CN108559678A - Four times of concentration liquid detergents of a kind of microcapsules perfume sweet smell and preparation method thereof - Google Patents
Four times of concentration liquid detergents of a kind of microcapsules perfume sweet smell and preparation method thereof Download PDFInfo
- Publication number
- CN108559678A CN108559678A CN201810630953.4A CN201810630953A CN108559678A CN 108559678 A CN108559678 A CN 108559678A CN 201810630953 A CN201810630953 A CN 201810630953A CN 108559678 A CN108559678 A CN 108559678A
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- CN
- China
- Prior art keywords
- fatty alcohol
- fragrant
- polyoxyethylene ether
- microcapsules
- feed liquid
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
- C11D3/502—Protected perfumes
- C11D3/505—Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay
Abstract
The invention discloses fragrant fragrant four times of concentrations liquid detergents of a kind of microcapsules and preparation method thereof, specially liquid detergent preparing technical field.Liquid detergent includes following raw material：Fatty alcohol polyoxyethylene ether AEO 3 10%, fatty alcohol polyoxyethylene ether AEO 9 15%, 70% sodium sulfate of polyethenoxy ether of fatty alcohol 15%, MULTISO 1,380 13%, washing synergist WR 2%, NATSURF 265 10%, natural soap agent HF 1,213 10%, polyethylene glycol 400 5%, 1,2 propylene glycol 5%, microcapsule essence 1%, washing proteinase-10 .1%, antiseptic 0.1%, deionized water 13.8%, this concentration liquid detergent dosage is few, it is light-weight, it is easy to carry, using natural organic degradable raw material and soap lye, lower the irritation of product, it is extremely low to the injury of clothing.
Description
Technical field
The present invention relates to fragrant fragrant four times of concentrations liquid detergents of a kind of microcapsules and preparation method thereof, and specially liquid detergent prepares skill
Art field.
Background technology
As the progress of economic society and environmental protection concept are gradually rooted in the hearts of the people, " saving water resource " is advocated in the whole society, " is protected
Retaining ring border " can not adapt to new market environment requirement using the expansion of amount as the development model of main means.In market competition
Abnormal fierce today, how to seek the new development opportunity of liquid detergent, is the problem of we have to face.Come from current situation
See, low-carbon environment-friendly by be articles for washing enterprise realize sustainable development only way, the hair in China's articles for washing industry future
Exhibition will be with fluidization, enrichment and green safe for homophony.
Superconcentrated washing liquid is with the fastest developing speed in the U.S..1992, the maximum detergent manufacturer P＆G in the whole world announced to push away
Go out concentrated type liquid detergent, and started all using Concentrated formulations in 2008.It was produced since hyperconcetration type liquid detergent has
Cheng Jieshui reduces plastics and uses, reduces the advantages of municipal solid waste discharge and greenhouse gas emission, while reducing warehousing capacity
And transportation cost.Only having the solidifying pearl of green unrestrained twice of concentration laundry and blue moon three times thickener to be washed till honor in the domestic market at present is
Belong to hyperconcetration type liquid detergent.From the point of view of the price war of current major liquid detergent producer, the retail price of liquid detergent is constantly down
It adjusts, promotion dynamics is also even more unprecedented, and such change promotes producer to want the higher Superconcentrated washing liquid of development technique content
To seize washing market.
Invention content
The purpose of the present invention is to provide fragrant fragrant four times of concentrations liquid detergents of a kind of microcapsules and preparation method thereof.
To achieve the above object, the present invention provides the following technical solutions：A kind of fragrant fragrant four times of concentrations liquid detergent packet of microcapsules
Raw material containing following mass fraction：
Fatty alcohol polyoxyethylene ether AEO-3 8-12%
Fatty alcohol polyoxyethylene ether AEO-9 12-18%
70% sodium sulfate of polyethenoxy ether of fatty alcohol 13-18%
MULTISO 1380 10-15%
Wash synergist WR 1-4%
NATSURF 265 8-12%
Natural soap agent HF-1213 8-12%
Polyethylene glycol 400 3-8%
1,2 propylene glycol 3-8%
Microcapsule essence 0.5-2%
Wash proteinase-10 .05-0.2%
Antiseptic 0.05-0.2%
Deionized water 10-15%
Further preferably, the fragrant fragrant four times of concentrations liquid detergent of the microcapsules includes the raw material of following mass fraction：
Fatty alcohol polyoxyethylene ether AEO-3 10%
Fatty alcohol polyoxyethylene ether AEO-9 15%
70% sodium sulfate of polyethenoxy ether of fatty alcohol 15%
MULTISO 1380 13%
Wash synergist WR 2%
NATSURF 265 10%
Natural soap agent HF-1213 10%
Polyethylene glycol 400 5%
1,2 propylene glycol 5%
Microcapsule essence 1%
Wash proteinase-10 .1%
Antiseptic 0.1%
Deionized water 13.8%
A kind of preparation method of the fragrant fragrant four times of concentrations liquid detergent of microcapsules：Step 1: pre-treatment, is accurately weighed by formula rate
70% sodium sulfate of polyethenoxy ether of fatty alcohol, NATSURF 265, polyethylene glycol 400 are placed in 50 kilograms of plastic barrel, place 2
Hour or more, so that 70% sodium sulfate of polyethenoxy ether of fatty alcohol is uniformly dissolved with nylon rod stirring, mixing time is 3-5 minutes, is used
Lid covers tightly spare, and pre-treatment feed liquid A is made；
Antiseptic, washing protease and deionized water are accurately weighed by formula rate in 50 kilograms of plastic barrel, are stirred evenly
It is covered tightly with lid spare, pre-treatment feed liquid B is made；
Step 2: feed liquid is prepared：1,2 propylene glycol, MULTISO 1380, aliphatic alcohol polyethenoxy are accurately weighed by formula rate
Ether AEO-3, fatty alcohol polyoxyethylene ether AEO-9, washing synergist WR, natural soap agent HF-1213 are sequentially added under stiring
It in stirred tank, stirs 30 minutes, is added slowly with stirring above-mentioned uniformly mixed pre-treatment feed liquid A, add stirring after ten minutes
Pre-treatment feed liquid B, microcapsule essence are sequentially added, stirring stops stirring after 30 minutes, feed liquid is poured into plastic barrel, and sealing is standby
With.
NATSURF 265 wherein in the present invention is that standing grain large group releases a kind of novel high-performance non-ionic surface active
Agent, this product aim at hard surface cleaning formula and the design of laundry product formula, and cleaning effect is good, can remove a variety of stubbornnesses
Spot.NatSurf265 can be used for producing concentration laundry product, and the product of production does not exist with gel state, or even in cold water
It can quickly dissolve, which improves the efficiency of laundry, realize fast low temperature laundry.NatSurf265 also has certain perfume (or spice)
Taste can dissolve grease, and the still ideal formulations agent of the friendly class product of ecology.It is washed using the NatSurf265 concentrations produced
Transportation and packaging cost can be reduced by washing product, reduce wash water amount and carbon footprint, while not interfering with its cleaning performance.
Natural soap agent HF-1213：The saturated carbon chains anion surfactant made of natural cocounut oil feed hydrogen
It compounds, has non-discolouring not spoiled by a certain percentage with the tridecanol ether carboxylic acid potassium anion surfactant of saturated carbon chains
Characteristic.After the two compounding, not only has the effect of collaboration decontamination synergy, but also low-temperature resistance, resistance to salting-out effect have and significantly carry
Height, while the easy performance rinsed, rinsed of potash soap is remained, it is a kind of surface-active of high effective green environmentally friendly of newest release
Agent.This product addition is convenient, easily addition dissolving, is one of raw material indispensable in laundry, bath product, and dosage is few, effect is aobvious
It writes.
Microcapsule essence：It is essence to be completely enclosed within a kind of technology that microcapsules are formed in a tunic, diameter is generally 1
~1000 nanometers.Microcapsule essence is an important branch in microcapsules technology, and one of microcapsules technology rather allusion quotation
The application of type.The wall material of Micro-encapsulation in Essence can depending on core material, it is general require be material property it is stable, it is nontoxic, without secondary work
With, it is nonirritant, play the role of compatibility, do not influence essence and flavoring agent, and to have satisfactory viscosity, permeability, have one
Determine intensity and plasticity etc..Essence is after microencapsulation, since the sealing function of cyst wall can effectively inhibit the volatilization of essence to damage
It loses, the stability for improving the storage of essence and using；Sensitive composition can be protected, oxytolerant, fast light and heat-resisting energy are greatly improved
Power increases its stability in clothing surface, essence can be made to have the function of slow release.
Compared with prior art, beneficial effects of the present invention are as follows：1, dosage is few, four times of hyperconcetration formulas, one gram of feed liquid
It can clean 1 clothes, general ordinary liquid laundry detergent surface-active contents 15%-17%, and this formula surface-active contents 65%
Left and right；
2, light-weight, easy to carry and transport, one bottle of 600g is equivalent to one bottle 3 kilograms of ordinary liquid laundry detergent（Four times of concentrations, five times
Clean power）；
3, fragrance remaining time is long, and this product adds microcapsule essence, can more than two weeks lasting；
4, easy-to-use quick, this product is packed using compressing pump type, and about 5 grams of a pump can clean 5 clothes, user
Just, measuring cup is not needed, without spill and leakage, is followed one's bent, laundry new paragon is opened；
5, using natural organic degradable raw material and soap lye, lower the irritation of product significantly, it is whole that alkalescent (pH value is presented
7.5~8.5), extremely low to the injury of clothing.
6, formula presses 2 by the big import new raw material NATSURF 265 of standing grain and polyethylene glycol 400,1,2 propylene glycol:1:1 ratio
It prepares, greatly improves table work solution rate in water, and surface-active contents are increased to 4 times of concentrations；5 grams of this product are added to
It in 100 grams of water, is gently mixed with glass bar, all dissolves not conglomeration in 1 minute.
7, this dispensing is solved by charging sequence and pre-treating method, can with the cold method of completing the square of common stirring at low speed come
It prepares, per kilogram feed liquid needs to consume the electricity charge less than 0.02 yuan, lowers dispensing cost significantly.
Specific implementation mode
The technical solution of present embodiment is clearly and completely described below in conjunction with the embodiment of the present invention,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1：
A kind of preparation method of the fragrant fragrant four times of concentrations liquid detergent of microcapsules：Step 1: pre-treatment, is accurately weighed by formula rate
70% sodium sulfate of polyethenoxy ether of fatty alcohol 15%, NATSURF 265 10%, polyethylene glycol 400 5% are in 50 kilograms of plastic barrel
In, place 2 hours or more, so that 70% sodium sulfate of polyethenoxy ether of fatty alcohol is uniformly dissolved with nylon rod stirring, mixing time 3-
It 5 minutes, is covered tightly with lid and spare pre-treatment feed liquid A is made：
Antiseptic 0.1%, washing proteinase-10 .1% and deionized water 13.8% are accurately weighed by formula rate in 50 kilograms of plastics
In bucket, stirs evenly to be covered tightly with lid and spare pre-treatment feed liquid B is made；
Step 2: feed liquid is prepared：1,2 propylene glycol 5%, MULTISO 1,380 13%, poly alkyl alcohol are accurately weighed by formula rate
Ethylene oxide ether AEO-3 10%, fatty alcohol polyoxyethylene ether AEO-9 15%, washing synergist WR 2%, natural soap agent HF-1213
10% sequentially adds in stirred tank under stiring, stirs 30 minutes, is added slowly with stirring above-mentioned uniformly mixed pre-treatment feed liquid
A adds stirring and sequentially adds pre-treatment feed liquid B, microcapsule essence 1% after ten minutes, and stirring stops stirring after 30 minutes, will expect
Liquid pours into plastic barrel, and sealing is spare.
Embodiment 2：
A kind of preparation method of the fragrant fragrant four times of concentrations liquid detergent of microcapsules：Step 1: pre-treatment, is accurately weighed by formula rate
70% sodium sulfate of polyethenoxy ether of fatty alcohol 13%, NATSURF 265 12%, polyethylene glycol 400 6% are in 50 kilograms of plastic barrel
In, place 2 hours or more, so that 70% sodium sulfate of polyethenoxy ether of fatty alcohol is uniformly dissolved with nylon rod stirring, mixing time 3-
It 5 minutes, is covered tightly with lid and spare pre-treatment feed liquid A is made：
Antiseptic 0.1%, washing proteinase-10 .1% and deionized water 12.8% are accurately weighed by formula rate in 50 kilograms of plastics
In bucket, stirs evenly to be covered tightly with lid and spare pre-treatment feed liquid B is made；
Step 2: feed liquid is prepared：1,2 propylene glycol 7%, MULTISO 1,380 11%, poly alkyl alcohol are accurately weighed by formula rate
Ethylene oxide ether AEO-3 12%, fatty alcohol polyoxyethylene ether AEO-9 13%, washing synergist WR 1%, natural soap agent HF-1213
11% sequentially adds in stirred tank under stiring, stirs 30 minutes, is added slowly with stirring above-mentioned uniformly mixed pre-treatment feed liquid
A adds stirring and sequentially adds pre-treatment feed liquid B, microcapsule essence 1% after ten minutes, and stirring stops stirring after 30 minutes, will expect
Liquid pours into plastic barrel, and sealing is spare.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (3)
1. a kind of fragrant fragrant four times of concentrations liquid detergent of microcapsules, it is characterised in that：The concentration liquid detergent includes following quality point
Several raw materials：
Fatty alcohol polyoxyethylene ether AEO-3 8-12%
Fatty alcohol polyoxyethylene ether AEO-9 12-18%
70% sodium sulfate of polyethenoxy ether of fatty alcohol 13-18%
MULTISO 1380 10-15%
Wash synergist WR 1-4%
NATSURF 265 8-12%
Natural soap agent HF-1213 8-12%
Polyethylene glycol 400 3-8%
1,2 propylene glycol 3-8%
Microcapsule essence 0.5-2%
Wash proteinase-10 .05-0.2%
Antiseptic 0.05-0.2%
Deionized water 10-15%.
2. the fragrant fragrant four times of concentrations liquid detergent of a kind of microcapsules according to claim 1, it is characterised in that：The concentration laundry
Liquid includes the raw material of following mass fraction：
Fatty alcohol polyoxyethylene ether AEO-3 10%
Fatty alcohol polyoxyethylene ether AEO-9 15%
70% sodium sulfate of polyethenoxy ether of fatty alcohol 15%
MULTISO 1380 13%
Wash synergist WR 2%
NATSURF 265 10%
Natural soap agent HF-1213 10%
Polyethylene glycol 400 5%
1,2 propylene glycol 5%
Microcapsule essence 1%
Wash proteinase-10 .1%
Antiseptic 0.1%
Deionized water 13.8%.
3. a kind of preparation method of the fragrant fragrant four times of concentrations liquid detergent of microcapsules, it is characterised in that specifically preparation method is：Step 1:
Pre-treatment is accurately weighed 70% sodium sulfate of polyethenoxy ether of fatty alcohol, NATSURF 265, polyethylene glycol 400 by formula rate and set
In 50 kilograms of plastic barrel, place 2 hours or more, so that 70% sodium sulfate of polyethenoxy ether of fatty alcohol is dissolved with nylon rod stirring
Uniformly, mixing time is 3-5 minutes, is covered tightly with lid spare, and pre-treatment feed liquid A is made；
Antiseptic, washing protease and deionized water are accurately weighed by formula rate in 50 kilograms of plastic barrel, are stirred evenly
It is covered tightly with lid spare, pre-treatment feed liquid B is made；
Step 2: feed liquid is prepared：1,2 propylene glycol, MULTISO 1380, fatty alcohol polyoxyethylene ether are accurately weighed by formula rate
AEO-3, fatty alcohol polyoxyethylene ether AEO-9, washing synergist WR, natural soap agent HF-1213 are sequentially added stir under stiring
Mix in kettle, stir 30 minutes, be added slowly with stirring above-mentioned uniformly mixed pre-treatment feed liquid A, add stirring after ten minutes according to
Secondary addition pre-treatment feed liquid B, microcapsule essence, stirring stop stirring after 30 minutes, feed liquid are poured into plastic barrel, and sealing is spare
.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810630953.4A CN108559678A (en) | 2018-06-19 | 2018-06-19 | Four times of concentration liquid detergents of a kind of microcapsules perfume sweet smell and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810630953.4A CN108559678A (en) | 2018-06-19 | 2018-06-19 | Four times of concentration liquid detergents of a kind of microcapsules perfume sweet smell and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108559678A true CN108559678A (en) | 2018-09-21 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810630953.4A Pending CN108559678A (en) | 2018-06-19 | 2018-06-19 | Four times of concentration liquid detergents of a kind of microcapsules perfume sweet smell and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111286414A (en) * | 2019-11-28 | 2020-06-16 | 纳爱斯浙江科技有限公司 | Clothing fragrance retaining bead and preparation method thereof |
| EP4206310A1 (en) * | 2021-12-29 | 2023-07-05 | Henkel IP & Holding GmbH | Unit dose product comprising a liquid composition with encapsulated fragrance |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105779159A (en) * | 2016-04-09 | 2016-07-20 | 福建省金鹿日化股份有限公司 | Softening clothes washing condensate ball and preparation method thereof |
| CN106047522A (en) * | 2016-06-27 | 2016-10-26 | 浙江绿果新材料有限公司 | Hyperconcentration anhydrous laundry detergent as well as preparation method and laundry beads thereof |
-
2018
- 2018-06-19 CN CN201810630953.4A patent/CN108559678A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105779159A (en) * | 2016-04-09 | 2016-07-20 | 福建省金鹿日化股份有限公司 | Softening clothes washing condensate ball and preparation method thereof |
| CN106047522A (en) * | 2016-06-27 | 2016-10-26 | 浙江绿果新材料有限公司 | Hyperconcentration anhydrous laundry detergent as well as preparation method and laundry beads thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111286414A (en) * | 2019-11-28 | 2020-06-16 | 纳爱斯浙江科技有限公司 | Clothing fragrance retaining bead and preparation method thereof |
| CN111286414B (en) * | 2019-11-28 | 2021-04-27 | 纳爱斯浙江科技有限公司 | Clothing fragrance retaining bead and preparation method thereof |
| EP4206310A1 (en) * | 2021-12-29 | 2023-07-05 | Henkel IP & Holding GmbH | Unit dose product comprising a liquid composition with encapsulated fragrance |
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|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180921 |
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| RJ01 | Rejection of invention patent application after publication |