CN108727101A - A kind of wheat fertilizer special for organic and its preparation method and application - Google Patents
A kind of wheat fertilizer special for organic and its preparation method and application Download PDFInfo
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- CN108727101A CN108727101A CN201810599321.6A CN201810599321A CN108727101A CN 108727101 A CN108727101 A CN 108727101A CN 201810599321 A CN201810599321 A CN 201810599321A CN 108727101 A CN108727101 A CN 108727101A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F1/00—Fertilisers made from animal corpses, or parts thereof
- C05F1/002—Fertilisers made from animal corpses, or parts thereof from fish or from fish-wastes
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/16—Ericaceae [Heath or Blueberry family], e.g. rhododendron, arbutus, pieris, cranberry or bilberry
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K17/00—Soil-conditioning materials or soil-stabilising materials
- C09K17/14—Soil-conditioning materials or soil-stabilising materials containing organic compounds only
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2101/00—Agricultural use
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- General Health & Medical Sciences (AREA)
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- Wood Science & Technology (AREA)
- Agronomy & Crop Science (AREA)
- Environmental Sciences (AREA)
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- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
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Abstract
The invention discloses a kind of wheat fertilizer special for organic and its preparation method and application.The wheat fertilizer special for organic includes the raw material of following parts by weight：25-36 parts of air bladder, 12-18 parts of glucorphanin, 6-17 parts of blueberry leaf, turns round 5-17 parts of Cactus Pedicel of thorn at 6-12 parts of puridoxine hydrochloride.The wheat fertilizer special for organic fertilizer efficiency of the present invention is high, and Plant Height in Wheat, survival rate and yield are improved；It is alternatively arranged as bacteriostatic agent and heavy metal processing soil treatment agent uses, Escherichia coli bacteriostasis rate and staphylococcus aureus bacteriostasis rate are above 98%, excellent to the adsorption effect of cadmium, cobalt and lead in soil, are worthy to be popularized.
Description
Technical field
The present invention relates to a kind of organic fertilizer, specifically a kind of wheat fertilizer special for organic and its preparation method and application.
Background technology
Wheat is important cereal crops and industrial crops, and statistics display, the yield and cultivated area of wheat are only secondary at present
In corn, second place of the world is occupied.China is one of the country that wheat is planted in the world earliest, and wheat accounts in the people's livelihood and national economy
There is critical role.Wheat yield per unit area is improved, the fertilising to soil is be unable to do without.Currently, in wheat growth, change
Fertilizer application is more spread unchecked；Although increasing the speed of growth of wheat, yield is improved, also results in degeneration, the plate in arable land
The more serious consequences such as knot；In addition, abuse chemical fertilizer also results in wheat quality continuous decrease, while the natural environments such as soil are made
At prodigious pollution.These consequences not only compromise the sustainable development of Wheat Production, or even jeopardize our mankind's
Long-range survival and development.
With the improvement of people's living standards, the demand of the free of contamination organic and green food of safety of residents health is continuous
Increase, vast farmers improve the market competitiveness of agricultural product there is an urgent need to application of organic fertilizers.Although currently used organic fertilizer
Free from environmental pollution, cost is relatively low, but has the following disadvantages：A, nutriment is lost in serious, and wheat yield is low；B, it has a single function,
Without bacteriostasis efficacy and heavy metal soil treatment function.
Invention content
The purpose of the present invention is to provide a kind of wheat fertilizer special for organic and its preparation method and application, to solve the above-mentioned back of the body
The problem of being proposed in scape technology.
To achieve the above object, the present invention provides the following technical solutions：
A kind of wheat fertilizer special for organic, includes the raw material of following parts by weight：25-36 parts of air bladder, puridoxine hydrochloride 6-12
Part, 12-18 parts of glucorphanin, 6-17 parts of blueberry leaf turn round 5-17 parts of Cactus Pedicel of thorn.
As a further solution of the present invention：Include the raw material of following parts by weight：28-32 parts of air bladder, puridoxine hydrochloride
8-11 parts, 14-17 parts of glucorphanin, 9-13 parts of blueberry leaf, turn round thorn 8-15 parts of Cactus Pedicel.
As a further solution of the present invention：Include the raw material of following parts by weight：30 parts of air bladder, puridoxine hydrochloride 10
Part, 15 parts of glucorphanin, 11 parts of blueberry leaf turn round 9 parts of Cactus Pedicel of thorn.
A kind of preparation method of wheat fertilizer special for organic, is prepared by following steps：
(1) air bladder, blueberry leaf are taken and turns round thorn Cactus Pedicel, 1-2h is soaked, smashes, add water and decoct 20-25min,
Extracting solution is obtained by filtration, extracting solution centrifugation discards insoluble matter, and supernatant is inhaled by loading the resin column of LX-8 macroporous absorbent resins
It is attached, it is primary to repeat loading；Then gains stand 2-5h, are first negative with water elution to eluent molish reactions, then with 50-
60% ethanol solution elution, is finally eluted with 75% ethanol solution, solvent is separately recovered in eluent, by 50-60% ethyl alcohol
Position and the mixing of 75% ethyl alcohol position, freeze-drying obtain mixed extract；
(2) glucorphanin and puridoxine hydrochloride are mixed, 65% ethyl alcohol of the two 0.5-1 times of weight of mixture is added, with
And the water of 0.5-1 times of weight of the two mixture, after stirring evenly, it is placed at 60-65 DEG C and is stirred to react 4-6h, then soak at room temperature
2-4h；
(3) upper step gains are mixed with mixed extract, is placed at 70-77 DEG C and is stirred 10-20min；Then subtract
Pressure is distilled to recover ethyl alcohol, and residue is wheat fertilizer special for organic.
A kind of bacteriostatic agent, including the wheat fertilizer special for organic.
One heavy metal species processing soil treatment agent, including the wheat fertilizer special for organic.
Compared with prior art, the beneficial effects of the invention are as follows：
The wheat fertilizer special for organic fertilizer efficiency of the present invention is high, and Plant Height in Wheat, survival rate and yield are improved；It is alternatively arranged as
Bacteriostatic agent and heavy metal processing soil treatment agent use, and Escherichia coli bacteriostasis rate and staphylococcus aureus bacteriostasis rate are above 98%,
It is excellent to the adsorption effect of cadmium, cobalt and lead in soil, it is worthy to be popularized.
Specific implementation mode
The technical solution of this patent is described in more detail With reference to embodiment.
Embodiment 1
A kind of wheat fertilizer special for organic, includes the raw material of following parts by weight：25 parts of air bladder, 6 parts of puridoxine hydrochloride, radish
12 parts of sulphur glycosides, 6 parts of blueberry leaf turn round 5 parts of Cactus Pedicel of thorn.
A kind of preparation method of wheat fertilizer special for organic, is prepared by following steps：(1) take air bladder, blueberry leaf and
Thorn Cactus Pedicel is turned round, 1h is soaked, smashes, adds water and decocts 20min, extracting solution is obtained by filtration, extracting solution centrifugation discards not
Molten object, supernatant are adsorbed by loading the resin column of LX-8 macroporous absorbent resins, and it is primary to repeat loading；Then gains are stood
2h is first negative with water elution to eluent molish reaction, then is eluted with 50% ethanol solution, finally with 75% ethyl alcohol
Solution elutes, and solvent is separately recovered in eluent, and 50% ethyl alcohol position and 75% ethyl alcohol position are mixed, and freeze-drying must mix extraction
Object；(2) glucorphanin and puridoxine hydrochloride are mixed, 65% ethyl alcohol and the two of the two 0.5 times of weight of mixture is added
The water of 0.5 times of weight of mixture after stirring evenly, is placed at 60 DEG C and is stirred to react 4h, then soak at room temperature 2h；(3) by upper step
Gains are mixed with mixed extract, are placed at 70 DEG C and are stirred 10min；Then vacuum distillation recycling ethyl alcohol, residue are
For wheat fertilizer special for organic.
The wheat fertilizer special for organic can be used for preparing bacteriostatic agent, metal processing soil treatment agent.
Embodiment 2
A kind of wheat fertilizer special for organic, includes the raw material of following parts by weight：36 parts of air bladder, 12 parts of puridoxine hydrochloride, radish
18 parts of sulphur glycosides, 17 parts of blueberry leaf turn round 17 parts of Cactus Pedicel of thorn.
A kind of preparation method of wheat fertilizer special for organic, is prepared by following steps：(1) take air bladder, blueberry leaf and
Thorn Cactus Pedicel is turned round, 2h is soaked, smashes, adds water and decocts 25min, extracting solution is obtained by filtration, extracting solution centrifugation discards not
Molten object, supernatant are adsorbed by loading the resin column of LX-8 macroporous absorbent resins, and it is primary to repeat loading；Then gains are stood
5h is first negative with water elution to eluent molish reaction, then is eluted with 60% ethanol solution, finally with 75% ethyl alcohol
Solution elutes, and solvent is separately recovered in eluent, and 60% ethyl alcohol position and 75% ethyl alcohol position are mixed, and freeze-drying must mix extraction
Object；(2) glucorphanin and puridoxine hydrochloride are mixed, 65% ethyl alcohol and the two that the two 1 times of weight of mixture is added are mixed
The water for closing 1 times of weight of object, after stirring evenly, is placed at 65 DEG C and is stirred to react 6h, then soak at room temperature 4h；It (3) will be obtained by upper step
Object is mixed with mixed extract, is placed at 77 DEG C and is stirred 20min；Then vacuum distillation recycling ethyl alcohol, residue are as small
Wheat fertilizer special for organic.
The wheat fertilizer special for organic can be used for preparing bacteriostatic agent, metal processing soil treatment agent.
Embodiment 3
A kind of wheat fertilizer special for organic, includes the raw material of following parts by weight：30 parts of air bladder, 10 parts of puridoxine hydrochloride, radish
15 parts of sulphur glycosides, 11 parts of blueberry leaf turn round 9 parts of Cactus Pedicel of thorn.
A kind of preparation method of wheat fertilizer special for organic, is prepared by following steps：(1) take air bladder, blueberry leaf and
Thorn Cactus Pedicel is turned round, 1.5h is soaked, smashes, adds water and decocts 23min, extracting solution is obtained by filtration, extracting solution centrifugation discards
Insoluble matter, supernatant are adsorbed by loading the resin column of LX-8 macroporous absorbent resins, and it is primary to repeat loading；Then gains are stood
2.6h is first negative with water elution to eluent molish reaction, then is eluted with 55% ethanol solution, finally with 75% second
Alcoholic solution elutes, and solvent is separately recovered in eluent, and 55% ethyl alcohol position and 75% ethyl alcohol position are mixed, and freeze-drying obtains mixing and carries
Take object；(2) glucorphanin and puridoxine hydrochloride are mixed, 65% ethyl alcohol and two of the two 0.8 times of weight of mixture is added
The water of 0.7 times of weight of person's mixture after stirring evenly, is placed at 62 DEG C and is stirred to react 5h, then soak at room temperature 3h；It (3) will be upper
Step gains are mixed with mixed extract, are placed at 72 DEG C and are stirred 15min；Then vacuum distillation recycling ethyl alcohol, residue
As wheat fertilizer special for organic.
The wheat fertilizer special for organic can be used for preparing bacteriostatic agent, metal processing soil treatment agent.
Embodiment 4
As different from Example 3, a kind of wheat fertilizer special for organic, includes the raw material of following parts by weight：28 parts of air bladder,
8 parts of puridoxine hydrochloride, 9 parts of blueberry leaf, turns round 8 parts of Cactus Pedicel of thorn at 14 parts of glucorphanin.
Embodiment 5
As different from Example 3, a kind of wheat fertilizer special for organic, includes the raw material of following parts by weight：32 parts of air bladder,
11 parts of puridoxine hydrochloride, 13 parts of blueberry leaf, turns round 15 parts of Cactus Pedicel of thorn at 17 parts of glucorphanin.
Comparative example 1
It is removed outside puridoxine hydrochloride in raw material, other are consistent with embodiment 3.Preparation process is consistent with embodiment 3.
Comparative example 2
It is removed outside glucorphanin in raw material, other are consistent with embodiment 3.Preparation process is consistent with embodiment 3.
Comparative example 3
It is removed outside puridoxine hydrochloride and glucorphanin in raw material, other are consistent with embodiment 3.Preparation process and embodiment 3 one
It causes.
Comparative example 4
Raw material is consistent with embodiment 3.Preparation process use common process, by all raw materials be mixed evenly to get.
Experimental example
One, fertilizer efficiency is tested
It chooses wheat planting base to be tested, the product of common fertilizer, embodiment 1-3 and comparative example 1-4 is applied respectively
Enter in 5 pieces of wheat planting fields, sowing amount is identical.Wheat is harvested, as a contrast with common fertilizer.Experimental result is shown in Table 1.
1 experimental result of table
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 |
| Plant height increases % | 15 | 12 | 14 | 6 | 7 | 5 | 10 |
| Wheat increase yield % | 32 | 30 | 35 | 22 | 24 | 18 | 26 |
| Survival rate increases % | 28 | 25 | 29 | 20 | 18 | 16 | 22 |
Two, fungistatic effect is tested
The product of embodiment 1-3 and comparative example 1-4 are carried out to carry out bacteriostasis property test, the results are shown in Table 2.
2 bacteriostasis property test result of table
Three, heavy metal soil treatment is tested
Before reparation, in soil cadmium concentration be 135.8mg/Kg, cobalt concentration 170.6mg/Kg, lead concentration 142.7mg/Kg,
By the product rehabilitating soil of above-described embodiment 1-3 and comparative example 1-4, the concentration of cadmium in soil, cobalt and lead is determined after 5 days,
As a result as follows：
| Project | Cadmium concentration mg/Kg | Cobalt concentration mg/Kg | Lead concentration mg/Kg |
| Embodiment 1 | 9.2 | 10.3 | 10.8 |
| Embodiment 2 | 10.3 | 11.2 | 9.6 |
| Embodiment 3 | 8.8 | 9.8 | 9.3 |
| Comparative example 1 | 35.8 | 48.9 | 37.9 |
| Comparative example 2 | 29.6 | 42.7 | 42.8 |
| Comparative example 3 | 48.1 | 55.6 | 46.2 |
| Comparative example 4 | 15.9 | 23.2 | 18.1 |
The better embodiment of this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
Formula, one skilled in the relevant art within the scope of knowledge, can also be under the premise of not departing from this patent objective
It makes a variety of changes.
Claims (6)
1. a kind of wheat fertilizer special for organic, which is characterized in that include the raw material of following parts by weight：25-36 parts of air bladder, hydrochloric acid pyrrole
Tremble 6-12 parts of alcohol, 12-18 parts of glucorphanin, 6-17 parts of blueberry leaf, turn round thorn 5-17 parts of Cactus Pedicel.
2. wheat fertilizer special for organic according to claim 1, which is characterized in that include the raw material of following parts by weight：Fish
28-32 parts of fish glue, 14-17 parts of glucorphanin, 9-13 parts of blueberry leaf, turns round 8-15 parts of Cactus Pedicel of thorn at 8-11 parts of puridoxine hydrochloride.
3. wheat fertilizer special for organic according to claim 1, which is characterized in that include the raw material of following parts by weight：Fish
30 parts of fish glue, 15 parts of glucorphanin, 11 parts of blueberry leaf, turns round 9 parts of Cactus Pedicel of thorn at 10 parts of puridoxine hydrochloride.
4. a kind of preparation method of wheat fertilizer special for organic as described in any one of claims 1-3, which is characterized in that by following
Step is prepared：
（1）It takes air bladder, blueberry leaf and turns round thorn Cactus Pedicel, soak 1-2h, smash, add water and decoct 20-25min, filtering
Extracting solution is obtained, extracting solution centrifugation discards insoluble matter, and supernatant is adsorbed by loading the resin column of LX-8 macroporous absorbent resins,
It is primary to repeat loading；Then gains stand 2-5h, are first negative with water elution to eluent molish reactions, then with 50-
60% ethanol solution elution, is finally eluted with 75% ethanol solution, solvent is separately recovered in eluent, by 50-60% ethyl alcohol
Position and the mixing of 75% ethyl alcohol position, freeze-drying obtain mixed extract；
（2）Glucorphanin and puridoxine hydrochloride are mixed, 65% ethyl alcohol and two of the two 0.5-1 times of weight of mixture is added
The water of 0.5-1 times of weight of person's mixture after stirring evenly, is placed at 60-65 DEG C and is stirred to react 4-6h, then soak at room temperature 2-
4h；
（3）Upper step gains are mixed with mixed extract, is placed at 70-77 DEG C and is stirred 10-20min；Then decompression is steamed
Recycling ethyl alcohol is evaporated, residue is wheat fertilizer special for organic.
5. a kind of bacteriostatic agent, including any wheat fertilizer special for organic of claim 1-3.
6. a heavy metal species processing soil treatment agent, including any wheat fertilizer special for organic of claim 1-3.
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