separation method Methods 0.000 claims abstract description 53
- 230000003139 buffering effect Effects 0.000 claims abstract description 19
- 239000000872 buffer Substances 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims abstract description 8
- 239000003305 oil spill Substances 0.000 claims abstract description 8
- 230000002093 peripheral effect Effects 0.000 claims description 3
- 230000001105 regulatory effect Effects 0.000 claims description 3
- 239000003921 oil Substances 0.000 description 15
- 238000000034 method Methods 0.000 description 10
- 230000000694 effects Effects 0.000 description 7
- 238000001256 steam distillation Methods 0.000 description 5
- 238000002156 mixing Methods 0.000 description 4
- 244000050510 Cunninghamia lanceolata Species 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- 241000218645 Cedrus Species 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- IRAQOCYXUMOFCW-CXTNEJHOSA-N cedrene Chemical group C1[C@]23[C@H](C)CC[C@H]3C(C)(C)[C@H]1C(C)=CC2 IRAQOCYXUMOFCW-CXTNEJHOSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- IRAQOCYXUMOFCW-UHFFFAOYSA-N di-epi-alpha-cedrene Natural products C1C23C(C)CCC3C(C)(C)C1C(C)=CC2 IRAQOCYXUMOFCW-UHFFFAOYSA-N 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000003550 marker Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
- B01D17/0211—Separation of non-miscible liquids by sedimentation with baffles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
- B01D17/0214—Separation of non-miscible liquids by sedimentation with removal of one of the phases
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The invention discloses a kind of fir essential oil production oily-water seperating equipment of optimization design, including separation container；The condensate line no less than one is provided with the top of separation container, separation container is provided with oil spill pipe by top sidewall, and separation container is provided with drainpipe by bottom sidewall；Center is provided with collecting pipe along the vertical direction in separation container, and the height of collecting pipe bottom face is suitable with position height at the middle waist of separation container；The bottom face of collecting pipe is provided with loop buffer dividing plate, buffers the internal face seamless connectivity of the side face of dividing plate largest contours and the corresponding position of separation container；Buffering dividing plate inner ring surface is all with the bottom of collecting pipe along seamless connectivity；Gathered on buffering dividing plate and be provided with multiple through holes；Condensate line quantity is two, is respectively first, second feed tube；First, second feed tube is each provided at the top of collecting pipe, and first feed tube is mutually arranged oppositely with second feed tube.Liquid level stationarity influence of the feed liquor on separation container is small, and oil-water separation is more preferable.
Description
Technical field
The invention belongs to the extractive technique field of fir essential oil, it is related to a kind of fir essential oil production profit of optimization design
Separator.
Background technology
Contain substantial amounts of fir essential oil in China fir, its main component is cedrene, cedar wood alcohol etc., can be used for perfume industry
In.At present, the extraction processing of fir essential oil is main using solvent extraction method, cracking process, steam distillation.Using solvent extraction
The oil yield that method extracts fir essential oil is high compared with the oil yield of steam distillation, but needs substantial amounts of solvent, and subsequent treatment is complicated,
There is a problem of high energy consumption, dissolvent residual.The oil yield for extracting fir essential oil using cracking process is higher, but it is a chemical mistake
Journey, the essential oil for obtaining contains the materials such as substantial amounts of tar, phenol, aldehyde and ketone, has a strong impact on the quality of fir essential oil.Steam distillation
Preferably, clear, aroma of pure are best suitable for for blending the fir essential oil quality that method is extracted, and its extraction process is pure thing
Reason process, it is pollution-free, but oil yield is relatively low.Several techniques compare, and steam distillation is the production work of preferred environment-friendly type
Skill, but should also optimize to improve yield and further reducing energy consumption.The step of steam distillation extracts fir essential oil
It is：A, China fir is ground into fir powder；B, in fir powder add dispensing be stirred mixing；C, the fir powder that will be mixed send
Enter in destilling tower, distilled to superheated steam is passed through in destilling tower, distillation time is 9-11 hours；That is discharged after D, distillation is mixed
Close gas be delivered in cooling tower cooled down after obtain oil mixing with water liquid；E, oil mixing with water liquid are obtained after water-oil separating
Fir essential oil.
Oily-water seperating equipment is the equipment of whole flow process most terminal, therefore the efficiency of oily-water seperating equipment is related to whole China fir
The efficiency of another name for oil production.The effect quality of water-oil separating is heavily dependent on separation container 2 during dynamic is continuously produced
The stationarity of liquid level.
The structure of fir essential oil production oily-water seperating equipment of the prior art is as shown in figure 1, including separation container 2；
The top of separation container 2 is provided with the condensate line 1 no less than, and the side wall by top of separation container 2 is provided with oil spill pipe
3, the side wall by bottom of separation container 2 is provided with drainpipe 4.
Using the oily-water seperating equipment of such technology it is of course possible to use, but because the feed liquor impact of condensate line 1 can be right
The stationarity of the liquid level of separation container 2 has relatively large influence, causes the effect of water-oil separating not good enough, and using effect is also
It is not ideal enough.
The content of the invention
To overcome the deficiencies in the prior art, the influence that the present invention provides a kind of stationarity of feed liquor to liquid level is small, profit point
From the more preferable optimization design of effect fir essential oil production oily-water seperating equipment, using effect is more preferable.
The technical scheme that is used to reach above-mentioned technical purpose of the present invention is：A kind of fir essential oil production of optimization design
With oily-water seperating equipment, including separation container；The condensate line no less than one is provided with the top of separation container, separation container
Side wall by top is provided with oil spill pipe, and the side wall by bottom of separation container is provided with drainpipe；Center in separation container
Place is inserted with collecting pipe along the vertical direction, and the position height of the bottom face of collecting pipe is high with position at the middle waist of separation container
Degree is suitable；The bottom face of collecting pipe is provided with the buffering dividing plate of annular, buffers the side face and separation container of the largest contours of dividing plate
The internal face seamless connectivity of corresponding position；The inner ring surface of dividing plate and the bottom week of collecting pipe are buffered along seamless connectivity；Buffer compartment
Gathered on plate and be provided with multiple through holes；The quantity of condensate line is two, is respectively first feed tube, second feed tube；First feed tube
With the top that second feed tube is each provided at collecting pipe, first feed tube is mutually arranged oppositely with second feed tube.
Described separation container is the separation container of cylinder；Described collecting pipe is columnar collecting pipe；Separate and hold
Device is coaxially disposed with collecting pipe；Described buffering dividing plate is the buffering dividing plate of annular, buffers the outer diameter of a circle of dividing plate and divides
From the inner peripheral surface equal diameters of container；Buffer the interior diameter of a circle of dividing plate and the cylindrical equal diameters of collecting pipe.
The bottom surface of described separation container is provided with funnelform conical bottom, and the lowermost end of conical bottom is provided with blow-off pipe.
Described oil spill pipe, drainpipe, the valve that regulating flow quantity is equipped with blow-off pipe three.
The advantage of the invention is that：Collecting pipe is inserted with due to the center in separation container along the vertical direction, is confluxed
The position height of the bottom face of pipe is suitable with the position height at the middle waist of separation container；The bottom face of collecting pipe is provided with annular
Buffering dividing plate, buffers the internal face seamless connectivity of the side face of the largest contours of dividing plate and the corresponding position of separation container；Buffer compartment
The inner ring surface of plate is all with the bottom of collecting pipe along seamless connectivity；Gathered on buffering dividing plate and be provided with multiple through holes；Condensate line
Quantity be two, be respectively first feed tube, second feed tube；First feed tube and second feed tube are each provided at the top of collecting pipe, first
Feed tube is mutually arranged oppositely with second feed tube.
Therefore, the two strands of feed liquors for being separately flowed into from first feed tube and second feed tube are imported after first relative eating up part of small impulsive force
Collecting pipe simultaneously flows out from bottom of the tube of confluxing to surrounding, and water body can sink to the bottom, and oil body can float, due to buffering the filtering resiliency of dividing plate
Stop, the process that oil body floats more relaxes, the slag charge in feed liquor can be blocked in the bottom surface of buffering dividing plate and sink, floating
With regard to very little, just more preferably, using effect is more preferable for the effect of water-oil separating for influence of the oil body to the stationarity of the liquid level of separation container.
Brief description of the drawings
The invention will be further described with reference to the accompanying drawings and examples.Wherein：
Fig. 1 is the schematic diagram of the oily-water seperating equipment of prior art；
Fig. 2 is subdivision schematic diagram of the invention.
Marker number in accompanying drawing is described as follows：Condensate line 1, first feed tube 1A, second feed tube 1B, separation container 2, overflow
Oil pipe 3, drainpipe 4, collecting pipe 5, buffering dividing plate 6, conical bottom 7, blow-off pipe 8
Specific embodiment
Embodiments of the invention, as shown in Fig. 2 a kind of fir essential oil production oily-water seperating equipment of optimization design, bag
Include separation container 2；The top of separation container 2 is provided with the condensate line no less than, on the side wall by top of separation container 2
Oil spill pipe 3 is provided with, the side wall by bottom of separation container 2 is provided with drainpipe 4；Center in separation container 2 is vertically
Direction is inserted with collecting pipe 5, and the position height of the bottom face of collecting pipe 5 is suitable with the position height at the middle waist of separation container 2；
The bottom face of collecting pipe 5 is provided with the buffering dividing plate 6 of annular, and the side face for buffering the largest contours of dividing plate 6 is corresponding with separation container 2
The internal face seamless connectivity at place；The inner ring surface of dividing plate 6 and the bottom week of collecting pipe 5 are buffered along seamless connectivity；Buffering dividing plate 6
Upper gathering is provided with multiple through holes；The quantity of condensate line is two, is respectively first feed tube 1A, second feed tube 1B；First feed liquor
Pipe 1A and second feed tube 1B are each provided at the top of collecting pipe 5, and first feed tube 1A is arranged oppositely with second feed tube 1B phases.
Described separation container 2 is the separation container 2 of cylinder；Described collecting pipe 5 is columnar collecting pipe 5；Point
It is coaxially disposed with collecting pipe 5 from container 2；Described buffering dividing plate 6 is the buffering dividing plate 6 of annular, buffers the cylindrical of dividing plate 6
The inner peripheral surface equal diameters of diameter and separation container 2；Buffer the interior diameter of a circle of dividing plate 6 and the outer diameter of a circle phase of collecting pipe 5
Deng.
The bottom surface of described separation container 2 is provided with funnelform conical bottom 7, and the lowermost end of conical bottom 7 is provided with blow-off pipe
8。
Described oil spill pipe 3, drainpipe 4, the valve that regulating flow quantity is equipped with the three of blow-off pipe 8.
Claims (4)
1. a kind of fir essential oil production oily-water seperating equipment of optimization design, including separation container；Set at the top of separation container
Have a condensate line no less than, the side wall by top of separation container is provided with oil spill pipe, separation container by bottom
Side wall is provided with drainpipe；It is characterized in that：Center in separation container is inserted with collecting pipe, collecting pipe along the vertical direction
The position height of bottom face it is suitable with the position height at the middle waist of separation container；The bottom face of collecting pipe is provided with the slow of annular
Dividing plate is rushed, the internal face seamless connectivity of the side face of the largest contours of dividing plate and the corresponding position of separation container is buffered；Buffering dividing plate
Inner ring surface and collecting pipe bottom week along seamless connectivity；Gathered on buffering dividing plate and be provided with multiple through holes；Condensate line
Quantity is two, is respectively first feed tube, second feed tube；First feed tube and second feed tube are each provided at the top of collecting pipe, and first is entered
Liquid pipe is mutually arranged oppositely with second feed tube.
2. the fir essential oil production oily-water seperating equipment of a kind of optimization design according to claim 1, it is characterised in that：
Described separation container is the separation container of cylinder；Described collecting pipe is columnar collecting pipe；Separation container with conflux
Pipe is coaxially disposed；Described buffering dividing plate is the buffering dividing plate of annular, buffers the outer diameter of a circle and separation container of dividing plate
Inner peripheral surface equal diameters；Buffer the interior diameter of a circle of dividing plate and the cylindrical equal diameters of collecting pipe.
3. the fir essential oil production oily-water seperating equipment of a kind of optimization design according to claim 2, it is characterised in that：
The bottom surface of described separation container is provided with funnelform conical bottom, and the lowermost end of conical bottom is provided with blow-off pipe.
4. the fir essential oil production oily-water seperating equipment of a kind of optimization design according to claim 3, it is characterised in that：
Described oil spill pipe, drainpipe, the valve that regulating flow quantity is equipped with blow-off pipe three.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710286827.7A CN106902550A (en) | 2017-04-27 | 2017-04-27 | A kind of fir essential oil production oily-water seperating equipment of optimization design |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710286827.7A CN106902550A (en) | 2017-04-27 | 2017-04-27 | A kind of fir essential oil production oily-water seperating equipment of optimization design |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106902550A true CN106902550A (en) | 2017-06-30 |
Family
ID=59211264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710286827.7A Pending CN106902550A (en) | 2017-04-27 | 2017-04-27 | A kind of fir essential oil production oily-water seperating equipment of optimization design |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106902550A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108905292A (en) * | 2018-09-25 | 2018-11-30 | 江西中医药大学 | A kind of alternating temperature oil water separator and volatile oil extracting system |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2463023Y (en) * | 2000-12-28 | 2001-12-05 | 陈彬扬 | Oil-water separator |
| US20120255900A1 (en) * | 2009-12-10 | 2012-10-11 | Noriyoshi Osawa | Oil-water separation device and refining device |
| CN202529889U (en) * | 2012-04-08 | 2012-11-14 | 营口市环境工程开发有限公司 | Oil-water separator for treating oil shale wastewater |
| CN203564817U (en) * | 2013-11-29 | 2014-04-30 | 浙江扬帆新材料股份有限公司 | Oil-water separator with improved separation effect |
| CN104404925A (en) * | 2014-10-08 | 2015-03-11 | 四川大学 | Porous inflow hedging energy dissipation structure of hydraulic structure |
| CN105214345A (en) * | 2015-10-21 | 2016-01-06 | 宁波新能电器科技有限公司 | A kind of oil water separator |
| CN206746047U (en) * | 2017-04-27 | 2017-12-15 | 福建鑫绿林产品开发有限公司 | A kind of fir essential oil production oily-water seperating equipment of optimization design |
-
2017
- 2017-04-27 CN CN201710286827.7A patent/CN106902550A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2463023Y (en) * | 2000-12-28 | 2001-12-05 | 陈彬扬 | Oil-water separator |
| US20120255900A1 (en) * | 2009-12-10 | 2012-10-11 | Noriyoshi Osawa | Oil-water separation device and refining device |
| CN202529889U (en) * | 2012-04-08 | 2012-11-14 | 营口市环境工程开发有限公司 | Oil-water separator for treating oil shale wastewater |
| CN203564817U (en) * | 2013-11-29 | 2014-04-30 | 浙江扬帆新材料股份有限公司 | Oil-water separator with improved separation effect |
| CN104404925A (en) * | 2014-10-08 | 2015-03-11 | 四川大学 | Porous inflow hedging energy dissipation structure of hydraulic structure |
| CN105214345A (en) * | 2015-10-21 | 2016-01-06 | 宁波新能电器科技有限公司 | A kind of oil water separator |
| CN206746047U (en) * | 2017-04-27 | 2017-12-15 | 福建鑫绿林产品开发有限公司 | A kind of fir essential oil production oily-water seperating equipment of optimization design |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108905292A (en) * | 2018-09-25 | 2018-11-30 | 江西中医药大学 | A kind of alternating temperature oil water separator and volatile oil extracting system |
| CN108905292B (en) * | 2018-09-25 | 2023-09-26 | 江西中医药大学 | Temperature-changing oil-water separator and volatile oil extraction system |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170630 |
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| RJ01 | Rejection of invention patent application after publication |