CN108904380A - A kind of hygenic towelette and its manufacturing method with bacteria resistance function - Google Patents
A kind of hygenic towelette and its manufacturing method with bacteria resistance function Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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Abstract
The present invention relates to hygenic towelette manufacturing fields, a kind of hygenic towelette and its manufacturing method with bacteria resistance function are provided, for improving the fungistatic effect of hygenic towelette.A kind of hygenic towelette and its manufacturing method with bacteria resistance function provided by the invention, including substrate and wet tissue lotion, load has wet tissue lotion on the substrate；The wet tissue lotion includes 1 ~ 2 mass parts of glycerol, 3 ~ 6 mass parts of hyaluronic acid, 2 ~ 4 mass parts of cetyl polyoxyethylene ether sodium phosphate, 4 ~ 6 mass parts of Chinese medical extract, 0.2 ~ 0.5 mass parts of EDETATE SODIUM, 60 ~ 70 mass parts of deionized water.The hygenic towelette of addition Chinese medical extract can effectively inhibit the growth of bacterium, while small to the irritation of skin.
Description
Technical field
The present invention relates to hygenic towelette manufacturing fields, and in particular to a kind of hygenic towelette and its manufacturer with bacteria resistance function
Method.
Background technique
Hygenic towelette is a kind of common cleaning supplies, since it contains certain moisture, sterilization component and cleansing, when
When be not easy in environment with water, hygenic towelette can preferably replace towel, and take it is more convenient so that the use model of hygenic towelette
It encloses increasingly wider.
But the disinfection and sterilization ingredient in existing hygenic towelette is usually that ethyl alcohol, Iodophor, Peracetic acid, bleaching powder crystalline substance etc. are changed
Medicament is learned, although which has certain bactericidal effect, but larger to the irritation of skin, while sterilizing ability is limited.
Summary of the invention
Present invention solves the technical problem that providing a kind of l Water Paper with bacteria resistance function to improve the fungistatic effect of hygenic towelette
Towel and its manufacturing method.
In order to solve the above technical problem, the present invention provides technical solution be：
A kind of hygenic towelette with bacteria resistance function, including substrate and wet tissue lotion, load has wet tissue lotion on the substrate；Institute
The wet tissue lotion stated includes 1 ~ 2 mass parts of glycerol, 3 ~ 6 mass parts of hyaluronic acid, 2 ~ 4 matter of cetyl polyoxyethylene ether sodium phosphate
Measure part, 4 ~ 6 mass parts of Chinese medical extract, 0.2 ~ 0.5 mass parts of EDETATE SODIUM, 60 ~ 70 mass parts of deionized water.
Include Chinese medical extract and a small amount of hyaluronic acid in wet tissue lotion, has both antibacterial and skin effect, it can be effective
Consistent wet tissue to the irritation of skin, while the bactericidal effect of Chinese medical extract is better than traditional medicament, while to skin
Irritation is small.
The hygenic towelette of addition Chinese medical extract can effectively inhibit the growth of bacterium, while irritation is small.
Preferably, the wet tissue lotion includes 1.5 ~ 2 mass parts of glycerol, 4 ~ 6 mass parts of hyaluronic acid, and cetyl is poly-
3 ~ 4 mass parts of ethylene oxide ether phosphoric acid sodium, 5 ~ 6 mass parts of Chinese medical extract, 0.3 ~ 0.5 mass parts of EDETATE SODIUM, deionized water 65 ~
70 mass parts.
Preferably, the wet tissue lotion includes 1.5 mass parts of glycerol, 4 mass parts of hyaluronic acid, cetyl polyoxy second
3 mass parts of alkene ether phosphoric acid sodium, 5 mass parts of Chinese medical extract, 0.3 mass parts of EDETATE SODIUM, 65 mass parts of deionized water.
Preferably, the Chinese medical extract includes 50 ~ 60 mass parts of Chinese medicinal component and modified 2 ~ 6 mass parts of component.Change
Property component can significantly improve the fungistatic effect of Chinese medicinal component.
Preferably, the Chinese medicinal component includes 1 ~ 2 mass parts of Fructus Corni, 2 ~ 3 mass parts of Medulla Tetrapanacis extract, and mistletoe mentions
Take 2 ~ 5 mass parts of object, 10 ~ 12 mass parts of rose of Sharon bark extract, 1 ~ 3 mass parts of Viscum album extract, 1 ~ 4 matter of Saururus chinensis extract
Measure part；After the Fructus Corni, the stem pith of the rice-paper plant, mistletoe, Cortex hibisus syriacus, herba taxilli and saururus chinensis are crushed, 60 ~ 80 mass parts are added
Deionized water impregnates 2h, takes filter residue after filtering；The filter residue is added to impregnated for 24 hours in the ethyl alcohol of 10 ~ 20 mass parts after, to leaching
Filter residue after bubble carries out diacolation, and diacolation rate is 80 ~ 90ml/min/Kg, and the dosage of the ethyl alcohol is the 10 ~ 16 of filter residue amount
Times, percolate is collected, percolate is subjected to heating concentration decrement, and recycle ethyl alcohol simultaneously, it is dry that obtained concentrate carries out vacuum
It is dry to obtain, Chinese medicinal component；The modification component is 2 ~ 5 mass parts of nano-titanium dioxide, and 5 ~ 6 mass parts of nano zine oxide are received
Above-mentioned nano-oxide is dissolved in deionized water, 40 DEG C by rice 0.5 ~ 1 mass parts of manganese dioxide, 40 ~ 50 mass parts of deionized water
Ultrasonic water bath 3h obtains modified component；Chinese medicinal component is dissolved in the deionized water of 20 ~ 30 mass parts with modified component, ultrasound
Chinese medical extract is obtained after dispersion.
Chinese medicinal component can further improve the fungistatic effect of hygenic towelette, while to skin with modified component compounding
Irritation is small；Fructus Corni, the stem pith of the rice-paper plant, mistletoe, Cortex hibisus syriacus, herba taxilli and saururus chinensis in wet tissue lotion after seepage pressure effects
There is significant fungistatic effect, this may be since Cortex hibisus syriacus has certain fungistatic effect, and same Fructus Corni, the stem pith of the rice-paper plant, Mongolian oak are posted
The fungistatic effect of extract has more significant raising after raw, herba taxilli and saururus chinensis compounding；Modified component itself has centainly
Fungistatic effect, but its main function is that same Chinese medicinal component generates synergy, further increases the fungistatic effect of Chinese medicinal component, together
When nano-scale particle can effectively disperse, and then significantly improve the fungistatic effect of Chinese medical extract.
Preferably, the Chinese medicinal component includes 1.5 ~ 2 mass parts of Fructus Corni, 2.5 ~ 3 mass parts of Medulla Tetrapanacis extract, and Mongolian oak is posted
Raw 3 ~ 5 mass parts of extract, 11 ~ 12 mass parts of rose of Sharon bark extract, 2 ~ 3 mass parts of Viscum album extract, Saururus chinensis extract 2
~ 4 mass parts；After the Fructus Corni, the stem pith of the rice-paper plant, mistletoe, Cortex hibisus syriacus, herba taxilli and saururus chinensis are crushed, 70 ~ 80 mass are added
The deionized water of part impregnates 2h, takes filter residue after filtering；The filter residue is added to impregnated for 24 hours in the ethyl alcohol of 15 ~ 20 mass parts after,
Diacolation carried out to the filter residue after immersion, diacolation rate is 85 ~ 90ml/min/Kg, the dosage of the ethyl alcohol be filter residue amount 12 ~
16 times, percolate is collected, percolate is subjected to heating concentration decrement, and recycle ethyl alcohol simultaneously, obtained concentrate carries out vacuum
It is dried to obtain Chinese medicinal component；The modification component be 3 ~ 5 mass parts of nano-titanium dioxide, 5.5 ~ 6 mass parts of nano zine oxide,
0.8 ~ 1 mass parts of nano-manganese dioxide, 45 ~ 50 mass parts of deionized water, above-mentioned nano-oxide are dissolved in deionized water, 40
DEG C ultrasonic water bath 3h obtains modified component；Chinese medicinal component is dissolved in the deionized water of 25 ~ 30 mass parts with modified component, is surpassed
Chinese medical extract is obtained after sound dispersion.
Preferably, the Chinese medicinal component includes 1.5 mass parts of Fructus Corni, 2.5 mass parts of Medulla Tetrapanacis extract, and mistletoe mentions
Take 3 mass parts of object, 11 mass parts of rose of Sharon bark extract, 2 mass parts of Viscum album extract, 2 mass parts of Saururus chinensis extract；By institute
After Fructus Corni, the stem pith of the rice-paper plant, mistletoe, Cortex hibisus syriacus, herba taxilli and the saururus chinensis stated crush, the deionized water that 70 mass parts are added is impregnated
2h takes filter residue after filtering；The filter residue is added to impregnated for 24 hours in the ethyl alcohol of 15 mass parts after, to after immersion filter residue carry out
Diacolation, diacolation rate are 85ml/min/Kg, and the dosage of the ethyl alcohol is 12 times of filter residue amount, percolate are collected, by percolate
Heating concentration decrement is carried out, and recycles ethyl alcohol simultaneously, obtained concentrate is dried in vacuo to obtain Chinese medicinal component；Described changes
Property component be 3 mass parts of nano-titanium dioxide, 5.5 mass parts of nano zine oxide, 0.8 mass parts of nano-manganese dioxide, deionization
45 mass parts of water, above-mentioned nano-oxide is dissolved in deionized water, 40 DEG C of ultrasonic water bath 3h, obtains modified component；By Chinese medicine
Component is dissolved in the deionized water of 25 mass parts with modified component, and Chinese medical extract is obtained after ultrasonic disperse.
Preferably, the nano-titanium dioxide is modified nano-titanium dioxide；The modified nano-titanium dioxide
Method of modifying is：Nano-titanium dioxide is added in the aqueous solution for the citric acid that pH is 4 ~ 5, high-speed stirred obtains mixed liquor；
Mixed liquor is subjected to constant temperature reflow treatment, reaction temperature is 90 DEG C, handles 3h, filters, be washed with deionized to washing water extremely
Neutrality, it is cooling after being placed in oven and dried, then be impregnated into the n-hexane solvent of methyl-silicone oil, it is evaporated, removes after mixing evenly
Pre- modified body is obtained after being placed in oven and dried after solvent, and pre- modified body is subjected to 500 DEG C of roastings, obtains modified nano-silica
Titanium；30 ~ 40 mass parts of nano-titanium dioxide, 10 ~ 20 mass parts of methyl-silicone oil.
Nano-titanium dioxide has the fungistatic effect that can further improve Chinese medical extract by modified, and then promotes
The fungistatic effect of hygenic towelette.
Preferably, the nano-titanium dioxide is modified nano-titanium dioxide；The modified nano-titanium dioxide
Method of modifying is：Nano-titanium dioxide is added in the aqueous solution for the citric acid that pH is 4.5, high-speed stirred obtains mixed liquor；
Mixed liquor is subjected to constant temperature reflow treatment, reaction temperature is 90 DEG C, handles 3h, filters, be washed with deionized to washing water extremely
Neutrality, it is cooling after being placed in oven and dried, then be impregnated into the n-hexane solvent of methyl-silicone oil, it is evaporated, removes after mixing evenly
Pre- modified body is obtained after being placed in oven and dried after solvent, and pre- modified body is subjected to 500 DEG C of roastings, obtains modified nano-silica
Titanium；35 mass parts of nano-titanium dioxide, 15 mass parts of methyl-silicone oil.
A kind of hygenic towelette manufacturing method with bacteria resistance function, includes the following steps：（1）, by glycerol, hyaluronic acid, ten
Six alkyl polyoxyethylene ether sodium phosphates, Chinese medical extract, EDETATE SODIUM are dissolved in deionized water, and wet tissue lotion is made in high-speed stirred
It is spare；（2）, by lotion spray to hygenic towelette, the substrate on substrate, is obtained be the substrate through folding, the Foldable square
Formula is to carry out vertical folding after the substrate uncoiling after manufacturing paper with pulp is unfolded；（3）, the substrate after spray cut, cross break, obtain that there is suppression
The hygenic towelette of bacterium function.
Lotion is loaded on substrate by way of spray, it is possible to reduce the dosage of lotion, while unemployed cream
Liquid can utilize again after collecting, save the cost；Substrate spray by folding is high-efficient, effectively improves production efficiency.
During Emulsion Spraying to substrate, chemical property and composition change smaller, the master of the Chinese medical extract in lotion
It wants ingredient to obtain sufficient reservation during spray, the whitening effect of lotion is enabled more completely to be transferred to paper handkerchief
On.
Compared with prior art, the device have the advantages that being：The hygenic towelette for adding Chinese medical extract can be effective
Inhibit the growth of bacterium, while small to the irritation of skin；Lotion is loaded on substrate by way of spray, it is possible to reduce
The dosage of lotion, while unemployed lotion can utilize again after collecting, save the cost；Substrate spray by folding
It is high-efficient, improve production efficiency；Chinese medicinal component can further improve the fungistatic effect of hygenic towelette with modified component compounding.
Specific embodiment
Following implementation column is to further explanation of the invention, is not limitation of the present invention.
Embodiment 1
A kind of hygenic towelette and its manufacturing method with bacteria resistance function, the wet tissue lotion includes 1.5 mass parts of glycerol, transparent
Matter 4 mass parts of acid, 3 mass parts of cetyl polyoxyethylene ether sodium phosphate, 5 mass parts of Chinese medical extract, 0.3 mass of EDETATE SODIUM
Part, 65 mass parts of deionized water.The Chinese medical extract includes 55 mass parts of Chinese medicinal component and modified 4 mass parts of component.Institute
The Chinese medicinal component stated includes 1.5 mass parts of Fructus Corni, 2.5 mass parts of Medulla Tetrapanacis extract, 3 mass parts of Herba Visci extract, the rose of Sharon
11 mass parts of bark extract, 2 mass parts of Viscum album extract, 2 mass parts of Saururus chinensis extract；By the Fructus Corni, the stem pith of the rice-paper plant,
After mistletoe, Cortex hibisus syriacus, herba taxilli and saururus chinensis crush, the deionized water that 70 mass parts are added impregnates 2h, takes filter residue after filtering；
The filter residue is added to impregnated for 24 hours in the ethyl alcohol of 15 mass parts after, diacolation is carried out to the filter residue after immersion, diacolation rate is
85ml/min/Kg, the dosage of the ethyl alcohol are 12 times of filter residue amount, collect percolate, and percolate is carried out heating concentration and is subtracted
Amount, and ethyl alcohol is recycled simultaneously, obtained concentrate is dried in vacuo to obtain Chinese medicinal component；The modification component is nanometer two
3 mass parts of titanium oxide, 5.5 mass parts of nano zine oxide, 0.8 mass parts of nano-manganese dioxide, 45 mass parts of deionized water will be upper
It states nano-oxide to be dissolved in deionized water, 40 DEG C of ultrasonic water bath 3h, obtains modified component；Chinese medicinal component is molten with modified component
In the deionized water of 25 mass parts, Chinese medical extract is obtained after ultrasonic disperse.The nano-titanium dioxide is modified Nano
Titanium dioxide；The method of modifying of the modified nano-titanium dioxide is：Nano-titanium dioxide is added to the lemon that pH is 4.5
In the aqueous solution of acid, high-speed stirred obtains mixed liquor；Mixed liquor is subjected to constant temperature reflow treatment, reaction temperature is 90 DEG C, processing
3h is filtered, and the cooling after being placed in oven and dried to washing water to neutrality is washed with deionized, then be impregnated into methyl-silicone oil
It in n-hexane solvent, is evaporated after mixing evenly, pre- modified body is obtained after being placed in oven and dried after removal solvent, by pre- modified body
500 DEG C of roastings are carried out, modified nano-titanium dioxide is obtained；35 mass parts of nano-titanium dioxide, the methyl-silicone oil
15 mass parts.
Include Chinese medical extract and a small amount of hyaluronic acid in wet tissue lotion, has both antibacterial and skin effect, it can be effective
Consistent wet tissue to the irritation of skin, while the bactericidal effect of Chinese medical extract is better than traditional medicament, while to skin
Irritation is small.
The hygenic towelette of addition Chinese medical extract can effectively inhibit the growth of bacterium, while irritation is small.Modified component can
Significantly to improve the fungistatic effect of Chinese medicinal component.
Chinese medicinal component can further improve the fungistatic effect of hygenic towelette, while to skin with modified component compounding
Irritation is small；Fructus Corni, the stem pith of the rice-paper plant, mistletoe, Cortex hibisus syriacus, herba taxilli and saururus chinensis in wet tissue lotion after seepage pressure effects
There is significant fungistatic effect, this may be since Cortex hibisus syriacus has certain fungistatic effect, and same Fructus Corni, the stem pith of the rice-paper plant, Mongolian oak are posted
The fungistatic effect of extract has more significant raising after raw, herba taxilli and saururus chinensis compounding；Modified component itself has centainly
Fungistatic effect, but its main function is that same Chinese medicinal component generates synergy, further increases the fungistatic effect of Chinese medicinal component, together
When nano-scale particle can effectively disperse, and then significantly improve the fungistatic effect of Chinese medical extract.
Nano-titanium dioxide has the fungistatic effect that can further improve Chinese medical extract by modified, and then promotes
The fungistatic effect of hygenic towelette.
A kind of hygenic towelette manufacturing method with bacteria resistance function, includes the following steps：（1）, by glycerol, hyaluronic acid, ten
Six alkyl polyoxyethylene ether sodium phosphates, Chinese medical extract, EDETATE SODIUM are dissolved in deionized water, and wet tissue lotion is made in high-speed stirred
It is spare；（2）, by lotion spray to hygenic towelette, the substrate on substrate, is obtained be the substrate through folding, the Foldable square
Formula is to carry out vertical folding after the substrate uncoiling after manufacturing paper with pulp is unfolded；（3）, the substrate after spray cut, cross break, obtain that there is suppression
The hygenic towelette of bacterium function.
Lotion is loaded on substrate by way of spray, it is possible to reduce the dosage of lotion, while unemployed cream
Liquid can utilize again after collecting, save the cost；Substrate spray by folding is high-efficient, improves production efficiency.
During Emulsion Spraying to substrate, chemical property and composition change smaller, the master of the Chinese medical extract in lotion
It wants ingredient to obtain sufficient reservation during spray, the whitening effect of lotion is enabled more completely to be transferred to paper handkerchief
On.
Embodiment 2
Embodiment 2 with embodiment 1 the difference is that, including substrate and wet tissue lotion, load has wet tissue newborn on the substrate
Liquid；The wet tissue lotion includes 1 mass parts of glycerol, 3 mass parts of hyaluronic acid, 2 matter of cetyl polyoxyethylene ether sodium phosphate
Measure part, 4 mass parts of Chinese medical extract, 0.2 mass parts of EDETATE SODIUM, 60 mass parts of deionized water.The Chinese medical extract packet
Include 50 mass parts of Chinese medicinal component and modified 3 mass parts of component.
Embodiment 3
Embodiment 3 with embodiment 1 the difference is that, including substrate and wet tissue lotion, load has wet tissue newborn on the substrate
Liquid；The wet tissue lotion includes 2 mass parts of glycerol, 6 mass parts of hyaluronic acid, 4 matter of cetyl polyoxyethylene ether sodium phosphate
Measure part, 6 mass parts of Chinese medical extract, 0.5 mass parts of EDETATE SODIUM, 70 mass parts of deionized water.The Chinese medical extract packet
Include 60 mass parts of Chinese medicinal component and modified 6 mass parts of component.
Embodiment 4
Embodiment 4 with embodiment 1 the difference is that, the Chinese medicinal component includes 1 mass parts of Fructus Corni, Medulla Tetrapanacis extract 2
Mass parts, 2 mass parts of Herba Visci extract, 10 mass parts of rose of Sharon bark extract, 1 mass parts of Viscum album extract, saururus chinensis mention
Take 1 mass parts of object；After the Fructus Corni, the stem pith of the rice-paper plant, mistletoe, Cortex hibisus syriacus, herba taxilli and saururus chinensis are crushed, 60 mass are added
The deionized water of part impregnates 2h, takes filter residue after filtering；The filter residue is added to impregnated for 24 hours in the ethyl alcohol of 10 mass parts after, it is right
Filter residue after immersion carries out diacolation, and diacolation rate is 80ml/min/Kg, and the dosage of the ethyl alcohol is 10 times of filter residue amount, receives
Collect percolate, percolate is subjected to heating concentration decrement, and recycle ethyl alcohol simultaneously, obtained concentrate be dried in vacuo
It arrives, Chinese medicinal component；The modification component is 2 mass parts of nano-titanium dioxide, 5 mass parts of nano zine oxide, nanometer titanium dioxide
0.5 ~ 1 mass parts of manganese, 40 ~ 50 mass parts of deionized water, above-mentioned nano-oxide is dissolved in deionized water, 40 DEG C of ultrasonic water baths
3h obtains modified component；Chinese medicinal component is dissolved in the deionized water of 20 mass parts with modified component, is obtained after ultrasonic disperse
Medicament extract.
Embodiment 5
Embodiment 5 with embodiment 1 the difference is that, the Chinese medicinal component includes 2 mass parts of Fructus Corni, Medulla Tetrapanacis extract 3
Mass parts, 5 mass parts of Herba Visci extract, 12 mass parts of rose of Sharon bark extract, 3 mass parts of Viscum album extract, saururus chinensis mention
Take 4 mass parts of object；After the Fructus Corni, the stem pith of the rice-paper plant, mistletoe, Cortex hibisus syriacus, herba taxilli and saururus chinensis are crushed, 80 mass are added
The deionized water of part impregnates 2h, takes filter residue after filtering；The filter residue is added to impregnated for 24 hours in the ethyl alcohol of 20 mass parts after, it is right
Filter residue after immersion carries out diacolation, and diacolation rate is 90ml/min/Kg, and the dosage of the ethyl alcohol is 16 times of filter residue amount, receives
Collect percolate, percolate is subjected to heating concentration decrement, and recycle ethyl alcohol simultaneously, obtained concentrate be dried in vacuo
It arrives, Chinese medicinal component；The modification component is 5 mass parts of nano-titanium dioxide, 6 mass parts of nano zine oxide, nanometer titanium dioxide
1 mass parts of manganese, 50 mass parts of deionized water, above-mentioned nano-oxide is dissolved in deionized water, and 40 DEG C of ultrasonic water bath 3h are obtained
Modified component；Chinese medicinal component is dissolved in the deionized water of 30 mass parts with modified component, traditional Chinese medicine extraction is obtained after ultrasonic disperse
Object.
Embodiment 6
Embodiment 6 with embodiment 1 the difference is that, the nano-titanium dioxide be modified nano-titanium dioxide；Described
The method of modifying of modified nano-titanium dioxide is：Nano-titanium dioxide is added in the aqueous solution for the citric acid that pH is 4, high speed
Stirring, obtains mixed liquor；Mixed liquor is subjected to constant temperature reflow treatment, reaction temperature is 90 DEG C, handles 3h, filters, use deionization
Water washing is to washing water to neutrality, cooling after being placed in oven and dried, then is impregnated into the n-hexane solvent of methyl-silicone oil, stirs
It is evaporated after uniformly, obtains pre- modified body after being placed in oven and dried after removal solvent, pre- modified body is subjected to 500 DEG C of roastings, is obtained
To modified nano-titanium dioxide；30 mass parts of nano-titanium dioxide, 10 mass parts of methyl-silicone oil.
Embodiment 7
Embodiment 7 with embodiment 1 the difference is that, the nano-titanium dioxide be modified nano-titanium dioxide；Described
The method of modifying of modified nano-titanium dioxide is：Nano-titanium dioxide is added in the aqueous solution for the citric acid that pH is 5, high speed
Stirring, obtains mixed liquor；Mixed liquor is subjected to constant temperature reflow treatment, reaction temperature is 90 DEG C, handles 3h, filters, use deionization
Water washing is to washing water to neutrality, cooling after being placed in oven and dried, then is impregnated into the n-hexane solvent of methyl-silicone oil, stirs
It is evaporated after uniformly, obtains pre- modified body after being placed in oven and dried after removal solvent, pre- modified body is subjected to 500 DEG C of roastings, is obtained
To modified nano-titanium dioxide；40 mass parts of nano-titanium dioxide, 20 mass parts of methyl-silicone oil.
Comparative example 1
Comparative example 1 with embodiment 1 the difference is that, the Chinese medical extract in the wet tissue lotion replaces with ethyl alcohol.
Comparative example 2
Comparative example 2 with embodiment 1 the difference is that, the nano-titanium dioxide is unmodified.
Comparative example 3
Comparative example 3 with same embodiment 1 the difference is that, without modified component in the Chinese medical extract.
Experimental example 1
Hygenic towelette made from embodiment 1 ~ 7 and comparative example 1 ~ 3 is built up into 2cm × 3cm size and carries out sterilizing rate detection test, experiment
Method is carried out referring to GB15979-2002, and experimental result is shown in Table 1.
1 hygenic towelette fungistatic effect of table
| Candida albicans | Staphylococcus aureus | Escherichia coli | |
| Embodiment 1 | 99.99% | 99.99% | 100% |
| Embodiment 2 | 99.12% | 98.16% | 99.21% |
| Embodiment 3 | 99.99% | 99.99% | 100% |
| Embodiment 4 | 97.12% | 96.13% | 99.95% |
| Embodiment 5 | 98.96% | 99.32% | 100% |
| Embodiment 6 | 96.13% | 95.21% | 94.18% |
| Embodiment 7 | 99.85% | 99.83% | 100% |
| Comparative example 1 | 66.15% | 67.23% | 70.15% |
| Comparative example 2 | 82.13% | 81.33% | 85.62% |
| Comparative example 3 | 77.36% | 79.25% | 81.15% |
Containing Chinese medicinal component and modified component in hygenic towelette prepared by embodiment 1 ~ 7, to Candida albicans, golden yellow grape
Coccus and Escherichia coli all have good inhibitory effect, and fungistatic effect is significantly better than comparative example preparation between each embodiment
The fungistatic effect of paper handkerchief, therefore, Chinese medical extract can significantly improve the fungistatic effect of paper handkerchief.
Embodiment 1 is preferably embodiment, and the additive amount of various components is relatively mild, and fungistatic effect is the same as embodiment 3
Be not much different, but be better than embodiment 2, this may be since the dosage of substances various in embodiment 2 is less, fungistatic effect by
It influences；The fungistatic effect of embodiment 3 is little with 1 difference of embodiment, but the dosage of each substance is larger, higher cost, therefore,
Embodiment 1 is more preferably embodiment.
The fungistatic effect of embodiment 4 and 5 is poor compared with embodiment 1, and the fungistatic effect of embodiment 4 will be weaker than implementation 5, more
It is weaker than embodiment 1, shows that the dosage of each substance in Chinese medical extract is unsuitable too low, be also not easy very few.Embodiment 6 it is antibacterial
Effect is weaker than embodiment 4, has absolutely proved nano-titanium dioxide modified necessity, has to the raising of hygenic towelette fungistatic effect
There is obvious action.The fungistatic effect of comparative example 2 is significantly weaker than embodiment 1 ~ 7, illustrates that the modification of nano-titanium dioxide can
Effectively to improve the fungistatic effect of hygenic towelette.
The fungistatic effect of comparative example 3 is most weak, shows Chinese medicinal component with the necessity of modified component compounding, made of compounding
Chinese medical extract can effectively improve the fungistatic effect of hygenic towelette.
Experimental example 2
30 18 ~ 50 years old Healthy Peoples are randomly selected as volunteer, the hygenic towelette of embodiment 1 ~ 7 and comparative example 1 ~ 3 is provided,
Then record counts the usage experience of each volunteer, and table 2 is experimental result.
User's using effect of 2 hygenic towelette of table
| Stingless excitation | Good antimicrobial effect | |
| Embodiment 1 | 30 | 30 |
| Embodiment 2 | 30 | 30 |
| Embodiment 3 | 30 | 30 |
| Embodiment 4 | 30 | 28 |
| Embodiment 5 | 29 | 30 |
| Embodiment 6 | 30 | 30 |
| Embodiment 7 | 29 | 30 |
| Comparative example 1 | 1 | 16 |
| Comparative example 2 | 29 | 18 |
| Comparative example 3 | 28 | 20 |
For embodiment 1 ~ 7 compared with comparative example 1, irritation is small, shows that Chinese medical extract is significantly smaller than second to the irritation of skin
Alcohol is superior to comparative example 1 ~ 3 to the irritation of skin, the fungistatic effect of embodiment 1 ~ 7, show Chinese medicinal component, modified component and
Modified nano-titanium dioxide compounding in modified component is significant to the promotion of hygenic towelette fungistatic effect.
Above-listed detailed description is illustrating for possible embodiments of the present invention, and above embodiments are not to limit this
The scope of the patents of invention, all equivalence enforcements or change without departing from carried out by the present invention, is intended to be limited solely by the scope of the patents of this case.
Claims (10)
1. a kind of hygenic towelette with bacteria resistance function, which is characterized in that including substrate and wet tissue lotion, loaded on the substrate
There is wet tissue lotion；The wet tissue lotion includes 1 ~ 2 mass parts of glycerol, 3 ~ 6 mass parts of hyaluronic acid, cetyl polyoxyethylene
2 ~ 4 mass parts of ether phosphoric acid sodium, 4 ~ 6 mass parts of Chinese medical extract, 0.2 ~ 0.5 mass parts of EDETATE SODIUM, 60 ~ 70 mass of deionized water
Part.
2. a kind of hygenic towelette with bacteria resistance function according to claim 1, which is characterized in that the wet tissue lotion packet
Include 1.5 ~ 2 mass parts of glycerol, 4 ~ 6 mass parts of hyaluronic acid, 3 ~ 4 mass parts of cetyl polyoxyethylene ether sodium phosphate, Chinese medicine mentions
Take 5 ~ 6 mass parts of object, 0.3 ~ 0.5 mass parts of EDETATE SODIUM, 65 ~ 70 mass parts of deionized water.
3. a kind of hygenic towelette with bacteria resistance function according to claim 2, which is characterized in that the wet tissue lotion packet
Include 1.5 mass parts of glycerol, 4 mass parts of hyaluronic acid, 3 mass parts of cetyl polyoxyethylene ether sodium phosphate, 5 matter of Chinese medical extract
Measure part, 0.3 mass parts of EDETATE SODIUM, 65 mass parts of deionized water.
4. a kind of hygenic towelette with bacteria resistance function according to claim 1, which is characterized in that the Chinese medical extract
Including 50 ~ 60 mass parts of Chinese medicinal component and modified 2 ~ 6 mass parts of component.
5. a kind of hygenic towelette with bacteria resistance function according to claim 4, which is characterized in that the Chinese medicinal component packet
Include 1 ~ 2 mass parts of Fructus Corni, 2 ~ 3 mass parts of Medulla Tetrapanacis extract, 2 ~ 5 mass parts of Herba Visci extract, rose of Sharon bark extract 10 ~ 12
Mass parts, 1 ~ 3 mass parts of Viscum album extract, 1 ~ 4 mass parts of Saururus chinensis extract；
After the Fructus Corni, the stem pith of the rice-paper plant, mistletoe, Cortex hibisus syriacus, herba taxilli and saururus chinensis are crushed, 60 ~ 80 mass parts are added
Deionized water impregnates 2h, takes filter residue after filtering；The filter residue is added to impregnated for 24 hours in the ethyl alcohol of 10 ~ 20 mass parts after, to leaching
Filter residue after bubble carries out diacolation, and diacolation rate is 80 ~ 90ml/min/Kg, and the dosage of the ethyl alcohol is the 10 ~ 16 of filter residue amount
Times, percolate is collected, percolate is subjected to heating concentration decrement, and recycle ethyl alcohol simultaneously, it is dry that obtained concentrate carries out vacuum
It is dry to obtain, Chinese medicinal component；
The modification component is 2 ~ 5 mass parts of nano-titanium dioxide, 5 ~ 6 mass parts of nano zine oxide, nano-manganese dioxide 0.5
~ 1 mass parts, 40 ~ 50 mass parts of deionized water, above-mentioned nano-oxide is dissolved in deionized water, and 40 DEG C of ultrasonic water bath 3h are obtained
To modified component；
Chinese medicinal component is dissolved in the deionized water of 20 ~ 30 mass parts with modified component, Chinese medical extract is obtained after ultrasonic disperse.
6. a kind of hygenic towelette with bacteria resistance function according to claim 5, which is characterized in that the Chinese medicinal component packet
Include 1.5 ~ 2 mass parts of Fructus Corni, 2.5 ~ 3 mass parts of Medulla Tetrapanacis extract, 3 ~ 5 mass parts of Herba Visci extract, rose of Sharon bark extract
11 ~ 12 mass parts, 2 ~ 3 mass parts of Viscum album extract, 2 ~ 4 mass parts of Saururus chinensis extract；
After the Fructus Corni, the stem pith of the rice-paper plant, mistletoe, Cortex hibisus syriacus, herba taxilli and saururus chinensis are crushed, 70 ~ 80 mass parts are added
Deionized water impregnates 2h, takes filter residue after filtering；The filter residue is added to impregnated for 24 hours in the ethyl alcohol of 15 ~ 20 mass parts after, to leaching
Filter residue after bubble carries out diacolation, and diacolation rate is 85 ~ 90ml/min/Kg, and the dosage of the ethyl alcohol is the 12 ~ 16 of filter residue amount
Times, percolate is collected, percolate is subjected to heating concentration decrement, and recycle ethyl alcohol simultaneously, it is dry that obtained concentrate carries out vacuum
It is dry to obtain Chinese medicinal component；
The modification component is 3 ~ 5 mass parts of nano-titanium dioxide, 5.5 ~ 6 mass parts of nano zine oxide, nano-manganese dioxide
0.8 ~ 1 mass parts, 45 ~ 50 mass parts of deionized water, above-mentioned nano-oxide is dissolved in deionized water, 40 DEG C of ultrasonic water baths
3h obtains modified component；
Chinese medicinal component is dissolved in the deionized water of 25 ~ 30 mass parts with modified component, Chinese medical extract is obtained after ultrasonic disperse.
7. a kind of hygenic towelette with bacteria resistance function according to claim 1, which is characterized in that the Chinese medicinal component packet
Include 1.5 mass parts of Fructus Corni, 2.5 mass parts of Medulla Tetrapanacis extract, 3 mass parts of Herba Visci extract, 11 mass of rose of Sharon bark extract
Part, 2 mass parts of Viscum album extract, 2 mass parts of Saururus chinensis extract；By the Fructus Corni, the stem pith of the rice-paper plant, mistletoe, Cortex hibisus syriacus,
After herba taxilli and saururus chinensis crush, the deionized water that 70 mass parts are added impregnates 2h, takes filter residue after filtering；The filter residue is added
After impregnating for 24 hours into the ethyl alcohol of 15 mass parts, diacolation is carried out to the filter residue after immersion, diacolation rate is 85ml/min/Kg, described
The dosage of ethyl alcohol be 12 times of filter residue amount, collect percolate, percolate be subjected to heating concentration decrement, and recycle second simultaneously
Alcohol, obtained concentrate are dried in vacuo to obtain Chinese medicinal component；The modification component is 3 mass parts of nano-titanium dioxide,
5.5 mass parts of nano zine oxide, 0.8 mass parts of nano-manganese dioxide, 45 mass parts of deionized water are molten by above-mentioned nano-oxide
In deionized water, 40 DEG C of ultrasonic water bath 3h obtain modified component；Chinese medicinal component is dissolved in going for 25 mass parts with modified component
In ionized water, Chinese medical extract is obtained after ultrasonic disperse.
8. a kind of hygenic towelette with bacteria resistance function according to claim 5, which is characterized in that the nanometer titanium dioxide
Titanium is modified nano-titanium dioxide；The method of modifying of the modified nano-titanium dioxide is：Nano-titanium dioxide is added to
In the aqueous solution for the citric acid that pH is 4 ~ 5, high-speed stirred obtains mixed liquor；Mixed liquor is subjected to constant temperature reflow treatment, reaction temperature
Degree is 90 DEG C, handles 3h, is filtered, and the cooling after being placed in oven and dried at neutrality is washed with deionized to washing water, then impregnate
It into the n-hexane solvent of methyl-silicone oil, is evaporated after mixing evenly, obtains pre- modification after being placed in oven and dried after removal solvent
Pre- modified body is carried out 500 DEG C of roastings, obtains modified nano-titanium dioxide by body；30 ~ 40 mass of nano-titanium dioxide
Part, 10 ~ 20 mass parts of methyl-silicone oil.
9. a kind of hygenic towelette with bacteria resistance function according to claim 8, which is characterized in that the nanometer titanium dioxide
Titanium is modified nano-titanium dioxide；The method of modifying of the modified nano-titanium dioxide is：Nano-titanium dioxide is added to
In the aqueous solution for the citric acid that pH is 4.5, high-speed stirred obtains mixed liquor；Mixed liquor is subjected to constant temperature reflow treatment, reaction temperature
Degree is 90 DEG C, handles 3h, is filtered, and the cooling after being placed in oven and dried at neutrality is washed with deionized to washing water, then impregnate
It into the n-hexane solvent of methyl-silicone oil, is evaporated after mixing evenly, obtains pre- modification after being placed in oven and dried after removal solvent
Pre- modified body is carried out 500 DEG C of roastings, obtains modified nano-titanium dioxide by body；35 mass parts of nano-titanium dioxide, institute
15 mass parts of methyl-silicone oil stated.
10. a kind of hygenic towelette manufacturing method with bacteria resistance function, which is characterized in that include the following steps：
（1）, by glycerol, hyaluronic acid, cetyl polyoxyethylene ether sodium phosphate, Chinese medical extract, EDETATE SODIUM be dissolved in from
In sub- water, it is spare that wet tissue lotion is made in high-speed stirred；
（2）, by lotion spray to hygenic towelette, the substrate on substrate, is obtained be the substrate through folding, the folding mode
To carry out vertical folding after the substrate uncoiling expansion after manufacturing paper with pulp；
（3）, the substrate after spray cut, cross break, obtain the hygenic towelette with bacteria resistance function.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115873662A (en) * | 2022-12-27 | 2023-03-31 | 高梵(浙江)信息技术有限公司 | Velvet down jacket care washing liquid and preparation method thereof |
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| JPH0940516A (en) * | 1995-08-02 | 1997-02-10 | Asahi Chem Ind Co Ltd | Antibacterial wet tissue |
| CN106511205A (en) * | 2016-12-09 | 2017-03-22 | 苏州宝丽洁日化有限公司 | Antiallergic skin-caring lotion and wet tissue and preparation methods of antiallergic skin-caring lotion and wet tissue |
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2018
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0940516A (en) * | 1995-08-02 | 1997-02-10 | Asahi Chem Ind Co Ltd | Antibacterial wet tissue |
| CN106511205A (en) * | 2016-12-09 | 2017-03-22 | 苏州宝丽洁日化有限公司 | Antiallergic skin-caring lotion and wet tissue and preparation methods of antiallergic skin-caring lotion and wet tissue |
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| 刘军等: "《化学与人类文明》", 31 July 2008 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115873662A (en) * | 2022-12-27 | 2023-03-31 | 高梵(浙江)信息技术有限公司 | Velvet down jacket care washing liquid and preparation method thereof |
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Effective date of registration: 20210908 Address after: 113000 No. 188-10, JINZI street, Shenfu New District, Fushun City, Liaoning Province (all) Applicant after: Americana (Liaoning) Pharmaceutical Co.,Ltd. Address before: 523000 Wanjiang Guyong Industrial Zone, Dongguan City, Guangdong Province Applicant before: DONGGUAN BAITIANE PAPER Co.,Ltd. |
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