KR100811594B1 - Composites and preparation method of toothpsate containing sulfur salts produced the andes mountains - Google Patents

Abstract

A toothpaste composition comprising sulfur salts of the Andes mountains is provided to show functional effects of preventing gingival ailment such as oral disease and gingivitis and inhibiting bad breath. A toothpaste composition comprising sulfur salts of the Andes mountains is characterized in that it is prepared by mixing pulverized Andes mountains sulfur salts with pulverized peel of pear to prepare a sulfur salt mixture, filtering the sulfur salt mixture through 80 mesh, mixing water with increased fine dissolved oxygen with the filtered mixture in a weight ratio of 4:1 to prepare a second mixture, storing the second mixture at a temperature of 13 deg.C for 7 days, sterilizing the stored mixture at a temperature of 65 deg.C for 20 minutes, and extracting the sterilized mixture.

Description

Compositions and preparation method of toothpsate containing sulfur salts produced the Andes Mountains

1 is a manufacturing process showing an embodiment of the present invention

The present invention is a method for producing a toothpaste composition containing the Andes rock salt, including the pre-treatment (mixing and water treatment, after 7 days storage, 65 ℃ 20 minutes sterilization extraction) with Andes rock salt and The present invention relates to a composition and a toothpaste containing the composition. More specifically, the present invention provides a functional toothpaste suitable for high value-added and consumer preferences by manufacturing a toothpaste by using a rock salt, which is a raw material of the present invention, together with a pear shell. will be.

Looking at the related prior art, Registration No. 10-0085705-0000 is 'Toothpaste composition containing bamboo salt' whose main purpose is to prevent periodontal disease prevention, treatment and tooth decay in combination with bamboo salt alone or sodium chloride, registration number 10-0067484-0000 relates to a method for the preparation of a transparent toothpaste composition containing granular salts, which includes complexities in the manufacturing process for mass production and industrialization due to pretreatment of raw materials and limitation of raw materials. There is a technical problem regarding the safety of raw materials. Also, related patents using rock salt, registration number 20-0332693-0000, 'crystal lamp using natural rock salt (fragment)' and 20-2005-0014841, 'internal structure of lighting equipment using rock salt or natural minerals' And the like has been filed. Therefore, there has been no report on the dentifrice composition grafted using pretreated natural rock salt.

Therefore, in the present invention, using the natural Andes rock salt, which is widely known for its high functionality, safety, and consumer preference, in preparing a composition capable of making functional toothpaste excellent for various health such as oral disease, whitening, dermatitis, and blood improvement, grinding The safety and economic efficiency of the toothpaste is considered by applying the composition to the toothpaste manufacturing, which is applied to the manufacture of toothpaste through pear shells, mixed treatment, water treatment and sterilization. The present invention has been completed in view of the technical problem of the present invention in providing a highly functional toothpaste composition.

The present invention is characterized by a composition that can be applied to the production of functional toothpaste using an Andes rock salt, a method for preparing the same and a toothpaste. Therefore, Figure 1 is a process diagram showing a preferred embodiment of the present invention when described in detail the configuration and operation of the present invention.

The Andes rock salt is purified and washed as the clean, clear water of the glacier melts, repeats for tens of thousands of years, removes impurities through clear wind and sun evaporation, and is a natural pure salt made from nature at 3,700m above sea level. One of its features is sulfur, which contains the biochemical functional aspects of sulfur and is used for natural hot spring baths and acne skin removal.The composition contains 0.1% water, 62.6% total chlorine, and 0.03% sulfate (5.3mg). It is known that sodium chloride (99.26g) is free from heavy metals (arsenic, lead, cadmium, mercury, etc.) and bacteria, and has many useful minerals compared to ordinary salts. In addition, it is known that there are no impurities at all, essential minerals are present in an ionic state, purity is good, and far-infrared salts have effects such as oral disease, odor removal, whitening, and blood improvement. On the other hand, sulfur in rock salt is a mineral that is absorbed only in the form of organic matter and is a mineral necessary for tissues of nails, toenails, joints and skin. Its action is known to maintain skin elasticity, skin immunity to control acne, rough skin, psoriasis, wrinkles, hair loss and scalp, eczema, skin eczema. In addition, the large amount of anions and far infrared rays generated from rock salt, along with minerals, help to balance the human body and facilitate metabolism, making the skin soft and elastic and removing mold, bacteria, or toxins from cells. .

In addition, the main application of calcium present in large amounts in rock salt is to form a skeleton and teeth, the main component of the tooth is a crystalline compound called hydroxy apatite composed of calcium and phosphorus. There are many factors that can damage teeth, but there are natural wear, damage caused by brushing habits, and corrosion caused by acid, a metabolite of bacteria. Therefore, the rock salt component is said to be effective in removing oral diseases of the teeth, bad breath, and the like.

Most of the pear sugar is fructose and low in glucose. Unlike apples, organic acids such as malic acid, tin acid and citric acid are only 0.1% and have little sour taste. There are many enzymes in the stomach that help digestion. If you mix pears with bulgogi or sashimi, meat will not only be softened by the action of enzymes but will also improve digestibility. When you're eating a pear, you'll feel embarrassed because there are stalacted stone cells. These stone cells are thick-filmed cells with thickened cell membranes composed of lignin and pentosan. Because these stone cells are present, eating a pear and brushing it with the rest of the stomach will clean the teeth. In addition, the oriental medicine has been used in various ways. The cough comes with a pear juice to eat ginger juice and honey is said to be effective. When I had a severe cough, I cut one pear and mixed it with sheep's milk or milk. When stomach pain is severe, pear leaves are richly sweet and often eaten.

Water is treated with ceramics to increase the dissolved oxygen by making water into ultra-fine bubbles with diameters ranging from 1 to several tens of micrometers, using a water softener having characteristics such as antibacterial, antibacterial, deodorization, bleaching, penetrating power, and surfactant action effects. Water was prepared and used using a microbubble device that has been scientifically proven to enhance the taste depth, promote fermentation, and the like on the final product.

Looking in detail the step-by-step manufacturing method of the present invention using the raw materials grafts,

① Grinding the raw Andes natural rock salt with a grinder (Halled SB-4, Sweden) for 20 minutes,

② grind the skin of the pear with a grinder (Halled SB-4, Sweden) for 10 minutes,

③ mixing the materials of ① and ② by filtration (80 mesh) at a ratio of 1:10 to form a rock salt mixture, and then mixing the rock salt mixture with water-treated water and ground rock salt (4: 1 w / w),

④ ③ After 7 days of storage at 13 ℃, 20 minutes sterilization step,

⑤ extract and concentrate the solution of ④ to powder,

The final powder and toothpaste composition of ⑥ ⑤, abrasive (precipitated calcium carbonate), wetting agent (glycerine, sorbitol liquid), foaming agent (sodium lauryl sulfate), sweetener (stevioside), PH regulator (sodium pyrophosphate), active ingredient (day Mixing with sodium phosphate), fragrance (menthol), solvent (purified water), binder (carboxymethyl cellulose sodium), brightener (titanium dioxide), etc.

⑦ the mixture and powder and flavoring, dilution (glycerol or sorbitol liquid) step,

⑧ is the packaging and product phase of the mixture of ⑦

Hereinafter, the invention will be described in detail with reference to the following examples.

<Example>

1. Materials and Methods

(1) Toothpaste compositions include abrasives (precipitated calcium carbonate), wetting agents (glycerine, sorbitol liquid), foaming agents (sodium lauryl sulfate), sweeteners (stevioside), PH regulators (sodium pyrophosphate), active ingredients (sodium fluorophosphate) ) The basic ingredients of toothpaste, such as fragrance (menthol), solvent (purified water), binder (sodium carboxymethyl cellulose) and brightener (titanium dioxide), were purchased commercially.

The ship was purchased commercially from Sangju Mountain (2006).

(2) Rock salt was purchased from Argentina's natural Andes rock salt.

(3) Preparation of rock salt and pear shells and extraction of water treatment-Raw rock salt is ground for 20 minutes using a grinder (Hallde SB-4, Sweden), and pear shells are pulverized for 10 minutes and then rock salt and pear shells. To a rock salt mixture by mixing 1:10 (w / w), and the rock salt was mixed with a rock salt mixture and a water softener treated water (20 ° C.) 1: 4 (rock salt mixture: a water softener treated water w / w). After dissolution and treatment with a water softener and stored at 13 ° C. for 7 days, sterilization was performed at 65 ° C. for 20 minutes, followed by extraction with a rotary evaporator as an extract.

At this time, the water-cooling machine manufacturing equipment used UP-200 (water-cooling machine) produced by Daewon Bio Co., Ltd., and the pump used for the water-cooling machine was used as a submersible pump Was used to adjust the intensity per 10 meters / second.

(4) Elimination of bad breath-After 20 men and women who are aware of bad breath have been subjected to clinical trials, the same type of meal was used, and the degree of bad breath using a halimeter (Model SB-17, USA) After the exclusion from the experiment, very strong people (over 350) were divided into 5 groups in the Comparative Examples and Examples, and the average value was adjusted to be similar between the groups. After the same meal, 20 people measured the initial bad breath degree after 45 minutes and 90 minutes, and provided the toothbrush and toothpaste according to each composition (Example), and then measured the final bad breath degree after 45 minutes and 90 minutes after 3 minutes

(5) Gingivitis Inhibition Test- This experiment was conducted on 20 subjects in a relatively same environment. The test method was a single blind method, in which all subjects were given the same detergent and toothbrush during the residual effect removal period of 4 weeks before the experiment.

Experimental method was calculated as the average value of the index by dividing the gingiva per tooth into the buccal and lingual. Each gingivitis was evaluated from 0 to 3 points according to Loe's and Silnis's evaluation criteria, and the gingivitis index was calculated on average. .

(6) Bacterial Membrane Index Comparison-20 subjects in the same environment were compared. All the subjects underwent a first-order oral examination before the test to obtain a baseline. The experiment was applied with a single blind method and all subjects were given the same dentifrice and toothbrush of the same standard during the residual effect removal period for 4 weeks prior to the experiment. In this method, 20 ml of water was mixed with 10 drops of plaque, mixed for 1 minute in the mouth, spited out, lightly brushed with water, and the coloration was applied to Quigley & Hein's Turesky modification criteria. .

(7) Andean Natural Salt Toothpaste Composition Preparation

Table 1. Preparation of Natural Salt Toothpaste Compositions

                                             (weight%)

number Ingredient Name Comparative Example 1 Example 1 Example 2 Example 3 One Precipitated Calcium Carbonate 37 25 40 35 2 glycerin - 40 - - 3 Sorbitol solution 45 20 45 44 4 Sodium Lauryl Sulfate 5.0 2.0 2.0 2.0 5 Stevio side 1.5 2.0 2.0 2,0 6 Sodium pyrophosphate 2.5 1.0 2.0 3.0 7 Sodium monofluorophosphate 0.5 1.0 0,5 1.0 8 Titanium dioxide 1.0 0.5 0.5 0.5 9 Carboxymethyl Cellulose Sodium 1.5 1.0 1.5 1.0 10 Tranexamic acid 0.5 0.5 0.5 0.5 11 Spices 1.0 1.5 1.0 1.0 12 Treated Andes Natural Rock Salt and Pear Shell Mixture - 0.01 3.0 9.0 13 Purified water Remaining amount Remaining amount Remaining amount Remaining amount 14 system 100 100 100 100

2. Results and Summary

Table 2. Bad Breath Removal Effects

Treatment sphere base line 45 minutes after eating 90 minutes after eating Comparative Example 1 210 160 170 Example 1 200 150 170 Example 2 220 140 160 Example 3 220 160 175

1) The given value is the average of two experiments

<Result>

 ① In Comparative Example 1, the bad breath removal rate was reduced by 19 ~ 24% after 45 minutes after eating and 90 minutes after eating.

 ② Examples 1, 2 and 3 showed a decrease of about 25 to 36% compared to the baseline. In particular, the case of Example 2 showed the largest decrease with a decrease of 27 to 36%.

Table 3. Comparison of gingivitis inhibition

Treatment sphere base line 3 months later 6 months later Comparative Example 1 0.63 0.57 0.66 Example 1 0.62 0.53 0.44 Example 2 0.61 0.50 0.28 Example 3 0.62 0.50 0.45

1) The given value is the average of two experiments

<Result>

 ① In Comparative Example 1, there is no significant change even after 3 to 6 months.

 ② In Examples 1 and 2, the case of Example 2 showed the greatest reduction.

Table 4. Comparison of Dental Bacterial Membrane Index

Treatment sphere base line 3 months later 6 months later Comparative Example 1 0.77 0.75 0.73 Example 1 0.78 0.73 0.65 Example 2 0.76 0.61 0.40 Example 3 0.76 0.66 0.54

1) The given value is averaged twice in the experiment.

<Result>

 ① Comparative Example 1 shows no significant change after 3 and 6 months.

 ② Example 2 shows the largest reduction among Examples 1, 2, and 3.

As described in detail above, the toothpaste composition containing the Andes rock salt of the present invention and the toothpaste using the same have a great effect that can provide users with functional effects such as oral disease, gum disease prevention or odor control, such as gingivitis. Invention.

Claims (3)

Andean natural rock salt and pear skin are ground and mixed to form a rock salt mixture, After filtering the rock salt mixture to 80 mesh and mixed with water and the mixture of 4: 1 w / w and increased the fine dissolved oxygen by a hydrophobic treatment, to form a secondary mixture, Toothpaste composition containing the Andes rock salt comprising the secondary mixture was stored for 7 days at 13 ℃, sterilized at 65 ℃ 20 minutes, extracted and concentrated extraction Claim 2 was abandoned when the setup registration fee was paid. Pulverizing the skin of andean natural rock salt and pear, respectively, and mixing the ratio of rock salt to pear 1:10 by weight to form a rock salt mixture; Filtration of the rock salt mixture with 80 mesh, followed by mixing with water to increase the microdissolved oxygen in a hydrophobic treatment, and mixing the mixture at a weight ratio of 4: 1 to form a secondary mixture; After storing the secondary mixture at 13 ° C. for 7 days, sterilizing at 65 ° C. for 20 minutes, and extracting and concentrated extracting, the toothpaste composition containing Andes rock salt comprising the step of being prepared. Claim 3 was abandoned when the setup registration fee was paid. In preparing toothpaste using a conventional toothpaste composition,

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