CN108587494A - A kind of glutinous rice glue and preparation method thereof with sedative action - Google Patents
A kind of glutinous rice glue and preparation method thereof with sedative action Download PDFInfo
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- CN108587494A CN108587494A CN201810831196.7A CN201810831196A CN108587494A CN 108587494 A CN108587494 A CN 108587494A CN 201810831196 A CN201810831196 A CN 201810831196A CN 108587494 A CN108587494 A CN 108587494A
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- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
- C09J4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09J159/00 - C09J187/00
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
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- A61L9/16—Disinfection, sterilisation or deodorisation of air using physical phenomena
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- C08B30/00—Preparation of starch, degraded or non-chemically modified starch, amylose, or amylopectin
- C08B30/12—Degraded, destructured or non-chemically modified starch, e.g. mechanically, enzymatically or by irradiation; Bleaching of starch
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
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Abstract
The invention discloses a kind of glutinous rice glues with sedative action, include the raw material of following parts by weight：Pre-process 30~50 parts of glutinous rice, 10~20 parts of potato, 15~25 parts of cornstarch, 3~7 parts of alum, 6~9 parts of acrylic acid, modified 8~12 parts of bamboo powder, 4~6 parts of lignin, 2~4 parts of citric acid, 3~5 parts of glucolactone, 2~4 parts of anionic additive, 2~5 parts of sorbierite, 1~2 part of lavender extracting solution, 1.3~2.7 parts of rose extracting solution, India 2~3 parts of extracting solution of flower, 3~6 parts of mixture of Chinese herbal medicines of sterilization, 3~5 parts of tackifier.Proportioning of the present invention by controlling between raw material and raw material, the product prepared does not discharge volatile organic matter, non-toxic to humans, and the caking property of glutinous rice glue is strong, has excellent bactericidal mould proof effect to the common mould of wallpaper, effectively improves its service life.
Description
Technical field
The invention belongs to glutinous rice glue technical fields, and in particular to a kind of glutinous rice glue and its preparation side with sedative action
Method.
Background technology
Instantly, requirement of the people for finishing material is higher and higher, and the environmental-protecting performance of finishing material considers as many people
One of necessary condition.Plank etc. gradually replaces the materials such as traditional calcimine, paint, and wallpaper etc. is with its good use
The performances such as property, the feature of environmental protection and dicoration, are also increasingly widely used by people, and wallpaper is adhered on plank and is often made with
Adhesive glue is sticked together, and general adhesive glue all can largely use the organic solvents such as formaldehyde substantially, can be caused greatly to human body
Harm.
Glutinous rice glue is also referred to as glutinous rice glue, be with pure natural glutinous rice or glutinous rice is raw material, by glutinous rice purification, grinding, dry etc.
12 procedures and the environment-protective adhesive formed, applied widely, viscosity is long.
But the viscosity of traditional glutinous rice glue generally existing is low, anti-aging bad, storage thickens the phenomenon that is hardened, and appearance is not
Good, frost resistance poorly causes viscosity to decline, high expensive and construction when impregnation it is laborious the problems such as.
The patent of application publication number CN107057603A discloses a kind of child room special environment protection glutinous rice rubber powder and its processing
Method is process by following step：It is steamed, HIGH PRESSURE TREATMENT, microwave treatment, immersion, primary drying, tabletting, redrying, close
Package fills.Child room special environment protection glutinous rice rubber powder provided by the invention, the raw material of use is environmentally protective, it is organic not discharge volatility
Object, non-toxic to humans, the caking property of glutinous rice rubber powder is strong, has excellent bactericidal mould proof effect to the common mould of wallpaper, has
Effect improves its service life.But preparation process is complicated, low production efficiency.
Invention content
The glutinous rice glue and preparation method thereof with sedative action that the present invention provides a kind of, solves asking in background technology
Topic, the proportioning of the present invention by controlling between raw material and raw material, the product prepared does not discharge volatile organic matter, to people
Body is nontoxic, and the caking property of glutinous rice glue is strong, has excellent bactericidal mould proof effect to the common mould of wallpaper, effectively improving it makes
Use the service life.
It is of the existing technology in order to solve the problems, such as, it adopts the following technical scheme that：
A kind of glutinous rice glue with sedative action, includes the raw material of following parts by weight：Pre-process 30~50 parts of glutinous rice, potato 10
~20 parts, 15~25 parts of cornstarch, 3~7 parts of alum, 6~9 parts of acrylic acid, modified 8~12 parts of bamboo powder, 4~6 parts of lignin,
2~4 parts of citric acid, 3~5 parts of glucolactone, 2~4 parts of anionic additive, 2~5 parts of sorbierite, lavender extracting solution 1
~2 parts, 1.3~2.7 parts of rose extracting solution, India flower 2~3 parts of extracting solution, sterilization 3~6 parts of mixture of Chinese herbal medicines, tackifier 3
~5 parts.
Preferably, the glutinous rice glue with sedative action, includes the raw material of following parts by weight：Pre-process glutinous rice 35~45
Part, 12~17 parts of potato, 18~23 parts of cornstarch, 4~6 parts of alum, 7~8 parts of acrylic acid, modified 9~11 parts of bamboo powder, wood
4.3~5.2 parts of quality, 2.4~3.2 parts of citric acid, 3.5~4.5 parts of glucolactone, anionic additive 2.8~3.3
Part, 3~4 parts of sorbierite, 1.2~1.7 parts of lavender extracting solution, 1.5~2.5 parts of rose extracting solution, India flower extracting solution 2.1~
2.9 parts, sterilization 4~5 parts of mixture of Chinese herbal medicines, 3.6~4.2 parts of tackifier.
Preferably, the glutinous rice glue with sedative action, includes the raw material of following parts by weight：Including following parts by weight
Raw material：Pre-process 40 parts of glutinous rice, 15 parts of potato, 21 parts of cornstarch, 5 parts of alum, 7.6 parts of acrylic acid, modified 10 parts of bamboo powder,
4.8 parts of lignin, 3.8 parts of glucolactone, 3.2 parts of anionic additive, 3.4 parts of sorbierite, smokes clothing at 2.7 parts of citric acid
1.6 parts of careless extracting solution, 2 parts of rose extracting solution, India 2.3 parts of extracting solution of flower, 4.4 parts of mixture of Chinese herbal medicines of sterilization, tackifier 3.9
Part.
Preferably, the preparation method of the pretreatment glutinous rice is as follows：
By glutinous rice be put into glacial acetic acid it is molten in, be warming up to 50~55 DEG C, ultrasonication power be 900~1100W under conditions of
It handles 15min and obtains the pretreatment glutinous rice after taking-up is dried.
Preferably, the preparation method of the modified bamboo powder is as follows：
Bamboo powder is impregnated 4 hours in a concentration of 4% dilute nitric acid solution, it is ultrasonic under supersonic frequency 22kHz, power 80W
Processing 20 minutes, is then added with stirring equivalent Sodium Polyacrylate, is warming up to 80 DEG C and reacts 50 minutes, filters after reaction,
Filter cake is washed three times, is most less than 5% through oven drying to moisture up to the modified starch afterwards.
Preferably, the anionic additive includes the raw material of following parts by weight：5 parts of tourmaline, lanthanide rare complex salt
5 parts of 10 parts of class, 6 parts of nano-titanium dioxide and Tourmaline mountain flour.
Preferably, the Fungicidai mixtures are the mixture of garlic, purslane, Chinese cassia tree, camphor ball and tulip, described big
Garlic, purslane, Chinese cassia tree, camphor ball and the mass ratio of tulip are 1:2:1:3:1.
Preferably, the tackifier are any one of food-grade acetylation diacid double sodium starch, maltodextrins.
A method of the glutinous rice glue with sedative action is prepared, is included the following steps：
（1）By above-mentioned formula weigh pretreatment glutinous rice, potato, cornstarch, alum, acrylic acid, modified bamboo powder, lignin,
Citric acid, glucolactone, anionic additive, sorbierite, lavender extracting solution, rose extracting solution, India flower extracting solution,
Mixture of Chinese herbal medicines, tackifier are sterilized, it is spare；
（2）By peeling potatoes, it is cut into small pieces, then is cooked using water vapour, then smashed to pieces, prepares mashed potato；
（3）Pretreatment glutinous rice, mashed potato, cornstarch and alum are mixed, added water, until water content is 60% in its material,
It is stirred, heats while stirring, be warming up to 70~80 DEG C, then acrylic acid, modified bamboo powder, wood is added in insulated and stirred 2 hours
Quality, citric acid, glucolactone and sorbierite, are uniformly mixed, and are then gelatinized, and gelatinization product is obtained；
（4）Surplus stock is added to step（4）In the gelatinization product of gained, high speed dispersion is uniform, and packaging has to get described
The glutinous rice glue of sedative action.
Preferably, the step（3）The speed of middle stirring is 30r/min.
Compared with prior art, the present invention it has the advantages that：
（1）The present invention is using pretreatment glutinous rice, potato, cornstarch, alum, acrylic acid, modified bamboo powder, lignin, lemon
Acid, glucolactone, anionic additive, sorbierite, lavender extracting solution, rose extracting solution, India flower extracting solution, sterilization
Mixture of Chinese herbal medicines, tackifier etc. are used as raw material, and the raw material of use is environmentally protective, does not discharge volatile organic matter, to human body without
Poison is harmless, and the caking property for preparing glutinous rice glue is strong, has excellent bactericidal mould proof effect to the common mould of wallpaper, effectively improves it
Service life；
（2）The present invention by pre-process glutinous rice, potato, cornstarch, alum, etc. a variety of specified raw material glue compounding energy
Its adhesive property is effectively improved, also, further combined with the pretreatment glutinous rice provided in the present invention, it is viscous can preferably to improve it
The performances such as knot；
（3）It is mixed that the present invention is added to lavender extracting solution, rose extracting solution, India flower extracting solution, sterilization Chinese herbal medicine in the feed
Object is closed, the extracts of Chinese herbal medicine is the mixture of garlic, purslane, Chinese cassia tree, camphor ball and tulip, and anion addition
Agent mutually acts synergistically, and can resist a variety of germs, to improve the antibiotic property of product, lavender extracting solution, rose extracting solution,
India spends extracting solution and anionic additive mutually to act synergistically, and the glutinous rice glue prepared can discharge anion and fragrance, tool
Play the role of purifying air, tranquilizing the mind.
Specific implementation mode
Present invention will be further explained below with reference to specific examples.These embodiments are merely to illustrate the present invention and do not have to
In limiting the scope of the invention.
Embodiment 1
The present embodiment is related to a kind of glutinous rice glue with sedative action, includes the raw material of following parts by weight：30 parts of glutinous rice of pretreatment,
10 parts of potato, 15 parts of cornstarch, 3 parts of alum, 6 parts of acrylic acid, modified 8 parts of bamboo powder, 4 parts of lignin, 2 parts of citric acid, Portugal
3 parts of grape saccharic acid lactone, 2 parts of anionic additive, 2 parts of sorbierite, 1 part of lavender extracting solution, 1.3 parts of rose extracting solution, India
2 parts of extracting solution of flower, 3 parts of mixture of Chinese herbal medicines of sterilization, 3 parts of tackifier.
Wherein, the preparation method of the pretreatment glutinous rice is as follows：
By glutinous rice be put into glacial acetic acid it is molten in, be warming up to 50 DEG C, ultrasonication power be 900W under conditions of handle 15min,
After taking-up is dried, the pretreatment glutinous rice is obtained.
Wherein, the preparation method of the modified bamboo powder is as follows：
Bamboo powder is impregnated 4 hours in a concentration of 4% dilute nitric acid solution, it is ultrasonic under supersonic frequency 22kHz, power 80W
Processing 20 minutes, is then added with stirring equivalent Sodium Polyacrylate, is warming up to 80 DEG C and reacts 50 minutes, filters after reaction,
Filter cake is washed three times, is most less than 5% through oven drying to moisture up to the modified starch afterwards.
Wherein, the anionic additive includes the raw material of following parts by weight：5 parts of tourmaline, lanthanide rare composite salt
5 parts of 10 parts, 6 parts of nano-titanium dioxide and Tourmaline mountain flour.
Wherein, the Fungicidai mixtures are the mixture of garlic, purslane, Chinese cassia tree, camphor ball and tulip, described big
Garlic, purslane, Chinese cassia tree, camphor ball and the mass ratio of tulip are 1:2:1:3:1.
Wherein, the tackifier are the double sodium starch of food-grade acetylation diacid.
A method of the glutinous rice glue with sedative action is prepared, is included the following steps：
（1）By above-mentioned formula weigh pretreatment glutinous rice, potato, cornstarch, alum, acrylic acid, modified bamboo powder, lignin,
Citric acid, glucolactone, anionic additive, sorbierite, lavender extracting solution, rose extracting solution, India flower extracting solution,
Mixture of Chinese herbal medicines, tackifier are sterilized, it is spare；
（2）By peeling potatoes, it is cut into small pieces, then is cooked using water vapour, then smashed to pieces, prepares mashed potato；
（3）Pretreatment glutinous rice, mashed potato, cornstarch and alum are mixed, added water, until water content is 60% in its material,
It is stirred, heats while stirring, be warming up to 70 DEG C, then insulated and stirred 2 hours is added acrylic acid, is modified bamboo powder, is wooden
Element, citric acid, glucolactone and sorbierite, are uniformly mixed, and are then gelatinized, and gelatinization product is obtained；
（4）Surplus stock is added to step（4）In the gelatinization product of gained, high speed dispersion is uniform, and packaging has to get described
The glutinous rice glue of sedative action.
Wherein, the step（3）The speed of middle stirring is 30r/min.
Embodiment 2
The present embodiment is related to a kind of glutinous rice glue with sedative action, includes the raw material of following parts by weight：50 parts of glutinous rice of pretreatment,
20 parts of potato, 25 parts of cornstarch, 7 parts of alum, 9 parts of acrylic acid, modified 12 parts of bamboo powder, 6 parts of lignin, 4 parts of citric acid, Portugal
5 parts of grape saccharic acid lactone, 4 parts of anionic additive, 5 parts of sorbierite, 2 parts of lavender extracting solution, 2.7 parts of rose extracting solution, India
3 parts of extracting solution of flower, 6 parts of mixture of Chinese herbal medicines of sterilization, 5 parts of tackifier.
Wherein, the preparation method of the pretreatment glutinous rice is as follows：
By glutinous rice be put into glacial acetic acid it is molten in, be warming up to 55 DEG C, ultrasonication power be 1100W under conditions of handle 15min,
After taking-up is dried, the pretreatment glutinous rice is obtained.
Wherein, the preparation method of the modified bamboo powder is as follows：
Bamboo powder is impregnated 4 hours in a concentration of 4% dilute nitric acid solution, it is ultrasonic under supersonic frequency 22kHz, power 80W
Processing 20 minutes, is then added with stirring equivalent Sodium Polyacrylate, is warming up to 80 DEG C and reacts 50 minutes, filters after reaction,
Filter cake is washed three times, is most less than 5% through oven drying to moisture up to the modified starch afterwards.
Wherein, the anionic additive includes the raw material of following parts by weight：5 parts of tourmaline, lanthanide rare composite salt
5 parts of 10 parts, 6 parts of nano-titanium dioxide and Tourmaline mountain flour.
Wherein, the Fungicidai mixtures are the mixture of garlic, purslane, Chinese cassia tree, camphor ball and tulip, described big
Garlic, purslane, Chinese cassia tree, camphor ball and the mass ratio of tulip are 1:2:1:3:1.
Wherein, the tackifier are maltodextrin.
A method of the glutinous rice glue with sedative action is prepared, is included the following steps：
（1）By above-mentioned formula weigh pretreatment glutinous rice, potato, cornstarch, alum, acrylic acid, modified bamboo powder, lignin,
Citric acid, glucolactone, anionic additive, sorbierite, lavender extracting solution, rose extracting solution, India flower extracting solution,
Mixture of Chinese herbal medicines, tackifier are sterilized, it is spare；
（2）By peeling potatoes, it is cut into small pieces, then is cooked using water vapour, then smashed to pieces, prepares mashed potato；
（3）Pretreatment glutinous rice, mashed potato, cornstarch and alum are mixed, added water, until water content is 60% in its material,
It is stirred, heats while stirring, be warming up to 80 DEG C, then insulated and stirred 2 hours is added acrylic acid, is modified bamboo powder, is wooden
Element, citric acid, glucolactone and sorbierite, are uniformly mixed, and are then gelatinized, and gelatinization product is obtained；
（4）Surplus stock is added to step（4）In the gelatinization product of gained, high speed dispersion is uniform, and packaging has to get described
The glutinous rice glue of sedative action.
Wherein, the step（3）The speed of middle stirring is 30r/min.
Embodiment 3
The present embodiment is related to a kind of glutinous rice glue with sedative action, includes the raw material of following parts by weight：35 parts of glutinous rice of pretreatment,
12 parts of potato, 18 parts of cornstarch, 4 parts of alum, 7 parts of acrylic acid, modified 9 parts of bamboo powder, 4.3 parts of lignin, citric acid 2.4
Part, 3.5 parts of glucolactone, 2.8 parts of anionic additive, 3 parts of sorbierite, 1.2 parts of lavender extracting solution, rose extracting solution
1.5 parts, India flower 2.1 parts of extracting solution, sterilization 4 parts of mixture of Chinese herbal medicines, 3.6 parts of tackifier.
Wherein, the preparation method of the pretreatment glutinous rice is as follows：
By glutinous rice be put into glacial acetic acid it is molten in, be warming up to 52 DEG C, ultrasonication power be 950W under conditions of handle 15min,
After taking-up is dried, the pretreatment glutinous rice is obtained.
Wherein, the preparation method of the modified bamboo powder is as follows：
Bamboo powder is impregnated 4 hours in a concentration of 4% dilute nitric acid solution, it is ultrasonic under supersonic frequency 22kHz, power 80W
Processing 20 minutes, is then added with stirring equivalent Sodium Polyacrylate, is warming up to 80 DEG C and reacts 50 minutes, filters after reaction,
Filter cake is washed three times, is most less than 5% through oven drying to moisture up to the modified starch afterwards.
Wherein, the anionic additive includes the raw material of following parts by weight：5 parts of tourmaline, lanthanide rare composite salt
5 parts of 10 parts, 6 parts of nano-titanium dioxide and Tourmaline mountain flour.
Wherein, the Fungicidai mixtures are the mixture of garlic, purslane, Chinese cassia tree, camphor ball and tulip, described big
Garlic, purslane, Chinese cassia tree, camphor ball and the mass ratio of tulip are 1:2:1:3:1.
Wherein, the tackifier are the double sodium starch of food-grade acetylation diacid.
A method of the glutinous rice glue with sedative action is prepared, is included the following steps：
（1）By above-mentioned formula weigh pretreatment glutinous rice, potato, cornstarch, alum, acrylic acid, modified bamboo powder, lignin,
Citric acid, glucolactone, anionic additive, sorbierite, lavender extracting solution, rose extracting solution, India flower extracting solution,
Mixture of Chinese herbal medicines, tackifier are sterilized, it is spare；
（2）By peeling potatoes, it is cut into small pieces, then is cooked using water vapour, then smashed to pieces, prepares mashed potato；
（3）Pretreatment glutinous rice, mashed potato, cornstarch and alum are mixed, added water, until water content is 60% in its material,
It is stirred, heats while stirring, be warming up to 72 DEG C, then insulated and stirred 2 hours is added acrylic acid, is modified bamboo powder, is wooden
Element, citric acid, glucolactone and sorbierite, are uniformly mixed, and are then gelatinized, and gelatinization product is obtained；
（4）Surplus stock is added to step（4）In the gelatinization product of gained, high speed dispersion is uniform, and packaging has to get described
The glutinous rice glue of sedative action.
Wherein, the step（3）The speed of middle stirring is 30r/min.
Embodiment 4
The present embodiment is related to a kind of glutinous rice glue with sedative action, includes the raw material of following parts by weight：45 parts of glutinous rice of pretreatment,
17 parts of potato, 23 parts of cornstarch, 6 parts of alum, 8 parts of acrylic acid, modified 11 parts of bamboo powder, 5.2 parts of lignin, citric acid 3.2
Part, 4.5 parts of glucolactone, 3.3 parts of anionic additive, 4 parts of sorbierite, 1.7 parts of lavender extracting solution, rose extracting solution
2.5 parts, India flower 2.9 parts of extracting solution, sterilization 5 parts of mixture of Chinese herbal medicines, 4.2 parts of tackifier.
Wherein, the preparation method of the pretreatment glutinous rice is as follows：
By glutinous rice be put into glacial acetic acid it is molten in, be warming up to 53 DEG C, ultrasonication power be 1000W under conditions of handle 15min,
After taking-up is dried, the pretreatment glutinous rice is obtained.
Wherein, the preparation method of the modified bamboo powder is as follows：
Bamboo powder is impregnated 4 hours in a concentration of 4% dilute nitric acid solution, it is ultrasonic under supersonic frequency 22kHz, power 80W
Processing 20 minutes, is then added with stirring equivalent Sodium Polyacrylate, is warming up to 80 DEG C and reacts 50 minutes, filters after reaction,
Filter cake is washed three times, is most less than 5% through oven drying to moisture up to the modified starch afterwards.
Wherein, the anionic additive includes the raw material of following parts by weight：5 parts of tourmaline, lanthanide rare composite salt
5 parts of 10 parts, 6 parts of nano-titanium dioxide and Tourmaline mountain flour.
Wherein, the Fungicidai mixtures are the mixture of garlic, purslane, Chinese cassia tree, camphor ball and tulip, described big
Garlic, purslane, Chinese cassia tree, camphor ball and the mass ratio of tulip are 1:2:1:3:1.
Wherein, the tackifier are maltodextrin.
A method of the glutinous rice glue with sedative action is prepared, is included the following steps：
（1）By above-mentioned formula weigh pretreatment glutinous rice, potato, cornstarch, alum, acrylic acid, modified bamboo powder, lignin,
Citric acid, glucolactone, anionic additive, sorbierite, lavender extracting solution, rose extracting solution, India flower extracting solution,
Mixture of Chinese herbal medicines, tackifier are sterilized, it is spare；
（2）By peeling potatoes, it is cut into small pieces, then is cooked using water vapour, then smashed to pieces, prepares mashed potato；
（3）Pretreatment glutinous rice, mashed potato, cornstarch and alum are mixed, added water, until water content is 60% in its material,
It is stirred, heats while stirring, be warming up to 75 DEG C, then insulated and stirred 2 hours is added acrylic acid, is modified bamboo powder, is wooden
Element, citric acid, glucolactone and sorbierite, are uniformly mixed, and are then gelatinized, and gelatinization product is obtained；
（4）Surplus stock is added to step（4）In the gelatinization product of gained, high speed dispersion is uniform, and packaging has to get described
The glutinous rice glue of sedative action.
Wherein, the step（3）The speed of middle stirring is 30r/min.
Embodiment 5
The present embodiment is related to a kind of glutinous rice glue with sedative action, includes the raw material of following parts by weight：40 parts of glutinous rice of pretreatment,
15 parts of potato, 21 parts of cornstarch, 5 parts of alum, 7.6 parts of acrylic acid, modified 10 parts of bamboo powder, 4.8 parts of lignin, citric acid
2.7 parts, 3.8 parts of glucolactone, 3.2 parts of anionic additive, 3.4 parts of sorbierite, 1.6 parts of lavender extracting solution, rose
2 parts of extracting solution, India 2.3 parts of extracting solution of flower, 4.4 parts of mixture of Chinese herbal medicines of sterilization, 3.9 parts of tackifier.
Wherein, the preparation method of the pretreatment glutinous rice is as follows：
By glutinous rice be put into glacial acetic acid it is molten in, be warming up to 54 DEG C, ultrasonication power be 1050W under conditions of handle 15min,
After taking-up is dried, the pretreatment glutinous rice is obtained.
Wherein, the preparation method of the modified bamboo powder is as follows：
Bamboo powder is impregnated 4 hours in a concentration of 4% dilute nitric acid solution, it is ultrasonic under supersonic frequency 22kHz, power 80W
Processing 20 minutes, is then added with stirring equivalent Sodium Polyacrylate, is warming up to 80 DEG C and reacts 50 minutes, filters after reaction,
Filter cake is washed three times, is most less than 5% through oven drying to moisture up to the modified starch afterwards.
Wherein, the anionic additive includes the raw material of following parts by weight：5 parts of tourmaline, lanthanide rare composite salt
5 parts of 10 parts, 6 parts of nano-titanium dioxide and Tourmaline mountain flour.
Wherein, the Fungicidai mixtures are the mixture of garlic, purslane, Chinese cassia tree, camphor ball and tulip, described big
Garlic, purslane, Chinese cassia tree, camphor ball and the mass ratio of tulip are 1:2:1:3:1.
Wherein, the tackifier are maltodextrin.
A method of the glutinous rice glue with sedative action is prepared, is included the following steps：
（1）By above-mentioned formula weigh pretreatment glutinous rice, potato, cornstarch, alum, acrylic acid, modified bamboo powder, lignin,
Citric acid, glucolactone, anionic additive, sorbierite, lavender extracting solution, rose extracting solution, India flower extracting solution,
Mixture of Chinese herbal medicines, tackifier are sterilized, it is spare；
（2）By peeling potatoes, it is cut into small pieces, then is cooked using water vapour, then smashed to pieces, prepares mashed potato；
（3）Pretreatment glutinous rice, mashed potato, cornstarch and alum are mixed, added water, until water content is 60% in its material,
It is stirred, heats while stirring, be warming up to 78 DEG C, then insulated and stirred 2 hours is added acrylic acid, is modified bamboo powder, is wooden
Element, citric acid, glucolactone and sorbierite, are uniformly mixed, and are then gelatinized, and gelatinization product is obtained；
（4）Surplus stock is added to step（4）In the gelatinization product of gained, high speed dispersion is uniform, and packaging has to get described
The glutinous rice glue of sedative action.
Wherein, the step（3）The speed of middle stirring is 30r/min.
Comparative example
A kind of child room special environment protection glutinous rice rubber powder and its processing method of the patent disclosure of application publication number CN107057603A.
Glutinous rice glue described in above-described embodiment 1~5, comparative example is detected into its wet viscosity (stripping according to JC/T548-2016 respectively
When length is 300mm, displacement distance), sliding, 180 ° of peel strengths, 7d working lives, 30d working lives and 180d working lives,
The results are shown in table below.Wherein, not corrupt, not thinning, mildew be qualification
As can be seen from the above table, the performance of glutinous rice glue of the present invention is better than comparative example.
In conclusion（1）The present invention is using pretreatment glutinous rice, potato, cornstarch, alum, acrylic acid, modified bamboo
Powder, lignin, citric acid, glucolactone, anionic additive, sorbierite, lavender extracting solution, rose extracting solution, day
Zhu spends extracting solution, sterilization mixture of Chinese herbal medicines, tackifier etc. to be used as raw material, and the raw material of use is environmentally protective, does not discharge volatility
Organic matter, non-toxic to humans, the caking property for preparing glutinous rice glue is strong, has excellent fungus and mildew resistance to the common mould of wallpaper
Effect effectively improves its service life；
（2）The present invention by pre-process glutinous rice, potato, cornstarch, alum, etc. a variety of specified raw material glue compounding energy
Its adhesive property is effectively improved, also, further combined with the pretreatment glutinous rice provided in the present invention, it is viscous can preferably to improve it
The performances such as knot；
（3）It is mixed that the present invention is added to lavender extracting solution, rose extracting solution, India flower extracting solution, sterilization Chinese herbal medicine in the feed
Object is closed, the extracts of Chinese herbal medicine is the mixture of garlic, purslane, Chinese cassia tree, camphor ball and tulip, and anion addition
Agent mutually acts synergistically, and can resist a variety of germs, to improve the antibiotic property of product, lavender extracting solution, rose extracting solution,
India spends extracting solution and anionic additive mutually to act synergistically, and the glutinous rice glue prepared can discharge anion and fragrance, tool
Play the role of purifying air, tranquilizing the mind.
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (10)
1. a kind of glutinous rice glue with sedative action, which is characterized in that include the raw material of following parts by weight：Pretreatment glutinous rice 30~
50 parts, 10~20 parts of potato, 15~25 parts of cornstarch, 3~7 parts of alum, 6~9 parts of acrylic acid, modified 8~12 parts of bamboo powder,
4~6 parts of lignin, 2~4 parts of citric acid, 3~5 parts of glucolactone, 2~4 parts of anionic additive, 2~5 parts of sorbierite,
1~2 part of lavender extracting solution, 1.3~2.7 parts of rose extracting solution, India 2~3 parts of extracting solution of flower, sterilization mixture of Chinese herbal medicines 3
~6 parts, 3~5 parts of tackifier.
2. the glutinous rice glue according to claim 1 with sedative action, which is characterized in that include the original of following parts by weight
Material：Pre-process 35~45 parts of glutinous rice, 12~17 parts of potato, 18~23 parts of cornstarch, 4~6 parts of alum, acrylic acid 7~8
Part, modified 9~11 parts of bamboo powder, 4.3~5.2 parts of lignin, 2.4~3.2 parts of citric acid, 3.5~4.5 parts of glucolactone,
2.8~3.3 parts of anionic additive, 3~4 parts of sorbierite, 1.2~1.7 parts of lavender extracting solution, rose extracting solution 1.5~2.5
Part, India 2.1~2.9 parts of extracting solution of flower, 4~5 parts of mixture of Chinese herbal medicines of sterilization, 3.6~4.2 parts of tackifier.
3. the glutinous rice glue according to claim 1 with sedative action, which is characterized in that include the original of following parts by weight
Material：Pre-process 40 parts of glutinous rice, 15 parts of potato, 21 parts of cornstarch, 5 parts of alum, 7.6 parts of acrylic acid, modified 10 parts of bamboo powder, wood
4.8 parts of quality, 2.7 parts of citric acid, 3.8 parts of glucolactone, 3.2 parts of anionic additive, 3.4 parts of sorbierite, lavender
1.6 parts of extracting solution, 2 parts of rose extracting solution, India 2.3 parts of extracting solution of flower, 4.4 parts of mixture of Chinese herbal medicines of sterilization, tackifier 3.9
Part.
4. the glutinous rice glue according to claim 1 with sedative action, which is characterized in that the preparation of the pretreatment glutinous rice
Method is as follows：
By glutinous rice be put into glacial acetic acid it is molten in, be warming up to 50~55 DEG C, ultrasonication power be 900~1100W under conditions of
It handles 15min and obtains the pretreatment glutinous rice after taking-up is dried.
5. the glutinous rice glue according to claim 1 with sedative action, which is characterized in that the preparation side of the modified bamboo powder
Method is as follows：
Bamboo powder is impregnated 4 hours in a concentration of 4% dilute nitric acid solution, it is ultrasonic under supersonic frequency 22kHz, power 80W
Processing 20 minutes, is then added with stirring equivalent Sodium Polyacrylate, is warming up to 80 DEG C and reacts 50 minutes, filters after reaction,
Filter cake is washed three times, is most less than 5% through oven drying to moisture up to the modified starch afterwards.
6. the glutinous rice glue according to claim 1 with sedative action, which is characterized in that the anionic additive includes
The raw material of following parts by weight：5 parts of tourmaline, 10 parts of lanthanide rare composite salt, 6 parts of nano-titanium dioxide and Tourmaline mountain flour 5
Part.
7. the glutinous rice glue according to claim 1 with sedative action, which is characterized in that the Fungicidai mixtures are big
Garlic, purslane, Chinese cassia tree, camphor ball and the mixture of tulip, the garlic, purslane, Chinese cassia tree, camphor ball and tulip matter
Amount is than being 1:2:1:3:1.
8. the glutinous rice glue according to claim 1 with sedative action, which is characterized in that the tackifier are food-grade second
Any one of acylated diacid double sodium starch, maltodextrins.
9. a kind of method preparing the glutinous rice glue with sedative action described in any one of claim 1~8, which is characterized in that packet
Include following steps：
（1）By above-mentioned formula weigh pretreatment glutinous rice, potato, cornstarch, alum, acrylic acid, modified bamboo powder, lignin,
Citric acid, glucolactone, anionic additive, sorbierite, lavender extracting solution, rose extracting solution, India flower extracting solution,
Mixture of Chinese herbal medicines, tackifier are sterilized, it is spare；
（2）By peeling potatoes, it is cut into small pieces, then is cooked using water vapour, then smashed to pieces, prepares mashed potato；
（3）Pretreatment glutinous rice, mashed potato, cornstarch and alum are mixed, added water, until water content is 60% in its material,
It is stirred, heats while stirring, be warming up to 70~80 DEG C, then acrylic acid, modified bamboo powder, wood is added in insulated and stirred 2 hours
Quality, citric acid, glucolactone and sorbierite, are uniformly mixed, and are then gelatinized, and gelatinization product is obtained；
（4）Surplus stock is added to step（4）In the gelatinization product of gained, high speed dispersion is uniform, and packaging has to get described
The glutinous rice glue of sedative action.
10. preparation method according to claim 9, which is characterized in that the step（3）The speed of middle stirring is 30r/
min。
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| CN113322674A (en) * | 2020-02-28 | 2021-08-31 | 成都菩提高能科技有限公司 | Method for manufacturing negative oxygen ion energy cloth |
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|---|---|---|---|---|
| CN107384245A (en) * | 2017-08-28 | 2017-11-24 | 上海前引科技有限公司 | A kind of antibacterial and mouldproof anion glutinous rice adhesive |
| CN108047990A (en) * | 2018-01-24 | 2018-05-18 | 合肥市大卓电力有限责任公司 | A kind of novel antibacterial glutinous rice glue and preparation method thereof |
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2018
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107384245A (en) * | 2017-08-28 | 2017-11-24 | 上海前引科技有限公司 | A kind of antibacterial and mouldproof anion glutinous rice adhesive |
| CN108047990A (en) * | 2018-01-24 | 2018-05-18 | 合肥市大卓电力有限责任公司 | A kind of novel antibacterial glutinous rice glue and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113322674A (en) * | 2020-02-28 | 2021-08-31 | 成都菩提高能科技有限公司 | Method for manufacturing negative oxygen ion energy cloth |
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Application publication date: 20180928 |