CN108477228A - A kind of bedding antiseptic and mite-proof agent and preparation method thereof - Google Patents
A kind of bedding antiseptic and mite-proof agent and preparation method thereof Download PDFInfo
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- CN108477228A CN108477228A CN201810367906.5A CN201810367906A CN108477228A CN 108477228 A CN108477228 A CN 108477228A CN 201810367906 A CN201810367906 A CN 201810367906A CN 108477228 A CN108477228 A CN 108477228A
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- mite
- antiseptic
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- proof agent
- leaf
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/34—Rosaceae [Rose family], e.g. strawberry, hawthorn, plum, cherry, peach, apricot or almond
Abstract
The invention discloses a kind of bedding antiseptic and mite-proof agents and preparation method thereof.The bedding antiseptic and mite-proof agent, by weight percentage, including the following raw material：Antiseptic 0.5~8%, mite-proof agent 1~10%, emulsifier 0.3~1%, dispersant 0.2~0.4%, crosslinking agent 0.1~0.3%, water surplus；Wherein, one or more in extract of the antiseptic selected from cayropteris incana, the extract of loguat leaf, the extract of myrica rubra leaf；The mite-proof agent is selected from one or both of volatile argyi leaf oil, stemonine.The preparation process of the bedding antiseptic and mite-proof agent is easy, not only safety and environmental protection, human body and the noxious material of Environmental security will not be had an impact, bactericidal can also effectively be pressed down, prevent the growth of acarid from multiplying, reduce the harm risk of acarid and bacterium to health, to play the role of preventing disease, have a very important significance and wide application prospect.
Description
Technical field
The present invention relates to antibiosis anti-acarien technical field, more particularly to a kind of bedding antiseptic and mite-proof agent and preparation method thereof
Background technology
With the improvement of living standards, people increasingly pay close attention to the health care of itself, the requirement to domestic environment is also continuous
It improves.Especially to work together have prevent bacteria breed, acarid breeding and other effects again safety and environmental protection multi-functional bedding it is more and more closeer
It looks at.Therefore research and development, which are prepared, has the function of antibacterial, the finishing agent of anti-mite function just can make bedding obtain health, health care, to
Play the role of preventing disease, have a very important significance and wide application prospect.
Bacterium and acarid are all invisible tiny organisms, under suitable environment, what they can be secreted with the mankind
Sweat, secretion and exuviae bits are bred rapidly as nutriment.In mattress, bedding, down toy, carpet, sand
There is their figure in the household supplies such as hair, kitchen, bathroom and environment.And secretion, metabolin and the corpse of acarid, all it is
The anaphylactogen that can be caused a disease easily causes allergic dermatitis, breathing problem.If dust mite brings some germs into, it is also easy to cause
The respiratory tract infection of human body or inflammation.According to the statistics of the World Health Organization, 70% asthma is caused by dust mite.
In damp and hot quilt, bacterium and acarid can grow rapidly, breed so that human skin infect and make to speckle with sweat and
The fabric of human secretion generates stench, and there is prodigious harm for this sleep quality and health to people.Therefore, make bedding
Possess the function of antibacterial and anti-mite deodorization as one of the research hotspot of current Mobyneb antiseptic and mite-proof agent.Now about antibacterial
In anti-mite research, some main matters for anti-acarus and bacteria are artificial synthesized mostly, and toxicity is big, this serious damage
The health of victimization body.
Therefore, it is necessary to provide a kind of antiseptic and mite-proof agent, you can be widely used in bedding, effectively sterilize it is anti-mite, to human body
Skin it is non-stimulated, safety and environmental protection, improve people’s lives environment.
Invention content
The technical problem to be solved in the present invention is to provide a kind of bedding antiseptic and mite-proof agent and preparation method thereof, which uses
The preparation process of antiseptic and mite-proof agent is easy, and not only safety and environmental protection, will not have an impact human body and the noxious material of Environmental security, also
Bactericidal can effectively be pressed down, prevent the growth of acarid from multiplying, reduce the harm risk of acarid and bacterium to health, to rise
To the effect for preventing disease, have a very important significance and wide application prospect.
In order to solve the above-mentioned technical problem, the technical scheme is that：
In a first aspect, a kind of bedding antiseptic and mite-proof agent provided by the invention, by weight percentage, including it is following former
Material：Antiseptic 0.5~8%, mite-proof agent 1~10%, emulsifier 0.3~1%, dispersant 0.2~0.4%, crosslinking agent 0.1~
0.3%, water surplus；
Wherein, one in extract of the antiseptic selected from cayropteris incana, the extract of loguat leaf, the extract of myrica rubra leaf
Kind is a variety of；
The mite-proof agent is selected from one or both of volatile argyi leaf oil, stemonine.
Preferably, the extract of the cayropteris incana is in ultrasonic extraction, microwave loss mechanisms, water extraction, alcohol extracting method
Any one is made；The described batch of extract leaf is appointing in ultrasonic extraction, microwave loss mechanisms, water extraction, alcohol extracting method
Meaning is a kind of to be made；The extract of the myrica rubra leaf is arbitrary in ultrasonic extraction, microwave loss mechanisms, water extraction, alcohol extracting method
One kind is made.
Preferably, the extract of the cayropteris incana is to be made using following methods：
After cayropteris incana is crushed, using water as solvent, in material-water ratio 1:5~20 (g/mL), the condition that temperature is 60~80 DEG C
1~3h of lower mechanical shaking extraction filters to take filtrate, and filter residue is brought up again once by above-mentioned steps, then the extracting solution merging of gained twice is dense
Contracting is the extract of cayropteris incana；
The described batch of extract leaf is to be made using following methods：
After loguat leaf is crushed, using water as solvent, in material-water ratio 1:5~20, temperature is that 60~80 DEG C of constant temperature oscillations extract 1
~3h filters to take filtrate, and filter residue is brought up again once by above-mentioned steps, then the extracting solution of gained twice is merged carrying for concentration loguat leaf
Take object；
The extract of the myrica rubra leaf is to be made using following methods：
After myrica rubra leaf is crushed, using water as solvent, by material-water ratio 1:5~20, temperature is that 60~80 DEG C of constant temperature oscillations extract 1
~3h filters to take filtrate, and filter residue is brought up again once by above-mentioned steps, then the extracting solution of gained twice is merged carrying for concentration loguat leaf
Take object.
Preferably, the antiseptic includes the extract of the extract of cayropteris incana, loguat leaf, wherein the cayropteris incana
The weight ratio of extract and the extract of the loguat leaf is 0.5~3:1.
Preferably, the mite-proof agent includes volatile argyi leaf oil, stemonine, wherein the volatile argyi leaf oil and the tuber of stemona
The weight ratio of alkali is 0.5~3:1.
Preferably, the emulsifier it is a kind of in Glycerin, mixed triester with caprylic acid capric acid, glycerin monostearate, propylene glycol fatty acid or
It is several.
Preferably, the dispersant is one or more of in pungent sodium tripolyphosphate, calgon, fiery sodium pyrophosphate.
Preferably, the crosslinking agent is aqueous polyurethane.
Preferably, the bedding antiseptic and mite-proof agent, by weight percentage, including the following raw material：Antiseptic 4~8%,
Mite-proof agent 5~10%, emulsifier 0.8~1%, dispersant 0.35~0.4%, crosslinking agent 0.25~0.3%, water surplus.
Second aspect, a kind of method of the bedding antiseptic and mite-proof agent prepared as described in relation to the first aspect provided by the invention,
Include the following steps：
By weight percentage, by antiseptic, mite-proof agent, emulsifier, dispersant, crosslinking agent, water at 1200~1800rpm
It is uniformly mixed up to antiseptic and mite-proof agent.
Compared with prior art, the beneficial effects of the present invention are：
(1) bedding of the present invention is with antiseptic and mite-proof agent selection is natural or safety and environmental protection, no skin irritation.
(2) the antibiosis anti-acarien effect of bedding antiseptic and mite-proof agent of the present invention is good：Antibiosis anti-acarien is Compositional type antiseptic and mite-proof agent,
Antibacterial anti-mite effect can be played simultaneously, 99% is both greater than to the bacteriostasis rate of staphylococcus aureus and Escherichia coli, to acarid
Inhibiting rate be more than 99%.
(3) use scope of bedding antiseptic and mite-proof agent of the present invention is wide：It can be used for textile, sofa, bedding, bathroom, dote on
It is non-discolouring after sprinkling or immersion article in object nest etc., product use value or appearance are not reduced.
(4) bedding antiseptic and mite-proof agent of the present invention is cost-effective：Used raw material is common, at low cost, has price advantage,
Its production operation step is few, with short production cycle.
(5) bedding of the present invention has the advantage of certain lasting effect with antiseptic and mite-proof agent：Wash resistant not easily runs off.
Specific implementation mode
The specific implementation mode of the present invention is described further below.It should be noted that for these implementations
The explanation of mode is used to help understand the present invention, but does not constitute limitation of the invention.In addition, invention described below
Involved technical characteristic can be combined with each other as long as they do not conflict with each other in each embodiment.
In a first aspect, a kind of bedding antiseptic and mite-proof agent provided by the invention, by weight percentage, including it is following former
Material：Antiseptic 0.5~8%, mite-proof agent 1~10%, emulsifier 0.3~1%, dispersant 0.2~0.4%, crosslinking agent 0.1~
0.3%, water surplus；
Wherein, one in extract of the antiseptic selected from cayropteris incana, the extract of loguat leaf, the extract of myrica rubra leaf
Kind is a variety of；
The mite-proof agent is selected from one or both of volatile argyi leaf oil, stemonine.
In an embodiment of the present invention, the extract of the cayropteris incana is ultrasonic extraction, microwave loss mechanisms, water carry
Any one in method, alcohol extracting method is made；The described batch of extract leaf be ultrasonic extraction, microwave loss mechanisms, water extraction,
Any one in alcohol extracting method is made；The extract of the myrica rubra leaf is ultrasonic extraction, microwave loss mechanisms, water extraction, alcohol
Any one in formulation is made.
In an embodiment of the present invention, the extract of the cayropteris incana is to be made using following methods：
After cayropteris incana is crushed, using water as solvent, in material-water ratio 1:5~20 (g/mL), the condition that temperature is 60~80 DEG C
1~3h of lower mechanical shaking extraction filters to take filtrate, and filter residue is brought up again once by above-mentioned steps, then the extracting solution merging of gained twice is dense
Contracting is the extract of cayropteris incana；
The described batch of extract leaf is to be made using following methods：
After loguat leaf is crushed, using water as solvent, in material-water ratio 1:5~20 (g/mL), the condition that temperature is 60~80 DEG C
Lower constant temperature oscillation extracts 1~3h, filters to take filtrate, and filter residue is brought up again once by above-mentioned steps, then the extracting solution of gained twice is closed
And concentrate the extract of loguat leaf；
The extract of the myrica rubra leaf is to be made using following methods：
After myrica rubra leaf is crushed, using water as solvent, in material-water ratio 1:5~20 (g/mL), the condition that temperature is 60~80 DEG C
Lower constant temperature oscillation extracts 1~3h, filters to take filtrate, and filter residue is brought up again once by above-mentioned steps, then the extracting solution of gained twice is closed
And concentrate the extract of loguat leaf.
Contain a kind of antibiotic effective ingredient of cayropteris incana element sodium in the cayropteris incana of the present invention, in root, stem, leaf, flower, herb
In content be respectively 1,5,10.4,5.5,4.7 gram of %, be faint yellow or yellow greenish powder, odorless, mildly bitter flavor is soluble easily in water.
Cayropteris incana element sodium to the bacillus such as staphylococcus aureus, typhoid fever, A type and paratyphoid B, green pus, large intestine, dysentery (Freund) with
And hemolytic streptococcus has resistance effect.
The folium artemisiae argyi of the present invention is the leaf of feverfew Chinese mugwort, and medicinal history is long, and the load that begins is seen《Mingyi Bielu》.The change of folium artemisiae argyi
Studying point mainly has volatile oil, flavones, eudesmane and triterpenes components, and there is good antibacterial action, decocting liquid to have preferably for it
Bacteriostasis, wound surface of burn patients after moxa stick sootiness, surface of a wound reduction in colony be 74.64%；Ward is carried out with folium artemisiae argyi
Sootiness sterilizes, and total number of bacteria rate of descent can be made in air up to 73.04%.
In an embodiment of the present invention, the antiseptic includes the extract of the extract of cayropteris incana, loguat leaf,
In, the weight ratio of the extract of the cayropteris incana and the extract of the loguat leaf is 0.5~3:1.
It is further preferred that in this embodiment, the extract of the cayropteris incana and the extract of the loguat leaf
Weight ratio is 2:1.
In an embodiment of the present invention, the mite-proof agent includes volatile argyi leaf oil, stemonine, wherein the folium artemisiae argyi is waved
The weight ratio of hair oil and the stemonine is 0.5~3:1.
It is further preferred that in this embodiment, the weight ratio of the volatile argyi leaf oil and the stemonine is 2:1.
In an embodiment of the present invention, the emulsifier is selected from Glycerin, mixed triester with caprylic acid capric acid, glycerin monostearate, propylene glycol
It is one or more of in aliphatic acid.
Further, in this embodiment, the emulsifier is Glycerin, mixed triester with caprylic acid capric acid.
In an embodiment of the present invention, the dispersant is selected from pungent sodium tripolyphosphate, calgon, fiery sodium pyrophosphate
Middle one or more.
Further, in this embodiment, the dispersant is pungent sodium tripolyphosphate.
In an embodiment of the present invention, the crosslinking agent is aqueous polyurethane.
In an embodiment of the present invention, the bedding antiseptic and mite-proof agent, by weight percentage, including it is following former
Material：Antiseptic 4~8%, mite-proof agent 5~10%, emulsifier 0.8~1%, dispersant 0.35~0.4%, crosslinking agent 0.25~
0.3%, water surplus.
Second aspect, a kind of method of the bedding antiseptic and mite-proof agent prepared as described in relation to the first aspect provided by the invention,
Include the following steps：
By weight percentage, by antiseptic, mite-proof agent, emulsifier, dispersant, crosslinking agent, water at 1200~1800rpm
It is uniformly mixed up to antiseptic and mite-proof agent.
In following embodiment, the extract of cayropteris incana is to be made using following methods：
Cayropteris incana is put in high speed disintegrator and is crushed uniformly, is 1 in material-water ratio using water as solvent:10 (g/mL), temperature
Constant temperature oscillation extracts 2h under conditions of being 70 DEG C, filters to take filtrate, filter residue is brought up again once by above-mentioned steps, then will be obtained by twice
Extracting solution merges the water extract that concentration is cayropteris incana.
In following embodiment, the extract of loguat leaf is to be made using following methods：
Loguat leaf is put in high speed disintegrator and is crushed uniformly, is 1 in material-water ratio using water as solvent:10 (g/mL), temperature
Constant temperature oscillation extracts 2h under conditions of being 70 DEG C, filters to take filtrate, filter residue is brought up again once by above-mentioned steps, then will be obtained by twice
Extracting solution merges the water extract of concentration loguat leaf.
In following embodiment, the extract of the myrica rubra leaf is to be made using following methods：
Myrica rubra leaf is put in high speed disintegrator and is crushed uniformly, using water as solvent, in material-water ratio 1:12 (g/mL), temperature are
Constant temperature oscillation extracts 2h under conditions of 70 DEG C, filters to take filtrate, and filter residue is brought up again once by above-mentioned steps, then carrying gained twice
Liquid is taken to merge the extract of concentration loguat leaf.
Embodiment 1
Take the raw material of following weight percent meters：Extract 0.5%, volatile argyi leaf oil 1%, the pungent capric acid glycerine of cayropteris incana
Above-mentioned raw materials are added in blender for ester 0.3%, sodium tripolyphosphate 0.2%, aqueous polyurethane 0.1%, distilled water surplus,
It is uniformly mixed under 1600rpm up to antiseptic and mite-proof agent.
Embodiment 2
Take the raw material of following weight percent meters：Extract 0.5%, stemonine 1%, the Glycerin, mixed triester with caprylic acid capric acid of cayropteris incana
0.3%, above-mentioned raw materials are added in blender for sodium tripolyphosphate 0.2%, aqueous polyurethane 0.1%, distilled water surplus,
It is uniformly mixed under 1600rpm up to antiseptic and mite-proof agent.
Embodiment 3
Take the raw material of following weight percent meters：The extract 0.25% of cayropteris incana criticizes the extract 0.25% leaf, Chinese mugwort
Leaf volatile oil 0.5%, stemonine 0.5%, Glycerin, mixed triester with caprylic acid capric acid 0.3%, sodium tripolyphosphate 0.2%, aqueous polyurethane 0.1%,
Above-mentioned raw materials are added in blender distilled water surplus, are uniformly mixed at 1600 rpm up to antiseptic and mite-proof agent.
Embodiment 4
Take the raw material of following weight percent meters：It criticizes the extract 0.5% of leaf, volatile argyi leaf oil 1%, pungent capric acid glycerine
Above-mentioned raw materials are added in blender for ester 0.3%, sodium tripolyphosphate 0.2%, aqueous polyurethane 0.1%, distilled water surplus,
It is uniformly mixed under 1600rpm up to antiseptic and mite-proof agent.
Embodiment 5
Take the raw material of following weight percent meters：Criticize the extract 0.5%, stemonine 1%, Glycerin, mixed triester with caprylic acid capric acid leaf
0.3%, above-mentioned raw materials are added in blender for sodium tripolyphosphate 0.2%, aqueous polyurethane 0.1%, distilled water surplus,
It is uniformly mixed under 1600rpm up to antiseptic and mite-proof agent.
Embodiment 6
Take the raw material of following weight percent meters：The extract 0.33% of cayropteris incana criticizes the extract 0.17% leaf, Chinese mugwort
Leaf volatile oil 0.66%, stemonine 0.34%, Glycerin, mixed triester with caprylic acid capric acid 0.3%, sodium tripolyphosphate 0.2%, aqueous polyurethane
0.1%, above-mentioned raw materials are added in blender distilled water surplus, are uniformly mixed at 1600 rpm up to antibiosis anti-acarien
Agent.
Embodiment 7
Take the raw material of following weight percent meters：The extract 0.17% of cayropteris incana criticizes the extract 0.33% leaf, Chinese mugwort
Leaf volatile oil 0.37%, stemonine 0.66%, Glycerin, mixed triester with caprylic acid capric acid 0.3%, sodium tripolyphosphate 0.2%, aqueous polyurethane
0.1%, above-mentioned raw materials are added in blender distilled water surplus, are uniformly mixed at 1600 rpm up to antibiosis anti-acarien
Agent.
Embodiment 8
Take the raw material of following weight percent meters：The extract 5.33% of cayropteris incana criticizes the extract 2.67% leaf, Chinese mugwort
Leaf volatile oil 6.6%, Glycerin, mixed triester with caprylic acid capric acid 1%, sodium tripolyphosphate 0.4%, aqueous polyurethane 0.3%, steams stemonine 3.4%
Above-mentioned raw materials are added in blender distilled water surplus, are uniformly mixed at 1600 rpm up to antiseptic and mite-proof agent.
Embodiment 9
Take the raw material of following weight percent meters：The extract 2.66% of cayropteris incana criticizes the extract 1.34% leaf, Chinese mugwort
Leaf volatile oil 3.3%, Glycerin, mixed triester with caprylic acid capric acid 1%, sodium tripolyphosphate 0.4%, aqueous polyurethane 0.3%, steams stemonine 1.7%
Above-mentioned raw materials are added in blender distilled water surplus, are uniformly mixed at 1600 rpm up to antiseptic and mite-proof agent.
Embodiment 10
Take the raw material of following weight percent meters：The extract 2.66% of cayropteris incana criticizes the extract 1.34% leaf, Chinese mugwort
Leaf volatile oil 3.3%, stemonine 1.7%, Glycerin, mixed triester with caprylic acid capric acid 0.3%, sodium tripolyphosphate 0.2%, aqueous polyurethane 0.1%,
Above-mentioned raw materials are added in blender distilled water surplus, are uniformly mixed at 1600 rpm up to antiseptic and mite-proof agent.
Embodiment 11
Take the raw material of following weight percent meters：The extract 3% of cayropteris incana criticizes the extract 1% leaf, folium artemisiae argyi volatilization
Oil 3.3%, stemonine 1.7%, Glycerin, mixed triester with caprylic acid capric acid 1%, sodium tripolyphosphate 0.4%, aqueous polyurethane 0.3%, more than distilled water
Above-mentioned raw materials are added in blender amount, are uniformly mixed at 1600 rpm up to antiseptic and mite-proof agent.
Embodiment 12
Take the raw material of following weight percent meters：The extract 3% of cayropteris incana criticizes the extract 1% leaf, folium artemisiae argyi volatilization
Oil 3.75%, stemonine 1.25%, Glycerin, mixed triester with caprylic acid capric acid 1%, sodium tripolyphosphate 0.4%, aqueous polyurethane 0.3%, distilled water
Above-mentioned raw materials are added in blender surplus, are uniformly mixed at 1600 rpm up to antiseptic and mite-proof agent.
Embodiment 13
Take the raw material of following weight percent meters：The extract 2.66% of cayropteris incana criticizes the extract 1.34% leaf, Chinese mugwort
Leaf volatile oil 3.3%, stemonine 1.7%, Glycerin, mixed triester with caprylic acid capric acid 0.8%, sodium tripolyphosphate 0.35%, aqueous polyurethane
0.25%, above-mentioned raw materials are added in blender distilled water surplus, are uniformly mixed at 1600 rpm up to antibiosis anti-acarien
Agent.
Embodiment 14
Take the raw material of following weight percent meters：The extract 0.66% of cayropteris incana criticizes the extract 0.34% leaf, Chinese mugwort
Leaf volatile oil 1.33%, stemonine 0.67%, Glycerin, mixed triester with caprylic acid capric acid 0.3%, sodium tripolyphosphate 0.2%, aqueous polyurethane
0.1%, above-mentioned raw materials are added in blender distilled water surplus, are uniformly mixed at 1600 rpm up to antibiosis anti-acarien
Agent.
Embodiment 15
Take the raw material of following weight percent meters：The extract 6.66% of cayropteris incana criticizes the extract 3.34% leaf, Chinese mugwort
Leaf volatile oil 9.9%, Glycerin, mixed triester with caprylic acid capric acid 1%, sodium tripolyphosphate 0.4%, aqueous polyurethane 0.3%, steams stemonine 5.1%
Above-mentioned raw materials are added in blender distilled water surplus, are uniformly mixed at 1600 rpm up to antiseptic and mite-proof agent.
Antiseptic and mite-proof agent obtained by the embodiment of the present invention is pressed into 5g/m2Sprinkling is used in bedding surface, waits for naturally dry
.Textile article also can directly be soaked in the antiseptic and mite-proof agent obtained by 10% embodiment of the present invention 15~20 points
Clock, after routinely washing dry.
Advantageous effect in order to further illustrate the present invention, using following methods to the product obtained by the embodiment of the present invention
Carry out measure of merit：
(1) acute dermal toxicity is tested：According to《Cosmetics safety technical specification》(version in 2015) chapter 6 toxicology is real
4 skin irritations of proved recipe method/corrosion test.
(2) acute eye irritation test：According to《Cosmetics safety technical specification》(version in 2015) second part is tested.
(3) antibacterium aptitude tests：Antiseptic and mite-proof agent treatment cloth is tested using oscillating culture, the use of strain is golden yellow
Staphylococcus and Escherichia coli, with specific reference to standard ASTM E2149.
(4) Durability of antimicrobial effect is tested：Antibiosis anti-acarien after antiseptic and mite-proof agent treatment cloth is washed 5 times arranges cloth according to standard
ASTM E2149 tests.
(5) anti-mite aptitude tests：Antiseptic and mite-proof agent treatment cloth drives mite effect detection, with specific reference to standard GB/T 24253-
The evaluation of the anti-mite performance of 2009 textiles.
(6) anti-mite sustainability test：Antibiosis anti-acarien after antiseptic and mite-proof agent treatment cloth is washed 5 times arranges cloth according to standard
GB/T 24253-2009 tests.
Testing result is as follows：
The test result statistical form of product obtained by 1 each embodiment of table
Test result analysis：
The product testing result of Examples 1 to 7 in table 1 is compared and analyzed, it is known that, the extract of cayropteris incana, loquat
The extract mixing of leaf is used as antiseptic, and there is synergetic antibacterial effect, antimicrobial efficiency to be apparently higher than using single cayropteris incana
The extract of extract or single loguat leaf；Volatile argyi leaf oil, stemonine mixing are used as mite-proof agent, have the anti-of synergy
Mite effect is driven mite rate and is apparently higher than using single volatile argyi leaf oil or single stemonine.
The product testing result of embodiment in table 13,6,7,9,11,12 is compared and analyzed, it is known that, as antiseptic
The extract of the cayropteris incana of ingredient, the extract of loguat leaf weight ratio be 2:Antimicrobial efficiency when 1 is significantly better than other proportionings.
It is 2 as the volatile argyi leaf oil of mite-proof agent ingredient, the weight ratio of stemonine:When 1 range it is anti-mite it is with obvious effects be better than it is other
Proportioning.
The product testing result of embodiment in table 16,9,10,13,14 is compared and analyzed, it is known that, when the use of antiseptic
When amount is higher than 1%, the dosage of mite-proof agent is higher than 2%, emulsifier, dispersant, crosslinking agent dosage should increase accordingly, emulsifier
Glycerin, mixed triester with caprylic acid capric acid is preferably not below 0.8%, pentasodium triphosphate of dispersing agent and is preferably not below 0.35%, crosslinking agent aqueous polyurethane
Preferably not below 0.25, when too low this is mainly due to emulsifier, dispersant, crosslinking agent, can make antiseptic and mite-proof agent with
Absorption between bedding surface is inadequate, to the antibacterial for influencing product and anti-mite effect.And emulsifier, dispersant, crosslinking agent are used
Measure it is excessively high also bring along adverse effect, this be mainly emulsifier, dispersant, crosslinking agent interaction, be easy package antiseptic and
Mite-proof agent, so that antiseptic and mite-proof agent are unable to give full play effect；Therefore, in the present invention, the dosage of emulsifier is excellent
The dosage for being selected as 0.8~1%, dispersant is preferably that the dosage of 0.35~0.4%, crosslinking agent is preferably 0.25~0.3%.
The product testing result of embodiment in table 16,8,9,14,15 is compared and analyzed, it is known that, when the use of antiseptic
It measures in range of the dosage 1~10% of 0.5~8%, mite-proof agent, the antibacterial of product and anti-mite effect are with antiseptic and anti-
The dosage of mite agent increases and enhances；When the dosage of antiseptic is higher than 8%, and the dosage of mite-proof agent is higher than 10%, the antibacterial of product,
Anti-mite effect has almost no change, from the point of view of economic cost and antibacterial, anti-mite effect, antiseptic and mite-proof agent of the invention
In, when the dosage preferably 4~8% of antiseptic, the dosage preferably 5~10% of mite-proof agent.
Advantageous effect in order to further illustrate the present invention, it is real that the present invention also uses the extract of myrica rubra leaf to replace the present invention
The extract criticized leaf in example 1~14 is applied, prepares antiseptic and mite-proof agent, the antibiosis anti-acarien performance of the product finally measured is obviously poor
In the antibiosis anti-acarien performance of 1~15 resulting product of the embodiment of the present invention.
Embodiments of the present invention are explained in detail above, but the present invention is not limited to described embodiments.It is right
For those skilled in the art, in the case where not departing from the principle of the invention and spirit, these embodiments are carried out more
Kind change, modification, replacement and modification, still fall in protection scope of the present invention.
Claims (10)
1. a kind of bedding antiseptic and mite-proof agent, it is characterised in that：By weight percentage, including the following raw material：Antiseptic 0.5~
8%, mite-proof agent 1~10%, emulsifier 0.3~1%, dispersant 0.2~0.4%, crosslinking agent 0.1~0.3%, water surplus；
Wherein, extract of the antiseptic selected from cayropteris incana, the extract of loguat leaf, one kind in the extract of myrica rubra leaf or
It is a variety of；
The mite-proof agent is selected from one or both of volatile argyi leaf oil, stemonine.
2. bedding antiseptic and mite-proof agent according to claim 1, it is characterised in that：The extract of the cayropteris incana is ultrasound
Any one in wave extraction method, microwave loss mechanisms, water extraction, alcohol extracting method is made；The described batch of extract leaf is ultrasonic wave
Any one in extraction method, microwave loss mechanisms, water extraction, alcohol extracting method is made；The extract of the myrica rubra leaf carries for ultrasonic wave
Follow the example of, in microwave loss mechanisms, water extraction, alcohol extracting method any one be made.
3. bedding antiseptic and mite-proof agent according to claim 1, it is characterised in that：The extract of the cayropteris incana is to use
Following methods are made：
After cayropteris incana is crushed, using water as solvent, in material-water ratio 1:5~20 (g/mL), temperature are shaken under conditions of being 60~80 DEG C
1~3h of extraction is swung, filtrate is filtered to take, filter residue is brought up again once by above-mentioned steps, then the extracting solution of gained twice is merged concentration and is
For the extract of cayropteris incana；
The described batch of extract leaf is to be made using following methods：
After loguat leaf is crushed, using water as solvent, in material-water ratio 1:5~20 (g/mL), temperature are permanent under conditions of being 60~80 DEG C
Warm 1~3h of mechanical shaking extraction filters to take filtrate, and filter residue is brought up again once by above-mentioned steps, then the extracting solution merging of gained twice is dense
The extract of contracting loguat leaf；
The extract of the myrica rubra leaf is to be made using following methods：
After myrica rubra leaf is crushed, using water as solvent, in material-water ratio 1:5~20 (g/mL), temperature are permanent under conditions of being 60~80 DEG C
Warm 1~3h of mechanical shaking extraction filters to take filtrate, and filter residue is brought up again once by above-mentioned steps, then the extracting solution merging of gained twice is dense
The extract of contracting loguat leaf.
4. bedding antiseptic and mite-proof agent according to claim 1, it is characterised in that：The antiseptic includes carrying for cayropteris incana
Take the extract of object, loguat leaf, wherein the weight ratio of the extract of the cayropteris incana and the extract of the loguat leaf is 0.5
~3:1.
5. bedding antiseptic and mite-proof agent according to claim 1, it is characterised in that：The mite-proof agent includes folium artemisiae argyi volatilization
Oil, stemonine, wherein the weight ratio of the volatile argyi leaf oil and the stemonine is 0.5~3:1.
6. bedding antiseptic and mite-proof agent according to claim 1, it is characterised in that：The emulsifier is selected from pungent capric acid glycerine
It is one or more of in ester, glycerin monostearate, propylene glycol fatty acid.
7. bedding antiseptic and mite-proof agent according to claim 1, it is characterised in that：The dispersant is selected from pungent tripolyphosphate
It is one or more of in sodium, calgon, fiery sodium pyrophosphate.
8. bedding antiseptic and mite-proof agent according to claim 1, it is characterised in that：The crosslinking agent is aqueous polyurethane.
9. bedding antiseptic and mite-proof agent according to claim 1, it is characterised in that：The bedding antiseptic and mite-proof agent, is pressed
Weight percent meter, including the following raw material：Antiseptic 4~8%, mite-proof agent 5~10%, emulsifier 0.8~1%, dispersant
0.35~0.4%, crosslinking agent 0.25~0.3%, water surplus.
10. a kind of preparing the method such as claim 1~9 any one of them bedding antiseptic and mite-proof agent, it is characterised in that：Packet
Include following steps：
By weight percentage, antiseptic, mite-proof agent, emulsifier, dispersant, crosslinking agent, water are stirred at 1200~1800rpm
It is uniformly mixed up to antiseptic and mite-proof agent.
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