CN108743494A - A kind of antibacterial anti-acne facial cleanser and preparation method thereof - Google Patents
A kind of antibacterial anti-acne facial cleanser and preparation method thereof Download PDFInfo
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- CN108743494A CN108743494A CN201811024211.3A CN201811024211A CN108743494A CN 108743494 A CN108743494 A CN 108743494A CN 201811024211 A CN201811024211 A CN 201811024211A CN 108743494 A CN108743494 A CN 108743494A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/02—Local antiseptics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/04—Antibacterial agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention discloses a kind of antibacterial anti-acne facial cleansers, include the raw material of following parts by weight：2-8 parts of 8-15 parts of glycerine, 3-6 parts of glycol distearate, 0.1-1 parts of fructus cannabis, 0.1-0.5 parts of lepidium seed, 1-4 parts of monkshood and tea root.The invention also discloses a kind of preparation methods of antibacterial anti-acne facial cleanser.The present invention has better antibacterial and anti-acne effect by adding fructus cannabis and lepidium seed in milk material of washing one's face.
Description
Technical field
The present invention relates to a kind of cosmetic field, specifically a kind of antibacterial anti-acne facial cleanser and preparation method thereof.
Background technology
Facial cleanser is a kind of senior face washing agent.Facial dirt, makeup removing can be cleaned.Facial cleanser best in quality should have clear
Clean, nutrition, protection skin and other effects.In general, common facial cleanser is without whitening effect, in general, facial cleanser
It is the liquiform product being made of ingredients such as oil phase thing, aqueous-phase material, surfactant, moisturizer, nutritional agents.Wherein butyrous is washed one's face
Milk contains oil-phase component, is suitable for dry skin and uses；Crystal clear product is free of oil-phase component, and such as formula conditioning is appropriate,
Most consumers can be met to use.Surfactant has wetting, dispersion, foaming, decontamination, five your writings of emulsification in facial cleanser
With being the chief active object of face cleaning product.In addition, according to the similar principle that mixes, during washing one's face, oil phase thing dissolving face can be borrowed
Oil-soluble fat dirt and extra grease；By means of water-soluble sweat stain dirt on its aqueous-phase material dissolving face.
Traditional facial cleanser only has cleaning action, cannot inhibit face's bacterial reproduction well, not have to acne etc.
There is direct repair.
Invention content
The purpose of the present invention is to provide a kind of antibacterial anti-acne facial cleansers, to solve mentioned above in the background art ask
Topic.
To achieve the above object, the present invention provides the following technical solutions：
A kind of antibacterial anti-acne facial cleanser, includes the raw material of following parts by weight：8-15 parts of glycerine, glycol distearate
2-8 parts of 3-6 parts, 0.1-1 parts of fructus cannabis, 0.1-0.5 parts of lepidium seed, 1-4 parts of monkshood and tea root.
Further scheme as the present invention：Include the raw material of following mass fraction：10-12 parts of glycerine, ethylene glycol two are hard
3-7 parts of 4-5 parts of resin acid ester, 0.2-0.6 parts of fructus cannabis, 0.3-0.4 parts of lepidium seed, 2-3 parts of monkshood and tea root.
Further scheme as the present invention：Include the raw material of following mass fraction：11 parts of glycerine, ethylene glycol distearyl acid
5 parts of 4.5 parts of ester, 0.5 part of fructus cannabis, 0.35 part of lepidium seed, 2.5 parts of monkshood and tea root.
A kind of preparation method of antibacterial anti-acne facial cleanser, includes the following steps：(1) fructus cannabis ethanol solution ultrasound is soaked
It carries, ultrafiltration is carried out after the completion of extraction, filtrate obtains fructus cannabis extracting solution by being concentrated under reduced pressure into the 1/4 of former filtrate volume；(2)
Lepidium seed is dry, crush, be put into boiling in pot and filter, 8-10 times of water is added and continues infusion, is carried out between 50-65 degrees Celsius
Refluxing extraction obtains lepidium seed extracting solution；(3) monkshood and tea root are crushed, dry and is extracted using ethyl alcohol, distillation and concentration obtains
To component C；(4) glycerine, glycol distearate are added in the first secondary reacting kettle, are stirred and are mixed and heated 60-
80 degrees Celsius；(5) fructus cannabis extracting solution, lepidium seed extracting solution and component C are added in the second width reaction kettle, it is Celsius is heated to 65
Degree；(6) main reaction kettle is preheating to 50-60 degrees Celsius and is evacuated to -1mpa, by the first secondary reacting kettle and the second secondary reacting kettle
In raw material be evacuated in main reaction kettle, homogeneous blender was opened with 4000-4500r/ minutes rotating speeds, homogeneous stirs after sixty minutes
(7) lactic acid, potassium hydroxide, essence, secondary agitation 1 hour are sequentially added, constant temperature is cooled to 40 degrees Celsius after 30 minutes, detect pH
To discharge when 6-7.
Further scheme as the present invention：The condition of ultrasound extraction is in step (1)：The quality of ethanol solution is dense Celsius
Degree is 60%, ultrasound extraction 2 times, 2 hours every time, solid-liquid ratio 1:10.
Further scheme as the present invention：The condition of boiling extraction is in step (2)：Solid-liquid ratio 1:8, return time is
2 hours, 55 degrees Celsius of refluxing extraction temperature degree Celsius.
Further scheme as the present invention：Preheating temperature degree Celsius is 65 degrees Celsius in step (4), and heating temperature degree Celsius is
75 degrees Celsius；
Further scheme as the present invention：Preheating temperature is 55 degrees Celsius in step (6), and homogeneous stirring speed degree Celsius is
4200r/ minutes；
Further scheme as the present invention：PH value is 6.5 dischargings in step (7).
Compared with prior art, the beneficial effects of the invention are as follows：The present invention in milk material of washing one's face by adding fructus cannabis
And lepidium seed, there is better antibacterial and anti-acne effect.
Specific implementation mode
The technical solution of this patent is described in more detail With reference to embodiment.
Embodiment 1
A kind of antibacterial anti-acne facial cleanser, which is characterized in that include the raw material of following parts by weight：Glycerine 8g, ethylene glycol two
Stearate 3g, fructus cannabis 0.1g, lepidium seed 0.1g, monkshood 1g and tea root 2g.
A kind of preparation method of antibacterial anti-acne facial cleanser, which is characterized in that include the following steps：(1) by fructus cannabis second
Alcoholic solution ultrasound extracts, and ultrafiltration is carried out after the completion of extraction, and filtrate obtains fiery fiber crops by being concentrated under reduced pressure into the 1/4 of former filtrate volume
Benevolence extracting solution；(2) lepidium seed is dry, crush, be put into boiling in pot and filter, 8 times of water are added and continue infusions, 50 degrees Celsius it
Between carry out refluxing extraction, obtain lepidium seed extracting solution；(3) monkshood and tea root are crushed, dry and is extracted using ethyl alcohol, distilled
It is concentrated to give component C；(4) glycerine, glycol distearate are added in the first secondary reacting kettle, are stirred and are mixed and heated
To 60 degrees Celsius；(5) fructus cannabis extracting solution, lepidium seed extracting solution and component C are added in the second width reaction kettle, are heated to 65 and take the photograph
Family name's degree；(6) main reaction kettle is preheating to 50 degrees Celsius and is evacuated to -1mpa, by the first secondary reacting kettle and the second secondary reacting kettle
In raw material be evacuated in main reaction kettle, homogeneous blender was opened with 4000/ minute rotating speed, (7) successively after sixty minutes for homogeneous stirring
Lactic acid, potassium hydroxide, essence, secondary agitation 1 hour is added, constant temperature is cooled to 40 degrees Celsius after 30 minutes, when detection pH is 6 into
Row discharging.
Embodiment 2
A kind of antibacterial anti-acne facial cleanser, includes the raw material of following parts by weight：Glycerine 15g, glycol distearate 6g,
Fructus cannabis 1g, lepidium seed 0.5g, monkshood 4g and tea root 8g.
A kind of preparation method of antibacterial anti-acne facial cleanser, includes the following steps：(1) fructus cannabis ethanol solution ultrasound is soaked
It carries, ultrafiltration is carried out after the completion of extraction, filtrate obtains fructus cannabis extracting solution by being concentrated under reduced pressure into the 1/4 of former filtrate volume；(2)
Lepidium seed is dry, crush, be put into boiling in pot and filter, 10 times of water are added and continue infusions, flow back between 65 degrees Celsius
Extraction, obtains lepidium seed extracting solution；(3) monkshood and tea root are crushed, dry and is extracted using ethyl alcohol, distillation and concentration obtains group
Divide C；(4) will glycerine, glycol distearate be added the first secondary reacting kettle in, be stirred be mixed and heated it is Celsius to 80
Degree；(5) fructus cannabis extracting solution, lepidium seed extracting solution and component C are added in the second width reaction kettle, are heated to 65 degrees Celsius；(6)
Main reaction kettle is preheating to 60 degrees Celsius and is evacuated to -1mpa, by the raw material in the first secondary reacting kettle and the second secondary reacting kettle
It is evacuated in main reaction kettle, homogeneous blender was opened with 4500r/ minutes rotating speeds, (7) sequentially add breast after sixty minutes for homogeneous stirring
Acid, potassium hydroxide, essence, secondary agitation 1 hour, constant temperature are cooled to 40 degrees Celsius after 30 minutes, detection pH is gone out when being 7
Material.
Embodiment 3
A kind of antibacterial anti-acne facial cleanser, includes the raw material of following mass fraction：Glycerine 10g, glycol distearate 4g,
Fructus cannabis 0.2g, lepidium seed 0.3g, monkshood 2-g and tea root 3g.
A kind of preparation method of antibacterial anti-acne facial cleanser, includes the following steps：(1) fructus cannabis ethanol solution ultrasound is soaked
It carries, ultrafiltration is carried out after the completion of extraction, filtrate obtains fructus cannabis extracting solution by being concentrated under reduced pressure into the 1/4 of former filtrate volume；(2)
Lepidium seed is dry, crush, be put into boiling in pot and filter, 10 times of water are added and continue infusions, flow back between 65 degrees Celsius
Extraction, obtains lepidium seed extracting solution；(3) monkshood and tea root are crushed, dry and is extracted using ethyl alcohol, distillation and concentration obtains group
Divide C；(4) will glycerine, glycol distearate be added the first secondary reacting kettle in, be stirred be mixed and heated it is Celsius to 80
Degree；(5) fructus cannabis extracting solution, lepidium seed extracting solution and component C are added in the second width reaction kettle, are heated to 65 degrees Celsius；(6)
Main reaction kettle is preheating to 60 degrees Celsius and is evacuated to -1mpa, by the raw material in the first secondary reacting kettle and the second secondary reacting kettle
It is evacuated in main reaction kettle, homogeneous blender was opened with 4500r/ minutes rotating speeds, (7) sequentially add breast after sixty minutes for homogeneous stirring
Acid, potassium hydroxide, essence, secondary agitation 1 hour, constant temperature are cooled to 40 degrees Celsius after 30 minutes, detection pH is gone out when being 7
Material.
Embodiment 4
A kind of antibacterial anti-acne facial cleanser, includes the raw material of following mass fraction：Glycerine 12g, glycol distearate 5g,
Fructus cannabis 0.6g, lepidium seed 0.4g, monkshood 3g and tea root 7g.
A kind of preparation method of antibacterial anti-acne facial cleanser, which is characterized in that include the following steps：(1) by fructus cannabis second
Alcoholic solution ultrasound extracts, and ultrafiltration is carried out after the completion of extraction, and filtrate obtains fiery fiber crops by being concentrated under reduced pressure into the 1/4 of former filtrate volume
Benevolence extracting solution；(2) lepidium seed is dry, crush, be put into boiling in pot and filter, 8 times of water are added and continue infusions, 50 degrees Celsius it
Between carry out refluxing extraction, obtain lepidium seed extracting solution；(3) monkshood and tea root are crushed, dry and is extracted using ethyl alcohol, distilled
It is concentrated to give component C；(4) glycerine, glycol distearate are added in the first secondary reacting kettle, are stirred and are mixed and heated
To 60 degrees Celsius；(5) fructus cannabis extracting solution, lepidium seed extracting solution and component C are added in the second width reaction kettle, are heated to 65 and take the photograph
Family name's degree；(6) main reaction kettle is preheating to 50 degrees Celsius and is evacuated to -1mpa, by the first secondary reacting kettle and the second secondary reacting kettle
In raw material be evacuated in main reaction kettle, homogeneous blender was opened with 4000/ minute rotating speed, (7) successively after sixty minutes for homogeneous stirring
Lactic acid, potassium hydroxide, essence, secondary agitation 1 hour is added, constant temperature is cooled to 40 degrees Celsius after 30 minutes, when detection pH is 6 into
Row discharging.
Embodiment 5
A kind of antibacterial anti-acne facial cleanser, includes the raw material of following mass fraction：Glycerine 11g, glycol distearate
4.5g, fructus cannabis 0.5g, lepidium seed 0.35g, monkshood 2.5g and tea root 5g.
A kind of preparation method of antibacterial anti-acne facial cleanser, includes the following steps：(1) fructus cannabis ethanol solution ultrasound is soaked
It carries, ultrafiltration is carried out after the completion of extraction, filtrate obtains fructus cannabis extracting solution by being concentrated under reduced pressure into the 1/4 of former filtrate volume；(2)
Lepidium seed is dry, crush, be put into boiling in pot and filter, 8 times of water are added and continue infusions, reflux is carried out between 55 degrees Celsius and is carried
It takes, obtains lepidium seed extracting solution；(3) monkshood and tea root are crushed, dry and is extracted using ethyl alcohol, distillation and concentration obtains component
C；(4) glycerine, glycol distearate are added in the first secondary reacting kettle, are stirred and are mixed and heated to 75 degrees Celsius；
(5) fructus cannabis extracting solution, lepidium seed extracting solution and component C are added in the second width reaction kettle, are heated to 65 degrees Celsius；(6) will
Main reaction kettle is preheating to 55 degrees Celsius and is evacuated to -1mpa, and the raw material in the first secondary reacting kettle and the second secondary reacting kettle is taken out
Into main reaction kettle, homogeneous blender was opened with 4200r/ minutes rotating speeds, homogeneous stirring after sixty minutes (7) sequentially add lactic acid,
Potassium hydroxide, essence, secondary agitation 1 hour, constant temperature are cooled to 40 degrees Celsius after 30 minutes, detection pH discharges when being 6.5.
Comparative example 1
This comparative example, which is removed, is free of fructus cannabis, remaining raw material and technique are same as Example 5.
Comparative example 2
This comparative example, which is removed, is free of lepidium seed, remaining raw material and technique are same as Example 5.
Comparative example 3
This comparative example, which is removed, is free of fructus cannabis and lepidium seed, remaining raw material and technique are same as Example 5.
Comparative example 4
Each raw material in embodiment 5 is directly added into reaction kettle and is directly mixed, heats reaction by this comparative example.
Antibacterial anti-acne facial cleanser made from embodiment 1-5 and comparative example 1-4 is tested for the property：
Anti-acne performance test：Select 9 groups, every group 10 totally 90 volunteers's (age 20-30 Sui) for suffering from acne, every group
The obtained facial cleanser of embodiment 1-5 and comparative example 1-4 is respectively adopted in volunteer, persistently uses 30 days, counts within every ten days every group of skin
The percentage situation of change of skin acne sum, as a result such as following table：
By counting volunteer's acne transformation of variables percentage, pass through comparative example product group and comparative example product group, it is known that
The facial cleanser of the present invention can reduce the acne number of volunteer, and facial cleanser of the invention has anti-acne effect.
Antibacterial effect is tested：Using the antibiotic property of plate dilution assay method facial cleanser, number system is carried out to gained clump count
Meter, operation are as follows：Facial cleanser 1ml made from Example 1-5 and comparative example 1-4 respectively, dilutes 30 times, takes 5ml facial cleansers dilute
It releases liquid to mix with agar culture solution, 200ml deionized waters is used to wash one's face as experiment bacterium solution, take 1ml experiments bacterium solution to mixing
It in culture solution, cultivates 48 hours, observe clump count and counts under 37 degrees celsius, as a result such as following table：
Pass through the Statistical Comparison of above-mentioned clump count, it is known that facial cleanser of the invention can inhibit bacterial growth, have preferable
Antibacterial action.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (9)
1. a kind of antibacterial anti-acne facial cleanser, which is characterized in that include the raw material of following parts by weight：8-15 parts of glycerine, ethylene glycol
2-8 parts of 3-6 parts of distearate, 0.1-1 parts of fructus cannabis, 0.1-0.5 parts of lepidium seed, 1-4 parts of monkshood and tea root.
2. antibacterial anti-acne facial cleanser according to claim 1, which is characterized in that include the raw material of following mass fraction：It is sweet
10-12 parts oily, 4-5 parts of glycol distearate, 0.2-0.6 parts of fructus cannabis, 0.3-0.4 parts of lepidium seed, 2-3 parts of monkshood and tea
3-7 parts of tree root.
3. antibacterial anti-acne facial cleanser according to claim 1, which is characterized in that include the raw material of following mass fraction：It is sweet
5 parts of 11 parts of oil, 4.5 parts of glycol distearate, 0.5 part of fructus cannabis, 0.35 part of lepidium seed, 2.5 parts of monkshood and tea root.
4. a kind of preparation method of antibacterial anti-acne facial cleanser as described in claims 1 to 3 is any, which is characterized in that including with
Lower step：(1) fructus cannabis ethanol solution ultrasound is extracted, ultrafiltration is carried out after the completion of extraction, filtrate is by being concentrated under reduced pressure into original
The 1/4 of filtrate volume obtains fructus cannabis extracting solution；(2) lepidium seed is dry, crush, be put into boiling in pot and filter, 8-10 is added
Times water continues infusion, and refluxing extraction is carried out between 50-65 degrees Celsius, obtains lepidium seed extracting solution；(3) by monkshood and tea root
Crushing, drying are simultaneously extracted using ethyl alcohol, and distillation and concentration obtains component C；(4) glycerine, glycol distearate are added first
In secondary reacting kettle, it is stirred and is mixed and heated 60-80 degrees Celsius；(5) by fructus cannabis extracting solution, lepidium seed extracting solution and group
Divide C to be added in the second width reaction kettle, is heated to 65 degrees Celsius；(6) main reaction kettle is preheating to 50-60 degrees Celsius and vacuumized
To -1mpa, the raw material in the first secondary reacting kettle and the second secondary reacting kettle is evacuated in main reaction kettle, with 4000-4500r/ minutes
Rotating speed opens homogeneous blender, and (7) sequentially add lactic acid, potassium hydroxide, essence after sixty minutes for homogeneous stirring, and secondary agitation 1 is small
When, constant temperature is cooled to 40 degrees Celsius after 30 minutes, detection pH discharges when being 6-7.
5. the preparation method of antibacterial anti-acne facial cleanser according to claim 4, which is characterized in that ultrasound leaching in step (1)
The condition carried is：Dense degree Celsius of the quality of ethanol solution is 60%, ultrasound extraction 2 times, 2 hours every time, solid-liquid ratio 1:10.
6. the preparation method of antibacterial anti-acne facial cleanser according to claim 4, which is characterized in that boiling carries in step (2)
The condition taken is：Solid-liquid ratio 1:8, return time is 2 hours, 55 degrees Celsius of refluxing extraction temperature degree Celsius.
7. the preparation method of antibacterial anti-acne facial cleanser according to claim 4, which is characterized in that heating temperature in step (4)
Degree Celsius be 75 degrees Celsius.
8. the preparation method of antibacterial anti-acne facial cleanser according to claim 4, which is characterized in that preheating temperature in step (6)
Degree is 55 degrees Celsius, and homogeneous stirring speed degree Celsius is 4200r/ minutes.
9. the preparation method of antibacterial anti-acne facial cleanser according to claim 4, which is characterized in that pH value is in step (7)
6.5 discharging.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112022759A (en) * | 2020-07-21 | 2020-12-04 | 云南西草资源开发有限公司 | Preservative and preparation method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112022759A (en) * | 2020-07-21 | 2020-12-04 | 云南西草资源开发有限公司 | Preservative and preparation method and application thereof |
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Application publication date: 20181106 |