CN108704116A - Powder and preparation method thereof is sterilized in lavipeditum - Google Patents
Powder and preparation method thereof is sterilized in lavipeditum Download PDFInfo
- Publication number
- CN108704116A CN108704116A CN201810984868.8A CN201810984868A CN108704116A CN 108704116 A CN108704116 A CN 108704116A CN 201810984868 A CN201810984868 A CN 201810984868A CN 108704116 A CN108704116 A CN 108704116A
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- powder
- lavipeditum
- parts
- skin
- raw material
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/82—Theaceae (Tea family), e.g. camellia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/70—Carbohydrates; Sugars; Derivatives thereof
- A61K31/7028—Compounds having saccharide radicals attached to non-saccharide compounds by glycosidic linkages
- A61K31/7034—Compounds having saccharide radicals attached to non-saccharide compounds by glycosidic linkages attached to a carbocyclic compound, e.g. phloridzin
- A61K31/704—Compounds having saccharide radicals attached to non-saccharide compounds by glycosidic linkages attached to a carbocyclic compound, e.g. phloridzin attached to a condensed carbocyclic ring system, e.g. sennosides, thiocolchicosides, escin, daunorubicin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/483—Gleditsia (locust)
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- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/18—Magnoliophyta (angiosperms)
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Abstract
The invention discloses a kind of lavipeditums to sterilize powder, and the raw material matched by following masses part is made：20~30 parts of camellia seed meal, 60~80 parts of sodium bicarbonate, 0.5~1 part of soap powder, 0.5~1 part of atlapulgite, 4~6 parts of sea salt, 0.5~2 part of ginger powder, 0.1~3 part of Chinese honey locust, 0.1~3 part of soapberry, 0.5~1 part of peppermint, 0.5~1 part of rosemary.It is non-toxic, nonirritant, without sensitization, can penetrate into skin, to blood circulation of human body and then is distributed to the whole body internal organs of human body, it promotes blood circulation, cleans skin, deep layer is nourished, peculiar smell is removed in sterilization, there is lasting moisturizing, repairing skin prevents dry and cracked, cutin-softening, it is fine and smooth that skin moisturizing is used for a long time, it relieves fatigue, promotes sleep, health care.
Description
Technical field
The invention belongs to nursing materials technical field, especially a kind of lavipeditum sterilization powder and preparation method thereof is mainly used
In people's daily nursing, advantages of nontoxic raw materials, it is nonirritant, without sensitization, safety, environmental protection can be used for a long time.
Background technology
Before thousands of years《The Yellow Emperor's Canon of Internal Medicine》It records：Cloudy arteries and veins combines in foot, and gathers in sole center.So-called passages through which vital energy circulates trip, three
Through all arising from foot.Both foot was the starting point of three yin channel, the terminal of three yang channels, well, Ying, Yu, the original etc. of six passages through which vital energy circulates of foot
Acupuncture point is respectively positioned on foot.Biped portion shares 66 acupuncture points on these passages through which vital energy circulates, these acupuncture points are to all very sensitive, the cave of various stimulations
Position is connected with each internal organs organ of whole body closely again, can play the role of promotion QI-blood circulation by Chinese herbal medicine lavipeditum, warm internal organs,
To reach inner disease outer treat, the effect for the treatment of disease in the upper by managing the lower.
Most lavipeditum powder is all natural traditional Chinese medicine on the market at present, for example controls tinea pedis, improves sleep, sterilizing and itch-relieving, is promoted
Into blood circulation, etc..Due to comprising Chinese herbal medicine difference, curative effect is also different.But there is no pass through for the product of most enterprises
Detailed product mechanism study, health care effectiveness unobvious, only publicizes conceptual issues, and antibacterial and anti-inflammatory effects are bad, was easy
Quick or even skin ambustion.Or effect, obviously when price is again fairly expensive, unsuitable common people use.
Invention content
An object of the present invention is to overcome the above-mentioned insufficient of the prior art and provide a kind of lavipeditum sterilization powder, nontoxic
Property, it is nonirritant, without sensitization, skin can be penetrated into, to blood circulation of human body and then be distributed to the whole body internal organs of human body,
It promotes blood circulation, cleans skin, deep layer is nourished, and peculiar smell is removed in sterilization, there is lasting moisturizing, and repairing skin prevents dry and cracked, softening angle
Matter, long-time service skin moisturizing is fine and smooth, relieves fatigue, and promotes sleep, health care.
It is simple for process it is a further object of the present invention to provide the preparation method that powder is sterilized in above-mentioned lavipeditum, raw material is common,
Cheaply.
The technical scheme is that：A kind of lavipeditum sterilization powder, the raw material matched by following masses part are made：Oil tea
20~30 parts of the seed dregs of rice, 60~80 parts of sodium bicarbonate, 0.5~1 part of soap powder, 0.5~1 part of atlapulgite, 4~6 parts of sea salt, ginger powder 0.5
~2 parts, 0.1~3 part of Chinese honey locust, 0.1~3 part of soapberry, 0.5~1 part of peppermint, 0.5~1 part of rosemary.
Preferably, powder is sterilized in a kind of lavipeditum, and the raw material matched by following masses part is made：It is 22 parts of camellia seed meal, small
67 parts of soda, 0.5 part of soap powder, 0.9 part of atlapulgite, 4 parts of sea salt, 0.9 part of ginger powder, 2.7 parts of Chinese honey locust, 2.5 parts of soapberry, peppermint
0.8 part, 1 part of rosemary.
The present invention another technical solution be：The preparation method of above-mentioned lavipeditum sterilization powder, in turn includes the following steps：
（1）Take raw material：Raw material is weighed according to the ratio；
（2）It crushes：It by raw material drying, is crushed respectively by pulverizer, obtains each raw material powder；
（3）Mixing：Each raw material powder is mixed, is stirred evenly；
（4）Sterilization：25-35min is sterilized by 120-130 DEG C of hot wind, then non-woven bag packs, obtains finished product lavipeditum sterilization
Powder.
The primary symbols and name resolving that the present invention uses are as follows：
~：Numberical range, such as 1~5 expression 1 to 5；mL：The abbreviation of milliliter, milliliter；g:Gram.
The primary raw material that the present invention uses is described as follows：
Non-woven fabrics：(English name:Non Woven Fabric or Nonwoven cloth) it is also known as nonwoven fabric, by orienting
Or random fiber and constitute.Because with cloth appearance and certain performances due tos be called cloth.Non-woven fabrics has moisture-proof, ventilative, soft
Tough, light, not combustion-supporting, easy the features such as decomposing, is nontoxic nonirritant, rich in color, cheap, recyclable.
Camellia seed meal：Camellia seed kernel is after squeezing, extract technology extraction, the remaining bits of institute, referred to as camellia seed meal,
Contain about 10% protein, 10% tea polysaccharide, 12% Tea Saponin, 50% cellulose and lignin.
Sodium bicarbonate(edible)：White powder or monoclinic crystal crystalline powder, it is odorless, taste is salty, soluble easily in water, but compare sodium carbonate
Solubility in water is small, does not dissolve in ethyl alcohol, and aqueous solution is in alkalescence.It is heated easily to decompose.It is slowly decomposed in humid air.About
Start to lose carbon dioxide at 50 DEG C, becomes sodium carbonate in 100 DEG C of wholes.It is decomposed rapidly in weak acid, aqueous solution is at 20 DEG C
When start to split the carbon dioxide off and sodium carbonate, all decomposed to when boiling point.It is dissolved in 10 parts of water at 25 DEG C, about 18 DEG C of whens are dissolved in 12
Part water, does not dissolve in ethyl alcohol.The solution not stirred made of its cold water is only in that alkalescence is reacted to phenolphthalein test paper, places or rise
High-temperature, alkalinity increase.The 0.1mol/L pH value of water solution of 25 DEG C of Fresh is 8.3, shows alkalinity, but be free of OH ﹣, no
Belong to alkali, belongs to acid carbonate (bicarbonate).Storage:It is dry, it is protected from light, is sealed.Purposes:Analytical reagent.Organic conjunction
At.Pharmacy（Treat hyperhydrochloria）.Leavening（Roasting cake）.Extinguishing chemical（Foam or dry powder）.
Chinese honey locust：《Dictionary of medicinal plant》It records：Chinese honey locust,【Different name】Chicken dwell son (《Wide will) }), gleditsia sinensis (《Handbook of Prescriptions for Emergencies》), big soap
Pod (《Prescriptions worth thousand gold》), long Chinese honey locust (《Bencao Tujing》), hang knife (《Outer red book on Chinese herbal medicine》), long gleditsia sinensis (《The side of directing at》).【Base】For beans
The fruit of section Gleditsia plant Chinese honey locust or sterile fruit.The former claims Chinese honey locust, the latter to claim fructus gleditsiae.【Pick and process】Cultivation 5~6 years
Afterwards i.e. as a result, when autumn fruit maturation blackening picks, dry.【Pharmacology】1. phlegm-dispelling functions, this product can stimulate stomach lining containing saponin(e,
Respiratory mucosa secretion is caused to increase reflectingly.Belong to nauseous expectorant.2. antibacterial action, Chinese honey locust preserved material is in vitro to violet
Trichophyta, star-shaped nocardia and certain dermatophytes have inhibiting effect.
Sea salt:From salt marsh, sea salt contains trace mineral, such as calcium, magnesium, potassium, bromide and other various micro members
Element.The mollusk (insect) that slug, snail, leech one kind have mucus can be killed.
Soapberry：（Scientific name：Sapindus mukorossi Gaertn.）, alias：Wood suffers from son（Compendium of Materia Medica）, oil is suffered from sub
（Sichuan）Hardship suffers from tree（Hainan）, yellow mesh tree, mesh wave tree（Taiwan）, You Luoshu, fruit of washing one's hands, name elsewhere：Rub mesh, false dragon with the hands
Eye, Devil Frown etc..Soapberry deciduous tree, branch are carried out, leaf alternate；Without stipule；There is handle；Panicle, basidixed and side life；Flower
Polygamy, corolla light green, there is shortly clawed；Floral disc cup-shaped；Filigree has fine, soft fur, medicine back life, and hermaphrodite flower stamen is small, and filigree has soft
Hair.Drupe is spherical, yellow or brown color when ripe.Seed is spherical, black, 6~July of florescence.9~October of fruiting period.Length originating in China
Various regions and South East Asia Mainland various regions, India and Japan on the south the basin of river.Pericarp contains saponin, can do boxboard for soap, timber
With wooden comb etc..Root, browse, seed：Bitter, micro-pungent is trembled with fear.It is slightly poisonous.Heat-clearing eliminating the phlegm, disperse accumulation desinsection.For diphtheria, throat is swollen
Bitterly, acute tonsillitis, cough, pertussis, food stagnation malnutrition due to parasitic infestation；It is used for Trichomonas vaginalis outside.Benevolence：It is pungent, it puts down.Disperse accumulation wards off evil.For infantile malnutrition due to digestive disturbances or intestinalparasites, roundworm
Disease, inflatable in abdomen, halitosis.
Soap powder：Tea Saponin also known as tea saponin are a kind of candy glucosides by being extracted in tea tree seed (tea seed, tea seeds)
Compound is a kind of natural surfactant of good performance, it can be widely applied to light industry, chemical industry, pesticide, feed, cultivation,
The fields such as weaving, oil recovery, mining, building materials and expressway construction.Manufacture emulsifier, abluent, insecticides adjuvant, feed addition
Agent, crab shrimp aquaculture protective agent, textile auxiliary, oilfield foaming agent, mining flotation agent and air entrained concrete foam stabilizer and concrete
Additive -- antifreezing agent etc..
Atlapulgite：It is raw material with clay (mainly bentonite), is handled through inorganic acidifying, then through water rinsing, dry system
At adsorbent, appearance is off-white powder, odorless, tasteless, nontoxic, and absorption property is very strong, can adsorb coloring matter, organic matter
Matter.The easy moisture absorption in air, placement can reduce absorption property too long.But it is heated to 300 degrees Celsius or more and just starts to lose knot
Brilliant water, makes structure change, and influences fading effect.Atlapulgite is not soluble in water, in organic solvent and various oils, almost complete
It is dissolved in entirely in hot caustic soda and hydrochloric acid, relative density 2.3-2.5, swelling is minimum in water and oil.
Ginger powder：Powder, main material are gingers, and the function of ginger powder has warm, excited, sweating, preventing or arresting vomiting, removing toxic substances, warm lung
The effects that cough-relieving, especially for ichthyophagy crab poison, the drug poisoning such as the tuber of pinellia, rhizoma arisaematis have detoxication.Suitable for catching cold, head
Bitterly, phlegm and retained fluid, cough, gastrofrigid vomiting;By ice and snow, water is wet, after cold invasion, anxious to drink it with ginger decoction, blood can be promoted, dispersed
Cold-evil.
Peppermint：The general name of Labiatae (Labiatae) Mentha (Mentha Linn) plant is perennial root grass
This.Europe and Mediterranean are originated in, there is cultivation all over the world now, its cauline leaf is mainly used to extract essential oil as natural perfume
Material.Peppermint is with all herbal medicine, and also edible, is mainly used to refine peppermint oil and menthol, the two to be the master that peppermint plays a role
Ingredient is wanted, the foundation of different peppermint kinds is also to discriminate between.Peppermint can be used for toothpaste and dental care product, food, cigarette, wine,
The flavoring of cold drink, cosmetics and perfumed soap.In medicine, it is widely used in the medicines such as wind-dispelling, anti-corrosion, anti-inflammatory, antipruritic
In product, such as cooling ointment, rheumatic oil.
Rosemary：（Classification system：Rosmarinus officinalis）Labiatae shrub.Property happiness temperature climate, originate in
The northern Mediterranean of European Region and Africa.China is just once introduced a fine variety far away from Caowei Kingdom in period.Occasionally there is application in present gardens.From fan
Repeatedly antioxidant and Rosemary Oil with excellent anti-oxidation characteristics can be extracted in fragrant flower and leaf.Rosemary antioxidant.
Medicine, fried food, rich oil food and the fresh-keeping of each quasi-grease is widely used in guarantee the quality；And rosemary essence is then used for fragrance, sky
The daily-use chemical industries industry such as gas freshener, driving ants and sterilization, desinsection.
Usage and dosage:2000ml cold water soaks are added 15 minutes in 15 grams of lavipeditum sterilization powder of the invention, are decocted 20 minutes,
It is cooled at 50 DEG C, obtains liquid, impregnate foot 20 minutes, 1~2 times/day, 15 grams/day, the course for the treatment of 2 weeks.
The present invention has following features compared with prior art：
1. bactericidal effect is good, can effectively anti-inflammation and sterilization control tinea pedis；
2. use feels pleasant, cleaning, nourishes skin at moisturizing；
3. non-toxic, nonirritant, without sensitization, safety, environmental protection can be used for a long time.
In order to illustrate more clearly of the present invention, following embodiment and detection test situation, but its range to invention are enumerated
It is without any restrictions.
Specific implementation mode
Embodiment 1
Take 25 kilograms of camellia seed meal, 60 kilograms of sodium bicarbonate, 0.7 kilogram of soap powder, 1 kilogram of atlapulgite, 5 kilograms of sea salt, ginger powder 1,000
Gram, 2 kilograms of Chinese honey locust, 2 kilograms of soapberry, 0.8 kilogram of peppermint, 1 kilogram of rosemary.
All these raw materials are dried sanitaries；Raw material will be obtained to crush by pulverizer respectively, cross 100 mesh
Sieve, obtains each raw material powder；
Each raw material powder is put into agitator tank, is mixed, mixing time 30min, mixing powder is obtained；
Gained mixing powder is sterilized into 30min by 120-130 DEG C of hot wind, then non-woven bag packs, obtains finished product foot
Bath sterilization powder.
Embodiment 2-6
Raw material and quality used in embodiment 2-6, comparative example 1-2 are as shown in Table 1 below, preparation method and embodiment 1
It is identical；Table 1 below illustrates specific raw material and quality used in embodiment 1-6.
Table 1, unit are kilogram
。
Comparative example 1 eliminates atlapulgite on the basis of embodiment 6, and comparative example 2 eliminates on the basis of embodiment 6
Ginger powder is other same as Example 6.
Detection and experiment
The lavipeditum sterilization powder of various embodiments of the present invention is sent to the detection and experiment that special detection mechanism has carried out system by applicant,
It is as follows that it predominantly detects test result.
One, powder is sterilized into the lavipeditum obtained by the above various embodiments, by examining pH etc., obtains detecting shown in following table 2
As a result：
Table 2
。
From with upper table 2 it can be seen that the lavipeditum sterilization powder of various embodiments of the present invention has the advantages that safety, hygienic, comparative example
1 apparent detection heavy metal；Comparative example 2 obviously detects microorganism.
Two, cleaning action detects
Purpose：The lavipeditum of various embodiments of the present invention and comparative example sterilization powder packet and sodium bicarbonate, camellia seed meal, standard detergent are taken,
Test its cleaning capacity.
Method：Lavipeditum sterilization powder packet 15g/packet, sodium bicarbonate 15g, the camellia seed meal of various embodiments of the present invention and comparative example
15g/packet, standard detergent 15g measure cleaning capacity with the methods of national standard GB9985-2000.
As a result：It see the table below shown in 3.
The contrasting detection result (N=6, %) of 3. cleaning action of table
。
Conclusion：As can be seen from Table 3, the cleaning force of the lavipeditum sterilization powder packet of various embodiments of the present invention is better than little Su
It beats, camellia seed meal and standard detergent, this absolutely proves that each raw material component of the cleaning packet of various embodiments of the present invention is cleaning
It has been to form synergistic effect in power, the cleaning force of the cleaning packet of various embodiments of the present invention is not only not all components cleaning
The average value of power, and the cleaning force higher than any group of point, if each component of the cleaning packet of various embodiments of the present invention does not have
It forms collaboration de-sludging and cleans effect, then the cleaning capacity of each component mixture of same quality can be less than most high definition in each component
The cleaning capacity of the camellia seed meal of the same quality of clean ability, i.e., present invention produces unexpected cleaning capacities.For effect
The factor penetrates into skin preparation.
Three, antibacterial action detects
1, antibacterium range detection（The measurement of inhibition zone diameter size）
Purpose：Powder solution is sterilized in the lavipeditum that various embodiments of the present invention are detected with agar slant dilution method（A concentration of 0.1g/
ml）And saleratus solution（A concentration of 0.1g/ml）, camellia seed meal solution（A concentration of 0.1g/ml）It is sexy to that can cause to suppurate
The antibacterial action of the pathogenic bacteria of dye specifies its antibacterial range.
Method：Diameter 12cm plates are taken, culture medium 15ml is poured into, are dipped for prescribed limit with the cotton swab of sterilizing after condensation
The test organisms bacterium solution of the exponential phase of density, is uniformly coated on media surface；Then sterilizing Oxford is gripped with aseptic nipper
Cup is put in tablet, and in every Oxford cup plus powder solution is sterilized in the lavipeditum of various embodiments of the present invention and comparative example（A concentration of 0.1g/
ml）200ul, and carry out parallel test three times；37 DEG C of constant temperature incubations are taken out after lower 24 hours, survey inhibition zone diameter, and find out three
The average value of the inhibition zone diameter of secondary parallel test.It is used in combination same method to carry out contrasting detection using sodium bicarbonate, camellia seed meal
Experiment.
As a result：Contrasting detection result see the table below shown in 4.
4. antibacterium range of table contrasting detection result (mm, ±s)
。
2, antibacterium degree detecting（MIC；The measurement of MBC）
Purpose：Powder solution is sterilized in the lavipeditum that various embodiments of the present invention are detected with liquid dilution method（A concentration of 0.1g/ml）With
Saleratus solution（A concentration of 0.1g/ml）, camellia seed meal solution（A concentration of 0.1g/ml）3 or more various concentration points are to energy
Cause the pathogenic bacteria antimicrobial levels of pyogenic infection, detects minimum inhibitory concentration（MIC）And minimum bactericidal concentration（MBC）, clear
Its antimicrobial levels.
Method：It takes sterile test tube several, dilutes various embodiments of the present invention and comparative example with fluid nutrient medium equimultiple
Lavipeditum sterilize powder solution（A concentration of 0.1g/ml）Afterwards, each pipe plus 0.1ml are for trying bacterium solution, while setting culture medium control tube and bacterium
Liquid control tube, 37 DEG C of cultures are taken out afterwards for 24 hours to be seen as a result, in the case where control tube meets the requirements, and observes each developmental tube one by one, with
It can inhibit the various embodiments of the present invention of test organisms growth and the lavipeditum sterilization powder solution of comparative example（A concentration of 0.1g/ml）Most
High dilution is minimum inhibitory concentration（MIC）, and the culture in the test tube of each asepsis growth is forwarded to corresponding culture medium
On agar plate, 37 DEG C of cultures take out observation as a result, to kill the various embodiments of the present invention of 99.9% test organisms thalline afterwards for 24 hours
Powder solution is sterilized in lavipeditum with comparative example（A concentration of 0.1g/ml）Highest dilution is minimum bactericidal concentration（MBC）.It is used in combination same
The method of sample carries out contrasting detection experiment using sodium bicarbonate, camellia seed meal.
As a result：It see the table below shown in 5.
The contrasting detection result (mg/mL) of 5. antibacterium degree of table
。
Conclusion：From table 4,5 as can be seen that the antibacterial and bactericidal effect that powder is sterilized in the lavipeditum of various embodiments of the present invention is better than
Comparative example 2, sodium bicarbonate, camellia seed meal.That is the lavipeditum of various embodiments of the present invention sterilizes powder relative to its primary raw material
Sodium bicarbonate, camellia seed meal have improved bactericidal effect, and the lavipeditum sterilization powder of various embodiments of the present invention is than being used alone oil tea
The seed dregs of rice are more preferable as nursing antiseptic property.
3, antifungic action detects
Purpose：The lavipeditum of the camellia seed meal solution, various embodiments of the present invention of various concentration is detected with agar slant dilution method
Powder solution is sterilized to fungi antibacterial range and antimicrobial levels.
Method：Respectively with the sabouraud culture medium melted to saleratus solution（A concentration of 0.1g/ml）, camellia seed meal solution
（A concentration of 0.1g/ml）, various embodiments of the present invention and comparative example lavipeditum sterilize powder solution（A concentration of 0.1g/ml）, former
Liquid and 1：1,1：2 dilutions, prepare inoculated fungi behind inclined-plane, while setting culture medium control tube and bacterium solution control tube, and 28 DEG C are cultivated 1 week
It takes out and is seen as a result, in the case where control tube meets the requirements afterwards, observe each developmental tube one by one, it is small test organisms can be inhibited to grow
Soda solution（A concentration of 0.1g/ml）, camellia seed meal solution（A concentration of 0.1g/ml）With the lavipeditum of various embodiments of the present invention
Sterilize powder solution（A concentration of 0.1g/ml）Highest dilution is minimum inhibitory concentration（MIC）, and each nothing will be washed with physiology salt
Bacterium growth tube culture inclined-plane, be forwarded on the agar plate of corresponding culture medium, 28 DEG C culture 1 week after take out observation knot
Fruit, to kill the saleratus solution of 99.9% test organisms thalline（A concentration of 0.1g/ml）, camellia seed meal solution（A concentration of 0.1g
/ml）Powder solution is sterilized in lavipeditum with various embodiments of the present invention（A concentration of 0.1g/ml）Highest dilution is minimum bactericidal concentration
（MBC）.
As a result：It is shown in Table 6.
The contrasting detection result (mg/mL) of 6. antifungic action of table
。
Conclusion：As can be seen from Table 6, the lavipeditum sterilization powder antifungic action of various embodiments of the present invention is substantially better than comparison
Example 2, sodium bicarbonate, camellia seed meal.That is the lavipeditum of various embodiments of the present invention sterilizes powder relative to its primary raw material little Su
It beats, camellia seed meal has improved antifungic action.
Three, skin sensibiligen is tested
Purpose：Observation rabbit intact skin and damaged skin contact the lavipeditum sterilization powder solution of various embodiments of the present invention in a short time
Generated toxic reaction afterwards is product with providing safety foundation.
Method：White New Zealand rabbits 12 are selected, are randomly divided into 3 groups, every group 4.A groups:Complete skin group, B groups:It is damaged
Skin group, C groups:Blank control group.Medicine-feeding part is skin of back, and control group is to distilled water, and test medicine group is to the present invention's
Powder solution is sterilized in the lavipeditum of each embodiment（Concentration：3.35g/ml), powder solution is sterilized in the lavipeditum of various embodiments of the present invention（It is dense
Degree：It 3.35g/ml) is coated directly on intact skin and damaged skin, is fixed coated with polyethylene film, then gauze after applying examination, ensured
Powder solution is sterilized in the lavipeditum of various embodiments of the present invention（Concentration：3.35g/ml) with skin contact after 24 hours, such as non-death by poisoning
It dies, the lavipeditum sterilization powder solution of tested various embodiments of the present invention can be cleaned with warm water or other nonirritant solvents（Concentration：
3.35g/ml).It is observed continuously 7 days, observes and records the systemic toxicity profiles performance to animal after tested material and death condition, packet daily
Include the variation of the weight of animals, skin, hair, eyes and mucous membrane, the change of breathing, cycle, central nervous system, four limbs activity etc.
Change.
As a result：White New Zealand rabbits give the lavipeditum sterilization powder solution of various embodiments of the present invention（Concentration：3.35g/ml)
After have no systemic toxicity profiles performance and death condition, the weight of animals increase, to breathing, cycle, central nervous system, four limbs activity etc.
Without influence.There is slight erythema to damaged skin individual animal and disappears for 24 hours without oedema, after drug withdrawal, medication area drug residue free
Spot.
Conclusion：The lavipeditum of various embodiments of the present invention sterilizes powder to white New Zealand rabbits intact skin and damaged skin without apparent
Toxic reaction.
Four, skin irritation test
Purpose：The skin irritation reaction for detecting the lavipeditum sterilization powder of various embodiments of the present invention, safety is provided for clinical application
Property foundation.
Method：According to《Skin irritation test and skin allergy test guideline》In related requirement carry out.Choosing
With new zealand rabbit 8, it is randomly divided into 2 groups, every group 4.Every animal sets 4 areas：Area, damaged skin administration is administered in intact skin
Area, intact skin check plot, damaged skin check plot.
Medicine-feeding part is skin of back, is lost hair or feathers after surgical scissors cropping, then with 8% vulcanized sodium.It is body surface area per area
3-5%, keep suitable distance between each area.Damaged skin sand paper polishing epidermis, is degree with slight oozing of blood.Area is administered to smear
Powder solution is sterilized in the lavipeditum of various embodiments of the present invention（A concentration of 0.335g/ml）Distilled water is smeared in 1ml, check plot.Two layers of yarn
Cloth covers, and every animal sub-cage rearing, proper method is fixed.Daily give a medicine, each drug effect 4 hours, continuous 7 days,
Observe local reaction.After the last administration, residual tested material is removed with warm water, removes the lavipeditum sterilization powder of various embodiments of the present invention
Solution（A concentration of 0.335g/ml）Afterwards 1h, for 24 hours, 48h, 72h to 7d, observation situations such as whether there is or not erythema and oedema at coating position,
And above-mentioned variation recovery situation and time.
As a result：Family's rabbit skin gives the lavipeditum sterilization powder solution of various embodiments of the present invention（A concentration of 0.335g/ml）Afterwards,
The skin wound repairs such as erythema, oedema are showed no to intact skin and damaged skin.
Conclusion：The lavipeditum sterilization bean sheet jelly skin of various embodiments of the present invention is non-stimulated to complete normal skin and damaged skin
Property.
Five, skin allergy test
Purpose：The allergic reaction for detecting the intact skin of the lavipeditum sterilization powder of various embodiments of the present invention, carries for clinical application
For safety foundation.
Method：According to《Skin irritation test and skin allergy test guideline》In related requirement carry out, examination
Test grouping：Cavy is randomly divided into 3 groups by weight, gender, every group 10, A groups:Powder is sterilized in lavipeditum（A concentration of 0.335g/
ml）, B groups:Negative control group（Distilled water）, C groups:Positive controls（1-CHLORO-2,4-DINITROBENZENE）.Sensitization contact：Take the present invention's
Powder solution is sterilized in the lavipeditum of each embodiment（A concentration of 0.335g/ml）0.1-0.2ml is coated in back hair removal section on the left of animal, uses
Proper method is fixed, and every animal sub-cage rearing continues 6 hours, is repeated once in the same way within the 7th day and the 14th day.Swash
Hair contact：14 days after last dose sensitization, powder solution is sterilized into the lavipeditum of various embodiments of the present invention（A concentration of 0.335g/
ml）0.1-0.2ml is coated in hair removal section on the right side of cavy, removes the lavipeditum sterilization powder solution of various embodiments of the present invention after 6 hours（It is dense
Degree is 0.335g/ml）, at once observe skin allergy situation, then in for 24 hours, 48h, 72h observe result again.
As a result：Cavy gives the lavipeditum sterilization powder solution of various embodiments of the present invention（A concentration of 0.335g/ml）It is examined
After survey, do not find that the allergic reactions such as erythema, oedema occurs in the local skin of tested cavy.
Conclusion：Various embodiments of the present invention lavipeditum sterilization powder without anaphylaxis.
Six, health-care effect
1, it is active to lead to blood：Foot is three yin meridians（Liver and spleen kidney）Beginning, three yang channels（Stomach courage bladder）Whole, foot has more than 60
There are close ties at acupuncture point with the vital organs of the human body.The warm water of the lavipeditum sterilization powder of various embodiments of the present invention steeps foot, and both hands is coordinated to press
It rubs vola, so that the lavipeditum of various embodiments of the present invention is sterilized powder preferably stimulates acupoint of foot and echo area, reaches promoting blood circulation and removing obstruction in channels
Effect.
2, tinea pedis clinical efficacy：
Purpose：The lavipeditum for detecting the embodiment of the present invention 6 sterilizes powder to tinea pedis clinical application curative effect, referring to testing crew tinea pedis disease
Shape is close, has comparison meaning.
Method：4 groups of experiment point：Control group（Ciclopirox olamine cream）, 20, daily external application Ciclopirox olamine cream 2 times is used in conjunction
2 weeks.Experimental group 60, using the embodiment of the present invention 6 and comparative example 1-2 lavipeditum sterilize powder, every group 20.Experimental group is daily
Foot is impregnated with the lavipeditum sterilization powder extracting solution of the embodiment of the present invention 6 and comparative example 1-2 30 minutes, be used in conjunction 2 weeks, user at night
Method：15 grams of lavipeditum sterilization powder of the invention are added in the warm water of foot basin, after stirring evenly, 2 times/day.Observe clinical symptoms
And sign, microscopy and culture fungi, judge curative effect.
As a result：It is shown in Table 7 and table 8.
74 groups of Clinical efficacy comparisons of table
。
84 groups of mycology curative effects of table compare
。
Conclusion：The lavipeditum sterilization powder of various embodiments of the present invention can significantly improve curative effect and fungi clearance rate.
3, moisturizing
Purpose：Camellia seed meal, sodium bicarbonate, sea salt, ginger powder are tested to skin to sufficient face moisturizing effect.
Method：According to embodiment 6, after removal camellia seed meal, sodium bicarbonate, sea salt, ginger powder any one single raw material, group
Pairs of ratio 2, comparative example 3, comparative example 4, comparative example 5, after lavipeditum, situation is felt in sufficient face.
9 embodiment 6 of table and comparative example 2, comparative example 3, comparative example 4, comparative example 5
。
As a result：It see the table below (70 people participate in experiment, are divided into A-G groups, every group of 10 people) shown in 10.
Feel in the application metapedes of table 10 face
。
Conclusion：After any one the single raw material removal of camellia seed meal, sodium bicarbonate, sea salt, ginger powder, hand is washed to formulation product
It is very big that portion feels that pleasant, lubricant effect influences, and wherein comparative example 2 is less comfortable after washing, but is exactly that surface skin is smooth, comparison
Example 4 be feel comfortable after washing, but skin lack it is moist.
Claims (3)
1. powder is sterilized in a kind of lavipeditum, it is characterised in that the raw material matched by following masses part is made：It is 20~30 parts of camellia seed meal, small
60~80 parts of soda, 0.5~1 part of soap powder, 0.5~1 part of atlapulgite, 4~6 parts of sea salt, 0.5~2 part of ginger powder, Chinese honey locust 0.1~3
Part, 0.1~3 part of soapberry, 0.5~1 part of peppermint, 0.5~1 part of rosemary.
2. powder is sterilized in lavipeditum according to claim 1, it is characterised in that be made of following raw materials according：It is 22 parts of camellia seed meal, small
67 parts of soda, 0.5 part of soap powder, 0.9 part of atlapulgite, 4 parts of sea salt, 0.9 part of ginger powder, 2.7 parts of Chinese honey locust, 2.5 parts of soapberry, peppermint
0.8 part, 1 part of rosemary.
3. the preparation method of lavipeditum sterilization powder according to claim 1, it is characterised in that in turn include the following steps：
（1）Take raw material：Raw material is weighed according to the ratio；
（2）It crushes：It by raw material drying, is crushed respectively by pulverizer, obtains each raw material powder；
（3）Mixing：Each raw material powder is mixed, is stirred evenly；
（4）Sterilization：25-35min is sterilized by 120-130 DEG C of hot wind, then non-woven bag packs, obtains finished product lavipeditum sterilization
Powder.
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| CN201810984868.8A CN108704116A (en) | 2018-08-28 | 2018-08-28 | Powder and preparation method thereof is sterilized in lavipeditum |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810984868.8A CN108704116A (en) | 2018-08-28 | 2018-08-28 | Powder and preparation method thereof is sterilized in lavipeditum |
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Family
ID=63873695
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102113983A (en) * | 2011-02-18 | 2011-07-06 | 四川省中医药科学院 | Pure Chinese medicinal health-care bath fluid and preparation method thereof |
| CN104178379A (en) * | 2014-08-08 | 2014-12-03 | 福州喜自然生物科技有限公司 | Natural washing product with strong oil and dirt removal capacity and preparation method of natural washing product with strong oil and dirt removal capacity |
| CN107811937A (en) * | 2017-10-30 | 2018-03-20 | 中盐工程技术研究院有限公司 | It is a kind of to warm the foot bath salt dispeled cold |
| CN107898882A (en) * | 2017-12-22 | 2018-04-13 | 贵州青龙农林股份有限公司 | A kind of soapberry lavipeditum powder and preparation method thereof |
-
2018
- 2018-08-28 CN CN201810984868.8A patent/CN108704116A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102113983A (en) * | 2011-02-18 | 2011-07-06 | 四川省中医药科学院 | Pure Chinese medicinal health-care bath fluid and preparation method thereof |
| CN104178379A (en) * | 2014-08-08 | 2014-12-03 | 福州喜自然生物科技有限公司 | Natural washing product with strong oil and dirt removal capacity and preparation method of natural washing product with strong oil and dirt removal capacity |
| CN107811937A (en) * | 2017-10-30 | 2018-03-20 | 中盐工程技术研究院有限公司 | It is a kind of to warm the foot bath salt dispeled cold |
| CN107898882A (en) * | 2017-12-22 | 2018-04-13 | 贵州青龙农林股份有限公司 | A kind of soapberry lavipeditum powder and preparation method thereof |
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Application publication date: 20181026 |