CN108785116A - A kind of mascara and preparation method thereof - Google Patents

A kind of mascara and preparation method thereof Download PDF

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Publication number
CN108785116A
CN108785116A CN201810842683.3A CN201810842683A CN108785116A CN 108785116 A CN108785116 A CN 108785116A CN 201810842683 A CN201810842683 A CN 201810842683A CN 108785116 A CN108785116 A CN 108785116A
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China
Prior art keywords
parts
mascara
wax
added
preparation
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Application number
CN201810842683.3A
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Chinese (zh)
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CN108785116B (en
Inventor
刘伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anke cosmetics (Zhejiang) Co.,Ltd.
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Hangzhou Zhongqi New Mstar Technology Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/10Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41Particular ingredients further characterized by their size
    • A61K2800/413Nanosized, i.e. having sizes below 100 nm

Abstract

The invention discloses a kind of mascaras and preparation method thereof.It is made of the raw material of following parts by weight:30-50 parts of sucrose stearate, 20-30 parts of wax, 10-20 parts of silicone oil, 3-8 parts of propylene glycol, 3-8 parts of hydroxyethyl methacrylate, 1-3 parts of linarin.Mascara prepared by the present invention, after use, the dense warpage of eyelashes can be kept, mascara energy retention property under low temperature and hot conditions is stablized, not stiff under low temperature, do not melt under high temperature, the product of the present invention contains linarin, can reduce the stimulation to skin, preparation method of the invention is simple, raw material sources are wide, are suitble to large-scale industrial production.

Description

A kind of mascara and preparation method thereof
Technical field
The invention belongs to cosmetic technical fields, and in particular to one kind is heat-resisting cold-resistant and to skin non-irritant mascara cream And preparation method thereof.
Background technology
Mascara is the cosmetics for being applied to eyelashes, it is therefore intended that keeps eyelashes dense, fibre is long, and volume is stuck up, and deepens eyelashes Color.It generally comprises brush and includes smearing red ink paste used for seals and can store combined by the pipe two large divisions of brush, brush sheet Body has flexure type also to have erect type, the quality of mascara that can be divided into emulsus lotion and powdery lotion.
When in use, in order to reach the using effect that dense volume is stuck up, often brush is with multiple for current mascara, residual cream or Residual powder can be fallen on eye part skin often, and existing mascara has skin certain irritation, be caused using human body not Suitable, mascara melts under the high temperature conditions, can also influence its using effect, under cryogenic easy embrittlement, for the volume of eyelashes Qu Xiaoguo has a greatly reduced quality.
Patent 201710303595.1 discloses a kind of mascara, includes mainly following mass percent component:Fe2O3@C Super-hydrophobic oleophylic nano particle:1-5%, native paraffin:1-4%, moisturizer:11-25%, emulsifier:1-5%, stabilizer:1- 5%.Although the mascara has good water resistance, non-refractory and low temperature.
Patent 200780039027.X discloses a kind of cosmetic composition of volume mascara.The mascara contains Have:I) the acceptable acrylic thickening polymer of cosmetics, when the acrylic acid is added into water with the concentration of 0.5-3 weight % When thickening polymer, the adhesion strength of the acrylic thickening polymer is 10-100g;Ii) cosmetics of 0.5-10 weight % can connect The polyisobutene received.Although after the mascara makeup cosmetic compositions coat eyelashes, keep its dense, have to skin Certain irritation, using effect are bad.
Invention content
The purpose of the present invention is to provide a kind of heat-resisting cold-resistant and to skin non-irritant mascara cream and preparation method thereof.
A kind of mascara is made of the raw material of following parts by weight:30-50 parts of sucrose stearate, 20-30 parts of wax, silicon It is 10-20 parts oily, 3-8 parts of propylene glycol, 3-8 parts of hydroxyethyl methacrylate, 1-3 parts of linarin.
The wax is beeswax, Chinese wax, bayberry wax, candelila wax, Jojoba Oil, spermaceti, one kind in ceresine or it is a kind of with On.
The mascara raw material further includes 2-4 parts of Flos Chrysanthemi Indici extract.
The extracting method of the Flos Chrysanthemi Indici extract is:Herb of Flos Chrysanthemi Indici is weighed, is dried, is crushed, 40-60 mesh sieve, dress are crossed Enter percolator, be swollen 0.5-1.5 hours using the ethanol solution of 1-2 times of weight, then 6-12 times of ethanol solution is added to carry out diacolation, Flow velocity 1-3mL/min, obtains percolate, is evaporated percolate, is made.
The mascara raw material further includes 0.5-2 parts of nano imvite.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, 30-50 parts of sucrose stearate, 20-30 parts of wax is taken to be heated to 60-80 DEG C, stirring is equal It is even;
(2) it is cooled to 40-55 DEG C, 10-20 parts of silicone oil, 3-8 parts of propylene glycol is added, 3-8 parts of hydroxyethyl methacrylate stirs It mixes uniformly;
(3) it is cooled to room temperature, 1-3 parts of linarin is added, stirs evenly, is made.
Preferably, it is additionally added 2-4 parts of Flos Chrysanthemi Indici extract in the step (3).
Preferably, it is additionally added 0.5-2 parts of nano imvite in the step (1).
Beneficial effects of the present invention:Mascara prepared by the present invention after use, can keep the dense warpage of eyelashes, eyelashes Cream energy retention property under low temperature and hot conditions is stablized, not stiff under low temperature, does not melt under high temperature, product of the invention contains There is linarin, the stimulation to skin can be reduced, preparation method of the invention is simple, and raw material sources are wide, is suitble to extensive work Industry metaplasia is produced.
Specific implementation mode
With reference to specific embodiment, the present invention will be further described.
Embodiment 1
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g, Propylene glycol 6g, hydroxyethyl methacrylate 6g, linarin 2g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g is taken to be heated to 70 DEG C, stir evenly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly;
(3) it is cooled to room temperature, linarin 2g is added, stirs evenly, is made.
Embodiment 2
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 30g, candelila wax 20g, silicone oil 10g, propylene glycol 3g, hydroxyethyl methacrylate 3g, linarin 1g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 30g, candelila wax 20g is taken to be heated to 60 DEG C, stir evenly;
(2) 40 DEG C are cooled to, silicone oil 10g is added, propylene glycol 3g, hydroxyethyl methacrylate 3g are stirred evenly;
(3) it is cooled to room temperature, linarin 1g is added, stirs evenly, is made.
Embodiment 3
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 50g, Jojoba Oil 30g, silicone oil 20g, propylene glycol 8g, hydroxyethyl methacrylate 8g, linarin 3g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 50g, Jojoba Oil 30g is taken to be heated to 80 DEG C, stir evenly;
(2) 55 DEG C are cooled to, silicone oil 20g is added, propylene glycol 8g, hydroxyethyl methacrylate 8g are stirred evenly;
(3) it is cooled to room temperature, linarin 3g is added, stirs evenly, is made.
Embodiment 4
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g, Propylene glycol 6g, hydroxyethyl methacrylate 6g, linarin 2g, Flos Chrysanthemi Indici extract 3g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g is taken to be heated to 70 DEG C, stir evenly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly;
(3) it is cooled to room temperature, linarin 2g is added, Flos Chrysanthemi Indici extract 3g is stirred evenly, is made;
The extracting method of the Flos Chrysanthemi Indici extract is:Herb of Flos Chrysanthemi Indici is weighed, is dried, is crushed, 50 mesh sieve is crossed, loading is oozed It filters cylinder, is swollen 1 hour using the ethanol solution of 1.5 times of weight, then 8 times of ethanol solution is added to carry out diacolation, flow velocity 2mL/min, Percolate is obtained, percolate is evaporated, is made.
Embodiment 5
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g, Propylene glycol 6g, hydroxyethyl methacrylate 6g, linarin 2g, nano imvite 1g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g, nano imvite 1g is taken to be heated to 70 DEG C, stir It mixes uniformly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly;
(3) it is cooled to room temperature, linarin 2g is added, stirs evenly, is made.
Embodiment 6
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g, Propylene glycol 6g, hydroxyethyl methacrylate 6g, linarin 2g, Australian beech sweetwood extract 2g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g is taken to be heated to 70 DEG C, stir evenly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly;
(3) it is cooled to room temperature, linarin 2g is added, Australian beech sweetwood extract 2g is stirred evenly, is made;
The extracting method of the Australian beech sweetwood extract is:Australian beech sweetwood blade is taken, is dried, is crushed, 50 mesh sieve is crossed, is packed into diacolation Cylinder is swollen 1 hour using the ethanol solution of 1.5 times of weight, then 8 times of ethanol solution is added to carry out diacolation, and flow velocity 2mL/min is obtained To percolate, it is evaporated percolate, is made.
Embodiment 7
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g, Propylene glycol 6g, hydroxyethyl methacrylate 6g, linarin 2g, more fruit eucalyptus extract 2g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g is taken to be heated to 70 DEG C, stir evenly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly;
(3) it is cooled to room temperature, linarin 2g is added, more fruit eucalyptus extract 2g are stirred evenly, are made;
The extracting method of more fruit eucalyptus extracts is:More fruit folium eucalypti pieces are taken, are dried, are crushed, 50 mesh sieve is crossed, is packed into diacolation Cylinder is swollen 1 hour using the ethanol solution of 1.5 times of weight, then 8 times of ethanol solution is added to carry out diacolation, and flow velocity 2mL/min is obtained To percolate, it is evaporated percolate, is made.
Comparative example 1
A kind of mascara is made of the raw material of following parts by weight:Sucrose stearate 40g, beeswax 25g, silicone oil 15g, Propylene glycol 6g, hydroxyethyl methacrylate 6g.
The preparation method of above-mentioned mascara carries out in accordance with the following steps:
(1) according to parts by weight, sucrose stearate 40g, beeswax 25g is taken to be heated to 70 DEG C, stir evenly;
(2) 45 DEG C are cooled to, silicone oil 15g is added, propylene glycol 6g, hydroxyethyl methacrylate 6g are stirred evenly, be made.
Experimental example 1
Mascara prepared by embodiment 1-7 and comparative example 1 applies on artificial eyelashes 15 times respectively, then measures every Increased weight after secondary coating;It averages and is shown in the following table 1 to measuring result.
Table 1
Note:* P is represented<0.05;* represents P<0.01.
As can be seen from Table 1, compared with Example 1, the weightening of embodiment 4 and embodiment 5 is apparently higher than embodiment 1, card Bright Flos Chrysanthemi Indici extract, nano imvite have the effect of increasing eyelashes thickness, dense, other embodiment and comparative example and implementation Example 1 is suitable.
Experimental example 2
Embodiment 1-7 and comparative example 1 the mascara adhesion stability prepared are tested.Test method is as follows:First The composition is applied on a glass with identical thickness using spreader, it is then fully dry;Then it is cut using crosscutting Off line forms grid pattern on the glass plates;Then described group is removed from the glass plate with identical power using adhesive tape Close the ingredient of object.In triplicate for each mascara, test result is summarized in the following table 2 for the test.
In table 2, " D " indicates that 50% or more of the gross area is removed by adhesive tape, and " C " indicates that the 30-50% of the gross area is shelled From " B " indicates that the 10-30% of the gross area is stripped, and " A " indicates that the 10% or less of the gross area is stripped.
Table 2
As can be seen from Table 2, compared with Example 1, the stripping grade of embodiment 2-5, embodiment 7 are suitable with embodiment 1, The stripping grade of embodiment 6 is better than embodiment 1, it was demonstrated that Australian beech sweetwood extract has effects that increase mascara viscosity, comparative example 1 Stripping grade be less than embodiment 1, it was demonstrated that linarin have effects that increase mascara viscosity.
Experimental example 3
Electro-heating standing-temperature cultivator is adjusted to 65 DEG C required of temperature in advance, takes 10mL to inject 20mL glass sample to be tested It in glass test tube, is vertically put into constant incubator, takes out observation in 36h, 72h, 128h, do not occur precipitating or foam person is steady It is fixed.Test result is shown in Table 3:
Table 3
As can be seen from Table 3, each embodiment and comparative example system is stablized in high temperature 36 hours, high temperature 72 hours, comparison Example 1 start it is unstable, generate foam, high temperature 128 hours, embodiment 1-3, embodiment 7, start it is unstable, there is foam, implement Example 5 precipitates, and comparative example 1 is extremely unstable, a large amount of foams occurs, and embodiment 4 and embodiment 6 still maintain stable.

Claims (8)

1. a kind of mascara, which is characterized in that be made of the raw material of following parts by weight:30-50 parts of sucrose stearate, wax 20-30 parts, 10-20 parts of silicone oil, 3-8 parts of propylene glycol, 3-8 parts of hydroxyethyl methacrylate, 1-3 parts of linarin.
2. mascara according to claim 1, which is characterized in that the wax is beeswax, Chinese wax, bayberry wax, candelila wax, lotus Lotus fragrant plant is oily, spermaceti, the one or more in ceresine.
3. mascara according to claim 1, which is characterized in that the mascara raw material further includes Flos Chrysanthemi Indici extract 2-4 Part.
4. mascara according to claim 1, which is characterized in that the extracting method of the Flos Chrysanthemi Indici extract is:Weigh open country Chrysanthemum herb, is dried, and is crushed, and is crossed 40-60 mesh sieve, is packed into percolator, and 0.5-1.5 is swollen using the ethanol solution of 1-2 times of weight Hour, then 6-12 times of ethanol solution is added to carry out diacolation, flow velocity 1-3mL/min obtains percolate, is evaporated percolate, is made.
5. mascara according to claim 1, which is characterized in that the mascara raw material further includes nano imvite 0.5-2 Part.
6. the preparation method of mascara described in claim 1, which is characterized in that carry out in accordance with the following steps:
(1) according to parts by weight, 30-50 parts of sucrose stearate, 20-30 parts of wax is taken to be heated to 60-80 DEG C, stir evenly;
(2) it is cooled to 40-55 DEG C, 10-20 parts of silicone oil is added, 3-8 parts of propylene glycol, 3-8 parts of hydroxyethyl methacrylate, stirring is It is even;
(3) it is cooled to room temperature, 1-3 parts of linarin is added, stirs evenly, is made.
7. the preparation method of mascara according to claim 6, which is characterized in that be additionally added wild chrysanthemum in the step (3) 2-4 parts of extract.
8. the preparation method of mascara according to claim 6, which is characterized in that be additionally added nanometer illiteracy in the step (1) De- 0.5-2 parts of soil.
CN201810842683.3A 2018-07-27 2018-07-27 Mascara and preparation method thereof Active CN108785116B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110433088A (en) * 2019-08-24 2019-11-12 江西联锴新材料有限公司 A kind of alcohol packet oil mascara and preparation method thereof
CN111480926A (en) * 2019-01-29 2020-08-04 鞍山欣晟美容品有限公司 A adsorption structure and makeup ornaments for making up ornaments

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102274134A (en) * 2010-06-12 2011-12-14 浙江美雪化妆品有限公司 Eyelash mascara and preparation method thereof
CN104997656A (en) * 2014-03-19 2015-10-28 玫琳凯有限公司 Mascara formulation
CN106102710A (en) * 2014-04-17 2016-11-09 雅芳产品公司 The mascara of incremental contribution
CN106214610A (en) * 2016-08-25 2016-12-14 金华市卡姿秀化妆品有限公司 A kind of qualitative material of macromolecule modified mascara
CN106821907A (en) * 2017-02-14 2017-06-13 玉林祺钟商贸有限公司 A kind of efficient cosmetic hair care and preparation method
CN107405280A (en) * 2015-04-03 2017-11-28 Elc 管理有限责任公司 Hiar treatment compositions

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102274134A (en) * 2010-06-12 2011-12-14 浙江美雪化妆品有限公司 Eyelash mascara and preparation method thereof
CN104997656A (en) * 2014-03-19 2015-10-28 玫琳凯有限公司 Mascara formulation
CN106102710A (en) * 2014-04-17 2016-11-09 雅芳产品公司 The mascara of incremental contribution
CN107405280A (en) * 2015-04-03 2017-11-28 Elc 管理有限责任公司 Hiar treatment compositions
CN106214610A (en) * 2016-08-25 2016-12-14 金华市卡姿秀化妆品有限公司 A kind of qualitative material of macromolecule modified mascara
CN106821907A (en) * 2017-02-14 2017-06-13 玉林祺钟商贸有限公司 A kind of efficient cosmetic hair care and preparation method

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111480926A (en) * 2019-01-29 2020-08-04 鞍山欣晟美容品有限公司 A adsorption structure and makeup ornaments for making up ornaments
CN110433088A (en) * 2019-08-24 2019-11-12 江西联锴新材料有限公司 A kind of alcohol packet oil mascara and preparation method thereof
CN110433088B (en) * 2019-08-24 2023-10-27 江西联锴新材料有限公司 Oil-in-alcohol mascara and preparation method thereof

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