CN108585505A - A kind of persimmon red pottery glaze and preparation method thereof and glazing method - Google Patents
A kind of persimmon red pottery glaze and preparation method thereof and glazing method Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
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- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
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Abstract
A kind of persimmon red pottery glaze and preparation method thereof and glazing method, a kind of persimmon red pottery glaze include the raw material of following parts by weight：15 20 parts of melilite, 22 25 parts of quartz, 18 24 parts of kaolinite, 8 12 parts of red soil, 68 parts of iron oxide red, 10 15 parts of ferrous oxalate, 58 parts of talcum, 5 10 parts of Bai Changshi, 35 parts of bone meal, 1.2 1.8 parts of potassium oxide, 0.6 1.2 parts of lanthana, 0.5 0.8 parts of zinc oxide, 0.3 0.5 parts of manganese carbonate, select ferrous oxalate, red soil, iron oxide red part, color developing agent of the melilite as glaze, pass through mutual cooperation between four and synergistic effect, keep glaze color obtained red in persimmon, and glaze obtained is formed with stable molecular structure, it is bright to form glaze, color and luster is obvious, the persimmon red pottery glaze of stable quality.
Description
Technical field
The invention belongs to ceramic glaze preparation fields, and in particular to a kind of persimmon red pottery glaze and preparation method thereof and upper
Glaze method.
Background technology
The art pottery is with a long history, and production method is：Moulded pottery not yet put in a kiln to bake forming, drying, glazing, sintering process complete because
Glaze is a kind of nature of glass, but its forming process is that first through glaze is melted the stage in high temperature kiln, and glaze starts to melt at this time, but
Do not have intact mobility, volatilizable foreign gas is arrived the glaze top just melted at big and small bubble in green body glaze layer
It is bubbles burst despumation gas that glaze, which melts the stage, and glaze showpiece forms vitreous smooth glaze, but existing
Glaze color is also relatively single fewer, and colored glaze is still hyperchromic up for innovating, to meet creation and decoration demand.
Invention content
The purpose of the present invention is overcoming the prior art, a kind of persimmon red pottery glaze is provided, another object is that carrying
For a kind of preparation method and glazing method of above-mentioned glaze.
The present invention adopts the following technical scheme that：
A kind of persimmon red pottery glaze, includes the raw material of following parts by weight：15-20 parts of melilite, 22-25 parts of quartz, height
Stone 18-24 parts of ridge, 8-12 parts of red soil, 6-8 parts of iron oxide red, 10-15 parts of ferrous oxalate, 5-8 parts of talcum, feldspar 5-10 parts white, bone
3-5 parts of powder, 1.2-1.8 parts of potassium oxide, 0.6-1.2 parts of lanthana, 0.5-0.8 parts of zinc oxide, 0.3-0.5 parts of manganese carbonate.
Further, the bone meal is bovine bone powder or lamb bone meal.
A kind of preparation method of persimmon red pottery glaze, the method step are：Each raw material is matched into honest material in proportion, respectively
100-150 mesh sieve was rolled, mixing is fitted into ball mill, by raw material：Ballstone：Water=1:1.2-1.8:1.2-1.4 ratio into
Row ball milling is processed, Ball-milling Time 8-12h, and 200-300 mesh sieve is crossed after ball milling is good, completes the preparation of persimmon red pottery glaze.
Further, a concentration of 35-40 Baume degrees of the persimmon red pottery glaze obtained.
A kind of glazing method of persimmon red pottery glaze, includes the following steps：
(1), it fires the green body of non-glazing to obtain carcass；
(2), it waits for that carcass is cooled to room temperature, green body is placed in glaze and is stopped 5-8 seconds, propose, the thickness of glaze layer is 0.5-
0.8mm；
(3), the carcass after glazing is sent into kiln, is sintered using oxidizing atmosphere, sintering temperature is 1150 DEG C, when heat preservation
Between be 72-90min.
Further, it in the step (3), when being sintered using oxidizing atmosphere, is first warming up to from room temperature with 1.5-2 DEG C/min
350 DEG C, 600 DEG C are warming up to 1.2-1.5 DEG C/min, then 750 DEG C are warming up to 1-1.2 DEG C/min, then with 1-1.2 DEG C/min
1050 DEG C are warming up to, is finally warming up to 1150 DEG C with 2-3 DEG C/min, 72-90min is kept the temperature at 1150 DEG C, is finally down to 120 DEG C
.
Further, in the step (1), green body is fired using oxidizing atmosphere, is first heated up from room temperature with 1.5-2 DEG C/min
To 300 DEG C, 600 DEG C are warming up to 2-3 DEG C/min, then 750 DEG C are warming up to 1.2-1.5 DEG C/min, then with 1.5-2 DEG C/min
850 DEG C are warming up to, is finally down to 120 DEG C, carcass is made.
By the above-mentioned description of this invention it is found that compared with prior art, the beneficial effects of the invention are as follows：The present invention according to
Colouration mechanism and substance micro molecule structural theory select the colour developing of ferrous oxalate, red soil, iron oxide red part, melilite as glaze
Agent keeps glaze color obtained red in persimmon, and glaze obtained is formed by mutual cooperation between four and synergistic effect
There is stable molecular structure, formation glaze is bright, color and luster is obvious, stable quality persimmon red pottery glaze.
Specific implementation mode
Below by way of specific implementation mode, the invention will be further described.
A kind of persimmon red pottery glaze, includes the raw material of following parts by weight：15-20 parts of melilite, 22-25 parts of quartz, height
Stone 18-24 parts of ridge, 8-12 parts of red soil, 6-8 parts of iron oxide red, 10-15 parts of ferrous oxalate, 5-8 parts of talcum, feldspar 5-10 parts white, bone
3-5 parts of powder, 1.2-1.8 parts of potassium oxide, 0.6-1.2 parts of lanthana, 0.5-0.8 parts of zinc oxide, 0.3-0.5 parts of manganese carbonate；
Specifically, bone meal is bovine bone powder or lamb bone meal；
The preparation method of above-mentioned persimmon red pottery glaze, specifically includes：Each raw material is matched into honest material in proportion, was rolled respectively
100-150 mesh sieves, and mixing is fitted into ball mill, by raw material：Ballstone：Water=1:1.2-1.8:The ratio of 1.2-1.4 carries out ball milling
Processing, Ball-milling Time 8-12h cross 200-300 mesh sieve, complete the preparation of persimmon red pottery glaze after ball milling is good；
Specifically, a concentration of 35-40 Baume degrees of persimmon red pottery glaze obtained；
The glazing method of the persimmon red pottery glaze of above-mentioned preparation, includes the following steps：
(1), fire the green body of non-glazing to obtain carcass, specifically, green body using oxidizing atmosphere fire, first from room temperature with
1.5-2 DEG C/min is warming up to 300 DEG C, is warming up to 600 DEG C with 2-3 DEG C/min, then be warming up to 750 DEG C with 1.2-1.5 DEG C/min, so
850 DEG C are warming up to 1.5-2 DEG C/min afterwards, is finally down to 120 DEG C, carcass is made；
(2), it waits for that carcass is cooled to room temperature, green body is placed in glaze and is stopped 5-8 seconds, propose, the thickness of glaze layer is 0.5-
0.8mm；
(3), the carcass after glazing is sent into kiln, is sintered using oxidizing atmosphere, sintering temperature is 1150 DEG C, when heat preservation
Between be 72-90min, specifically, when being sintered using oxidizing atmosphere, be first warming up to 350 DEG C from room temperature with 1.5-2 DEG C/min, with
1.2-1.5 DEG C/min is warming up to 600 DEG C, then is warming up to 750 DEG C with 1-1.2 DEG C/min, is then warming up to 1-1.2 DEG C/min
1050 DEG C, 1150 DEG C finally are warming up to 2-3 DEG C/min, 72-90min is kept the temperature at 1150 DEG C, is finally down to 120 DEG C.
Embodiment 1
A kind of persimmon red pottery glaze, includes the raw material of following parts by weight：15 parts of melilite, quartzy 25 parts, kaolinite 18
Part, 12 parts of red soil, 6 parts of iron oxide red, 15 parts of ferrous oxalate, 8 parts of talcum, 5 parts of white feldspar, 5 parts of bone meal, 1.8 parts of potassium oxide, oxidation
0.6 part of lanthanum, 0.8 part of zinc oxide, 0.3 part of manganese carbonate.
Specifically, bone meal is bovine bone powder；
The preparation method of above-mentioned persimmon red pottery glaze, specifically includes：Each raw material is matched into honest material in proportion, was rolled respectively
150 mesh sieve, and mixing is fitted into ball mill, by raw material：Ballstone：Water=1:1.2:1.4 ratio carries out ball milling processing, Ball-milling Time
For 12h, 300 mesh sieve is crossed after ball milling is good, completes the preparation of persimmon red pottery glaze；
Specifically, a concentration of 35-40 Baume degrees of persimmon red pottery glaze obtained；
The glazing method of the persimmon red pottery glaze of above-mentioned preparation, includes the following steps：
(1), fire the green body of non-glazing to obtain carcass, specifically, green body using oxidizing atmosphere fire, first from room temperature with
1.5 DEG C/min is warming up to 300 DEG C, 600 DEG C is warming up to 2 DEG C/min, then be warming up to 750 DEG C with 1.5 DEG C/min, then with 1.5
DEG C/min is warming up to 850 DEG C, is finally down to 120 DEG C, carcass is made；
(2), it waits for that carcass is cooled to room temperature, green body is placed in glaze and is stopped 5 seconds, propose, the thickness of glaze layer is 0.5mm；
(3), the carcass after glazing is sent into kiln, is sintered using oxidizing atmosphere, sintering temperature is 1150 DEG C, when heat preservation
Between be 90min, specifically, when being sintered using oxidizing atmosphere, first 350 DEG C are warming up to from room temperature with 2 DEG C/min, with 1.2 DEG C/min
600 DEG C are warming up to, then 750 DEG C are warming up to 1.2 DEG C/min, then 1050 DEG C are warming up to 1 DEG C/min, finally with 3 DEG C/min
1150 DEG C are warming up to, 90min is kept the temperature at 1150 DEG C, is finally down to 120 DEG C.
Embodiment 2
A kind of persimmon red pottery glaze, includes the raw material of following parts by weight：20 parts of melilite, quartzy 22 parts, kaolinite 24
Part, 8 parts of red soil, 8 parts of iron oxide red, 10 parts of ferrous oxalate, 5 parts of talcum, 10 parts of white feldspar, 3 parts of bone meal, 1.2 parts of potassium oxide, oxidation
1.2 parts of lanthanum, 0.5 part of zinc oxide, 0.5 part of manganese carbonate；
Specifically, bone meal is lamb bone meal；
The preparation method of above-mentioned persimmon red pottery glaze, specifically includes：Each raw material is matched into honest material in proportion, was rolled respectively
100 mesh sieve, and mixing is fitted into ball mill, by raw material：Ballstone：Water=1:1.8:1.2 ratio carries out ball milling processing, Ball-milling Time
For 8h, 200 mesh sieve is crossed after ball milling is good, completes the preparation of persimmon red pottery glaze；
Specifically, a concentration of 35-40 Baume degrees of persimmon red pottery glaze obtained；
The glazing method of the persimmon red pottery glaze of above-mentioned preparation, includes the following steps：
(1), fire the green body of non-glazing to obtain carcass, specifically, green body using oxidizing atmosphere fire, first from room temperature with
2 DEG C/min is warming up to 300 DEG C, is warming up to 600 DEG C with 3 DEG C/min, then be warming up to 750 DEG C with 1.2 DEG C/min, then with 2 DEG C/
Min is warming up to 850 DEG C, is finally down to 120 DEG C, and carcass is made；
(2), it waits for that carcass is cooled to room temperature, green body is placed in glaze and is stopped 8 seconds, propose, the thickness of glaze layer is 0.8mm；
(3), the carcass after glazing is sent into kiln, is sintered using oxidizing atmosphere, sintering temperature is 1150 DEG C, when heat preservation
Between be 72min, specifically, when being sintered using oxidizing atmosphere, be first warming up to 350 DEG C from room temperature with 1.5 DEG C/min, with 1.5 DEG C/
Min is warming up to 600 DEG C, then is warming up to 750 DEG C with 1 DEG C/min, is then warming up to 1050 DEG C with 1.2 DEG C/min, finally with 2 DEG C/
Min is warming up to 1150 DEG C, and 72min is kept the temperature at 1150 DEG C, is finally down to 120 DEG C.
Embodiment 3
A kind of persimmon red pottery glaze, includes the raw material of following parts by weight：18 parts of melilite, quartzy 23 parts, kaolinite 21
Part, 10 parts of red soil, 7 parts of iron oxide red, 12 parts of ferrous oxalate, 6 parts of talcum, 7 parts of white feldspar, 4 parts of bone meal, 1.5 parts of potassium oxide, oxidation
0.9 part of lanthanum, 0.6 part of zinc oxide, 0.4 part of manganese carbonate；
Specifically, bone meal is lamb bone meal；
The preparation method of above-mentioned persimmon red pottery glaze, specifically includes：Each raw material is matched into honest material in proportion, was rolled respectively
120 mesh sieve, and mixing is fitted into ball mill, by raw material：Ballstone：Water=1:1.5:1.3 ratio carries out ball milling processing, Ball-milling Time
For 10h, 250 mesh sieve is crossed after ball milling is good, completes the preparation of persimmon red pottery glaze；
Specifically, a concentration of 35-40 Baume degrees of persimmon red pottery glaze obtained；
The glazing method of the persimmon red pottery glaze of above-mentioned preparation, includes the following steps：
(1), fire the green body of non-glazing to obtain carcass, specifically, green body using oxidizing atmosphere fire, first from room temperature with
1.8 DEG C/min is warming up to 300 DEG C, is warming up to 600 DEG C with 2.5 DEG C/min, then be warming up to 750 DEG C with 1.3 DEG C/min, then with
1.8 DEG C/min is warming up to 850 DEG C, is finally down to 120 DEG C, and carcass is made；
(2), it waits for that carcass is cooled to room temperature, green body is placed in glaze and is stopped 6 seconds, propose, the thickness of glaze layer is 0.7mm；
(3), the carcass after glazing is sent into kiln, is sintered using oxidizing atmosphere, sintering temperature is 1150 DEG C, when heat preservation
Between be 82min, specifically, when being sintered using oxidizing atmosphere, be first warming up to 350 DEG C from room temperature with 1.8 DEG C/min, with 1.3 DEG C/
Min is warming up to 600 DEG C, then is warming up to 750 DEG C with 1.1 DEG C/min, then 1050 DEG C is warming up to 1.1 DEG C/min, finally with 2.4
DEG C/min is warming up to 1150 DEG C, 82min is kept the temperature at 1150 DEG C, is finally down to 120 DEG C.
The present invention selects ferrous oxalate, red soil, iron oxide red part, Huang according to colouration mechanism and substance micro molecule structural theory
Color developing agent of the feldspar as glaze, by mutual cooperation between four and synergistic effect, it is in persimmon to make glaze color obtained
It is red, and glaze obtained is formed with stable molecular structure, formation glaze is bright, color and luster is obvious, stable quality persimmon red pottery
Glaze.
The foregoing is only a preferred embodiment of the present invention, therefore cannot be limited the scope of implementation of the present invention with this, i.e.,
According to equivalent changes and modifications made by scope of the present invention patent and description, it all should still belong to what patent of the present invention covered
In range.
Claims (7)
1. a kind of persimmon red pottery glaze, it is characterised in that：Include the raw material of following parts by weight：15-20 parts of melilite, quartz
22-25 parts, 18-24 parts of kaolinite, 8-12 parts of red soil, 6-8 parts of iron oxide red, 10-15 parts of ferrous oxalate, 5-8 parts of talcum, white feldspar
5-10 parts, 3-5 parts of bone meal, 1.2-1.8 parts of potassium oxide, 0.6-1.2 parts of lanthana, 0.5-0.8 parts of zinc oxide, manganese carbonate 0.3-
0.5 part.
2. a kind of persimmon red pottery glaze according to claim 1, it is characterised in that：The bone meal is bovine bone powder or sheep
Bone meal.
3. a kind of preparation method of persimmon red pottery glaze according to claim 1 or 2, it is characterised in that：The method
Step is：Each raw material is matched into honest material in proportion, rolled 100-150 mesh sieve respectively, mixing is fitted into ball mill, by raw material：Ball
Stone：Water=1:1.2-1.8:The ratio of 1.2-1.4 carries out ball milling processing, and Ball-milling Time 8-12h crosses 200-300 after ball milling is good
Mesh sieves, and completes the preparation of persimmon red pottery glaze.
4. a kind of preparation method of persimmon red pottery glaze according to claim 3, it is characterised in that：The persimmon obtained
Sub- a concentration of 35-40 Baume degrees of red pottery glaze.
5. a kind of glazing method of persimmon red pottery glaze according to claim 1 or 2, it is characterised in that：Including as follows
Step：
(1), it fires the green body of non-glazing to obtain carcass；
(2), it waits for that carcass is cooled to room temperature, green body is placed in glaze and is stopped 5-8 seconds, propose, the thickness of glaze layer is 0.5-
0.8mm；
(3), the carcass after glazing is sent into kiln, is sintered using oxidizing atmosphere, sintering temperature is 1150 DEG C, and soaking time is
72-90min。
6. a kind of glazing method of persimmon red pottery glaze according to claim 5, it is characterised in that：The step (3)
In, when being sintered using oxidizing atmosphere, 350 DEG C first are warming up to from room temperature with 1.5-2 DEG C/min, is warming up to 1.2-1.5 DEG C/min
600 DEG C, then 750 DEG C are warming up to 1-1.2 DEG C/min, be then warming up to 1050 DEG C with 1-1.2 DEG C/min, finally with 2-3 DEG C/
Min is warming up to 1150 DEG C, and 72-90min is kept the temperature at 1150 DEG C, is finally down to 120 DEG C.
7. a kind of glazing method of persimmon red pottery glaze according to claim 5, it is characterised in that：The step (1)
In, green body is fired using oxidizing atmosphere, is first warming up to 300 DEG C from room temperature with 1.5-2 DEG C/min, 600 are warming up to 2-3 DEG C/min
DEG C, then 750 DEG C are warming up to 1.2-1.5 DEG C/min, 850 DEG C then are warming up to 1.5-2 DEG C/min, is finally down to 120 DEG C, system
Obtain carcass.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111333327A (en) * | 2020-04-27 | 2020-06-26 | 德化县德鸿陶瓷有限公司 | Golden red glaze, ceramic product with golden red glaze and preparation method |
| CN115611515A (en) * | 2022-10-24 | 2023-01-17 | 福建省德化县百得隆陶瓷有限责任公司 | Matte glaze and method for preparing matte ceramic product by using same |
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| CN115611515B (en) * | 2022-10-24 | 2023-12-15 | 福建省德化县百得隆陶瓷有限责任公司 | Matte glaze and method for preparing matte ceramic product by using same |
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