CN108619062A - Acne-removing composition and its application - Google Patents
Acne-removing composition and its application Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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Abstract
The invention discloses a kind of acne-removing composition and its applications, belong to cosmetic technical field.The acne-removing composition is prepared from the following materials：Tea oil, hamamelis extract, camomile extract, Radix et Caulis Opuntiae Dillenii extract, aloe extract, niacinamide, tea extract, ethyl alcohol and butanediol.Above-mentioned composition addition is little less influence ultimate product appearance and smell in the case of, showing a kind of extraordinary anti-acne convergence pore improves skin quality effect, can make long acne and be easy the skin of long acne to improve comprehensively.The composition contains the ethyl alcohol and butanediol of sufficient amount, and the composition is made not have to that preservative is added, and for no anticorrosive composite, the trend of ecosystem is pursued in fitting instantly；And the composition is almost colourless, smell is very light, and addition is convenient, can be widely used in all kinds of cosmetics.
Description
Technical field
The present invention relates to cosmetic technical fields, more particularly to a kind of acne-removing composition and its preparation method and application.
Background technology
Acne, also known as small pox or whelk occur mainly to block, carefully with hypersteatosis, pilosebaceous duct
Bacterium infects related with inflammatory reaction etc..And long acne can be coarse with pore, there are pockmark, skin sensitivity, skin quality is poor, and prognosis is not
It is good, it is formed the skin quality that small pox easily occurs in the course of time.
Have many anti-acne class product mixes at present, but such product is usually processed just for small pox, to desalination acne print,
Pore refining, improvement skin quality etc. are ineffective；Or with raw materials used of high cost, have compared with dark colour, there is larger smell,
It is not easy to maintain, the problems such as long-term effect is not known.
Invention content
The purpose of the present invention, exactly overcome the deficiencies of the prior art and provide a kind of acne-removing composition and preparation method thereof and
Using the acne-removing composition cost of material is low, has preferable anti-acne effect, and in anti-acne while energy pore refining, improve skin
Matter.
In order to achieve the above object, it adopts the following technical scheme that：
A kind of acne-removing composition, is prepared from the following materials：Tea oil, hamamelis extract, camomile extract, celestial being
People slaps extract, aloe extract, niacinamide, tea extract, ethyl alcohol and butanediol.
In above-mentioned acne-removing composition, tea oil and Radix et Caulis Opuntiae Dillenii extract play the effect that anti-acne is sterilized, hamamelis extract
Have effects that restrain pore, aloe extract and niacinamide can desalinate acne print trace, and tea extract and aloe can moisten
Skin restores skin normal physiological function, it is made to be not easy again long acne.Above-mentioned raw materials cooperate, respectively from different angles to Cuo
Sore prevents and treats, and plays synergistic effect.
The composition is prepared by the raw material of following mass fraction in one of the embodiments,：
Combine each raw material with said ratio, there is the anti-acne effect of preferable anti-acne, and because the ethyl alcohol containing sufficient amount and
Butanediol makes the composition it is not necessary that preservative is added, for no anticorrosive composite.
The composition is prepared by the raw material of following mass fraction in one of the embodiments,：
The tea oil is the oily ingredient extracted in tea free in one of the embodiments,；The witch hazel extraction
Object is the extract of witch hazel complete stool；The camomile extract is the extract of chamomile complete stool；The Radix et Caulis Opuntiae Dillenii extract
For the extract of cactus complete stool；The aloe extract is the extract of aloe barbadensis Miller complete stool.
The tea oil is the oily ingredient that ethyl alcohol extraction extracts in tea free in one of the embodiments,；It is described
It with solid-liquid ratio is 1 that hamamelis extract, which is witch hazel complete stool,:5 addition volume ratios are 1:2 water：Butanediol mixed solvent, 15
~25 DEG C of Microwave Extractions, after recycling design to obtain the final product；It with solid-liquid ratio is 1 that the camomile extract, which is chamomile complete stool,:5 are added body
Product is than being 1:2 water：Butanediol mixed solvent, after 15~25 DEG C of Microwave Extractions, recycling design to obtain the final product；The cactus carries
It with solid-liquid ratio is 1 that take object, which be cactus complete stool,:5 addition volume ratios are 1:2 water：Butanediol mixed solvent, it is micro- at 15~25 DEG C
Wave extracts, after recycling design to obtain the final product；It with solid-liquid ratio is 1 that the aloe extract, which is aloe barbadensis Miller complete stool,:5, which are added volume ratios, is
1:2 water：Butanediol mixed solvent, after 15~25 DEG C of Microwave Extractions, recycling design to obtain the final product；The tea extract is tealeaves
With solid-liquid ratio for 1:5 addition volume ratios are 1:2 water：Butanediol mixed solvent, in 15~25 DEG C of Microwave Extractions, recycling design
Afterwards to obtain the final product.
Each raw material is extracted using aforesaid way, can preferably propose wherein active constituent, have preferable effect.
The invention also discloses the preparation methods of above-mentioned acne-removing composition, include the following steps：By the tea tree of predetermined amount
Oil, hamamelis extract, camomile extract, Radix et Caulis Opuntiae Dillenii extract, aloe extract, niacinamide, tea extract be added to
In ethyl alcohol and butanediol, dissolve and be uniformly mixed to get.
Above-mentioned preparation method, due to containing certain ethyl alcohol and butanediol in composition, when preparation, need not additionally incorporate
Solubilizer, room temperature simple agitation can prepare.Have the advantages that process is simple, stablizes.
The invention also discloses application of the above-mentioned acne-removing composition in preparing cosmetics.
Above-mentioned acne-removing composition not only has excellent cooperative synergism effect, and also almost colourless, smell is very light, addition side
Just, it can be widely used in all kinds of cosmetics.
The cosmetics include toner, lotion, emulsifiable paste, newborn gel, facial cleanser, BB frosts in one of the embodiments,.
In one of the embodiments, it is described it is used for cosmetic in prevent and improve there are the skin conditions of acne problems.
Compared with prior art, the beneficial effects of the present invention are：
In the acne-removing composition of the present invention, tea oil and Radix et Caulis Opuntiae Dillenii extract play the effect that anti-acne is sterilized, and witch hazel carries
Object is taken to have effects that restrain pore, aloe extract and niacinamide can desalinate acne print trace, and tea extract and aloe can
Moisturizing restores skin normal physiological function, it is made to be not easy again long acne.Above-mentioned composition is little in addition, less influences eventually
In the case of pole product appearance and smell, showing a kind of extraordinary anti-acne convergence pore improves skin quality effect, can make long acne
Improve comprehensively with the skin for being easy long acne.The composition contains the ethyl alcohol and butanediol of sufficient amount, and the composition is made not have to be added
Preservative meets the trend for pursuing ecosystem instantly for no anticorrosive composite；And the composition is almost colourless, smell is very light, adds
Add conveniently, can be widely used in all kinds of cosmetics.
Specific implementation mode
Below in conjunction with specific implementation method, the present invention will be described in detail, is used in the exemplary embodiment and description of the present invention
Explain the present invention, but not as a limitation of the invention.
During following embodiment is raw materials used, tea oil is the oily ingredient extracted with ethyl alcohol extraction in tea free；Golden thread
Prunus mume extract is the extract of witch hazel complete stool water distillation；Camomile extract is the extract of chamomile complete stool water distillation；It is celestial
People slaps the extract that extract is the distillation of cactus complete stool water；Aloe extract is the extraction of aloe barbadensis Miller complete stool water distillation
Object；Tea extract is the extract of Aqua Folium Camelliae sinensis distillation, respectively with solid-liquid ratio for 1:5 addition volume ratios are 1:2 water：Fourth two
Alcohol mixed solvent impregnates 8-24hr, then in 15~25 DEG C of Microwave Extractions 2-3 hours, after recycling design to obtain the final product,.
Remaining raw material is commercially available.
Embodiment 1
A kind of acne-removing composition, is prepared from the following materials：
The preparation method of above-mentioned acne-removing composition is as follows：、
Weigh tea oil, hamamelis extract, camomile extract, Radix et Caulis Opuntiae Dillenii extract, aloe extract, niacinamide and
Tea extract adds ethyl alcohol, butanediol and deionized water, dissolves, stirs evenly to get acne-removing composition.
Embodiment 2
A kind of composition in acne-removing composition and embodiment 1 is essentially identical, differ only in, and wherein tea oil contains
Amount is 0.1%.
Embodiment 3
A kind of composition in acne-removing composition and embodiment 1 is essentially identical, differ only in, and wherein niacinamide contains
Amount is 0.3%.
Embodiment 4
A kind of comprehensive anti-acne U.S. flesh emulsifiable paste, is prepared by the following method to obtain：
It is prepared by water phase：5% glycerine and 3%1.3- butanediols are added in deionized water, stir by the deionized water for taking 61.1%
After mixing dissolving, it is warming up to 70~75 DEG C, it is spare；
It is prepared by oil phase：By 2% cetostearyl alcohol, 1% ceteareth -6,2% polyethers -25,5% saualane, 8%
Octyl-decyl glyceryl ester, 2% octyl heptamethyltrisiloxane is added oil phase, 75~80 degree is warming up under stirring and is melted, standby
With；
Mixing：The oil phase is added to the aqueous phase stirs homogeneous 10 minutes, and 40 DEG C are cooled under stirring, adds 0.1% essence,
0.5% Microcare, 9010 (preservatives：Phenoxyethanol and Sensiva SC50), what the embodiment 1 of 10wt% was prepared
Acne-removing composition stirs 5 minutes.Being eventually adding 0.3%Aristoflex AVC, (acrylamide dimethyltaurine ammonium/VP is total
Polymers) homogeneous stir 10 minutes, be cooled to 35 DEG C to get.
Embodiment 5
A kind of comprehensive anti-acne U.S. flesh breast gel, is prepared by the following method to obtain：
Take 72.1% deionized water, 8% glycerine, 5%1.3- butanediols, 0.05%EDTA Na2, stirring and dissolving is good, stirs
It mixes down and is slowly added into 0.2% card wave 940, stir 30 minutes；Then 0.1% xanthan gum is added to stir 20 minutes, 3% reed fragrant plant is added
Glue oil, 0.8%PEG-40 rilanit specials, 0.1% essence, 9010 (preservatives of 0.5%Microcare：Phenoxyethanol and second
Base hexyl glycerine) homogeneous stirs 5 minutes, it is added the acne-removing composition that the embodiment 1 of 10wt% is prepared, homogeneous stirs 5 points
Clock, be eventually adding 0.2% triethanolamine stir 5 minutes to get.
Comparative example 1
A kind of composition in composition and embodiment 1 is essentially identical, differs only in, 1 anti-acne group of embodiment is omitted
Close the witch hazel in object.
Comparative example 2
A kind of composition in composition and embodiment 1 is essentially identical, differs only in, 1 anti-acne group of embodiment is omitted
Close the aloe in object.
Comparative example 3
A kind of composition in composition and embodiment 1 is essentially identical, differs only in, implementation is substituted with salicylic acid
Tea oil in 1 acne-removing composition of example.
Comparative example 4
A kind of commercially available product for resolving poxes, mark ingredient are：Water, propylene glycol, isopropyl myristate, stereth -21 are stearic
Alcohol polyethers -2, stearine, cetostearyl alcohol support leaf rheum officinale root extract, saualane, polydimethyl siloxane fluid, hydroxypropyl
Starch phosphate, peony root extractive, Tocopherol acetate ester, chapter brain, peppermint, Chinese corktree extract, methyl hydroxybenzoate, benzene oxygen second
Alcohol.
Comparative example 5
A kind of emulsifiable paste and comprehensive anti-acne U.S. flesh emulsifiable paste of embodiment 4 are essentially identical, differ only in：Implementation is not added
The acne-removing composition that example 1 is prepared.
Comparative example 6
A kind of comprehensive anti-acne U.S. flesh emulsifiable paste and comprehensive anti-acne U.S. flesh emulsifiable paste of embodiment 4 are essentially identical, differ only in,
Using 1 acne-removing composition of composition alternate embodiment in comparative example 1.
Comparative example 7
A kind of comprehensive anti-acne U.S. flesh emulsifiable paste and comprehensive anti-acne U.S. flesh emulsifiable paste of embodiment 4 are essentially identical, differ only in,
Using 1 acne-removing composition of composition alternate embodiment in comparative example 2.
Comparative example 8
A kind of comprehensive anti-acne U.S. flesh emulsifiable paste and comprehensive anti-acne U.S. flesh emulsifiable paste of embodiment 4 are essentially identical, differ only in,
Using 1 acne-removing composition of composition alternate embodiment in comparative example 3.
Experimental example 1
Propionibacterium acnes bacteriostatic test.
The composition that above-described embodiment and comparative example are prepared carries out propionibacterium acnes bacteriostatic test.
One, method.
With culture medium, bacterium solution prepares and inocalation method, is tested according to 2015 editions operations of cosmetics health specification.
Two, result.
The results are shown in table below：
1. propionibacterium acnes bacteriostatic test result of table
| Group | Concentration (wt%) | Antibacterial degree (%) |
| 1 composition of embodiment | 1% | 98% |
| 1 composition of embodiment | 2% | 100% |
| 1 composition of embodiment | 3% | 100% |
| 2 composition of embodiment | 1% | 85% |
| 2 composition of embodiment | 2% | 90% |
| 2 composition of embodiment | 3% | 97% |
| 3 composition of comparative example | 1% | 80% |
| 3 composition of comparative example | 2% | 86% |
| 3 composition of comparative example | 3% | 90% |
| 4 composition of comparative example | 1% | 90% |
| 4 composition of comparative example | 2% | 95% |
| 4 composition of comparative example | 3% | 100% |
It can be seen that in from the above：The composition of embodiment 1 has a good bacteriostasis efficacy, and low concentration just have it is bright
Aobvious fungistatic effect.And content of the embodiment 2 due to reducing tea oil, fungistatic effect are poor.In comparative example 3 as a result of
Salicylic acid can not reach preferable effect instead of tea oil.
Experimental example 2
The observation experiment of subject's spread compositions aqueous solution.
Choosing 25 has pore coarse and 20~45 years old personnel of acne print, smears embodiment and comparative example daily and is prepared
Composition solution, it is continuous to smear 28 days, then analyzed with skin image analysis system, the results are shown in table below.
2. subject composition of table observes test result
| Group | Concentration (wt%) | Pore restrains (%) | Acne print pigment is thin out (%) |
| 1 composition of embodiment | 10% | 33% | 36% |
| 1 composition of comparative example | 10% | 15% | 18% |
| 2 composition of comparative example | 10% | 23% | 20% |
| 3 composition of comparative example | 10% | 26% | 28% |
Note：Pore convergence refers to：Pore average diameter is obviously reduced than original, and skin polishes.
Acne print pigment is thin out：Pigmentation caused by small pox is thin out, replys original surrounding skin color
As can be seen that the composition of embodiment 1 has best pore convergence and the thin out effect of acne print in from the above
Fruit, and the composition of comparative example 1-3, since the ingredient of selection is different, effect is poor.
Experimental example 3
Subject smears emulsifiable paste observation experiment.
Object on probation：The crowd of 20~45 years old face head's acnes, has acne print and claims easy long acne.
Every group of 15 people, try out different emulsifiable pastes 15 days respectively, and process on probation cannot use other any product for resolving poxes and cosmetics,
The results are shown in table below.
3. subject's emulsifiable paste of table observes test result
Note：Anti-acne is notable：Refer to most of small poxs to subside, replys original skin state
Anti-acne is effective：Finger has small part small pox recession, part to reply original skin state substantially
Anti-acne is invalid：Refer to no any small pox to subside, or continues have small pox generation
It is notable that skin replys water profit：It is full that the state that finger skin follows the string from water deficient is completely recovered to moisture abundance
Moist state.
It is effective that skin replys water profit：It is substantially sufficient but full to refer to the state recovery moisture that skin follows the string from water deficient
Full scale is inadequate
It is invalid that skin replys water profit：Referring to the state that skin follows the string from water deficient does not have any recovery, with original one
Sample.
As can be seen that the composition of embodiment 4 and 5 has the best long acne crowd skin condition of improvement in from the above
Effect, and the composition of comparative example 4-8, since the ingredient of selection is different, effect is poor.
It is provided for the embodiments of the invention technical solution above to be described in detail, specific case used herein
The principle and embodiment of the embodiment of the present invention are expounded, the explanation of above example is only applicable to help to understand this
The principle of inventive embodiments；Meanwhile for those of ordinary skill in the art, embodiment according to the present invention, in specific embodiment party
There will be changes in formula and application range, in conclusion the content of the present specification should not be construed as limiting the invention.
Claims (9)
1. a kind of acne-removing composition, which is characterized in that be prepared from the following materials：Tea oil, hamamelis extract, chamomile
Extract, Radix et Caulis Opuntiae Dillenii extract, aloe extract, niacinamide, tea extract, ethyl alcohol and butanediol.
2. acne-removing composition according to claim 1, it is characterised in that：It is prepared by the raw material of following mass fraction：
3. acne-removing composition according to claim 2, it is characterised in that：It is prepared by the raw material of following mass fraction：
4. according to claim 1-3 any one of them acne-removing compositions, it is characterised in that：
The tea oil is the oily ingredient extracted in tea free；
The hamamelis extract is the extract of witch hazel complete stool；
The camomile extract is the extract of chamomile complete stool；
The Radix et Caulis Opuntiae Dillenii extract is the extract of cactus complete stool；
The aloe extract is the extract of aloe barbadensis Miller complete stool.
5. acne-removing composition according to claim 3, it is characterised in that：
The tea oil is the oily ingredient extracted with ethyl alcohol extraction in tea free.
It with solid-liquid ratio is 1 that the hamamelis extract, which is witch hazel complete stool,:5 addition volume ratios are 1:2 water：Butanediol mixing is molten
Agent, after 15~25 DEG C of Microwave Extractions, recycling design to obtain the final product；
It with solid-liquid ratio is 1 that the camomile extract, which is chamomile complete stool,:5 addition volume ratios are 1:2 water：Butanediol mixing is molten
Agent, after 15~25 DEG C of Microwave Extractions, recycling design to obtain the final product；
It with solid-liquid ratio is 1 that the Radix et Caulis Opuntiae Dillenii extract, which is cactus complete stool,:5 addition volume ratios are 1:2 water：Butanediol mixing is molten
Agent, after 15~25 DEG C of Microwave Extractions, recycling design to obtain the final product；
It with solid-liquid ratio is 1 that the aloe extract, which is aloe barbadensis Miller complete stool,:5 addition volume ratios are 1:2 water：Butanediol mixes
Solvent, after 15~25 DEG C of Microwave Extractions, recycling design to obtain the final product；
It with solid-liquid ratio is 1 that the tea extract, which is tealeaves,:5 addition volume ratios are 1:2 water：Butanediol mixed solvent, 15
~25 DEG C of Microwave Extractions, after recycling design to obtain the final product.
6. the preparation method of claim 1-5 any one of them acne-removing compositions, which is characterized in that include the following steps：It will
Tea oil, hamamelis extract, camomile extract, Radix et Caulis Opuntiae Dillenii extract, aloe extract, niacinamide, the tealeaves of predetermined amount
Extract is added into ethyl alcohol and butanediol, dissolve and be uniformly mixed to get.
7. application of the claim 1-5 any one of them acne-removing compositions in preparing cosmetics.
8. application of the acne-removing composition according to claim 7 in preparing cosmetics, it is characterised in that：The cosmetics
Including toner, lotion, emulsifiable paste, newborn gel, facial cleanser, BB frosts.
9. application of the acne-removing composition according to claim 7 in preparing cosmetics, it is characterised in that：The cosmetics
For preventing and improving the skin conditions there are acne problems.
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| CN201810784707.4A CN108619062B (en) | 2018-07-17 | 2018-07-17 | Acne-removing composition and application thereof |
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| CN201810784707.4A CN108619062B (en) | 2018-07-17 | 2018-07-17 | Acne-removing composition and application thereof |
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| CN1219880A (en) * | 1996-03-25 | 1999-06-16 | 第一曼司达投资有限公司 | Acne treatment |
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| CN108619062B (en) | 2020-06-19 |
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