CN108524418A - A kind of natural antiscale whitening toothpaste and preparation method thereof - Google Patents
A kind of natural antiscale whitening toothpaste and preparation method thereof Download PDFInfo
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- CN108524418A CN108524418A CN201810508575.2A CN201810508575A CN108524418A CN 108524418 A CN108524418 A CN 108524418A CN 201810508575 A CN201810508575 A CN 201810508575A CN 108524418 A CN108524418 A CN 108524418A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/02—Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/32—Phosphates of magnesium, calcium, strontium, or barium
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
Abstract
The invention discloses a kind of natural antiscale whitening toothpastes, including antiscale component, whitening component and the antibacterial component of cleaning, the weight ratio of antiscale component, whitening component and the antibacterial component of cleaning to be（1‑3）：（2‑5）：（2‑3）.In antiscale component, whitening component and the antibacterial component of cleaning that the present invention uses, wherein antiscale component with remove tartar and inhibit tartar grow based on, and whitening component is eliminated with tooth-whitening based on the pigmentation object on tooth, and clean antibacterial, it is normal cleaning tooth and using traditional Chinese medicine ingredients gum and enamel and improves based on oral environment have the function of intersecting between three.
Description
Technical field
The present invention relates to daily chemical product field, specifically a kind of natural antiscale whitening toothpaste and preparation method thereof.
Background technology
It is to remove plaque, soft dirt and swill by toothbrush to brush teeth, and keeps a kind of method of oral cleaning；It is also people
Self remove bacterial plaque, prevent periodontosis occur, development and recurrence main means.And during brushing teeth, the work(of toothpaste
It can also take care of one's teeth without the function of having lubrication cleaning and scale removal, tooth is avoided to be damaged by toothbrush.Simultaneously with human body body
Phenomena such as aging of body, tooth will appear loosening and fall off, be a kind of performance that function of human body is degenerated, and causes the edible food of people
The inconvenience of object, is unfavorable for health.The whitening of tooth is also most important simultaneously.
Face tooth mobility, Chinese traditional treatment tooth mobility pass through " kidney tonifying marrow facilitating, swelling and pain relieving, righting based on kidney tonifying
The method of eliminating evil " dredges periodontal blood circulation, increases periodontal sclerotin, into tooth calcification, fast quick-recovery periodontium and alveolar bone life
Function is managed, the purpose of permanent tooth shield gum is finally reached.Therefore common drug is as follows in Chinese medicine：
Pseudo-ginseng cauline leaf：Acrid flavour temperature enters liver, stomach two passes through.Hemostasis analgesic therapy, pesticide and disinfectant, ancient medicine book say " the same ginseng of pseudo-ginseng work(, old friend
Claim ginseng nugrsery seven, is the most precious person of Chinese medicine." oral bacterial infections, haematemesis, traumatic hemorrhage, carbuncle swells carbuncle etc. are controlled, contribute to mouth
Chamber is sterilized, and alveolus is cleaned, and restores fresh breath.
Hundred hay-scenteds：Acrid flavour temperature enters liver, stomach two passes through.Stop blooding analgesic therapy, pesticide and disinfectant, ancient medicine book say " the same ginseng of pseudo-ginseng work(, therefore
People claims ginseng nugrsery seven, is the most precious person of Chinese medicine." oral bacterial infections, haematemesis, traumatic hemorrhage, carbuncle swells carbuncle etc. are controlled, contribute to
Sterilizing oral cleans alveolus, restores fresh breath.
Cuttlebone：It is called cuttle bone, cuttlebone, nature and flavor are salty, puckery, temperature.Returns spleen, kidney channel.Stop with astringing to arrest bleeding, relieving haperacidity
Bitterly, the function of hygroscopic sore.It includes clean ingredient, is finely ground into powder, brushes teeth except tooth stain with this side, makes tooth can be by xanthochromia
In vain, it is the common good medicine for cleaning tooth.
Willow powder：It is bitterly puckery, there are fragrant wind-dispelling, removing toxic substances analgesic, the work(of apocenosis detumescence and the permanent tooth that cleans the teeth.Gu has " poplar branch
Wipe tooth method " say,《Platform is secret wants at place》In be loaded with and " often stung towards branch of the willow soft, point takes medicine to wipe tooth, fragrant and bright and clean." therefore, willow
Powder is indispensable one of the formula that cleans one's teeth at all times.
But the living habit of modern, especially various foods it is edible etc., cause tooth can be by different degrees of
Damage, and the tooth-brushing habit that people think little of can not make up the damage of tooth, it is therefore desirable to a kind of toothpaste of excellent effect,
During people's use, tooth can not only be cleaned, moreover it is possible to which long-acting takes care of one's teeth.
Invention content
A variety of Chinese medicine composition is used the purpose of the present invention is to provide a kind of so that toothpaste does not stimulate human oral cavity,
Improve natural antiscale whitening toothpaste of oral environment and preparation method thereof simultaneously, to solve mentioned above in the background art ask
Topic.
To achieve the above object, the present invention provides the following technical solutions：
A kind of natural antiscale whitening toothpaste, including antiscale component, whitening component and the antibacterial component of cleaning, antiscale component, whitening group
Point and clean the weight ratio of antibacterial component and be（1-3）：（2-5）：（2-3）；
The antiscale component：3-5 parts of alum powder, 10-15 parts of pseudo-ginseng cauline leaf powder, 10-15 parts of hundred hay-scented powder, pounce 10-
16 parts, 3-7 parts of willow powder；
The whitening component：8-12 parts of orange peel powder, 3-5 parts of brown sugar, 8-12 parts of dried peppermint leaf powder, 8-12 parts of celery powder；
The antibacterial component of cleaning：8-16 parts of Astragalus Root P.E, 3-7 parts of ginseng extract, 2-6 parts of Notogineng Extract, food-grade
7-13 parts of silica, 2-4 parts of chamomile extract, 10-16 parts of plant fiber abrasive grain, strontium-incorporated hydroxyapatite nanoparticle 12-14
Part, 1-3 parts of foaming agent, 1-3 parts of surfactant, 5-7 parts of moisturizer, 1-3 parts of thickener, 30-40 parts of deionized water, polypropylene
8-12 parts of acid polymer.
Preferably, the weight ratio of antiscale component, whitening component and the antibacterial component of cleaning is 2：3.5：2.5；
The antiscale component：4 parts of alum powder, 12.5 parts of pseudo-ginseng cauline leaf powder, 12.5 parts of hundred hay-scented powder, 13 parts of pounce, poplar
5 parts of willow powder；
The whitening component：10 parts of orange peel powder, 4 parts of brown sugar, 10 parts of dried peppermint leaf powder, 10 parts of celery powder；
The antibacterial component of cleaning：12 parts of Astragalus Root P.E, 5 parts of ginseng extract, 4 parts of Notogineng Extract, food-grade titanium dioxide
10 parts of silicon, 3 parts of chamomile extract, 13 parts of plant fiber abrasive grain, 13 parts of strontium-incorporated hydroxyapatite nanoparticle, 2 parts of foaming agent, surface
2 parts of activating agent, 6 parts of moisturizer, 2 parts of thickener, 35 parts of deionized water, 10 parts of acrylic acid polymer.
As a further solution of the present invention：The moisturizer is D-sorbite, and surfactant is lecithin, thickener
It is the raw material of food-grade for sodium carboxymethylcellulose, hydroxyethyl cellulose or carbomer, ensures the safety used.
As a further solution of the present invention：The alum powder, pseudo-ginseng cauline leaf powder, hundred hay-scented powder, pounce, willow
Powder, orange peel powder, dried peppermint leaf powder, celery powder are to be ground into the powder that grain size reaches 20-30 μm by milling apparatus by raw material
Last particle, by alum powder, pseudo-ginseng cauline leaf powder, hundred hay-scented powder, pounce, willow powder constitute antiscale component with tooth
When contact, the dirt of dental surface can be rubbed off, adequately cleans tooth, while its tiny structure can be filled into and be formed sediment
The position of the swills such as powder accumulation, plays the role of the effect of long lasting scale prevention, and play firm tooth, while in whitening component
Orange peel powder in acidic materials can soften dental surface pigementation, and dried peppermint leaf powder（Peppermint oil）And celery powder（It is fine
Dimension element and multivitamin）In nutritional ingredient can dilute acidic materials, while can help to protect tooth with anti-inflammatory analgetic
Gum avoids stimulating；
As a further solution of the present invention：The plant fiber abrasive grain and food grade silicon dioxide are ground by milling apparatus
Grain size reaches 40-60 μm of powder particle, and strontium-incorporated hydroxyapatite nanoparticle is nano level material, and cleaning is antibacterial to pass through Chinese medicine
Ingredient improves tooth environment, while strontium-incorporated hydroxyapatite nanoparticle can restore the enamel of dental surface so that toothpaste can
It keeps dental health and improves resistance.
As a further solution of the present invention：The preparation method of the natural antiscale whitening toothpaste, is as follows：
（1）The preparation of raw material, wherein alum powder, pseudo-ginseng cauline leaf powder, hundred hay-scented powder, pounce, willow powder, orange peel powder,
Dried peppermint leaf powder, plant fiber abrasive grain and food grade silicon dioxide are prepared by milling apparatus cryogrinding, cryogrinding, plant
Fiber abrasive grain is prepared using recombination hair method, and strontium-incorporated hydroxyapatite nanoparticle is prepared using chemical combination method；
（2）By the mixing of antiscale component, in the high-speed mixer that each component is placed, control mixing temperature is 3-10 DEG C of progress
It is spare after mixing；
（3）The mixing of whitening component, in the high-speed mixer that each component is placed, and it is spare after being mixed under room temperature；
（4）The mixing of antibacterial component is cleaned, first by food grade silicon dioxide part, plant fiber abrasive grain part, strontium-incorporated hydroxyapatite
It is mixed in nanoparticle part, acrylic acid polymer and deionized water merging high-speed mixer, then controls the mixing of mixing apparatus
Temperature sequentially adds chamomile extract, Astragalus Root P.E, ginseng extract and Notogineng Extract after 3-10 DEG C, and makes it
After mixing, the mixing temperature of mixing apparatus is increased at 20-25 DEG C, finally by foaming agent, surfactant, moisturizer, increasing
Thick dose, acrylic acid polymer sequentially add, it is spare after the completion of mixing；
（5）Antiscale component, whitening component and antibacterial three components of component of cleaning are proportionally stirred, after standing 24 hours
It can pack.
Whole needs of the invention are mixed in the environment of bacteria-and dust-free, ensure the safe and healthy of product.
As a further solution of the present invention：The step（1）The preparation method of middle strontium-incorporated hydroxyapatite nanoparticle is as follows：
Ammonium dibasic phosphate solution side is added and is stirred in calcium nitrate solution, and calcium hydroxyl phosphorus is obtained after adjusting solution Ph values to 9-11
Lime stone suspension, while ultrasonic generator being placed in reaction vessel, it is gradually added into ammonium dibasic phosphate solution and passes through stirring
Device cooperation is uniformly mixed, and strontium nitrate solution is finally added dropwise, strontium-incorporated hydroxyapatite nanoparticle is can be obtained after being precipitated,
It is stored after drying spare.
As a further solution of the present invention：The step（1）The preparation method of middle plant fiber abrasive grain is as follows：Using water
Solution obtains plant cellulose, and then plant cellulose is shaped and dried at bulk, then powder in present grinding device
It is broken, it is ground finally by grinder, obtains granular plant fiber abrasive grain and can be good at brush them, have simultaneously
Suction-operated can adsorb the pollutants such as bacterium.
As a further solution of the present invention：The step（1）Middle grinding temperature is 0-3 DEG C.
As a further solution of the present invention：The step（2）Middle mixing temperature is 3-10 DEG C.
Compared with prior art, the beneficial effects of the invention are as follows：
In antiscale component, whitening component and the antibacterial component of cleaning that the present invention uses, wherein antiscale component is to remove tartar and press down
Based on tartar processed growth, and whitening component is eliminated with tooth-whitening based on the pigmentation object on tooth, and cleans antibacterial, is
It is normal to clear up tooth and use traditional Chinese medicine ingredients gum and enamel and improve based on oral environment, there is intersection between three
Function.
Then the present invention is being mixed, can made during manufacturing, according to each by individually matching each component
Component designs preparation process, utmostly retains beneficiating ingredient, is finally mixed with so that the nutrition of raw material and active principle are most
The passage of smallization.
The present invention is equipped with the effect of scale removal and whitening so that the damage of tooth can to improve based on human oral cavity environment
It is gradually repaired, improves the effect brushed teeth, while ingredient is natural, it is non-stimulated to human body.
Specific implementation mode
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of natural antiscale whitening toothpaste, including antiscale component, whitening component and the antibacterial component of cleaning,
The weight ratio of antiscale component, whitening component and the antibacterial component of cleaning is 1：2：2；
The antiscale component：3 parts of alum powder, 10 parts of pseudo-ginseng cauline leaf powder, 10 parts of hundred hay-scented powder, 10 parts of pounce, willow powder 3
Part；
The whitening component：8 parts of orange peel powder, 3 parts of brown sugar, 8 parts of dried peppermint leaf powder, 8 parts of celery powder；
The antibacterial component of cleaning：8 parts of Astragalus Root P.E, 3 parts of ginseng extract, 2 parts of Notogineng Extract, food grade silicon dioxide
7 parts, 2 parts of chamomile extract, 10 parts of plant fiber abrasive grain, 12 parts of strontium-incorporated hydroxyapatite nanoparticle, 1 part of foaming agent, surface live
1 part of agent of property, 5 parts of moisturizer, 1 part of thickener, 30 parts of deionized water, 8 parts of acrylic acid polymer.
The preparation method of the natural antiscale whitening toothpaste, is as follows：
（1）The preparation of raw material, wherein alum powder, pseudo-ginseng cauline leaf powder, hundred hay-scented powder, pounce, willow powder, orange peel powder,
Dried peppermint leaf powder, plant fiber abrasive grain and food grade silicon dioxide are prepared by milling apparatus cryogrinding, cryogrinding temperature
It it is 0 DEG C, to ensure the activity of ingredient；
The preparation method of the strontium-incorporated hydroxyapatite nanoparticle is as follows：Ammonium dibasic phosphate solution side is added and is stirred to calcium nitrate
In solution, and solution Ph values are adjusted to obtaining calcium hydroxyapatite suspension after 9, while ultrasonic generator is placed in reaction
In container, it is gradually added into ammonium dibasic phosphate solution and is uniformly mixed by agitating device cooperation, strontium nitrate solution is finally added dropwise,
It can be obtained strontium-incorporated hydroxyapatite nanoparticle after being precipitated, stored after dry spare；
The preparation method of the plant fiber abrasive grain is as follows：Plant cellulose is obtained using Hydrolyze method, then by plant cellulose
It is shaped and is dried at bulk, then crushed in present grinding device, ground finally by grinder, obtain graininess
Plant fiber abrasive grain can be good at brush them, while there is suction-operated, the pollutants such as bacterium can be adsorbed；
（2）By the mixing of antiscale component, in the high-speed mixer that each component is placed, control mixing temperature, which is 3 DEG C, to be mixed
It is spare after conjunction；
（3）The mixing of whitening component, in the high-speed mixer that each component is placed, and it is spare after being mixed under room temperature；
（4）The mixing of antibacterial component is cleaned, first by food grade silicon dioxide part, plant fiber abrasive grain part, strontium-incorporated hydroxyapatite
It is mixed in nanoparticle part, acrylic acid polymer and deionized water merging high-speed mixer, then controls the mixing of mixing apparatus
Temperature sequentially adds chamomile extract, Astragalus Root P.E, ginseng extract and Notogineng Extract after 3-10 DEG C, and makes it
After mixing, the mixing temperature of mixing apparatus is increased at 20 DEG C, finally by foaming agent, surfactant, moisturizer, thickening
Agent, acrylic acid polymer sequentially add, spare after the completion of mixing.
（5）Antiscale component, whitening component and antibacterial three components of component of cleaning are proportionally stirred, it is small to stand 24
When after can pack.
Embodiment 2
In the embodiment of the present invention, a kind of natural antiscale whitening toothpaste, including antiscale component, whitening component and the antibacterial component of cleaning,
The weight ratio of antiscale component, whitening component and the antibacterial component of cleaning is 2：3.5：2.5；
The antiscale component：4 parts of alum powder, 12.5 parts of pseudo-ginseng cauline leaf powder, 12.5 parts of hundred hay-scented powder, 13 parts of pounce, poplar
5 parts of willow powder；
The whitening component：10 parts of orange peel powder, 4 parts of brown sugar, 10 parts of dried peppermint leaf powder, 10 parts of celery powder；
The antibacterial component of cleaning：12 parts of Astragalus Root P.E, 5 parts of ginseng extract, 4 parts of Notogineng Extract, food-grade titanium dioxide
10 parts of silicon, 3 parts of chamomile extract, 13 parts of plant fiber abrasive grain, 13 parts of strontium-incorporated hydroxyapatite nanoparticle, 2 parts of foaming agent, surface
2 parts of activating agent, 6 parts of moisturizer, 2 parts of thickener, 35 parts of deionized water, 10 parts of acrylic acid polymer.
The preparation method of the natural antiscale whitening toothpaste, is as follows：
（1）The preparation of raw material, wherein alum powder, pseudo-ginseng cauline leaf powder, hundred hay-scented powder, pounce, willow powder, orange peel powder,
Dried peppermint leaf powder, plant fiber abrasive grain and food grade silicon dioxide are prepared by milling apparatus cryogrinding, cryogrinding temperature
It it is 2 DEG C, to ensure the activity of ingredient；
The preparation method of the strontium-incorporated hydroxyapatite nanoparticle is as follows：Ammonium dibasic phosphate solution side is added and is stirred to calcium nitrate
In solution, and solution Ph values are adjusted to obtaining calcium hydroxyapatite suspension after 10, while ultrasonic generator being placed in instead
It answers in container, is gradually added into ammonium dibasic phosphate solution and is uniformly mixed by agitating device cooperation, it is molten that strontium nitrate is finally added dropwise
Liquid can be obtained strontium-incorporated hydroxyapatite nanoparticle, be stored after dry spare after being precipitated；
The preparation method of the plant fiber abrasive grain is as follows：Plant cellulose is obtained using Hydrolyze method, then by plant cellulose
It is shaped and is dried at bulk, then crushed in present grinding device, ground finally by grinder, obtain graininess
Plant fiber abrasive grain can be good at brush them, while there is suction-operated, the pollutants such as bacterium can be adsorbed；
（2）By the mixing of antiscale component, in the high-speed mixer that each component is placed, control mixing temperature is 6.5 DEG C of progress
It is spare after mixing；
（3）The mixing of whitening component, in the high-speed mixer that each component is placed, and it is spare after being mixed under room temperature；
（4）The mixing of antibacterial component is cleaned, first by food grade silicon dioxide part, plant fiber abrasive grain part, strontium-incorporated hydroxyapatite
It is mixed in nanoparticle part, acrylic acid polymer and deionized water merging high-speed mixer, then controls the mixing of mixing apparatus
Temperature sequentially adds chamomile extract, Astragalus Root P.E, ginseng extract and Notogineng Extract after 6.5 DEG C, and makes it
After mixing, the mixing temperature of mixing apparatus is increased at 22.5 DEG C, finally by foaming agent, surfactant, moisturizer, thickening
Agent, acrylic acid polymer sequentially add, spare after the completion of mixing.
（5）Antiscale component, whitening component and antibacterial three components of component of cleaning are proportionally stirred, it is small to stand 24
When after can pack.
Embodiment 3
In the embodiment of the present invention, a kind of natural antiscale whitening toothpaste, including antiscale component, whitening component and the antibacterial component of cleaning,
The weight ratio of antiscale component, whitening component and the antibacterial component of cleaning is 3：5：3；
The antiscale component：5 parts of alum powder, 15 parts of pseudo-ginseng cauline leaf powder, 15 parts of hundred hay-scented powder, 16 parts of pounce, willow powder 7
Part；
The whitening component：12 parts of orange peel powder, 5 parts of brown sugar, 12 parts of dried peppermint leaf powder, 12 parts of celery powder；
The antibacterial component of cleaning：16 parts of Astragalus Root P.E, 7 parts of ginseng extract, 6 parts of Notogineng Extract, food-grade titanium dioxide
13 parts of silicon, 4 parts of chamomile extract, 16 parts of plant fiber abrasive grain, 14 parts of strontium-incorporated hydroxyapatite nanoparticle, 3 parts of foaming agent, surface
3 parts of activating agent, 7 parts of moisturizer, 3 parts of thickener, 40 parts of deionized water, 12 parts of acrylic acid polymer.
The preparation method of the natural antiscale whitening toothpaste, is as follows：
（1）The preparation of raw material, wherein alum powder, pseudo-ginseng cauline leaf powder, hundred hay-scented powder, pounce, willow powder, orange peel powder,
Dried peppermint leaf powder, plant fiber abrasive grain and food grade silicon dioxide are prepared by milling apparatus cryogrinding, cryogrinding temperature
It it is 3 DEG C, to ensure the activity of ingredient；
The preparation method of the strontium-incorporated hydroxyapatite nanoparticle is as follows：Ammonium dibasic phosphate solution side is added and is stirred to calcium nitrate
In solution, and solution Ph values are adjusted to obtaining calcium hydroxyapatite suspension after 11, while ultrasonic generator being placed in instead
It answers in container, is gradually added into ammonium dibasic phosphate solution and is uniformly mixed by agitating device cooperation, it is molten that strontium nitrate is finally added dropwise
Liquid can be obtained strontium-incorporated hydroxyapatite nanoparticle, be stored after dry spare after being precipitated；
The preparation method of the plant fiber abrasive grain is as follows：Plant cellulose is obtained using Hydrolyze method, then by plant cellulose
It is shaped and is dried at bulk, then crushed in present grinding device, ground finally by grinder, obtain graininess
Plant fiber abrasive grain can be good at brush them, while there is suction-operated, the pollutants such as bacterium can be adsorbed；
（2）By the mixing of antiscale component, in the high-speed mixer that each component is placed, control mixing temperature, which is 10 DEG C, to be mixed
It is spare after conjunction；
（3）The mixing of whitening component, in the high-speed mixer that each component is placed, and it is spare after being mixed under room temperature；
（4）The mixing of antibacterial component is cleaned, first by food grade silicon dioxide part, plant fiber abrasive grain part, strontium-incorporated hydroxyapatite
It is mixed in nanoparticle part, acrylic acid polymer and deionized water merging high-speed mixer, then controls the mixing of mixing apparatus
Temperature sequentially adds chamomile extract, Astragalus Root P.E, ginseng extract and Notogineng Extract after 10 DEG C, and so that it is mixed
After closing uniformly, increase the mixing temperature of mixing apparatus at 25 DEG C, finally by foaming agent, surfactant, moisturizer, thickener,
Acrylic acid polymer sequentially adds, spare after the completion of mixing.
（5）Antiscale component, whitening component and antibacterial three components of component of cleaning are proportionally stirred, it is small to stand 24
When after can pack.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (10)
1. a kind of natural antiscale whitening toothpaste, including antiscale component, whitening component and the antibacterial component of cleaning, which is characterized in that anti-
The weight ratio of dirty component, whitening component and the antibacterial component of cleaning is（1-3）：（2-5）：（2-3）；
The antiscale component：3-5 parts of alum powder, 10-15 parts of pseudo-ginseng cauline leaf powder, 10-15 parts of hundred hay-scented powder, pounce 10-
16 parts, 3-7 parts of willow powder；
The whitening component：8-12 parts of orange peel powder, 3-5 parts of brown sugar, 8-12 parts of dried peppermint leaf powder, 8-12 parts of celery powder；
The antibacterial component of cleaning：8-16 parts of Astragalus Root P.E, 3-7 parts of ginseng extract, 2-6 parts of Notogineng Extract, food-grade
7-13 parts of silica, 2-4 parts of chamomile extract, 10-16 parts of plant fiber abrasive grain, strontium-incorporated hydroxyapatite nanoparticle 12-14
Part, 1-3 parts of foaming agent, 1-3 parts of surfactant, 5-7 parts of moisturizer, 1-3 parts of thickener, 30-40 parts of deionized water, polypropylene
8-12 parts of acid polymer.
2. natural antiscale whitening toothpaste according to claim 1, which is characterized in that antiscale component, whitening component and cleaning
The weight ratio of antibacterial component is 2：3.5：2.5；
The antiscale component：4 parts of alum powder, 12.5 parts of pseudo-ginseng cauline leaf powder, 12.5 parts of hundred hay-scented powder, 13 parts of pounce, poplar
5 parts of willow powder；
The whitening component：10 parts of orange peel powder, 4 parts of brown sugar, 10 parts of dried peppermint leaf powder, 10 parts of celery powder；
The antibacterial component of cleaning：12 parts of Astragalus Root P.E, 5 parts of ginseng extract, 4 parts of Notogineng Extract, food-grade titanium dioxide
10 parts of silicon, 3 parts of chamomile extract, 13 parts of plant fiber abrasive grain, 13 parts of strontium-incorporated hydroxyapatite nanoparticle, 2 parts of foaming agent, surface
2 parts of activating agent, 6 parts of moisturizer, 2 parts of thickener, 35 parts of deionized water, 10 parts of acrylic acid polymer.
3. natural antiscale whitening toothpaste according to claim 1 or 2, which is characterized in that the moisturizer is D-sorbite,
Surfactant is lecithin, and thickener is sodium carboxymethylcellulose, hydroxyethyl cellulose or carbomer, is food-grade
Raw material, ensure the safety used.
4. natural antiscale whitening toothpaste according to claim 1 or 2, which is characterized in that the alum powder, pseudo-ginseng cauline leaf
Powder, hundred hay-scented powder, pounce, willow powder, orange peel powder, dried peppermint leaf powder, celery powder are to pass through milling apparatus by raw material
It is ground into the powder particle that grain size reaches 20-30 μm.
5. natural antiscale whitening toothpaste according to claim 1 or 2, which is characterized in that the plant fiber abrasive grain and food
Grade silica is ground into the powder particle that grain size reaches 40-60 μm by milling apparatus.
6. a kind of preparation method of natural antiscale whitening toothpaste according to any one of claims 1 to 5, which is characterized in that the day
The preparation method of right antiscale whitening toothpaste, is as follows：
（1）The preparation of raw material, wherein alum powder, pseudo-ginseng cauline leaf powder, hundred hay-scented powder, pounce, willow powder, orange peel powder,
Dried peppermint leaf powder, plant fiber abrasive grain and food grade silicon dioxide are prepared by milling apparatus cryogrinding, cryogrinding, plant
Fiber abrasive grain is prepared using recombination hair method, and strontium-incorporated hydroxyapatite nanoparticle is prepared using chemical combination method；
（2）By the mixing of antiscale component, in the high-speed mixer that each component is placed, control mixing temperature is 3-10 DEG C of progress
It is spare after mixing；
（3）The mixing of whitening component, in the high-speed mixer that each component is placed, and it is spare after being mixed under room temperature；
（4）The mixing of antibacterial component is cleaned, first by food grade silicon dioxide part, plant fiber abrasive grain part, strontium-incorporated hydroxyapatite
It is mixed in nanoparticle part, acrylic acid polymer and deionized water merging high-speed mixer, then controls the mixing of mixing apparatus
Temperature sequentially adds chamomile extract, Astragalus Root P.E, ginseng extract and Notogineng Extract after 3-10 DEG C, and makes it
After mixing, the mixing temperature of mixing apparatus is increased at 20-25 DEG C, finally by foaming agent, surfactant, moisturizer, increasing
Thick dose, acrylic acid polymer sequentially add, it is spare after the completion of mixing；
（5）Antiscale component, whitening component and antibacterial three components of component of cleaning are proportionally stirred, after standing 24 hours
It can pack.
7. the preparation method of natural antiscale whitening toothpaste according to claim 6, which is characterized in that the step（1）In
The preparation method of strontium-incorporated hydroxyapatite nanoparticle is as follows：Ammonium dibasic phosphate solution side is added and is stirred in calcium nitrate solution,
And calcium hydroxyapatite suspension is obtained after adjusting solution Ph values to 9-11, while ultrasonic generator is placed in reaction vessel
It is interior, it is gradually added into ammonium dibasic phosphate solution and is uniformly mixed by agitating device cooperation, strontium nitrate solution is finally added dropwise, carries out
It can be obtained strontium-incorporated hydroxyapatite nanoparticle after precipitation, stored after dry spare.
8. the preparation method of natural antiscale whitening toothpaste according to claim 1, which is characterized in that the step（1）In
The preparation method of plant fiber abrasive grain is as follows：Using Hydrolyze method obtain plant cellulose, then by plant cellulose at bulk into
Row shapes and dries, and then crushes in present grinding device, is ground finally by grinder, and it is fine to obtain granular plant
Dimension abrasive grain can be good at brush them.
9. the preparation method of natural antiscale whitening toothpaste according to claim 1, which is characterized in that the step（1）In
Grinding temperature is 0-3 DEG C.
10. the preparation method of natural antiscale whitening toothpaste according to claim 1, which is characterized in that the step（2）In
Mixing temperature is 3-10 DEG C.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109820125A (en) * | 2019-04-02 | 2019-05-31 | 冯德良 | A kind of vegetable beverage prescription |
| CN110775953A (en) * | 2019-11-27 | 2020-02-11 | 中山市科信生物技术有限公司 | Method for synthesizing thermodynamically stable hydroxyapatite with microscopic kinetic reaction limitation |
| CN110859779A (en) * | 2019-11-29 | 2020-03-06 | 重庆登康口腔护理用品股份有限公司 | Oral care product containing plant fiber abrasive and preparation method thereof |
-
2018
- 2018-05-25 CN CN201810508575.2A patent/CN108524418A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109820125A (en) * | 2019-04-02 | 2019-05-31 | 冯德良 | A kind of vegetable beverage prescription |
| CN110775953A (en) * | 2019-11-27 | 2020-02-11 | 中山市科信生物技术有限公司 | Method for synthesizing thermodynamically stable hydroxyapatite with microscopic kinetic reaction limitation |
| CN110859779A (en) * | 2019-11-29 | 2020-03-06 | 重庆登康口腔护理用品股份有限公司 | Oral care product containing plant fiber abrasive and preparation method thereof |
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