CN108812714A - For preventing and treating the medicament and preparation method thereof of longan longicorn - Google Patents
For preventing and treating the medicament and preparation method thereof of longan longicorn Download PDFInfo
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- A—HUMAN NECESSITIES
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- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
- A01N57/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing acyclic or cycloaliphatic radicals
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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Abstract
The invention discloses a kind of for preventing and treating the medicament and preparation method thereof of longan longicorn, which includes following raw material:4-15 parts of fungi concentrate, 6-12 parts of amargosa, 5-8 parts of Chinese prickly ash, 1-3 parts of ginkgo leaf, 7-9 parts of indigo naturalis, 1-2 parts of diatomite, 0.5-1.6 parts of konjac glucomannan, 1-2 parts of chitosan, 6-10 parts of sepiolite, 3-5 parts of oil ben, 1-3 parts of perilla herb oil, 7-10 parts of diafenthiuron, 3-6 parts of tea polyphenols, 10-14 parts of isopropyl phosphoric acid ester, 10-12 parts of dimethylformamide, 3-7 parts of earthworm ester chitin, 3-5 parts of fatty alcohol polyoxyethylene ether, 2-6 parts of alkyl polyoxyethylene ether;By extract preparation, fungi concentrate preparation, raw material mixing and etc. be made.The present invention realizes preferable longicorn using fungi and kills effect, influences on fruit tree and environment less.Medicament of the invention does not have configuration simple process, feature easy to use.
Description
Technical field
The invention belongs to pest control technology fields, and in particular to a kind of medicament and its preparation for preventing and treating longan longicorn
Method.
Background technique
Longan is one of China's tropical fruit (tree) kind, with its pulp have anti-oxidant, antianxiety, anticancer, lipid-loweringing shield heart and
The effects of antibacterial.The study found that containing full sugar 12-23%, glucose 26.91%, tartaric acid 1.26%, egg in every 100g longan pulp
White matter 1.41%, fatty 0.45%, vitamin C 163.7mg, vitamin K1 96.6mg, there are also vitamin B1s, B2, P etc., by place
Reason is made dried fruit, every 100g 74.6g containing sugar, Fe35mg, Ca2mg, several mineral materials such as P110mg, K1200mg and a variety of
Amino acid, saponin, X- glycine, tannin, choline etc., this is the source of its powerful nourishing ability.Longan containing glucose abundant,
Sucrose and protein etc., iron-content is also relatively high, can promote hemoglobin regeneration while improving thermal energy, supplementing the nutrients, from
And achieve the effect that enrich blood.The study found that arillus longan is other than having benefiting action to whole body, and it is especially effective to brain cell, it can increase
Hypermnesia is recalled, and fatigue is eliminated.Arillus longan can also dry and longan is made in addition to fresh food, be processed into longan cream, longan fruit juice and with one
Determine the health liquor of effect, therefore, longan is as a kind of fresh food fruit and processes raw material and all has the stronger market demand.
Longicorn, also known as old carpenter worm, a kind of common pests main harm bearing tree as longan.It is carried out at present using pesticide
Killing has certain effect, but since long-time uses, disease is easy to generate resistance, causes drug effect to reduce, to increase
The dosage of pesticide extends and uses the time, causes pollution by pesticides, influences the quality of longan fruit, reduces economic value.
Summary of the invention
The present invention provide it is a kind of for preventing and treating the medicament and preparation method thereof of longan longicorn, to realize longan insect pest longicorn
Efficiently kill.
For preventing and treating the medicament of longan longicorn, the medicament includes following raw material:4-15 parts of fungi concentrate, hardship
6-12 parts of neem bark, 5-8 parts of Chinese prickly ash, 1-3 parts of ginkgo leaf, 7-9 parts of indigo naturalis, 1-2 parts of diatomite, 0.5-1.6 parts of konjac glucomannan, shell are poly-
1-2 parts sugared, 6-10 parts of sepiolite, 3-5 parts of oil ben, 1-3 parts of perilla herb oil, 7-10 parts of diafenthiuron, 3-6 parts of tea polyphenols, isopropyl
10-14 parts of phosphate, 10-12 parts of dimethylformamide, 3-7 parts of earthworm ester chitin, 3-5 parts of fatty alcohol polyoxyethylene ether, alkyl
2-6 parts of polyoxyethylene ether.
The medicament includes following raw material:8-12 parts of fungi concentrate, 8-10 parts of amargosa, 6-8 parts of Chinese prickly ash,
1.2-2.3 parts of ginkgo leaf, 8.1-8.8 parts of indigo naturalis, 1.2-1.6 parts of diatomite, 0.6-1.2 parts of konjac glucomannan, 1.4-2 parts of chitosan,
8-10 parts of sepiolite, 3.8-4.5 parts of oil ben, 1.2-1.8 parts of perilla herb oil, 8-9 parts of diafenthiuron, 4.6-5.7 parts of tea polyphenols, isopropyl
11-13 parts of base phosphate, 10.6-11.7 parts of dimethylformamide, 4-6 parts of earthworm ester chitin, fatty alcohol polyoxyethylene ether 3.4-
4.5 parts, 3-5.5 parts of alkyl polyoxyethylene ether.
The medicament includes following raw material:10 parts of fungi concentrate, 9.6 parts of amargosa, 7 parts of Chinese prickly ash, ginkgo
1.9 parts of leaf, 8.8 parts of indigo naturalis, 1.4 parts of diatomite, 0.8 part of konjac glucomannan, 1.6 parts of chitosan, 9.2 parts of sepiolite, oil ben 4.1
Part, 1.6 parts of perilla herb oil, 8.3 parts of diafenthiuron, 5.5 parts of tea polyphenols, 12 parts of isopropyl phosphoric acid ester, 11.4 parts of dimethylformamide, earthworm
5.7 parts of ester chitin, 3.9 parts of fatty alcohol polyoxyethylene ether, 5.1 parts of alkyl polyoxyethylene ether.
The fungi concentrate refers to the quasi- blueness of muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, Wan Shi
It is mould to be concentrated and dried again after expanding culture respectively, it remixes and is uniformly made.
The muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti weight ratio point
It Wei 1:0.5-0.8:0.3-0.5:0.2-0.7:0.6-0.9:0.6-1.3.
The muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti are after expanding culture
Viable count is 1.8 × 109CFU/g-1.2 × 1010CFU/g.
The present invention also provides a kind of for preventing and treating the medicament preparation method of longan longicorn, includes the following steps:
S1, amargosa, Chinese prickly ash, ginkgo leaf, indigo naturalis drying, crush, the ethanol solution that 6-8 times of margosa tare weight is added is surpassed
Sound wave extracts 0.5-1.2h, and filtering takes filtrate, is concentrated and dried to obtain extract A;
S2, muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti are respectively after expanding culture
Vacuum freeze drying is carried out, uniform fungi concentrate is then remixed;
S3, extract A, fungi concentrate and sepiolite, konjac glucomannan, chitosan, tea polyphenols mix, then again with oil ben, purple
Soviet Union oil, diatomite, diafenthiuron, isopropyl phosphoric acid ester, dimethylformamide, earthworm ester chitin, fatty alcohol polyoxyethylene ether, alkyl
The medicament is made in polyoxyethylene ether mixing.
The volumes of aqueous ethanol score is 60-85%.
The ultrasonic power is 300-500W.
The vacuum is 20-30Pa.
The medicament using when be diluted with water 300-500 times.
The beneficial effects of the present invention are:The present invention realizes preferable biological control effect using fungi, to fruit tree and
Environment influence is less, while the ingredients such as fatty alcohol polyoxyethylene ether, alkyl polyoxyethylene ether can preferably destroy the shell of longicorn,
So that medicament gradually penetrates into longicorn body celestial being, preferable longicorn killing effect is obtained.Medicament configuration simple process of the invention uses
Convenient feature.
【Specific embodiment】
To facilitate a better understanding of the present invention, it is illustrated by the following examples, these examples are belonged to the scope of protection of the present invention,
But it does not limit the scope of the invention.
Embodiment 1
For preventing and treating the medicament of longan longicorn, medicament includes following raw material:4 parts of fungi concentrate, 6 parts of amargosa,
5 parts of Chinese prickly ash, 1 part of ginkgo leaf, 7 parts of indigo naturalis, 1 part of diatomite, 0.5 part of konjac glucomannan, 1 part of chitosan, 6 parts of sepiolite, oil ben 3
Part, 1 part of perilla herb oil, 7-10 parts of diafenthiuron, 3 parts of tea polyphenols, 10 parts of isopropyl phosphoric acid ester, 10 parts of dimethylformamide, earthworm ester first
3-7 parts of shell element, 3 parts of fatty alcohol polyoxyethylene ether, 2 parts of alkyl polyoxyethylene ether.
Fungi concentrate refers to muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti point
It is not concentrated and dried again after expanding culture, remixes and be uniformly made.
Muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti weight ratio be respectively
1:0.5:0.3:0.2:0.6:0.6.
Muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, the paecilomyces varioti viable bacteria after expanding culture
Number is 1.8 × 109CFU/g。
For preventing and treating the medicament preparation method of longan longicorn, include the following steps:
S1, amargosa, Chinese prickly ash, ginkgo leaf, indigo naturalis drying, crush, the ethanol solution that 6-8 times of margosa tare weight is added is surpassed
Sound wave extracts 0.5h, and filtering takes filtrate, is concentrated and dried to obtain extract A;
S2, muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti are respectively after expanding culture
Vacuum freeze drying is carried out, uniform fungi concentrate is then remixed;
S3, extract A, fungi concentrate and sepiolite, konjac glucomannan, chitosan, tea polyphenols mix, then again with oil ben, purple
Soviet Union oil, diatomite, diafenthiuron, isopropyl phosphoric acid ester, dimethylformamide, earthworm ester chitin, fatty alcohol polyoxyethylene ether, alkyl
Polyoxyethylene ether, which mixes, is made medicament.
Volumes of aqueous ethanol score is 60%.
Ultrasonic power is 300W.
Vacuum is 20Pa.
Medicament using when be diluted with water 300 times.
Embodiment 2
For preventing and treating the medicament of longan longicorn, medicament includes following raw material:10 parts of fungi concentrate, amargosa 9.6
Part, 7 parts of Chinese prickly ash, 1.9 parts of ginkgo leaf, 8.8 parts of indigo naturalis, 1.4 parts of diatomite, 0.8 part of konjac glucomannan, 1.6 parts of chitosan, sepiolite
9.2 parts, 4.1 parts of oil ben, 1.6 parts of perilla herb oil, 8.3 parts of diafenthiuron, 5.5 parts of tea polyphenols, 12 parts of isopropyl phosphoric acid ester, dimethyl
11.4 parts of formamide, 5.7 parts of earthworm ester chitin, 3.9 parts of fatty alcohol polyoxyethylene ether, 5.1 parts of alkyl polyoxyethylene ether.
Fungi concentrate refers to muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti point
It is not concentrated and dried again after expanding culture, remixes and be uniformly made.
Muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti weight ratio be respectively
1:0.6:0.4:0.5:0.7:0.9.
Muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, the paecilomyces varioti viable bacteria after expanding culture
Number is 3.6 × 109CFU/g。
For preventing and treating the medicament preparation method of longan longicorn, include the following steps:
S1, amargosa, Chinese prickly ash, ginkgo leaf, indigo naturalis drying, crush, the ethanol solution that 6-8 times of margosa tare weight is added is surpassed
Sound wave extracts 0.8h, and filtering takes filtrate, is concentrated and dried to obtain extract A;
S2, muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti are respectively after expanding culture
Vacuum freeze drying is carried out, uniform fungi concentrate is then remixed;
S3, extract A, fungi concentrate and sepiolite, konjac glucomannan, chitosan, tea polyphenols mix, then again with oil ben, purple
Soviet Union oil, diatomite, diafenthiuron, isopropyl phosphoric acid ester, dimethylformamide, earthworm ester chitin, fatty alcohol polyoxyethylene ether, alkyl
Polyoxyethylene ether, which mixes, is made medicament.
Volumes of aqueous ethanol score is 75%.
Ultrasonic power is 400W.
Vacuum is 260Pa.
Medicament using when be diluted with water 350 times.
Embodiment 3
For preventing and treating the medicament of longan longicorn, medicament includes following raw material:15 parts of fungi concentrate, amargosa 12
Part, 8 parts of Chinese prickly ash, 3 parts of ginkgo leaf, 9 parts of indigo naturalis, 2 parts of diatomite, 1.6 parts of konjac glucomannan, 2 parts of chitosan, 10 parts of sepiolite, Moringa
Oily 5 parts, 3 parts of perilla herb oil, 10 parts of diafenthiuron, 6 parts of tea polyphenols, 14 parts of isopropyl phosphoric acid ester, 12 parts of dimethylformamide, earthworm ester first
Shell element 7 parts, 5 parts of fatty alcohol polyoxyethylene ether, 6 parts of alkyl polyoxyethylene ether.
Fungi concentrate refers to muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti point
It is not concentrated and dried again after expanding culture, remixes and be uniformly made.
Muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti weight ratio be respectively
1:0.8:0.5:0.7:0.9:1.3.
Muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, the paecilomyces varioti viable bacteria after expanding culture
Number is 1.2 × 1010CFU/g。
For preventing and treating the medicament preparation method of longan longicorn, include the following steps:
S1, amargosa, Chinese prickly ash, ginkgo leaf, indigo naturalis drying, crush, and 8 times of margosa tare weight of ethanol solution is added and carries out ultrasound
Wave extracts 1.2h, and filtering takes filtrate, is concentrated and dried to obtain extract A;
S2, muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti are respectively after expanding culture
Vacuum freeze drying is carried out, uniform fungi concentrate is then remixed;
S3, extract A, fungi concentrate and sepiolite, konjac glucomannan, chitosan, tea polyphenols mix, then again with oil ben, purple
Soviet Union oil, diatomite, diafenthiuron, isopropyl phosphoric acid ester, dimethylformamide, earthworm ester chitin, fatty alcohol polyoxyethylene ether, alkyl
Polyoxyethylene ether, which mixes, is made medicament.
Volumes of aqueous ethanol score is 85%.
Ultrasonic power is 500W.
Vacuum is 30Pa.
Medicament using when be diluted with water 500 times.
Comparative example 1
Same as Example 3 prepares raw material and technique, but fat-free alcohol polyoxyethylene ether, alkyl polyoxyethylene ether in raw material.
Comparative example 2
The killing of 350 times of progress longan longicorns is diluted with water using 40% flolimat emulsion.
5 groups are divided into 200 normal adult longan longicorns, every group 40, every group of longicorn is marked respectively,
Labeled as 1#, 2#, 3#, 4#, 5#, longicorn is placed on orchard different zones respectively(With having the transition of wide 5-10m between different zones
Band, it is 1#, 2#, 3#, 4#, 5# that region, which is also numbered,), then fruit tree is sprayed using the medicament of embodiment 1-3 and comparative example 1 respectively, 2
The killing situation of longicorn is observed after it, statistical result is as shown in the table.
Number | After sprinkling 2 day day after tomorrow kill situation/only | Killing rate/% |
1# | 38 | 95 |
2# | 36 | 90 |
3# | 39 | 97.5 |
4# | 28 | 70 |
5# | 26 | 0.65 |
By the data of 1-3# and 5# in table 1 it is found that the medicament that the present invention prepares tool has preferable longicorn killing effect,
This be primarily due to using fungi concentrate and other raw materials mutual cooperation play good killing effect.The number of 3# and 4#
According to it is found that fatty alcohol polyoxyethylene ether in the present invention, alkyl polyoxyethylene ether cooperation play preferable synergistic effect can be with
The shell of longicorn is dissolved, is invaded in longicorn body conducive to medicament to be killed.
The above content is combine it is specific/further detailed description of the invention for preferred embodiment, cannot
Assert that specific implementation of the invention is only limited to these instructions.General technical staff of the technical field of the invention is come
It says, without departing from the inventive concept of the premise, some replacements or modifications can also be made to the embodiment that these have been described,
And these substitutions or variant all shall be regarded as belonging to protection scope of the present invention.
Claims (10)
1. the medicament for preventing and treating longan longicorn, which is characterized in that the medicament includes following raw material:Fungi concentrate
4-15 parts, 6-12 parts of amargosa, 5-8 parts of Chinese prickly ash, 1-3 parts of ginkgo leaf, 7-9 parts of indigo naturalis, 1-2 parts of diatomite, konjac glucomannan 0.5-
1.6 parts, 1-2 parts of chitosan, 6-10 parts of sepiolite, 3-5 parts of oil ben, 1-3 parts of perilla herb oil, 7-10 parts of diafenthiuron, tea polyphenols 3-6
Part, 10-14 parts of isopropyl phosphoric acid ester, 10-12 parts of dimethylformamide, 3-7 parts of earthworm ester chitin, fatty alcohol polyoxyethylene ether 3-
5 parts, 2-6 parts of alkyl polyoxyethylene ether.
2. according to claim 1 for preventing and treating the medicament of longan longicorn, which is characterized in that the medicament includes following weight
Part raw material:8-12 parts of fungi concentrate, 8-10 parts of amargosa, 6-8 parts of Chinese prickly ash, 1.2-2.3 parts of ginkgo leaf, indigo naturalis 8.1-8.8
Part, 1.2-1.6 parts of diatomite, 0.6-1.2 parts of konjac glucomannan, 1.4-2 parts of chitosan, 8-10 parts of sepiolite, oil ben 3.8-4.5
Part, 1.2-1.8 parts of perilla herb oil, 8-9 parts of diafenthiuron, 4.6-5.7 parts of tea polyphenols, 11-13 parts of isopropyl phosphoric acid ester, dimethyl formyl
10.6-11.7 parts of amine, 4-6 parts of earthworm ester chitin, 3.4-4.5 parts of fatty alcohol polyoxyethylene ether, alkyl polyoxyethylene ether 3-5.5
Part.
3. according to claim 2 for preventing and treating the medicament of longan longicorn, which is characterized in that the medicament includes following weight
Part raw material:10 parts of fungi concentrate, 9.6 parts of amargosa, 7 parts of Chinese prickly ash, 1.9 parts of ginkgo leaf, 8.8 parts of indigo naturalis, diatomite 1.4
Part, 0.8 part of konjac glucomannan, 1.6 parts of chitosan, 9.2 parts of sepiolite, 4.1 parts of oil ben, 1.6 parts of perilla herb oil, 8.3 parts of diafenthiuron, tea
5.5 parts of polyphenol, 12 parts of isopropyl phosphoric acid ester, 11.4 parts of dimethylformamide, 5.7 parts of earthworm ester chitin, aliphatic alcohol polyethenoxy
3.9 parts of ether, 5.1 parts of alkyl polyoxyethylene ether.
4. according to claim 1 for preventing and treating the medicament of longan longicorn, which is characterized in that the fungi concentrate refers to white
Stiff bacterium, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti are concentrated after expanding culture dry again respectively
It is dry, it remixes and is uniformly made.
5. according to claim 4 for preventing and treating the medicament of longan longicorn, which is characterized in that the muscardine, green muscardine fungus, light
Purple Paecilomyces varioti, Verticillium lecanii, Trichoderma, paecilomyces varioti weight ratio be respectively 1:0.5-0.8:0.3-0.5:0.2-
0.7:0.6-0.9:0.6-1.3.
6. according to claim 4 for preventing and treating the medicament of longan longicorn, which is characterized in that the muscardine, green muscardine fungus, light
Purple Paecilomyces varioti, Verticillium lecanii, Trichoderma, the paecilomyces varioti viable count after expanding culture are 1.8 × 109CFU/g-1.2×
1010CFU/g。
7. according to claim 1 for preventing and treating the medicament preparation method of longan longicorn described in -6 any one, which is characterized in that described
Method includes the following steps:
S1, amargosa, Chinese prickly ash, ginkgo leaf, indigo naturalis drying, crush, the ethanol solution that 6-8 times of margosa tare weight is added is surpassed
Sound wave extracts 0.5-1.2h, and filtering takes filtrate, is concentrated and dried to obtain extract A;
S2, muscardine, green muscardine fungus, Paecilomyces lilacinus, Verticillium lecanii, Trichoderma, paecilomyces varioti are respectively after expanding culture
Vacuum freeze drying is carried out, uniform fungi concentrate is then remixed;
S3, extract A, fungi concentrate and sepiolite, konjac glucomannan, chitosan, tea polyphenols mix, then again with oil ben, purple
Soviet Union oil, diatomite, diafenthiuron, isopropyl phosphoric acid ester, dimethylformamide, earthworm ester chitin, fatty alcohol polyoxyethylene ether, alkyl
The medicament is made in polyoxyethylene ether mixing.
8. according to claim 7 for preventing and treating the medicament preparation method of longan longicorn, which is characterized in that the ethanol solution
Volume fraction is 60-85%.
9. according to claim 7 for preventing and treating the medicament preparation method of longan longicorn, which is characterized in that the ultrasonic wave function
Rate is 300-500W.
10. according to claim 7 for preventing and treating the medicament preparation method of longan longicorn, which is characterized in that the vacuum is
20-30Pa。
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