CN108517253A - 一种水基润滑膏及其制备方法 - Google Patents

一种水基润滑膏及其制备方法 Download PDF

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CN108517253A
CN108517253A CN201810459559.9A CN201810459559A CN108517253A CN 108517253 A CN108517253 A CN 108517253A CN 201810459559 A CN201810459559 A CN 201810459559A CN 108517253 A CN108517253 A CN 108517253A
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毛杰
曲波
李子荣
汪徐春
陈君华
张雪梅
刘川
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Anhui University of Science and Technology
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    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/14—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/141—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings monocarboxylic
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    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
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    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
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Abstract

本发明公开了一种水基润滑膏及其制备方法，该润滑膏是由以下重量份原料组成：硬脂酸钠4‑6份，硬脂酸锌1‑3份，石墨微粉1‑4份，乙二醇，5‑10份，季戊四醇，5‑8份，硅油5‑8份，三乙醇胺3‑5份，蒸馏水100‑120份，苯甲酸钠0.5‑1份亚硝酸钠1‑1.5份。本发明的有益效果是具有低软化点，低摩擦系数，抗冲击性和渗透性，减摩性能好，能有效防止器械受损，并且具有优异的抗腐蚀、防锈性能，保证设备在高强度环境下正常工作。

Description

一种水基润滑膏及其制备方法
技术领域：
本发明涉及润滑剂技术领域，具体涉及一种水基润滑膏及其制备方法。
背景技术：
润滑剂是用来降低摩擦阻力，减缓磨损的润滑介质，并且还能对摩擦部件起到冷却和清洗的作用。随着机械自动化程度的不断提高，生产对机械的使用寿命要求越来越高，为了满足机械润滑性能，对润滑膏提出了更多要求。目前的润滑膏种类繁多，但是普遍的导热性能差，软化点高，渗透力不强等缺点，无法同时满足人们对润滑膏的要求。
发明内容：
为解决上述问题，本发明的目的是提供一种润滑膏及其制备方法。
本发明为实现上述目的，通过以下技术方案实现：
一种水基润滑膏，以重量份计，由以下成分组成：硬脂酸钠4-6份，硬脂酸锌1-3份，石墨微粉1-4份，乙二醇，5-10份，季戊四醇，5-8份，硅油5-8份，三乙醇胺3-5份，蒸馏水100-120份，苯甲酸钠0.5-1份，亚硝酸钠1-1.5份；
所述润滑膏按以下方法得到：
①原料预混合：硬脂酸锌1-3份，石墨微粉1-4份，硅油5-8份，三乙醇胺3-5份，，苯甲酸钠0.5-1份，亚硝酸钠1-1.5份，放入搅拌罐搅拌均匀，待用。
②润滑膏的制备：以重量份计，将硬脂酸钠4-6份，乙二醇，5-10份，季戊四醇，5-8份，蒸馏水100-120份，加入到反应釜中，加热到90℃，将步骤①预混合原料加入到反应釜中，搅拌0.5小时，均匀后，趁热灌装，冷却固化后，得到润滑膏产品。
优选的一种润滑膏，以重量份计，由以下方法得到
①原料预混合：以重量份计，将硬脂酸锌2份，石墨微粉2份，硅油6份，三乙醇胺4份，，苯甲酸钠0.8份，亚硝酸钠1.2份，放入搅拌罐搅拌均匀，待用。
②润滑膏的制备：以重量份计，将硬脂酸钠5份，乙二醇，6份，季戊四醇，6份，蒸馏水110份，加入到反应釜中，加热到90℃，将步骤①预混合原料加入到反应釜中，搅拌0.5小时，均匀后，趁热灌装，冷却固化后，得到润滑膏产品。
本发明的优点在于：
本发明的润滑膏软化点低，硬度适中，抗冲击性和渗透性，减摩性能好，能有效防止器械受损，并且具有优异的抗腐蚀、防锈性能，保证设备在高强度环境下正常工作。
具体实施方式：
下面通过实施例对本发明作进一步的说明。
实施例1
一种润滑膏，以重量份计，由以下成分组成：所述润滑膏按以下方法得到：
①原料预混合：硬脂酸锌1份，石墨微粉1份，硅油5份，三乙醇胺3份，，苯甲酸钠0.5份，亚硝酸钠1份，放入搅拌罐搅拌均匀，待用。
②润滑膏的制备：以重量份计，将硬脂酸钠4份，乙二醇，5份，季戊四醇，5份，蒸馏水100份，加入到反应釜中，加热到90℃，将步骤①预混合原料加入到反应釜中，搅拌0.5小时，均匀后，趁热灌装，冷却固化后，得到润滑膏产品。
实施例2
一种润滑膏，以重量份计，由以下成分组成：所述润滑膏按以下方法得到：
①原料预混合：硬脂酸锌2份，石墨微粉4份，硅油8份，三乙醇胺5份，，苯甲酸钠1份，亚硝酸钠1.5份，放入搅拌罐搅拌均匀，待用。
②润滑膏的制备：以重量份计，将硬脂酸钠6份，乙二醇，10份，季戊四醇，8份，蒸馏水120份，加入到反应釜中，加热到90℃，将步骤①预混合原料加入到反应釜中，搅拌0.5小时，均匀后，趁热灌装，冷却固化后，得到润滑膏产品。
实施例3
一种润滑膏，以重量份计，由以下成分组成：所述润滑膏按以下方法得到：
①原料预混合：硬脂酸锌2份，石墨微粉3份，硅油6份，三乙醇胺4份，，苯甲酸钠0.8份，亚硝酸钠1.2份，放入搅拌罐搅拌均匀，待用。
②润滑膏的制备：以重量份计，将硬脂酸钠5份，乙二醇，6份，季戊四醇，6份，蒸馏水110份，加入到反应釜中，加热到90℃，将步骤①预混合原料加入到反应釜中，搅拌0.5小时，均匀后，趁热灌装，冷却固化后，得到润滑膏产品。
锥入度/mm 软化点/℃ 摩擦系数 腐蚀性/钢片
实施例1 15.7 65 0.10 合格
实施例2 14.1 73 0.15 合格
实施例3 14.8 70 0.13 合格

Claims (2)

1.一种水基润滑膏，其特征在于：以重量份计，由以下成分组成：硬脂酸钠4-6份，硬脂酸锌1-3份，石墨微粉1-4份，乙二醇，5-10份，季戊四醇，5-8份，硅油5-8份，三乙醇胺3-5份，蒸馏水100-120份，苯甲酸钠0.5-1份，亚硝酸钠1-1.5份；
所述润滑膏的制备方法包括以下步骤：
①原料预混合：硬脂酸锌1-3份，石墨微粉1-4份，硅油5-8份，三乙醇胺3-5份，，苯甲酸钠0.5-1份，亚硝酸钠1-1.5份，放入搅拌罐搅拌均匀，待用。
②润滑膏的制备：以重量份计，将硬脂酸钠4-6份，乙二醇，5-10份，季戊四醇，5-8份，蒸馏水100-120份，加入到反应釜中，加热到90℃，将步骤①预混合原料加入到反应釜中，搅拌0.5小时，均匀后，趁热灌装，冷却固化后，得到润滑膏产品。
2.根据权利要求1所述的一种水基润滑膏，其特征在于：制备方法包括以下步骤：
①原料预混合：以重量份计，将硬脂酸锌2份，石墨微粉2份，硅油6份，三乙醇胺4份，，苯甲酸钠0.8份，亚硝酸钠1.2份，放入搅拌罐搅拌均匀，待用。
②润滑膏的制备：以重量份计，将硬脂酸钠5份，乙二醇，6份，季戊四醇，6份，蒸馏水110份，加入到反应釜中，加热到90℃，将步骤①预混合原料加入到反应釜中，搅拌0.5小时，均匀后，趁热灌装，冷却固化后，得到润滑膏产品。
CN201810459559.9A 2018-05-15 2018-05-15 一种水基润滑膏及其制备方法 Pending CN108517253A (zh)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111944595A (zh) * 2020-08-21 2020-11-17 江苏省健尔康医用敷料有限公司 一种医用外科器械用润滑剂及其制备和使用方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1405286A (zh) * 2001-08-13 2003-03-26 衡阳市高新技术金化实业有限责任公司 水基石墨芯棒润滑剂
CN104694240A (zh) * 2015-02-13 2015-06-10 衡阳市金化科技有限公司 水基粘土润滑剂
CN105154203A (zh) * 2015-10-20 2015-12-16 湖南金化科技集团有限公司 一种水基石墨精轧润滑剂

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1405286A (zh) * 2001-08-13 2003-03-26 衡阳市高新技术金化实业有限责任公司 水基石墨芯棒润滑剂
CN104694240A (zh) * 2015-02-13 2015-06-10 衡阳市金化科技有限公司 水基粘土润滑剂
CN105154203A (zh) * 2015-10-20 2015-12-16 湖南金化科技集团有限公司 一种水基石墨精轧润滑剂

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111944595A (zh) * 2020-08-21 2020-11-17 江苏省健尔康医用敷料有限公司 一种医用外科器械用润滑剂及其制备和使用方法
CN111944595B (zh) * 2020-08-21 2022-08-09 健尔康医疗科技股份有限公司 一种医用外科器械用润滑剂及其制备和使用方法

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