A kind of mascara and preparation method thereof
Technical field
The invention belongs to cosmetic technical fields, and in particular to one kind is heat-resisting cold-resistant and to skin non-irritant mascara cream
And preparation method thereof.
Background technology
Mascara is the cosmetics for being applied to eyelashes, it is therefore intended that keeps eyelashes dense, fibre is long, and volume is stuck up, and deepens eyelashes
Color.It generally comprises brush and includes smearing red ink paste used for seals and can store combined by the pipe two large divisions of brush, brush sheet
Body has flexure type also to have erect type, the quality of mascara that can be divided into emulsus lotion and powdery lotion.
When in use, in order to reach the using effect that dense volume is stuck up, often brush is with multiple for current mascara, residual cream or
Residual powder can be fallen on eye part skin often, and existing mascara has skin certain irritation, be caused using human body not
Suitable, mascara melts under the high temperature conditions, can also influence its using effect, under cryogenic easy embrittlement, for the volume of eyelashes
Qu Xiaoguo has a greatly reduced quality.
Patent 201710303595.1 discloses a kind of mascara, includes mainly following mass percent component:Fe2O3@C
Super-hydrophobic oleophylic nano particle:1-5%, native paraffin:1-4%, moisturizer:11-25%, emulsifier:1-5%, stabilizer:1-
5%.Although the mascara has good water resistance, non-refractory and low temperature.
Patent 200780039027.X discloses a kind of cosmetic composition of volume mascara.The mascara contains
Have:I) the acceptable acrylic thickening polymer of cosmetics, when the acrylic acid is added into water with the concentration of 0.5-3 weight %
When thickening polymer, the adhesion strength of the acrylic thickening polymer is 10-100g;Ii) cosmetics of 0.5-10 weight % can connect
The polyisobutene received.Although after the mascara makeup cosmetic compositions coat eyelashes, keep its dense, have to skin
Certain irritation, using effect are bad.
Invention content
The purpose of the present invention is to provide a kind of heat-resisting cold-resistant and to skin non-irritant mascara cream and preparation method thereof.
A kind of mascara is made of the raw material of following parts by weight:30-50 parts of sucrose stearate, 20-30 parts of wax, silicon
It is 10-20 parts oily, 3-8 parts of propylene glycol, 3-8 parts of hydroxyethyl methacrylate, 1-3 parts of linarin.
The wax is beeswax, Chinese wax, bayberry wax, candelila wax, Jojoba Oil, spermaceti, one kind in ceresine or it is a kind of with
On.
The mascara raw material further includes 2-4 parts of Flos Chrysanthemi Indici extract.
The extracting method of the Flos Chrysanthemi Indici extract is:Herb of Flos Chrysanthemi Indici is weighed, is dried, is crushed, 40-60 mesh sieve, dress are crossed
Enter percolator, be swollen 0.5-1.5 hours using the ethanol solution of 1-2 times of weight, then 6-12 times of ethanol solution is added to carry out diacolation,
Flow velocity 1-3mL/min, obtains percolate, is evaporated percolate, is made.
The mascara raw material further includes 0.5-2 parts of nano imvite.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, 30-50 parts of sucrose stearate, 20-30 parts of wax is taken to be heated to 60-80 DEG C, stirring is equal
It is even;
(2) it is cooled to 40-55 DEG C, 10-20 parts of silicone oil, 3-8 parts of propylene glycol is added, 3-8 parts of hydroxyethyl methacrylate stirs
It mixes uniformly;
(3) it is cooled to room temperature, 1-3 parts of linarin is added, stirs evenly, is made.
Preferably, it is additionally added 2-4 parts of Flos Chrysanthemi Indici extract in the step (3).
Preferably, it is additionally added 0.5-2 parts of nano imvite in the step (1).
Beneficial effects of the present invention:Mascara prepared by the present invention after use, can keep the dense warpage of eyelashes, eyelashes
Cream energy retention property under low temperature and hot conditions is stablized, not stiff under low temperature, does not melt under high temperature, product of the invention contains
There is linarin, the stimulation to skin can be reduced, preparation method of the invention is simple, and raw material sources are wide, is suitble to extensive work
Industry metaplasia is produced.
Specific implementation mode
With reference to specific embodiment, the present invention will be further described.
Embodiment 1
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g,
Propylene glycol 6g, hydroxyethyl methacrylate 6g, linarin 2g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g is taken to be heated to 70 DEG C, stir evenly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly;
(3) it is cooled to room temperature, linarin 2g is added, stirs evenly, is made.
Embodiment 2
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 30g, candelila wax 20g, silicone oil
10g, propylene glycol 3g, hydroxyethyl methacrylate 3g, linarin 1g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 30g, candelila wax 20g is taken to be heated to 60 DEG C, stir evenly;
(2) 40 DEG C are cooled to, silicone oil 10g is added, propylene glycol 3g, hydroxyethyl methacrylate 3g are stirred evenly;
(3) it is cooled to room temperature, linarin 1g is added, stirs evenly, is made.
Embodiment 3
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 50g, Jojoba Oil 30g, silicone oil
20g, propylene glycol 8g, hydroxyethyl methacrylate 8g, linarin 3g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 50g, Jojoba Oil 30g is taken to be heated to 80 DEG C, stir evenly;
(2) 55 DEG C are cooled to, silicone oil 20g is added, propylene glycol 8g, hydroxyethyl methacrylate 8g are stirred evenly;
(3) it is cooled to room temperature, linarin 3g is added, stirs evenly, is made.
Embodiment 4
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g,
Propylene glycol 6g, hydroxyethyl methacrylate 6g, linarin 2g, Flos Chrysanthemi Indici extract 3g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g is taken to be heated to 70 DEG C, stir evenly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly;
(3) it is cooled to room temperature, linarin 2g is added, Flos Chrysanthemi Indici extract 3g is stirred evenly, is made;
The extracting method of the Flos Chrysanthemi Indici extract is:Herb of Flos Chrysanthemi Indici is weighed, is dried, is crushed, 50 mesh sieve is crossed, loading is oozed
It filters cylinder, is swollen 1 hour using the ethanol solution of 1.5 times of weight, then 8 times of ethanol solution is added to carry out diacolation, flow velocity 2mL/min,
Percolate is obtained, percolate is evaporated, is made.
Embodiment 5
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g,
Propylene glycol 6g, hydroxyethyl methacrylate 6g, linarin 2g, nano imvite 1g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g, nano imvite 1g is taken to be heated to 70 DEG C, stir
It mixes uniformly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly;
(3) it is cooled to room temperature, linarin 2g is added, stirs evenly, is made.
Embodiment 6
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g,
Propylene glycol 6g, hydroxyethyl methacrylate 6g, linarin 2g, Australian beech sweetwood extract 2g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g is taken to be heated to 70 DEG C, stir evenly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly;
(3) it is cooled to room temperature, linarin 2g is added, Australian beech sweetwood extract 2g is stirred evenly, is made;
The extracting method of the Australian beech sweetwood extract is:Australian beech sweetwood blade is taken, is dried, is crushed, 50 mesh sieve is crossed, is packed into diacolation
Cylinder is swollen 1 hour using the ethanol solution of 1.5 times of weight, then 8 times of ethanol solution is added to carry out diacolation, and flow velocity 2mL/min is obtained
To percolate, it is evaporated percolate, is made.
Embodiment 7
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g,
Propylene glycol 6g, hydroxyethyl methacrylate 6g, linarin 2g, more fruit eucalyptus extract 2g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g is taken to be heated to 70 DEG C, stir evenly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly;
(3) it is cooled to room temperature, linarin 2g is added, more fruit eucalyptus extract 2g are stirred evenly, are made;
The extracting method of more fruit eucalyptus extracts is:More fruit folium eucalypti pieces are taken, are dried, are crushed, 50 mesh sieve is crossed, is packed into diacolation
Cylinder is swollen 1 hour using the ethanol solution of 1.5 times of weight, then 8 times of ethanol solution is added to carry out diacolation, and flow velocity 2mL/min is obtained
To percolate, it is evaporated percolate, is made.
Comparative example 1
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g,
Propylene glycol 6g, hydroxyethyl methacrylate 6g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g is taken to be heated to 70 DEG C, stir evenly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly, be made.
Experimental example 1
Mascara prepared by embodiment 1-7 and comparative example 1 applies on artificial eyelashes 15 times respectively, then measures every
Increased weight after secondary coating;It averages and is shown in the following table 1 to measuring result.
Table 1
Note:* P is represented<0.05;* represents P<0.01.
As can be seen from Table 1, compared with Example 1, the weightening of embodiment 4 and embodiment 5 is apparently higher than embodiment 1, card
Bright Flos Chrysanthemi Indici extract, nano imvite have the effect of increasing eyelashes thickness, dense, other embodiment and comparative example and implementation
Example 1 is suitable.
Experimental example 2
Embodiment 1-7 and comparative example 1 the mascara adhesion stability prepared are tested.Test method is as follows:First
The composition is applied on a glass with identical thickness using spreader, it is then fully dry;Then it is cut using crosscutting
Off line forms grid pattern on the glass plates;Then described group is removed from the glass plate with identical power using adhesive tape
Close the ingredient of object.In triplicate for each mascara, test result is summarized in the following table 2 for the test.
In table 2, " D " indicates that 50% or more of the gross area is removed by adhesive tape, and " C " indicates that the 30-50% of the gross area is shelled
From " B " indicates that the 10-30% of the gross area is stripped, and " A " indicates that the 10% or less of the gross area is stripped.
Table 2
As can be seen from Table 2, compared with Example 1, the stripping grade of embodiment 2-5, embodiment 7 are suitable with embodiment 1,
The stripping grade of embodiment 6 is better than embodiment 1, it was demonstrated that Australian beech sweetwood extract has effects that increase mascara viscosity, comparative example 1
Stripping grade be less than embodiment 1, it was demonstrated that linarin have effects that increase mascara viscosity.
Experimental example 3
Electro-heating standing-temperature cultivator is adjusted to 65 DEG C required of temperature in advance, takes 10mL to inject 20mL glass sample to be tested
It in glass test tube, is vertically put into constant incubator, takes out observation in 36h, 72h, 128h, do not occur precipitating or foam person is steady
It is fixed.Test result is shown in Table 3:
Table 3
As can be seen from Table 3, each embodiment and comparative example system is stablized in high temperature 36 hours, high temperature 72 hours, comparison
Example 1 start it is unstable, generate foam, high temperature 128 hours, embodiment 1-3, embodiment 7, start it is unstable, there is foam, implement
Example 5 precipitates, and comparative example 1 is extremely unstable, a large amount of foams occurs, and embodiment 4 and embodiment 6 still maintain stable.