CN108542863B - Blackhead-removing flour and preparation method thereof - Google Patents

Abstract

The invention relates to blackhead-removing cleansing powder and a preparation method thereof, relates to the technical field of daily chemical cleaning products, and solves the problem of uncomfortable feeling of tight and dry face. The amino acid surfactant and the soapberry fruit extract are matched, so that the face cleaning powder can generate rich and stable foam, is beneficial to cleaning facial skin, and is mild in texture; the combination of the radix Trichosanthis Cucumeroidis powder and herba Spinaciae extract is helpful for cleaning blackhead and astringing follicular orifice; the combination of the skimmed milk powder, the pawpaw extract and the collagen powder is beneficial to moistening the facial skin and reducing the face tightening and discomfort.

Description

Blackhead-removing flour and preparation method thereof

Technical Field

The invention relates to the technical field of daily chemical cleaning products, and particularly relates to blackhead removing flour and a preparation method thereof.

Background

With the acceleration of the pace of life of people and the aggravation of urban air pollution, the face exposed outside is always full of oil. The cosmetics products are also increasingly popular, and as an important branch of cosmetics, the cosmetics take an important position in modern life, and the cleaning is the first step of vital skin care. The clean skin can absorb the following essences, lotions, creams and other nursing items to moisten each cell. Particularly in summer, the skin is subjected to high temperature and violent solarization, and isolation, sun protection, foundation make-up, color make-up, even dust, bacteria and the like in the atmosphere are also used for increasing the pressure of the skin, so that the skin is especially important to be cleaned. If the grease and dirt on the surface layer of the skin are not washed clean, the retained grease and dirt not only damage the skin, but also form a closed barrier to influence the penetration and absorption of nutrients in the subsequent skin care products.

At present, the variety of face cleaning products is very large, and particularly, the face cleaning products for deep cleaning and blackhead removal are also very large, wherein the face cleaning powder is a product for cleaning facial skin, is a powdery substance, and is used for removing facial stains by kneading out foams after water is added. The user usually needs to timely converge the pores after removing the blackheads and deeply cleaning the pores, and after the use of a lot of flour capable of deeply cleaning and converging the pores, the face can be tense and dry, so that the experience of the user is influenced.

Disclosure of Invention

The invention aims to provide blackhead removing cleansing powder which has the advantages of blackhead removing, pore astringing, mildness and facial skin moistening.

The technical purpose of the invention is realized by the following technical scheme:

the blackhead-removing flour comprises the following raw materials in parts by weight: 20-35 parts of amino acid surfactant, 10-18 parts of soapberry fruit extract, 5-10 parts of pawpaw extract, 2-5 parts of collagen powder, 3-8 parts of xylitol, 2-8 parts of radix trichosanthis powder and 1-2 parts of skimmed milk powder.

The amino acid surfactant is an amino acid salt with foaming decontamination capability; the weak-acid amino acid surfactant and the pawpaw extract enable the pH value of the cleansing powder to be 5.5-6.5, the cleansing powder is close to the skin of a human body, and the weak-acid amino acid surfactant is mild, skin-friendly and non-irritant when being applied to the cleansing powder.

The soapberry fruit extract is used as a natural surfactant, has small irritation to the skin, is matched with an amino acid surfactant for use, is beneficial to enhancing the foaming effect of the cleansing powder and enabling the cleansing powder to generate abundant foam, and on the other hand, the amino acid surfactant is milder, so that the irritation of foaming components to the skin is further reduced.

The pawpaw contains rich amino acid, and the amino acid surfactant is matched with the face cleaning powder, so that the face cleaning powder is favorable for keeping the weak acidity property, is more favorable for removing redundant oil on the face, and is more suitable for the face of a human body.

The root of the cucurbita pepo is the root of the cucurbita pepo as the name suggests, contains rich fatty acid and contains components such as kaempferitrin, amino acid, carotene, choline and the like, and is helpful for preventing the loss of facial moisture. The facial cleansing powder containing the radix Trichosanthis Cucumeroidis powder is used for massaging facial skin when it is in contact with water to generate foam, and helps to promote metabolism, remove facial blackheads, inhibit excessive sebum secretion, and astringe pores.

When pores are converged, the skin is often tense, the skimmed milk powder is prepared by removing fat from fresh milk and drying, and the skimmed milk powder is added to massage the face by using foam generated by the face cleaning powder, so that the face is moistened, the discomfort of tense face is relieved, and the face cleaning powder is milder. The fat content in the skimmed milk powder is extremely low, and the skimmed milk powder is beneficial to reducing greasy feeling of the face while moistening the face. The skim milk powder, the pawpaw extract and the collagen powder are mutually matched and act on the skin of the area, so that the skin is moistened and the tension and discomfort of the skin are reduced.

Xylitol is dissolved in water to absorb heat, so that a user can feel cool when cleaning the face by using the face cleaning powder, and the tightening and uncomfortable feeling of the face is further reduced.

Preferably, at least one of oat flour and spinach extract is also included.

Preferably, 2-4 parts of oat flour and 3-6 parts of spinach extract by weight.

Through the technical scheme, the oat flour and the spinach extract both have an anti-oxidation effect, are beneficial to inhibiting the oxidation of the skim milk powder and prolonging the quality guarantee period of the clean flour. The main ingredient of the oat flour is starch which has moisture absorption and moisture retention and is helpful for improving the moisture retention of the clean flour. Thereby reducing the sense of tension and discomfort of the facial skin. The spinach extract also has the effect of shrinking pores, and is matched with the cantaloupe root powder to enhance the effect of shrinking pores.

Preferably, the feed consists of the following raw materials in parts by weight: 20-25 parts of amino acid surfactant, 15-18 parts of soapberry fruit extract, 8-10 parts of pawpaw extract, 2-3.5 parts of collagen powder, 5-8 parts of xylitol, 5.8-8 parts of radix trichosanthis powder, 1-2 parts of skimmed milk powder, 2-3.5 parts of oat powder and 3-4.2 parts of spinach extract.

Through the technical scheme, the synergistic effect of the components is beneficial to removing the blackheads on the face, and after the blackheads on the face are removed, the blackheads on the face can be shrunk, and in addition, the skin is moistened, and the uncomfortable feeling of tight skin is reduced.

Preferably, the amino acid surfactant is selected from at least one of sodium lauroyl glutamate and sodium cocoyl glutamate.

Through the technical scheme, sodium lauroyl glutamate and sodium cocoyl glutamate are used as the surfactants in the cleansing powder, abundant foams are easily generated, the generated foams are stable, dirt on the surface of the face and in pores can be removed, and the cleansing effect is good.

Preferably, the preparation of the soapberry fruit extract comprises the following steps: crushing dried soapberry into soapberry powder, adding the soapberry powder into an ethanol solution with the mass fraction of 60-70%, stirring for 2-3 h under a closed condition at 50-60 ℃, standing for 20-30 min, filtering, taking filtrate, and drying the filtrate under a vacuum condition at 85-90 ℃ to obtain the soapberry extract.

By adopting the technical scheme, the temperature of 85-90 ℃ is higher than the boiling point of ethanol, so that the ethanol in the filtrate can be removed more conveniently, and the soapberry fruit extract with residual ethanol can be obtained.

Preferably, the preparation of the papaya extract comprises the following steps: slicing fresh pawpaw, placing the sliced fresh pawpaw in a vacuum drying oven, drying the sliced pawpaw for 24 hours at the temperature of 65-70 ℃, crushing the pawpaw to obtain pawpaw powder, mixing the pawpaw powder with ethanol with the mass fraction of 70-75%, carrying out ultrasonic treatment at room temperature for 30-40 min, standing for 20-30 min, and filtering to obtain filter residue I and filtrate I; mixing the filter residue I with distilled water, performing ultrasonic treatment at room temperature for 30-40 min, standing for 20-30 min, and filtering again to obtain filter residue II and filtrate II; and mixing the filtrate I and the filtrate II, concentrating in a rotary evaporator in vacuum to obtain a concentrated solution, and drying the concentrated solution at 85-90 ℃ in vacuum to obtain the pawpaw extract.

Through the technical scheme, the yield of the pawpaw extract is improved by the aid of two times of ultrasonic treatment, in addition, ethanol is contained in the first filtrate and the second filtrate, the ethanol directly contacts with skin and has an irritation effect on the skin, the concentrated solution is dried at the temperature of 85-90 ℃, the boiling point of the ethanol is 78 ℃, the ethanol in the mixed solution is removed, the pawpaw extract without ethanol residues is obtained, and the pawpaw extract is more suitable for being used in mild face cleaning powder.

Preferably, the preparation of the spinach extract comprises the following steps:

cleaning fresh spinach, crushing the spinach into spinach paste after cleaning, and performing reduced pressure suction filtration on the spinach paste to obtain filtrate; and (3) concentrating the filtrate in vacuum in a rotary evaporator to obtain a concentrated solution, and drying in vacuum at the temperature of 60-70 ℃ to obtain the spinach extract.

Through the technical scheme, the spinach extract is directly obtained from the spinach paste, and other auxiliary agents are not added, so that the spinach extract is more natural.

The invention also aims to provide a preparation method of the blackhead-removed flour, which enables the components in the flour to be mixed more uniformly.

In order to achieve the second purpose, the invention provides the following technical scheme:

a preparation method of blackhead-removing flour comprises the following operation steps:

the method comprises the following steps: uniformly mixing the soapberry fruit extract, the papaya extract and the spinach extract, and then carrying out ball milling to obtain a first mixture;

step two: uniformly mixing amino acid surfactant, xylitol, oat flour, potato root powder and skim milk powder, and grinding to obtain a second mixture;

step three: and uniformly mixing the first mixture and the second mixture to obtain the prepared flour.

By adopting the method, on one hand, the particle sizes of the soapberry fruit extract, the pawpaw extract and the spinach extract are finer through ball milling, so that the soapberry fruit extract, the pawpaw extract and the spinach extract are mixed more uniformly, and the first mixture obtained after ball milling is mixed with the second mixture to be adsorbed on the outer surfaces of the components in the second component more easily, so that the uniformity of mixing of the components of the flour can be improved.

The amino acid surfactant, the xylitol, the oat flour, the potato root powder and the skim milk powder are uniformly mixed and then ground, so that the dispersion uniformity of each component in the second mixture can be improved.

Preferably: the first mixture in step one can pass through a 320 mesh screen and the second mixture in step two can pass through a 100 mesh screen.

By adopting the method, the particle sizes of the soapberry fruit extract, the pawpaw extract and the spinach extract are fine, which is beneficial to enhancing the adsorption of the soapberry fruit extract, the pawpaw extract and the spinach extract on the surfaces of other components.

In conclusion, the invention has the following beneficial effects:

1. the amino acid surfactant is matched with the soapberry fruit extract, so that the face cleaning powder can generate rich and stable foam, is beneficial to cleaning facial skin, and is mild in texture;

2. the combination of the radix Trichosanthis Cucumeroidis powder and herba Spinaciae extract is helpful for cleaning blackhead and astringing follicular orifice;

3. the combination of the skimmed milk powder, the pawpaw extract and the collagen powder is beneficial to moistening the facial skin and reducing the face tightening and discomfort.

Detailed Description

The present invention will be described in further detail with reference to examples.

Example 1

Preparing the soapberry fruit extract:

pulverizing dried fructus Sapindi Mukouossi into fructus Sapindi Mukouossi powder, adding the fructus Sapindi Mukouossi powder into 60% ethanol solution, stirring at 50 deg.C under sealed condition for 2 hr, standing for 20min, filtering, and oven drying the filtrate at 85 deg.C under vacuum condition to obtain fructus Sapindi Mukouossi extract.

Preparing a pawpaw extract:

slicing fresh pawpaw, drying in a vacuum drying oven at 65 ℃ for 24h, crushing the pawpaw slices to obtain pawpaw powder, mixing the pawpaw powder with ethanol with the mass fraction of 70%, performing ultrasonic treatment at room temperature for 30min, standing for 20min, and filtering to obtain filter residue I and filtrate I. Mixing the filter residue I with distilled water, performing ultrasonic treatment at room temperature for 40min, standing for 30min, and filtering again to obtain filter residue II and filtrate II; mixing the first filtrate and the second filtrate, vacuum concentrating in a rotary evaporator to obtain concentrated solution, and oven drying the concentrated solution at 85 deg.C under vacuum to obtain fructus Chaenomelis extract.

The preparation of spinach extract comprises the following steps:

cleaning fresh spinach, crushing the spinach into spinach paste after cleaning, and performing reduced pressure suction filtration on the spinach paste to obtain filtrate; concentrating the filtrate in a rotary evaporator under vacuum to obtain concentrated solution, and vacuum drying at 60 deg.C to obtain herba Spinaciae extract.

Preparing blackhead-removing flour:

and (3) uniformly mixing 10g of the soapberry fruit extract, 5g of the pawpaw extract and 3g of the spinach extract, then carrying out ball milling for 1h to obtain a first mixture capable of passing through a 320-mesh screen. Uniformly mixing 20g of sodium lauroyl glutamate, 3g of xylitol, 2g of oat flour, 2g of radix Trichosanthis Cucumeroidis powder and 1g of skimmed milk powder, grinding for 30min to obtain a second mixture capable of passing through a 100-mesh sieve. And uniformly mixing the first mixture and the second mixture to obtain the prepared blackhead-removed flour.

Example 2

Preparing the soapberry fruit extract:

pulverizing dried fructus Sapindi Mukouossi into fructus Sapindi Mukouossi powder, adding 70 wt% ethanol solution, stirring at 60 deg.C under sealed condition for 3 hr, standing for 30min, filtering, and oven drying the filtrate at 90 deg.C under vacuum condition to obtain fructus Sapindi Mukouossi extract.

Preparing a pawpaw extract:

slicing fresh pawpaw, drying in a vacuum drying oven at 70 ℃ for 24h, crushing the pawpaw slices to obtain pawpaw powder, mixing the pawpaw powder with 75% of ethanol by mass, performing ultrasonic treatment at room temperature for 40min, standing for 30min, and filtering to obtain filter residue I and filtrate I; mixing the filter residue I with distilled water, performing ultrasonic treatment at room temperature for 30min, standing for 20min, and filtering again to obtain filter residue II and filtrate II; mixing the first filtrate and the second filtrate, vacuum concentrating in a rotary evaporator to obtain concentrated solution, and oven drying the concentrated solution at 90 deg.C under vacuum to obtain fructus Chaenomelis extract.

The preparation of spinach extract comprises the following steps:

cleaning fresh spinach, crushing the spinach into spinach paste after cleaning, and performing reduced pressure suction filtration on the spinach paste to obtain filtrate; vacuum concentrating the filtrate in rotary evaporator to obtain concentrated solution, and vacuum drying at 70 deg.C to obtain herba Spinaciae extract.

Preparing blackhead-removing flour:

and (3) uniformly mixing 18g of the soapberry fruit extract, 10g of the pawpaw extract and 6g of the spinach extract, then carrying out ball milling, and obtaining a first mixture capable of passing through a 320-mesh screen after 1h of ball milling. Uniformly mixing 35g of sodium cocoyl glutamate, 8g of xylitol, 4g of oat flour, 5.8g of radix Trichosanthis Cucumeroidis powder and 1.5g of skimmed milk powder, grinding for 30min to obtain a second mixture capable of passing through a 100-mesh sieve. And uniformly mixing the first mixture and the second mixture to obtain the prepared blackhead-removed flour.

Examples 3 to 6

The preparation of the soapberry fruit extract, the spinach extract and the papaya extract is the same as the example, the preparation method of the flour is the same as the example 1, and the specific dosage of each component is shown in table 1.

TABLE 1 Components and amounts thereof in examples 3-6

Comparative example 1

The whole wheat flour was the same as in example 1 except that it did not contain the powder of potato roots and the extract of spinach.

Comparative example 2

The procedure of example 1 was repeated except that the cleansing flour contained no xylitol and no skim milk powder.

Xylitol in examples 1-6 and comparative example 1 was purchased from Western No Yuhua biotechnology, Inc.

And (4) testing results:

80 testers with blackheads on their faces were selected and divided into 8 groups, each group of the testers used the cleansing powders of examples 1-6 and comparative examples 1-2, respectively, once a day for 7 days, and the blackheads on the testers' faces were compared with the blackheads before 7 days, and the users were asked to evaluate whether the faces were tight after the cleansing powders were used. The moisture value of the face of the testee after the flour is used for 30min by using a skin moisture detector, and the average value of each group of people is calculated.

TABLE 2 evaluation criteria of face powders

TABLE 3 test results table

As can be seen from the data in the table 3, the blackhead removing cleansing powder prepared by the formula and the method has good blackhead removing effect, and the skin is moist and has no tight discomfort after use. The data of comparative example and comparative example 1 show that the combination of the cantaloupe root powder and spinach extract contributes to the improvement of the blackhead removing effect of the cleaning flour. The data of the comparative example and the comparative example 2 show that the combination of the xylitol, the skim milk powder and the pawpaw extract is helpful for improving the skin comfort of the cleaning flour after use, moistening the skin and reducing the tightening and uncomfortable feeling of the skin.

The above description is only a preferred embodiment of the present invention, and the protection scope of the present invention is not limited to the above embodiments, and all technical solutions belonging to the idea of the present invention belong to the protection scope of the present invention. It should be noted that modifications and embellishments within the scope of the invention may occur to those skilled in the art without departing from the principle of the invention, and are considered to be within the scope of the invention.

Claims (2)

1. The preparation method of the blackhead removing cleansing powder is characterized by comprising the following raw materials in parts by weight: 25-35 parts of amino acid surfactant, 15-18 parts of soapberry fruit extract, 8-10 parts of pawpaw extract, 3.5-5 parts of collagen powder, 5-8 parts of xylitol, 5.8-8 parts of radix trichosanthis powder and 1.5-2 parts of skimmed milk powder;

oat flour and spinach extract are also included; 3.5-4 parts of oat powder and 4.2-6 parts of spinach extract by weight;

the amino acid surfactant is selected from at least one of sodium lauroyl glutamate and sodium cocoyl glutamate;

the preparation method of the blackhead-removing flour comprises the following steps:

the method comprises the following steps: uniformly mixing the soapberry fruit extract, the papaya extract and the spinach extract, and then carrying out ball milling to obtain a first mixture;

the preparation method of the soapberry fruit extract comprises the following steps: crushing dried soapberry into soapberry powder, adding the soapberry powder into an ethanol solution with the mass fraction of 60-70%, stirring for 2-3 h under a closed condition at 50-60 ℃, standing for 20-30 min, filtering, taking filtrate, and drying the filtrate under a vacuum condition at 85-90 ℃ to obtain a soapberry extract;

the preparation method of the pawpaw extract comprises the following steps: slicing fresh pawpaw, placing the sliced fresh pawpaw in a vacuum drying oven, drying the sliced pawpaw for 24 hours at the temperature of 65-70 ℃, crushing the pawpaw to obtain pawpaw powder, mixing the pawpaw powder with ethanol with the mass fraction of 70-75%, carrying out ultrasonic treatment at room temperature for 30-40 min, standing for 20-30 min, and filtering to obtain filter residue I and filtrate I; mixing the filter residue I with distilled water, performing ultrasonic treatment at room temperature for 30-40 min, standing for 20-30 min, and filtering again to obtain filter residue II and filtrate II; mixing the filtrate I and the filtrate II, concentrating in a rotary evaporator in vacuum to obtain a concentrated solution, and drying the concentrated solution at 85-90 ℃ in vacuum to obtain a pawpaw extract;

the preparation method of the spinach extract comprises the following steps: cleaning fresh spinach, crushing the spinach into spinach paste after cleaning, and performing reduced pressure suction filtration on the spinach paste to obtain filtrate; concentrating the filtrate in a rotary evaporator in vacuum to obtain a concentrated solution, and drying in vacuum at 60-70 ℃ to obtain a spinach extract;

step two: uniformly mixing amino acid surfactant, xylitol, oat flour, potato root powder and skimmed milk powder, and grinding to obtain a second mixture;

step three: and uniformly mixing the first mixture and the second mixture to obtain the prepared flour.

2. The method as claimed in claim 1, wherein the first mixture in the first step can pass through a 320-mesh screen, and the second mixture in the second step can pass through a 100-mesh screen.