CN107854370A - A kind of antibacterial delicate fragrance type hand cleanser and preparation method thereof - Google Patents
A kind of antibacterial delicate fragrance type hand cleanser and preparation method thereof Download PDFInfo
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- CN107854370A CN107854370A CN201711418152.3A CN201711418152A CN107854370A CN 107854370 A CN107854370 A CN 107854370A CN 201711418152 A CN201711418152 A CN 201711418152A CN 107854370 A CN107854370 A CN 107854370A
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- antibacterial
- extract solution
- delicate fragrance
- hand cleanser
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention provides a kind of antibacterial delicate fragrance type hand cleanser and preparation method thereof, the antibacterial delicate fragrance type hand cleanser includes following material:Methyl sodiosul foaliphatate, ethoxylation modified grease, Coconut Fatty Acid Monoethanolamide, dodecanamide propyl dimethylamine caprolactone, dodecanamide propyl hydroxyl Huang base glycine betaine, polyoxyethylene polyoxypropylene pentaerythrite ether, glycerine, Herba Houttuyniae extract, dark plum extract solution, pomelo peel extract solution, essential oil, distilled water.Hand sanitizer formula provided by the invention is gentle, and viscosity is suitable, and each raw material, which cooperates, can effectively play antibacterial, moisturizing, the effect of cleaning, and not damage hand skin, and the soft and smooth impression of nature is brought to hand skin, safe and healthy.
Description
Technical field
The invention belongs to daily chemical product field, and in particular to a kind of antibacterial delicate fragrance type hand cleanser and preparation method thereof.
Background technology
The main function of hand cleanser is to play a part of cleaning skin care, and some specific compositions can play sterilization, sterilization
Effect, such as Escherichia coli etc. increasingly improve with the living standard of people, to the quality requirement of hand cleanser also increasingly
It is high.Hand cleanser on the market is although various, but many products more or less with the addition of some harmful materials:
Such as bleaching powder, mercury, cleaning agent, corrosive agent.The skin received not can so be caused damage.
The content of the invention
The deficiency for more than, the invention provides a kind of antibacterial delicate fragrance type hand cleanser and preparation method thereof, by addition
Medicine plant type bacteriostatic agent, and gentle formula is used, the hand cleanser of antibacterial delicate fragrance type is prepared, its effect of cleaning to hand
Fruit is obvious, will not stimulate hand skin, have moisturizing moisturizing and it is antibacterial the effect of, and be easy to degrade, for environment green ring
Protect.
The technical scheme that the present invention takes is:
A kind of antibacterial delicate fragrance type hand cleanser, include the raw material of following parts by weight:
Further, it is preferable to it is the raw material for including following parts by weight:
The methyl sodiosul foaliphatate is carbochain in C14/16Or C14Following methyl sodiosul foaliphatate, it is relatively more suitable
For being used as surfactant in liquid detergent.
The preparation method of the Herba Houttuyniae extract is:Herba houttuyniae powder is broken into powder, be put into 5~10 times 75~95%
Ethanol in refluxing extraction 3~6 hours, extract solution is then concentrated into 1/5th of original volume.
The preparation method of the dark plum extract solution is:Dark plum is ground into powder, is put into 5~10 times of 75~95% second
Refluxing extraction 3~6 hours in alcohol, then extract solution is concentrated into a quarter of original volume.
The preparation method of the pomelo peel extract solution is:Pomelo peel is soaked into 30~60min in 5~8 times of water, soaked repeatedly
Bubble three times, merges leaching liquor, and leaching liquor is concentrated into a quarter of original volume, you can obtains pomelo peel extract solution.
The essential oil includes Rosa Damascana, clove oil, Lavender, refined jasmine oil, chamomile essential oil, lemon extract
Oil, in one's early teens orange essential oil, one kind in essential oil.
Present invention also offers the preparation method of the antibacterial delicate fragrance type hand cleanser, the preparation method includes following step
Suddenly:
(1) distilled water of formula ratio is heated to 40~60 DEG C, then added successively into distilled water in the case of stirring
Enter methyl sodiosul foaliphatate, ethoxylation modified grease, Coconut Fatty Acid Monoethanolamide, the dodecanamide propyl diformazan of formula ratio
Amine caprolactone, dodecanamide propyl hydroxyl Huang base glycine betaine, are uniformly mixed;
(2) pomelo peel extract solution, the cordate houttuynia of the formula ratio of formula ratio are sequentially added into step (1) while stirring
Extract solution, dark plum extract solution, are stirring evenly and then adding into glycerine and are well mixed, and natural cooling;
(3) polyoxyethylene polyoxypropylene pentaerythrite ether and essential oil are added into step (2) while stirring, stirring is equal
It is even to can obtain antibacterial delicate fragrance type hand cleanser.
In the formula of hand cleanser provided by the invention, the effect of each composition is as follows:
In the ethanol extract of dark plum, rich in a variety of organic acids, such as oxalic acid, tartaric acid, citric acid, it can suppress more
The growth of kind of bacterium, and after being compounded with Herba Houttuyniae extract, the enhancing of its bacteriostasis is notable.
Contain a variety of aldehydes matters in the extract solution of cordate houttuynia, these aldehydes matters during antibacterial mutually make by collaboration
With making it that all there is stronger inhibitory action to various bacterias such as Escherichia coli, staphylococcus aureuses.
Pomelo peel extract solution, pomelo peel are to eat the pericarp discarded after shaddock, and it has the smell of delicate fragrance, can remove different
Taste, the present invention add the Aqueous extracts of pomelo peel into the formula of hand cleanser, are remarkably improved the cleaning effect of hand cleanser, and keep
The faint scent of hand cleanser.
Glycerine has the effect of preserving moisture and protecting skin, can effectively take good care of the skin of hand, and glycerine can also rise in formula in addition
To the effect of defoaming.
Defoamer of the polyoxyethylene polyoxypropylene pentaerythrite ether as food grade, it can effectively suppress several surface-actives
Foam is enriched caused by agent compounding, in the case where not reducing hand cleanser cleaning effect so that hand cleanser is readily cleaned, and is reduced and is used
Water, and it is safe and healthy.
Several gentle surfactant compounds, the cleaning clean effect of hand cleanser is considerably increased, and with excellent
Thickening property and moisturizing, bacteriostasis.
The addition of essential oil improves the delicate fragrance degree of hand cleanser while preserving moisture and protecting skin is carried out, and gives smell enjoyment.
Hand sanitizer formula provided by the invention is gentle, and viscosity is suitable, each raw material cooperate can effectively play it is antibacterial,
Moisturizing, the effect of cleaning, and hand skin is not damaged, the soft and smooth impression of nature is brought to hand skin, it is safe and healthy.
Embodiment
With reference to embodiment, the present invention is described in detail.
Embodiment 1
A kind of antibacterial delicate fragrance type hand cleanser, include the raw material of following parts by weight:
The preparation method of the Herba Houttuyniae extract is:Herba houttuyniae powder is broken into powder, is put into 6 times of 85% ethanol
Refluxing extraction 5 hours, is then concentrated into 1/5th of original volume by extract solution;
The preparation method of the dark plum extract solution is:Dark plum is ground into powder, is put into 7 times of 85% ethanol and flows back
Extraction 6 hours, then extract solution is concentrated into a quarter of original volume;
The preparation method of the pomelo peel extract solution is:Pomelo peel is soaked into 50min in 7 times of water, soaked repeatedly three times,
Merge leaching liquor, and leaching liquor is concentrated into a quarter of original volume, you can obtain pomelo peel extract solution.
The preparation method of the antibacterial delicate fragrance type hand cleanser is:
(1) distilled water of formula ratio is heated to 45 DEG C, then adds and match somebody with somebody into distilled water successively in the case of stirring
The methyl sodiosul foaliphatate just measured, ethoxylation modified grease, Coconut Fatty Acid Monoethanolamide, dodecanamide propyl dimethylamine oneself
Lactone, dodecanamide propyl hydroxyl Huang base glycine betaine, are uniformly mixed;
(2) pomelo peel extract solution, the cordate houttuynia of the formula ratio of formula ratio are sequentially added into step (1) while stirring
Extract solution, dark plum extract solution, are stirring evenly and then adding into glycerine and are well mixed, and natural cooling;
(3) polyoxyethylene polyoxypropylene pentaerythrite ether and essential oil are added into step (2) while stirring, stirring is equal
It is even to can obtain antibacterial delicate fragrance type hand cleanser.
Embodiment 2
A kind of antibacterial delicate fragrance type hand cleanser, include the raw material of following parts by weight:
The preparation method of the Herba Houttuyniae extract is:Herba houttuyniae powder is broken into powder, is put into 7 times of 80% ethanol
Refluxing extraction 6 hours, is then concentrated into 1/5th of original volume by extract solution;
The preparation method of the dark plum extract solution is:Dark plum is ground into powder, is put into 10 times of 75% ethanol and returns
Stream extraction 4 hours, then extract solution is concentrated into a quarter of original volume;
The preparation method of the pomelo peel extract solution is:Pomelo peel is soaked into 60min in 6 times of water, soaked repeatedly three times,
Merge leaching liquor, and leaching liquor is concentrated into a quarter of original volume, you can obtain pomelo peel extract solution.
The preparation method of the antibacterial delicate fragrance type hand cleanser is:
(1) distilled water of formula ratio is heated to 50 DEG C, then adds and match somebody with somebody into distilled water successively in the case of stirring
The methyl sodiosul foaliphatate just measured, ethoxylation modified grease, Coconut Fatty Acid Monoethanolamide, dodecanamide propyl dimethylamine oneself
Lactone, dodecanamide propyl hydroxyl Huang base glycine betaine, are uniformly mixed;
(2) pomelo peel extract solution, the cordate houttuynia of the formula ratio of formula ratio are sequentially added into step (1) while stirring
Extract solution, dark plum extract solution, are stirring evenly and then adding into glycerine and are well mixed, and natural cooling;
(3) polyoxyethylene polyoxypropylene pentaerythrite ether and essential oil are added into step (2) while stirring, stirring is equal
It is even to can obtain antibacterial delicate fragrance type hand cleanser.
Embodiment 3
A kind of antibacterial delicate fragrance type hand cleanser, include the raw material of following parts by weight:
The preparation method of the Herba Houttuyniae extract is:Herba houttuyniae powder is broken into powder, is put into 10 times of 75% ethanol
Middle refluxing extraction 4 hours, is then concentrated into 1/5th of original volume by extract solution;
The preparation method of the dark plum extract solution is:Dark plum is ground into powder, is put into 8 times of 80% ethanol and flows back
Extraction 5 hours, then extract solution is concentrated into a quarter of original volume;
The preparation method of the pomelo peel extract solution is:Pomelo peel is soaked into 40min in 7 times of water, soaked repeatedly three times,
Merge leaching liquor, and leaching liquor is concentrated into a quarter of original volume, you can obtain pomelo peel extract solution.
The preparation method of the antibacterial delicate fragrance type hand cleanser is:
(1) distilled water of formula ratio is heated to 55 DEG C, then adds and match somebody with somebody into distilled water successively in the case of stirring
The methyl sodiosul foaliphatate just measured, ethoxylation modified grease, Coconut Fatty Acid Monoethanolamide, dodecanamide propyl dimethylamine oneself
Lactone, dodecanamide propyl hydroxyl Huang base glycine betaine, are uniformly mixed;
(2) pomelo peel extract solution, the cordate houttuynia of the formula ratio of formula ratio are sequentially added into step (1) while stirring
Extract solution, dark plum extract solution, are stirring evenly and then adding into glycerine and are well mixed, and natural cooling;
(3) polyoxyethylene polyoxypropylene pentaerythrite ether and essential oil are added into step (2) while stirring, stirring is equal
It is even to can obtain antibacterial delicate fragrance type hand cleanser.
Embodiment 4
The bacteria inhibition assay of Chinese medical extract
The Herba Houttuyniae extract in embodiment and dark plum extract solution are concentrated and dried into dry powder respectively, then respectively with 75%
Ethanol be configured to concentration be 300mg/L drug solution;10 test tubes through high temperature high pressure process are taken, and in every test tube
1mL MH broth bouillons are added, while the drug solution 1mL that mass concentration is 300mg/mL is added in first test tube, and
Carry out doubling dilution to the 9th test tube from the 1st test tube, every test tube mass concentration is followed successively by 300,150,75,37.5,
18.8th, 9.4,4.7,2.4,1.2mg/mL, the 10th test tube is that control group adds isometric 1mL physiological saline.Again in every examination
100 μ L clump counts are added in pipe as 107~108The bacterium solution of CFU/mL Escherichia coli, 37 DEG C culture 24h after take out, with control group
Bacterial growth situation in test tube is observed for reference, by the least concentration to observe asepsis growth as the minimum antibacterial dense of this Chinese medicine
Spend (MIC).As a result show, the MIC of Herba Houttuyniae extract and dark plum extract solution is 18.8mg/mL, 18.8mg/mL.
The Combination of 2 kinds of Chinese medicine extracts is measured, is respectively with the MIC value setting drug concentration of every kind of medicine
2MIC, MIC, 1/2MIC, 1/4MIC, 1/8MIC concentration carry out every group of Combination susceptibility testing and are repeated 3 times respectively.Drug combination judges
Foundation:FICI≤0.5 is synergy;0.5 < FICI≤1 is summation action;1 < FICI≤2 are unrelated effect;FICI > 2
For antagonism.After both use in conjunction, MIC value when Herba Houttuyniae extract is individually antibacterial falls below 4.7 by 18.8;Dark plum carries
MIC value when taking liquid individually antibacterial falls below 4.7 by 18.8;Calculate and understand that FICI values are 0.5.It can be seen that Herba Houttuyniae extract and crow
Plum extract solution drug combination shows the bacteriostasis of collaboration to Escherichia coli.
Comparative example 1
Other simply wherein eliminate Herba Houttuyniae extract and wherein methyl sodiosul foaliphatate, dark plum carry with embodiment 1
The parts by weight for taking liquid are 14 parts.
Comparative example 2
Other simply wherein eliminate dark plum extract solution and dodecanamide propyl hydroxyl Huang base glycine betaine, fish raw meat with embodiment 1
The parts by weight of careless extract solution are 14 parts.
1-3 of the embodiment of the present invention is determined in defined method of testing and comparative example three compares by GB/15979-2002 appendix Cs
The fungistatic effect of anti-bacterial hand lotion prepared by example 1~2, test structure are as shown in table 1.
Table 1
Choose water-retaining property and the cleaning decontamination for the hand cleanser that 100 volunteers obtain to various embodiments of the present invention and comparative example
Ability is evaluated, and 10 points are best result, and evaluation result is as shown in table 2:
Table 2
The sterilizing rate for the hand cleanser that each embodiment provided by the invention is prepared is all higher than 98%, and fungistatic effect is notable,
It has stronger cleaning dirt-removing power and excellent preserving moisture and protecting skin performance.
The above-mentioned detailed description carried out with reference to embodiment to a kind of antibacterial delicate fragrance type hand cleanser and preparation method thereof, is explanation
Property rather than it is limited, can include several embodiments according to limited scope, therefore of the invention overall not departing from
Changing and modifications under design, should belong within protection scope of the present invention.
Claims (8)
1. a kind of antibacterial delicate fragrance type hand cleanser, it is characterised in that include the raw material of following parts by weight:
2~8 parts of methyl sodiosul foaliphatate;
4~9 parts of ethoxylation modified grease;
3~6 parts of Coconut Fatty Acid Monoethanolamide;
1~5 part of dodecanamide propyl dimethylamine caprolactone;
3~7 parts of dodecanamide propyl hydroxyl Huang base glycine betaine;
2~10 parts of polyoxyethylene polyoxypropylene pentaerythrite ether;
5~10 parts of glycerine;
5~10 parts of Herba Houttuyniae extract;
5~10 parts of dark plum extract solution;
2~10 parts of pomelo peel extract solution;
0.5~3 part of essential oil;
38~85 parts of distilled water.
2. antibacterial delicate fragrance type hand cleanser according to claim 1, it is characterised in that include the raw material of following parts by weight:
5 parts of methyl sodiosul foaliphatate;
6 parts of ethoxylation modified grease;
5 parts of Coconut Fatty Acid Monoethanolamide;
3 parts of dodecanamide propyl dimethylamine caprolactone;
6 parts of dodecanamide propyl hydroxyl Huang base glycine betaine;
5 parts of polyoxyethylene polyoxypropylene pentaerythrite ether;
8 parts of glycerine;
7 parts of Herba Houttuyniae extract;
7 parts of dark plum extract solution;
8 parts of pomelo peel extract solution;
2 parts of essential oil;
50 parts of distilled water.
3. antibacterial delicate fragrance type hand cleanser according to claim 1 or 2, it is characterised in that the methyl sodiosul foaliphatate
It is carbochain in C14/16Or C14Following methyl sodiosul foaliphatate.
4. antibacterial delicate fragrance type hand cleanser according to claim 1 or 2, it is characterised in that the system of the Herba Houttuyniae extract
Preparation Method is:Herba houttuyniae powder is broken into powder, is put into refluxing extraction 3~6 hours in 5~10 times of 75~95% ethanol, so
Extract solution is concentrated into 1/5th of original volume afterwards.
5. antibacterial delicate fragrance type hand cleanser according to claim 1 or 2, it is characterised in that the preparation of the dark plum extract solution
Method is:Dark plum is ground into powder, is put into refluxing extraction 3~6 hours in 5~10 times of 75~95% ethanol, then will
Extract solution is concentrated into a quarter of original volume.
6. antibacterial delicate fragrance type hand cleanser according to claim 1 or 2, it is characterised in that the system of the pomelo peel extract solution
Preparation Method is:Pomelo peel is soaked into 30~60min in 5~8 times of water, soaks repeatedly three times, merges leaching liquor, and by leaching liquor
It is concentrated into a quarter of original volume, you can obtain pomelo peel extract solution.
7. antibacterial delicate fragrance type hand cleanser according to claim 1 or 2, it is characterised in that the essential oil include Rosa Damascana,
Clove oil, Lavender, refined jasmine oil, chamomile essential oil, lemon, in one's early teens orange essential oil, one kind in essential oil.
8. the preparation method of antibacterial delicate fragrance type hand cleanser according to claim 1 or 2, it is characterised in that the preparation side
Method comprises the following steps:
(1) distilled water of formula ratio is heated to 40~60 DEG C, then adds and match somebody with somebody into distilled water successively in the case of stirring
The methyl sodiosul foaliphatate just measured, ethoxylation modified grease, Coconut Fatty Acid Monoethanolamide, dodecanamide propyl dimethylamine oneself
Lactone, dodecanamide propyl hydroxyl Huang base glycine betaine, are uniformly mixed;
(2) pomelo peel extract solution, the cordate houttuynia extraction of the formula ratio of formula ratio are sequentially added into step (1) while stirring
Liquid, dark plum extract solution, are stirring evenly and then adding into glycerine and are well mixed, and natural cooling;
(3) polyoxyethylene polyoxypropylene pentaerythrite ether and essential oil are added into step (2) while stirring, stirred i.e.
It can obtain antibacterial delicate fragrance type hand cleanser.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110123710A (en) * | 2019-05-15 | 2019-08-16 | 西华大学 | A kind of plum fruit bath salt and preparation method thereof, application |
CN113304072A (en) * | 2021-05-26 | 2021-08-27 | 建昌帮药业有限公司 | Floral water |
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CN103550124A (en) * | 2013-11-08 | 2014-02-05 | 张言军 | Shaddock peel skin-care hand sanitizer |
CN107468595A (en) * | 2017-09-29 | 2017-12-15 | 洛娃日化(江苏)股份有限公司 | A kind of plant bacteriostatic hand sanitizer and preparation method |
-
2017
- 2017-12-25 CN CN201711418152.3A patent/CN107854370A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103550124A (en) * | 2013-11-08 | 2014-02-05 | 张言军 | Shaddock peel skin-care hand sanitizer |
CN107468595A (en) * | 2017-09-29 | 2017-12-15 | 洛娃日化(江苏)股份有限公司 | A kind of plant bacteriostatic hand sanitizer and preparation method |
Non-Patent Citations (1)
Title |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110123710A (en) * | 2019-05-15 | 2019-08-16 | 西华大学 | A kind of plum fruit bath salt and preparation method thereof, application |
CN113304072A (en) * | 2021-05-26 | 2021-08-27 | 建昌帮药业有限公司 | Floral water |
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Application publication date: 20180330 |